CN111978870A - Cerate for redwood furniture and preparation method thereof - Google Patents
Cerate for redwood furniture and preparation method thereof Download PDFInfo
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- CN111978870A CN111978870A CN202010916190.7A CN202010916190A CN111978870A CN 111978870 A CN111978870 A CN 111978870A CN 202010916190 A CN202010916190 A CN 202010916190A CN 111978870 A CN111978870 A CN 111978870A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
- C09G1/12—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin mixtures of wax and silicon-containing polycondensates
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/06—Waxes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a wax paste for redwood furniture and a preparation method thereof, wherein the wax paste for the redwood furniture comprises 40-50 parts of beeswax, 20-30 parts of sweet orange oil, 5-10 parts of polyurethane adhesive, 2-5 parts of plasticizer, 3-5 parts of organic silicon resin, 3-5 parts of modified silicon oil, 0.5-1 part of photoinitiator, 0.015-0.02 part of antioxidant and the balance of absolute ethyl alcohol, and the wax paste for the redwood furniture has excellent performance, the loss mass of the prepared wax paste in an abrasion resistance test is 25-41 parts, the melting point is 97-126 ℃, and the curing speed is 2.6-3.7h, wherein the wax paste for the redwood furniture provided by the third embodiment has the optimal effect, the loss mass of the wax paste in the abrasion resistance test is only 25 parts, the melting point reaches 126 ℃, and the curing speed is only 2.6 h; through the adjustment to the wax ointment composition for the rosewood furniture now for wax ointment for the rosewood furniture wearability promotes, the melting point risees, solidification speed is accelerated, makes furniture more wear-resisting, and it is more convenient to maintain.
Description
Technical Field
The invention relates to a cerate, in particular to a cerate for redwood furniture.
Background
Wood furniture waxing can block the circulation of water and the outside of the solid wood furniture, so that the structural deformation of the solid wood furniture can be effectively avoided, wood fibers of the solid wood furniture can be moistened, and the solid wood furniture is enabled to be kept in a glossy state all the time.
However, when the wood furniture wax prepared by the existing preparation method is applied to wood furniture, the moisture-proof and scratch-proof effects are not particularly ideal, so that the appearance maintenance of the furniture is greatly influenced, and the service life of the wood furniture is also greatly shortened.
Disclosure of Invention
In order to solve the defects of the prior art, the invention provides the cerate for the redwood furniture and the preparation method thereof, and the cerate for the redwood furniture has the advantages that the wear resistance, the moisture resistance and the color retention degree are greatly improved and the protection effect is better by adjusting the components of the cerate for the redwood furniture.
The specific technical scheme is as follows:
the cerate for the redwood furniture comprises the following components in percentage by mass:
30-40 parts of beewax, 20-30 parts of sweet orange oil, 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer, 3-5 parts of organic silicon resin, 3-5 parts of modified silicon oil, 0.5-1 part of photoinitiator, 0.015-0.02 part of antioxidant and the balance of absolute ethyl alcohol.
Preferably, 35 parts of beeswax, 25 parts of sweet orange oil, 5 parts of polyurethane adhesive, 3.5 parts of plasticizer, 4 parts of silicone resin, 4 parts of modified silicon oil, 0.75 part of photoinitiator and 0.02 part of antioxidant.
Further, the invention provides a preparation method of the cerate for the redwood furniture, which comprises the following specific steps:
(1) heating beeswax in a water bath kettle at 70-80 deg.C for 2-3 hr until beeswax is completely melted, filtering liquid beeswax for 3-5 times step by step until no impurities are in beeswax, and keeping the temperature at 60-65 deg.C;
(2) preparing 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer and 0.015-0.02 part of saturated absolute ethyl alcohol solution of antioxidant according to the proportion;
(3) sequentially filling 30-40 parts of filtered beeswax, 20-30 parts of sweet orange oil, 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer and 0.015-0.02 part of antioxidant into a saturated absolute ethyl alcohol solution, 3-5 parts of organic silicon resin, 3-5 parts of modified silicon oil and 0.5-1 part of photoinitiator into an emulsifying machine preheated at 62 ℃, filling nitrogen into the emulsifying machine, slowly heating to 70-80 ℃, stirring at 700rpm for 2-4h, and observing the stirring process, and adding absolute ethyl alcohol until the stirred substance is pasty;
(4) and (4) releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the cerate obtained by stirring in the step (3) and strictly storing in a dark place.
Preferably, in the preparation method of the wax ointment for the redwood furniture, the beeswax is heated in a water bath at 74 ℃ for 3 hours until the beeswax is completely melted, the liquid beeswax is filtered for 5 times step by step until no impurities exist in the beeswax, and the temperature is kept at 62 ℃.
Preferably, in the preparation method of the cerate for the redwood furniture, the emulsifying machine is used for stirring for 4 hours at the stirring speed of 700rpm, the temperature in the container is 76 ℃ in the stirring process, and the container is kept in a dark state, so that the beneficial effects obtained by the invention are as follows:
(1) the wax paste for the redwood furniture prepared by the invention has excellent wear resistance, wherein the wax paste for the redwood furniture provided by the third embodiment has the best effect, and has the mass loss of only 25 parts in a wear resistance test, the melting point of 126 ℃ and the curing speed of only 2.6 hours under the mixture ratio of 35 parts of beeswax, 25 parts of sweet orange oil, 5 parts of polyurethane adhesive, 3.5 parts of plasticizer, 4 parts of organic silicon resin, 4 parts of sulfur-based modified silicone oil, 0.75 part of photoinitiator, 0.02 part of antioxidant and the balance of absolute ethyl alcohol.
(2) According to the invention, through adjusting the components of the existing wax paste for the redwood furniture, the wear resistance of the wax paste for the redwood furniture is improved, the melting point is increased, the curing speed is accelerated, the furniture is more wear-resistant, and the maintenance is more convenient.
(3) The performances of the cerate for the redwood furniture prepared in the first to fifth embodiments of the invention are all superior to those of the currently marketed wood wax oil, wherein the cerate prepared by the method of the invention has the loss of 25-41 parts in the wear resistance test, the melting point of 97-126 ℃, and the curing speed of 2.6-3.7h, and the cerate for the redwood furniture provided in the third embodiment has the optimal performance, the loss of 25 parts in the wear resistance test, the melting point of 126 ℃, and the curing speed of 2.6h, which are all far superior to those of the marketed wood wax oil.
Detailed Description
The invention will be better understood from the following examples. However, those skilled in the art will readily appreciate that the specific material ratios, process conditions and results thereof described in the examples are illustrative only and should not be taken as limiting the invention as detailed in the claims.
The first embodiment is as follows:
the cerate for the redwood furniture comprises the following components in percentage by mass: 30 parts of beeswax, 20 parts of sweet orange oil, 4 parts of polyurethane adhesive, 2 parts of plasticizer, 3 parts of organic silicon resin, 3 parts of modified silicon oil, 0.5 part of photoinitiator, 0.015 part of antioxidant and the balance of absolute ethyl alcohol.
In the embodiment, the preparation method of the cerate for the redwood furniture comprises the following specific steps: heating beeswax in a water bath kettle at 70 ℃ for 2 hours in a water bath until the beeswax is completely melted, filtering liquid beeswax for 3 times step by step until no impurities exist in the beeswax, and keeping the temperature at 60 ℃; preparing 4 parts of polyurethane adhesive, 2 parts of plasticizer and 0.015 part of antioxidant by using a saturated absolute ethyl alcohol solution according to the proportion; sequentially filling 30 parts of filtered beewax, 20 parts of sweet orange oil, 4 parts of polyurethane adhesive, 2 parts of plasticizer and 0.015 part of antioxidant in a saturated absolute ethyl alcohol solution, 3 parts of organic silicon resin, 3 parts of hydrophobic modified silicone oil and 0.5 part of photoinitiator into an emulsifying machine preheated at 62 ℃, filling nitrogen into the emulsifying machine, slowly heating to 70 ℃, stirring at 500rpm for 2 hours, and observing the stirring process and adding absolute ethyl alcohol until the stirred substance is pasty; and releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the wax paste obtained by stirring, and strictly keeping away from light.
Example two:
the cerate for the redwood furniture comprises the following components in percentage by mass: 33 parts of beewax, 22 parts of sweet orange oil, 4.5 parts of polyurethane adhesive, 3 parts of plasticizer, 3.5 parts of organic silicon resin, 3.5 parts of modified silicon oil, 0.6 part of photoinitiator, 0.016 part of antioxidant and the balance of absolute ethyl alcohol.
In the embodiment, the preparation method of the cerate for the redwood furniture comprises the following specific steps: heating beeswax in a water bath kettle at 72 ℃ for 2.5 hours in a water bath until the beeswax is completely melted, filtering liquid beeswax for 4 times step by step until no impurities exist in the beeswax, and keeping the temperature at 61 ℃; preparing 4.5 parts of polyurethane adhesive, 3 parts of plasticizer and 0.016 part of antioxidant according to the proportion; according to the proportion, 33 parts of filtered beewax, 22 parts of sweet orange oil, 4.5 parts of polyurethane adhesive, 3 parts of plasticizer and 0.016 part of antioxidant, 3.5 parts of organic silicon resin, 3.5 parts of sulfhydryl modified silicone oil and 0.6 part of photoinitiator are sequentially filled into an emulsifying machine preheated at 62 ℃, nitrogen is filled into the emulsifying machine, after the mixture is slowly heated to 72 ℃, the mixture is stirred at 550rpm for 2.5 hours, and the absolute ethyl alcohol is added during the stirring process until the mixture is pasty; and releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the wax paste obtained by stirring, and strictly keeping away from light.
Example three:
the cerate for the redwood furniture comprises the following components in percentage by mass: 35 parts of beeswax, 25 parts of sweet orange oil, 5 parts of polyurethane adhesive, 3.5 parts of plasticizer, 4 parts of organic silicon resin, 4 parts of modified silicon oil, 0.75 part of photoinitiator, 0.02 part of antioxidant and the balance of absolute ethyl alcohol.
In the embodiment, the preparation method of the cerate for the redwood furniture comprises the following specific steps: heating beeswax in a water bath at 74 ℃ for 3 hours in a water bath until the beeswax is completely melted, filtering liquid beeswax for 5 times step by step until no impurities exist in the beeswax, and keeping the temperature at 62 ℃; preparing 5 parts of polyurethane adhesive, 3.5 parts of plasticizer and 0.02 part of antioxidant according to the proportion; sequentially filling 35 parts of filtered beeswax, 25 parts of sweet orange oil, 5 parts of polyurethane adhesive, 3.5 parts of plasticizer and 0.02 part of antioxidant into a saturated absolute ethyl alcohol solution, 4 parts of organic silicon resin, 4 parts of sulfenyl modified silicone oil and 0.75 part of photoinitiator into an emulsifying machine preheated at 62 ℃, filling nitrogen into the emulsifying machine, slowly heating to 76 ℃, stirring at 700rpm for 4 hours, and observing the stirring process and adding absolute ethyl alcohol until the stirred substance is pasty; and releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the wax paste obtained by stirring, and strictly keeping away from light.
Example four:
the cerate for the redwood furniture comprises the following components in percentage by mass: 37 parts of beeswax, 28 parts of sweet orange oil, 5.5 parts of polyurethane adhesive, 4 parts of plasticizer, 4.5 parts of organic silicon resin, 4.5 parts of modified silicon oil, 0.75 part of photoinitiator, 0.017 part of antioxidant and the balance of absolute ethyl alcohol.
In the embodiment, the preparation method of the cerate for the redwood furniture comprises the following specific steps: heating beeswax in a water bath kettle at 78 deg.C for 2.7 in water bath until beeswax is completely melted, filtering liquid beeswax for 4 times step by step until no impurities are in beeswax, and keeping the temperature at 64 deg.C; preparing 5.5 parts of polyurethane adhesive, 45 parts of plasticizer and 0.017 part of antioxidant according to the proportion; according to the proportion, the filtered beewax 37 parts, the filtered sweet orange oil 28 parts, the filtered polyurethane adhesive 5.5 parts, the filtered plasticizer 4 parts and the filtered antioxidant 0.017 parts of saturated absolute ethyl alcohol solution, the filtered polyurethane adhesive 4.5 parts and the filtered antioxidant 0.017 part of saturated absolute ethyl alcohol solution, the filtered polyurethane adhesive 4.5 parts and the filtered polyurethane adhesive 4.5 parts, the filtered polyurethane adhesive 4.5 parts and; and releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the wax paste obtained by stirring, and strictly keeping away from light.
Example five:
the cerate for the redwood furniture comprises the following components in percentage by mass: 40 parts of beeswax, 30 parts of sweet orange oil, 6 parts of polyurethane adhesive, 5 parts of plasticizer, 5 parts of organic silicon resin, 5 parts of modified silicon oil, 1 part of photoinitiator, 0.02 part of antioxidant and the balance of absolute ethyl alcohol.
In the embodiment, the preparation method of the cerate for the redwood furniture comprises the following specific steps: heating beeswax in a water bath kettle at 80 deg.C for 3 hr until the beeswax is completely melted, filtering liquid beeswax for 5 times step by step until no impurities are in the beeswax, and keeping the temperature at 65 deg.C; preparing 6 parts of polyurethane adhesive, 5 parts of plasticizer and 0.02 part of antioxidant according to the proportion; sequentially filling 40 parts of filtered beeswax, 30 parts of sweet orange oil, 6 parts of polyurethane adhesive, 5 parts of plasticizer and 0.02 part of antioxidant into a saturated absolute ethyl alcohol solution, 5 parts of organic silicon resin, 5 parts of modified silicon oil and 1 part of photoinitiator which are preheated at 62 ℃, filling nitrogen into an emulsifying machine, slowly heating to 80 ℃, stirring at 700rpm for 4 hours, and observing the stirring process and adding absolute ethyl alcohol until the stirred substance is pasty; and releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the wax paste obtained by stirring, and strictly keeping away from light.
Example six:
the cerams prepared in examples one to five were applied to rosewood and their wear resistance, melting point and curing speed were measured and averaged, the results are shown in table 1.
Table 1: EXAMPLES first to fifth Properties of the cerate for redwood furniture
| Serial number | Loss of mass%/5 min/50rpm | Melting Point/. degree.C | Curing speed/h |
| Example one | 41 | 97 | 3.5 |
| Example two | 36 | 105 | 3.2 |
| EXAMPLE III | 25 | 126 | 2.6 |
| Example four | 33 | 112 | 3.3 |
| EXAMPLE five | 39 | 105 | 3.7 |
| Commercial wood wax oil | 53 | 80 | 5.5 |
Abrasion resistance measurement method: according to GB/T1768-1989.
As can be seen from Table 1, compared with commercially available wood wax oil, the wax paste for redwood furniture prepared in the first to fifth embodiments of the present invention has excellent wear resistance, the wax paste prepared by the method of the present invention has a loss of 25-41% in a wear resistance test, a melting point of 97-126 ℃, and a curing speed of 2.6-3.7h, wherein the wax paste for redwood furniture provided in the third embodiment has an optimal effect, the loss of 25% in the wear resistance test, the melting point of 126 ℃, and the curing speed of 2.6 h.
In conclusion, the technical scheme provided by the invention improves the wear resistance, increases the melting point and accelerates the curing speed of the cerate for the redwood furniture, so that the furniture is more wear-resistant and is more convenient to maintain.
Claims (5)
1. A wax paste for redwood furniture is characterized in that: the polyurethane adhesive comprises, by mass, 30-40 parts of beeswax, 20-30 parts of sweet orange oil, 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer, 3-5 parts of organic silicon resin, 3-5 parts of modified silicon oil, 0.5-1 part of photoinitiator, 0.015-0.02 part of antioxidant and the balance of absolute ethyl alcohol.
2. The cerate for redwood furniture according to claim 1, wherein: the adhesive is characterized by comprising, by weight, 35 parts of beeswax, 25 parts of sweet orange oil, 5 parts of a polyurethane adhesive, 3.5 parts of a plasticizer, 4 parts of an organic silicon resin, 4 parts of sulfur-based modified silicone oil, 0.75 part of a photoinitiator and 0.02 part of an antioxidant.
3. A cerate for redwood furniture as claimed in claim 1, wherein: the preparation method of the cerate for the redwood furniture comprises the following specific steps:
(1) heating beeswax in a water bath kettle at 70-80 deg.C for 2-3 hr until beeswax is completely melted, filtering liquid beeswax for 3-5 times step by step until no impurities are in beeswax, and keeping the temperature at 60-65 deg.C;
(2) preparing 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer and 0.015-0.02 part of saturated absolute ethyl alcohol solution of antioxidant according to the proportion;
(3) sequentially filling 30-40 parts of filtered beeswax, 20-30 parts of sweet orange oil, 4-6 parts of polyurethane adhesive, 2-5 parts of plasticizer and 0.015-0.02 part of antioxidant into a saturated absolute ethyl alcohol solution, 3-5 parts of organic silicon resin, 3-5 parts of modified silicon oil and 0.5-1 part of photoinitiator into an emulsifying machine preheated at 62 ℃, filling nitrogen into the emulsifying machine, slowly heating to 70-80 ℃, stirring at 700rpm for 2-4h, and observing the stirring process, and adding absolute ethyl alcohol until the stirred substance is pasty;
(4) and (4) releasing nitrogen in the emulsifying machine, cooling to normal temperature, subpackaging the cerate obtained by stirring in the step (3) and strictly storing in a dark place.
4. The cerate for redwood furniture according to claim 3, wherein: in the preparation method of the wax ointment for the redwood furniture, the beeswax is heated in a water bath at 74 ℃ for 3 hours in a water bath until the beeswax is completely melted, the liquid beeswax is filtered for 5 times step by step until no impurities exist in the beeswax, and the temperature is kept at 62 ℃.
5. The cerate for redwood furniture according to claim 3, wherein: in the preparation method of the cerate for the redwood furniture, the emulsifying machine is used for stirring for 4 hours at the stirring speed of 700rpm, the temperature in the container is 76 ℃ in the stirring process, and the container is kept in a dark state.
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| CN202010916190.7A CN111978870A (en) | 2020-09-03 | 2020-09-03 | Cerate for redwood furniture and preparation method thereof |
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| 李兴畅等: "红木家具表面"蜡"处理技术的对比性研究 ", 《家具》 * |
| 王登武等: "红木家具涂料用改性石蜡的制备与性能研究 ", 《涂料工业》 * |
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Application publication date: 20201124 |