CN111972667A - Composite agilawood leaf concentrated powder for relaxing bowel and preparation method thereof - Google Patents
Composite agilawood leaf concentrated powder for relaxing bowel and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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Abstract
The invention provides a compound agilawood leaf concentrated powder for relaxing bowel and a preparation method thereof, which comprises the following steps of (1) taking agilawood leaves, carrying out steam de-enzyming, drying, and crushing at room temperature to obtain agilawood leaf powder; (2) taking Mallotus furetianus tea, steaming, deactivating enzyme, drying, and carrying out low-temperature ultra-pulverization to obtain Mallotus furetianus tea powder; (3) taking agilawood leaf powder, mallotus oblongifolius muell-Arg powder and large leaf tea powder, respectively adding water, and heating and soaking at constant temperature; (4) filtering, and mixing 50-60 parts of agilawood leaf leaching liquor, 25-30 parts of mallotus oblongifolius tea leaching liquor and 10-25 parts of large-leaf seed tea leaching liquor according to the proportion; (5) filtering and drying to 1/12-1/8 of the original liquid volume; (6) spray drying the concentrated leaching solution to obtain compound agilawood leaf concentrated powder; the compound agilawood leaf concentrated powder product obtained by the invention has the characteristics of more convenient drinking, stable taste and good flavor, can effectively adjust intestinal flora, improves the integral purification function of a gastrointestinal system, and has milder and more obvious effect of relaxing bowel.
Description
Technical Field
The invention relates to the technical field of food processing, in particular to compound agilawood leaf concentrated powder for relaxing bowel and a preparation method thereof.
Background
The agilawood is a low-yield traditional Chinese medicine in Lingnan, has the effects of promoting qi circulation, relieving pain, warming middle energizer, stopping vomiting and absorbing qi and relieving asthma as a traditional Chinese medicine in China, and is used for treating chest and abdomen swelling pain, stomach cold, vomiting and hiccup, kidney deficiency and qi regurgitation and asthma. The agilawood leaves are non-medicinal parts of agilawood, and related researches are relatively few, and experiments show that the agilawood leaf water extract has the functions of relaxing bowels, expelling toxin, promoting sleep, reducing fat, tonifying qi and the like. However, the single eaglewood leaf water extract has limited effect on intestinal tract regulation and is not easy to store. The concentrated powder prepared from the single aquilaria sinensis leaf water extract has the defects of poor solubility, low mouthfeel, insufficient flavor, obvious astringency, limited regulating function effect on the gastrointestinal system and the like.
Disclosure of Invention
In view of the above, the invention provides a compound agilawood leaf concentrated powder for relaxing bowel and a preparation method thereof.
The technical scheme of the invention is realized as follows:
the invention provides a preparation method of composite agilawood leaf concentrated powder for relaxing bowel, which comprises the following steps:
(1) pretreatment of agilawood leaves: taking fresh agilawood leaves, deactivating enzyme under steam at 100-110 ℃, drying for 15-18 h at 55-65 ℃, crushing at room temperature, and sieving with a 40-60-mesh sieve to obtain agilawood leaf powder;
(2) pretreatment of Mallotus furetianus tea: taking fresh partridge tea leaves, deactivating enzymes under the steam of 115-120 ℃, and drying for 20-22 h at 60-75 ℃; carrying out superfine grinding on the dried Mallotus furetianus tea at the temperature of-10 to-15 ℃ for 60 to 120s, and sieving the Mallotus furetianus tea with a 100 to 120-mesh sieve to obtain Mallotus furetianus tea powder;
(3) and (3) independent leaching: taking the agilawood leaf powder, the partridge tea powder and the large-leaf seed tea powder, respectively adding water, heating and soaking at constant temperature to respectively obtain an agilawood leaf leaching liquor, a partridge tea leaching liquor and a large-leaf seed tea leaching liquor;
(4) primary filtering and mixing: filtering the leaching liquor obtained in the step (3) by a filter membrane with the diameter less than or equal to 50 microns, mixing 50-60 parts of agilawood leaf leaching liquor, 25-30 parts of mallotus oblongifolius linnaeus leaching liquor and 10-25 parts of large-leaf tea leaching liquor according to the proportion, and uniformly stirring to obtain a total mixed liquor;
(5) fine filtering and concentrating: filtering the total mixed solution by a filter membrane with the diameter less than or equal to 3.0 microns, drying the total mixed solution to 1/12-1/8 of the volume of the original liquid at the temperature of 55-65 ℃ and the pressure of 0.1-0.2 Mpa to obtain a concentrated leaching solution;
(6) spray milling: the concentrated leaching liquor is subjected to spray drying to obtain the composite agilawood leaf concentrated powder, and the obtained composite agilawood leaf concentrated powder product has the characteristics of more convenience in drinking, stable taste and good flavor, and can effectively adjust intestinal flora, improve the integral purification function of a gastrointestinal system, and achieve a milder and more remarkable bowel relaxing effect.
Further, in the step (2), the partridge tea leaves are dried until the moisture content is less than 5%, and then are subjected to superfine grinding for 80 seconds at the temperature of minus 13 ℃. The partridge tea powder with low water content is subjected to low-temperature super-grinding, so that the dissolubility of the partridge tea powder in a high-temperature leaching process is improved, effective components in the partridge tea are fully extracted to obtain a partridge tea leaching liquid, and finally, the taste and the flavor of the obtained composite eaglewood leaf concentrated powder are obviously improved.
Further, in the step (3), the agilawood powder, the mallotus oblongifolius muell-Arg powder and the large-leaf tea powder are extracted by the method that agilawood leaf powder is taken, water is added into the powder according to the material-liquid ratio of 1 (20-25) g/ml for soaking, the mixed solution is heated to 88-92 ℃, then the water temperature is controlled to be 85-95 ℃, and the constant temperature heating is continuously carried out for 30-40 min, so that an agilawood leaf extract liquid is obtained; soaking francolin tea powder in water according to the material-liquid ratio of 1 (30-35) g/ml, heating the mixed solution to 108-110 ℃, controlling the water temperature to be 105-115 ℃, and continuously heating at constant temperature for 5-10 min to obtain francolin tea leaching liquor; soaking the large leaf seed tea powder in water according to the material-liquid ratio of 1 (22-28) g/ml, heating the mixed solution to 84-86 ℃, controlling the water temperature to be 80-90 ℃, and continuously heating for 30-50 min at constant temperature to obtain a large leaf seed tea leaching solution.
The processing method comprises the steps of pretreating to obtain the eaglewood leaf powder, the partridge tea powder and the large-leaf tea powder with certain particle sizes, heating and soaking in an independent constant-temperature heating mode to be beneficial to fully dissolving and extracting active ingredients of all components to obtain different leaching solutions, and reasonably allocating the eaglewood leaf leaching solution, the partridge tea leaching solution and the large-leaf tea leaching solution in proportion, so that the taste and flavor of products are obviously improved, the fragrance and the lubrication are realized, the combined action among all the components is effectively promoted, the action unicity of intestinal tracts is avoided, the intestinal immunity is enhanced, the intestinal flora is improved, and the milder intestine moistening and bowel relaxing effects are realized.
Further, in the step (4), in the total mixed solution, the weight parts of each leaching solution are as follows: 55 parts of agilawood leaf leaching liquor, 28 parts of mallotus oblongifolius leaching liquor and 17.5 parts of large-leaf seed tea leaching liquor. The total mixed liquid is prepared by processing and mixing natural herbaceous plants of agilawood leaf, partridge tea and large-leaf tea, and the agilawood leaf leaching liquor, the partridge tea leaching liquor and the large-leaf tea leaching liquor are reasonably matched, so that the constipation relieving effect is enhanced, and the taste and the dissolution stability of the product are effectively improved.
Further, in the step (4), the leaching solutions are mixed according to a proportion and stirred for 15-25 min at the temperature of 40-70 ℃ at the speed of 350-550 r/min to obtain a total mixed solution. The blending and mixing of the components are enhanced, so that the composite agilawood leaf concentrated powder prepared by fine filtration concentration and spraying is good in liquidity, and is beneficial to brewing and easy to store.
Further, the large-leaf tea powder is obtained by kneading and twisting large-leaf tea twice, deactivating enzymes for 15-20 min respectively, drying at 55-65 ℃, crushing and sieving with a 60-80-mesh sieve.
Further, the water removing time of the agilawood leaves is 5-10 min, and the water removing time of the partridge tea is 4-8 min.
Further, the filter membrane filter diameter in the step (4) is 30-50 μm; the filter membrane in the step (5) has a filter diameter of 0.65-1.5 μm.
Further, in the step (6), the spray drying is carried out at the air inlet temperature of 140-180 ℃, the air outlet temperature of 80-95 ℃, the rotational speed of the atomizer of 260-280 r/s and the air inlet volume of 0.30-0.35 m3And preparing the concentrated extract into compound agilawood leaf concentrated powder under the condition of min.
The compound agilawood leaf concentrated powder for relaxing bowel is prepared according to the preparation method.
Compared with the prior art, the invention has the beneficial effects that: the invention is based on the matching of the agilawood leaves, the partridge tea leaves and the large-leaf tea, and obtains corresponding agilawood leaf leaching liquor, partridge tea leaching liquor and large-leaf tea leaching liquor by adopting a steam high-temperature enzyme deactivation and low-temperature crushing pretreatment combined with an independent constant-temperature heating leaching process; by utilizing a reasonable mixing mode of the leaching liquor, the flavors of the partridge tea, the large-leaf tea and the agilawood leaves are better combined, the holy fragrance of the unique compound tea fragrance is formed, the taste is moist and free of astringency, the combined action of the agilawood leaves and the partridge tea is effectively enhanced, the integral regulation function of a gastrointestinal system is further improved by combining the large-leaf tea, the gastrointestinal peristalsis is promoted, the intestinal immunity is effectively enhanced, the intestinal flora is improved, and the milder and remarkable effect of relaxing bowel is realized; and finally, the compound agilawood leaf concentrated powder obtained is good in fluidity and easy to store by combining the process treatments of primary filtering mixing, fine filtering concentration and spraying preparation, so that the compound agilawood leaf concentrated powder product which is more convenient to brew and drink, stable in taste and good in flavor, can effectively promote gastrointestinal peristalsis, adjust intestinal flora, improve the overall adjustment function of a gastrointestinal system and has a milder effect of relaxing bowel is obtained.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.
The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.
Embodiment 1-a method for preparing a compound agilawood leaf concentrated powder for relaxing bowel, comprising the following steps:
(1) pretreatment of agilawood leaves: taking fresh agilawood leaves, deactivating enzyme for 5min under steam at 100 ℃, removing surface water, drying at 55 ℃ for 15h, crushing at room temperature, and sieving with a 40-mesh sieve to obtain agilawood leaf powder;
(2) pretreatment of Mallotus furetianus tea: de-enzyming fresh Francolini pintadeani tea leaf with steam at 120 deg.C for 4min, and drying at 60 deg.C for 20 hr; carrying out superfine grinding on the dried Mallotus oblongifolius muell-Arg leaves for 60s at the temperature of-10 ℃, and sieving with a 100-mesh sieve to obtain Mallotus oblongifolius muell-Arg powder;
(3) and (3) independent leaching: putting the agilawood leaf powder into a container, adding water to soak the agilawood leaf powder according to the material-liquid ratio of 1:20g/ml, heating the mixed solution to 88 ℃, controlling the water temperature to be 85-95 ℃, and continuously heating for 30min at constant temperature to obtain an agilawood leaf leaching solution; putting the partridge tea powder into a container, adding water according to a material-liquid ratio of 1:30g/ml for soaking, heating the mixed solution to 108 ℃, controlling the water temperature to be 105-115 ℃, and continuously heating at a constant temperature for 5min to obtain a partridge tea leaching solution; putting the large leaf seed tea powder into a container, adding water according to the material-liquid ratio of 1:22g/ml for soaking, heating the mixed solution to 84 ℃, controlling the water temperature to be 80-90 ℃, and continuously heating for 30min at constant temperature to obtain a large leaf seed tea leaching solution;
wherein the large-leaf seed tea powder is prepared by kneading and twisting large-leaf seed tea twice, deactivating enzyme for 15min, drying at 55 deg.C, pulverizing at room temperature, and sieving with 60 mesh sieve;
(4) primary filtering and mixing: filtering the leaching liquor obtained in the step (3) through 30-micron filter membranes respectively, mixing 50 parts of agilawood leaf leaching liquor, 25 parts of mallotus oblongifolius leaching liquor and 10 parts of large-leaf tea leaching liquor in proportion, and stirring for 15min at the temperature of 40 ℃ at 350r/min to obtain a total mixed liquor;
(5) fine filtering and concentrating: filtering the total mixed solution with 0.65 μm filter membrane, drying at 55 deg.C and 0.1Mpa to 1/12 of original liquid volume to obtain concentrated leaching solution;
(6) spray milling: the concentrated leaching liquor is treated at the air inlet temperature of 140 ℃, the air outlet temperature of 80 ℃, the rotational speed of an atomizer of 260r/s and the air inlet amount of 0.30m3Spray drying at/min to obtain compound concentrated powder of folium Aquilariae Resinatum.
Embodiment 2-a method for preparing a compound agilawood leaf concentrated powder for relaxing bowel, comprising the following steps:
(1) pretreatment of agilawood leaves: taking fresh agilawood leaves, deactivating enzyme for 10min under steam at 110 ℃, removing surface water, drying at 65 ℃ for 18h, crushing at room temperature, and sieving with a 60-mesh sieve to obtain agilawood leaf powder;
(2) pretreatment of Mallotus furetianus tea: taking fresh Mallotus oblongifolius muell-Arg, deactivating enzyme for 8min under the steam of 115 ℃, and drying for 22h at 75 ℃; carrying out superfine grinding on the dried Mallotus oblongifolius muell-Arg leaves for 120s at the temperature of-15 ℃, and sieving with a 120-mesh sieve to obtain Mallotus oblongifolius muell-Arg powder;
(3) and (3) independent leaching: putting the agilawood leaf powder into a container, adding water to soak the agilawood leaf powder according to the material-liquid ratio of 1:25g/ml, heating the mixed solution to 92 ℃, controlling the water temperature to be 85-95 ℃, and continuously heating for 40min at constant temperature to obtain an agilawood leaf leaching solution; putting the partridge tea powder into a container, adding water according to the material-liquid ratio of 1:35g/ml for soaking, heating the mixed solution to 110 ℃, controlling the water temperature to be 105-115 ℃, and continuously heating for 10min at constant temperature to obtain partridge tea leaching liquor; putting the large leaf seed tea powder into a container, adding water according to the material-liquid ratio of 1:28g/ml for soaking, heating the mixed solution to 86 ℃, controlling the water temperature to be 80-90 ℃, and continuously heating for 50min at constant temperature to obtain a large leaf seed tea leaching solution;
wherein the large-leaf seed tea powder is prepared by kneading and twisting large-leaf seed tea twice, deactivating enzyme for 20min, drying at 65 deg.C, pulverizing at room temperature, and sieving with 80 mesh sieve;
(4) primary filtering and mixing: filtering the leaching liquor obtained in the step (3) through 50-micron filter membranes respectively, mixing 60 parts of agilawood leaf leaching liquor, 30 parts of mallotus oblongifolius Leng leaching liquor and 25 parts of large-leaf tea leaching liquor in proportion, and stirring for 25min at the temperature of 70 ℃ at 550r/min to obtain a total mixed liquor;
(5) fine filtering and concentrating: filtering the total mixed solution with 1.5 μm filter membrane, drying at 65 deg.C and 0.2Mpa to 1/8 of original liquid volume to obtain concentrated leaching solution;
(6) spray milling: the concentrated leaching liquor is treated at the air inlet temperature of 180 ℃, the air outlet temperature of 95 ℃, the rotational speed of an atomizer of 280r/s and the air inlet amount of 0.35m3Spray drying at/min to obtain compound concentrated powder of folium Aquilariae Resinatum.
Embodiment 3-a method for preparing a compound agilawood leaf concentrated powder for relaxing bowel, comprising the following steps:
(1) pretreatment of agilawood leaves: taking fresh agilawood leaves, deactivating enzyme for 8min under steam at 105 ℃, removing surface water, drying at 60 ℃ for 17h, crushing at room temperature, and sieving with a 50-mesh sieve to obtain agilawood leaf powder;
(2) pretreatment of Mallotus furetianus tea: taking fresh Mallotus furetianus tea, deactivating enzyme for 6min under 117 deg.C steam, drying at 70 deg.C until the water content is less than 5%, micronizing the dried Mallotus furetianus tea at-13 deg.C for 100s with micronizer, and sieving with 110 mesh sieve to obtain Mallotus furetianus tea powder;
(3) and (3) independent leaching: putting the agilawood leaf powder into a container, adding water to soak the agilawood leaf powder according to the material-liquid ratio of 1:22g/ml, heating the mixed solution to 90 ℃, controlling the water temperature to be 85-95 ℃, and continuously heating for 35min at constant temperature to obtain an agilawood leaf leaching solution; putting the partridge tea powder into a container, adding water for soaking according to the material-liquid ratio of 1:33g/ml, heating the mixed solution to 110 ℃, controlling the water temperature to be 105-115 ℃, and continuously heating for 7.5min at constant temperature to obtain partridge tea leaching liquor; putting the large-leaf seed tea powder into a container, adding water according to the material-liquid ratio of 1:25g/ml for soaking, heating the mixed solution to 85 ℃, controlling the water temperature to be 80-90 ℃, and continuously heating for 40min at constant temperature to obtain a large-leaf seed tea leaching solution;
wherein the large-leaf seed tea powder is prepared by kneading and twisting large-leaf seed tea twice, deactivating enzyme for 18min, drying at 60 deg.C, pulverizing at room temperature, and sieving with 70 mesh sieve;
(4) primary filtering and mixing: filtering the leaching liquor obtained in the step (3) through 40-micron filter membranes respectively, mixing 55 parts of agilawood leaf leaching liquor, 28 parts of mallotus oblongifolius Leng leaching liquor and 17.5 parts of large-leaf tea leaching liquor in proportion, and stirring for 20min at the temperature of 55 ℃ at 450r/min to obtain a total mixed liquor;
(5) fine filtering and concentrating: filtering the total mixed solution with 1.15 μm filter membrane, drying at 60 deg.C and 0.15Mpa to 1/10 of original liquid volume to obtain concentrated leaching solution;
(6) spray milling: the concentrated leaching liquor is treated at the air inlet temperature of 160 ℃, the air outlet temperature of 88 ℃, the rotation speed of an atomizer of 270r/s and the air inlet amount of 0.32m3Spray drying at/min to obtain compound concentrated powder of folium Aquilariae Resinatum.
Comparative example 1-preparation method of a compound agilawood leaf concentrated powder for relaxing bowel according to example 3, the difference is that: drying the de-enzymed partridge tea leaves until the water content is 10%, crushing at room temperature, and sieving with a 110-mesh sieve to obtain partridge tea powder; the remaining steps were the same as in example 3.
Comparative example 2-preparation method of a composite agilawood leaf concentrated powder for relaxing bowel according to example 3, the difference is that: in the step (3), the weight portions are as follows: directly mixing 55 parts of agilawood leaf powder, 28 parts of partridge tea powder and 17.5 parts of large leaf seed tea powder, adding water to soak the mixture according to the material-liquid ratio of 1:25g/ml, heating the mixed solution to 90 ℃, controlling the water temperature to be continuously heated at the constant temperature of 85-95 ℃ for 35min to obtain a mixed leaching solution, sequentially filtering the mixed leaching solution through a 40-micron filter membrane and a 1.15-micron filter membrane, and concentrating, wherein the rest steps are the same as the step in the embodiment 3.
Comparative example 3-preparation method of compound agilawood leaf concentrated powder for relaxing bowel according to example 3, the difference is that: in the step (4), the total mixed liquid only comprises the following components in parts by weight: 83 parts of agilawood leaf leaching liquor and 17.5 parts of big-leaf tea leaching liquor, and the rest steps are the same as example 3.
Comparative example 4-method for preparing a compound agilawood leaf concentrated powder for relaxing bowel according to example 3, the difference is that: in the step (4), all the leaching solutions are mixed according to a proportion, stirred for 20min at the normal temperature at 450r/min to obtain a total mixed solution, and the total mixed solution is directly sprayed and prepared into powder after being filtered by a filter membrane with the diameter of 1.15 mu m, and the rest steps are the same as those of the embodiment 3.
1. Sensory evaluation was performed on the composite type eaglewood leaf concentrated powder obtained in each of the examples and comparative examples.
The compound agilawood leaf concentrated powder of the embodiment and the comparative example is subjected to sensory evaluation by randomly extracting 20 persons from the population with professional sensory evaluation experience, and the evaluation criteria are as follows:
the brewing method comprises the following steps: soaking compound agilawood leaf concentrated powder and 100 ℃ boiled water for 5min according to the material-liquid ratio of 10:500 g/ml.
The sensory evaluation results of the compound agilawood leaf concentrated powder are as follows:
according to the sensory evaluation results in the table above, the compound agilawood leaf concentrated powder prepared by the invention has the advantages of full taste, smooth taste without astringent taste, stable color and luster, and unique holy basil fragrance of compound tea fragrance. Compared with the comparative examples 1 and 4, the embodiment 3 has the advantages that the low-temperature superfine grinding of the partridge tea leaves with low water content is beneficial to improving the solubility of the partridge tea powder in the high-temperature leaching process, so that the effective components in the partridge tea leaves are fully extracted, and the taste and flavor of the obtained compound agilawood leaf concentrated powder are obviously improved; and the mixing, stirring and concentration treatment are carried out at a certain temperature, so that the blending and mixing among the components are favorably enhanced, and the composite agilawood leaf concentrated powder prepared by fine filtration concentration and spraying is good in fluidity, and is favorable for brewing and easy to store. Compared with the comparative examples 2 and 3, the embodiment 3 shows that the combined taste and flavor of the Mallotus furetianus, the big-leaf tea and the agilawood leaves are favorably improved by combining the low-temperature crushing pretreatment with the independent constant-temperature heating leaching process and utilizing the reasonable blending mode of the leaching liquor, and the combined taste and flavor of the Mallotus furetianus, the big-leaf tea and the agilawood leaves are free from astringent retention, smooth, transparent in color and strong in smell.
2. Composite agilawood leaf concentrated powder bowel relaxing function experiment
(1) Establishment of Slow Transit Constipation (STC) animal model
Adult healthy male mice were selected, weighing 20 mice (20. + -.2) g.
The test pieces were divided into model control group and blank control group, each group containing 10 animals. The model control group was gavage with 5mg/kg.BW of loperamide hydrochloride every day, and the blank control group was fed normally for 7 days. On the 7 th day, after the model control group is filled with loperamide hydrochloride for 30min, the model control group and the blank control group are filled with stomach ink (the stomach filling amount of the ink is 0.2 ml/piece), and compared with the blank control group, the model control group obviously has the phenomena of prolonged defecation time and reduced defecation grain number; and (3) killing the mice after the ink is infused for 25-30 min, comparing the ink propulsion rates of the two groups of mice, and judging that the model building is successful if the small intestine ink propulsion rate of the model control group of mice is obviously reduced.
(2) Influence of compound agilawood leaf concentrated powder on gastrointestinal driving force of STC mice
Adult healthy male mice were selected, weighing (20. + -.2) g, and divided into 5 groups of 10 mice each.
The 5 groups are respectively: 2 experimental groups, model control group, positive control group and blank control group with high dose and low dose.
The method comprises the following specific steps:
2 experimental groups at both high and low doses: dissolving 0.5g of compound agilawood leaf concentrated powder (prepared in example 3) in 100ml of distilled water to serve as a low-dose liquid medicine; dissolving 2.5g of compound agilawood leaf concentrated powder in 100ml of distilled water to be used as high-dose liquid medicine; on the basis of normal feeding, per stomach is irrigated with 0.6ml of the low-dose liquid medicine/high-dose liquid medicine and 5mg/kg of loperamide hydrochloride for 14 days;
positive control group: dissolving 2g fructus Cannabis pill in 100ml distilled water as positive control liquid medicine; on the basis of normal feeding, performing intragastric administration on 0.6ml of the positive control liquid medicine and 5mg/kg of loperamide hydrochloride for 14 days every day;
model control group: the feed is normally fed, and the stomach is drenched with 0.6 ml/pig of distilled water and 5mg/kg.BW of loperamide hydrochloride every day for 14 days.
Blank control group: feeding normally, and feeding with 0.6 ml/per stomach distilled water every day for 14 days;
during the period, daily records:
weight change, food intake and water intake of the mice;
② observing the health condition and mental state of the mouse and various physiological activities. Stool color and shape;
③ the number of the defecation grains, the water content of the excrement and the dry weight of the excrement.
On day 14, the gavage was performed 30min after gavage with loperamide hydrochloride. After a further 30min (i.e. the ink was gavage for 30min) the mice were sacrificed.
Opening the intestinal cavity to separate mesentery, cutting the intestinal canal from pylorus, lower end to ileocecal part, placing on a tray, slightly drawing the small intestine into a straight line, measuring the length of the intestinal canal as the total length of the small intestine, and measuring the length of the intestinal canal from the pylorus to the front edge of ink as the advancing length of the ink.
The ink propulsion rate was calculated as follows:
the ink propulsion rate (%) — the ink propulsion length (cm)/total small intestine length (cm) × 100%. (ii) a
Results of the experiment
TABLE 1 influence of the concentrated powder of the compound eaglewood leaves on the intestinal motility (mean value)
And (4) conclusion:
the ink propulsion rate of each dosage group of the sample is obviously different from that of a model control group (P <0.01), and the high dosage group and a positive control group are not obviously different (P >0.05), so that the compound agilawood leaf concentrated powder can obviously promote the intestinal peristalsis of a tested animal and enables feces to be discharged out of the body more quickly.
In addition: under the same experimental conditions as above, the results of the tests of the examples and the comparative examples are as follows:
as can be seen from the table above, the compound agilawood leaf concentrated powder for relaxing bowel, prepared by the invention, has a good effect of promoting intestinal peristalsis. Compared with the comparative examples 2 and 3, the embodiment 3 has the advantages that the agilawood leaf leaching liquor and the partridge tea leaching liquor are combined to synergistically promote intestinal peristalsis, so that a milder and effective bowel relaxing effect is realized, meanwhile, the combined action of the agilawood leaf and the partridge tea can be further enhanced through an independent constant-temperature heating leaching process and a reasonable blending mode of the leaching liquors, the intestinal peristalsis is effectively promoted by combining the large-leaf seed tea, and the remarkable and efficient bowel relaxing effect is achieved.
3. The compound agilawood leaf concentrated powder obtained in the examples and the comparative examples respectively was subjected to clinical efficacy tests.
The experimental method comprises the following steps: randomly selecting 210 habitual constipation patients, 75 men patients and 65 women patients, wherein the patients are 8-70 old and clinically show symptoms of constipation, difficult defecation, hard feces, incomplete defecation, long defecation interval time and the like, and randomly dividing the patients into 7 groups;
the treatment method comprises the following steps: the compound agilawood leaf concentrated powder is brewed with boiled water every day, and 10 days of continuous drinking is a treatment course;
the curative effect standard is as follows: the effect is shown: the symptoms of constipation and difficult defecation disappear, and the defecation is smooth every day and is continuously kept for more than 2 weeks; the method has the following advantages: the symptoms of constipation and difficult defecation are relieved, and the defecation is more than 5 times per week but the difficult defecation sometimes occurs; and (4) invalidation: the symptoms of constipation and difficult defecation are not improved.
The above table shows that the compound agilawood leaf concentrated powder for relaxing bowel, prepared by the invention, has the advantages of unique holy fragrance of compound tea fragrance, moist mouthfeel, no astringent taste, good effect of relaxing bowel, total effective rate of 100% and significant efficiency of more than 80%. Compared with the comparative examples 2 and 3, the total significant efficiency reduction in the comparative examples 2 and 3 can be seen, and the fact that the combination of the eaglewood leaf leaching liquor and the francolin tea leaching liquor is adopted by the invention is shown, the self-regulation function of a gastrointestinal system can be better and synergistically regulated, the intestinal flora can be regulated, the gastrointestinal peristalsis is promoted, the intestinal immunity is enhanced, and the milder and more efficient bowel relaxing effect is realized.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. A preparation method of compound agilawood leaf concentrated powder for relaxing bowel is characterized by comprising the following steps:
(1) pretreatment of agilawood leaves: taking fresh agilawood leaves, deactivating enzyme under steam at 100-110 ℃, drying for 15-18 h at 55-65 ℃, crushing at room temperature, and sieving with a 40-60-mesh sieve to obtain agilawood leaf powder;
(2) pretreatment of Mallotus furetianus tea: taking fresh partridge tea leaves, deactivating enzymes under the steam of 115-120 ℃, and drying for 20-22 h at 60-75 ℃; carrying out superfine grinding on the dried Mallotus furetianus tea at the temperature of-10 to-15 ℃ for 60 to 120s, and sieving the Mallotus furetianus tea with a 100 to 120-mesh sieve to obtain Mallotus furetianus tea powder;
(3) and (3) independent leaching: taking the agilawood leaf powder, the partridge tea powder and the large-leaf seed tea powder, respectively adding water, heating and soaking at constant temperature to respectively obtain an agilawood leaf leaching liquor, a partridge tea leaching liquor and a large-leaf seed tea leaching liquor;
(4) primary filtering and mixing: filtering the leaching liquor obtained in the step (3) by a filter membrane with the diameter less than or equal to 50 microns, mixing 50-60 parts of agilawood leaf leaching liquor, 25-30 parts of mallotus oblongifolius linnaeus leaching liquor and 10-25 parts of large-leaf tea leaching liquor according to the proportion, and uniformly stirring to obtain a total mixed liquor;
(5) fine filtering and concentrating: filtering the total mixed solution by a filter membrane with the diameter less than or equal to 3.0 microns, drying the total mixed solution to 1/12-1/8 of the volume of the original liquid at the temperature of 55-65 ℃ and the pressure of 0.1-0.2 Mpa to obtain a concentrated leaching solution;
(6) spray milling: and (4) carrying out spray drying on the concentrated leaching solution to obtain compound agilawood leaf concentrated powder.
2. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: in the step (2), the partridge tea leaves are dried until the water content is less than 5 percent, and then are subjected to superfine grinding for 80 seconds at the temperature of minus 13 ℃.
3. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: in the step (3), the extraction method of the agilawood powder, the partridge tea powder and the large leaf seed tea powder comprises the following steps of,
soaking the agilawood leaf powder in water according to the material-liquid ratio of 1 (20-25) g/ml, heating the mixed solution to 88-92 ℃, controlling the water temperature to be 85-95 ℃, and continuously heating for 30-40 min at constant temperature to obtain an agilawood leaf leaching solution; soaking francolin tea powder in water according to the material-liquid ratio of 1 (30-35) g/ml, heating the mixed solution to 108-110 ℃, controlling the water temperature to be 105-115 ℃, and continuously heating at constant temperature for 5-10 min to obtain francolin tea leaching liquor; soaking the large leaf seed tea powder in water according to the material-liquid ratio of 1 (22-28) g/ml, heating the mixed solution to 84-86 ℃, controlling the water temperature to be 80-90 ℃, and continuously heating for 30-50 min at constant temperature to obtain a large leaf seed tea leaching solution.
4. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 3, wherein the preparation method comprises the following steps: in the step (4), in the total mixed liquid, the weight parts of each leaching solution are as follows: 55 parts of agilawood leaf leaching liquor, 28 parts of mallotus oblongifolius leaching liquor and 17.5 parts of large-leaf seed tea leaching liquor.
5. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 4, wherein the preparation method comprises the following steps: in the step (4), the leaching solutions are mixed in proportion and stirred for 15-25 min at the temperature of 40-70 ℃ at the speed of 350-550 r/min to obtain a total mixed solution.
6. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: the large-leaf tea powder is prepared by kneading and twisting large-leaf tea twice, deactivating enzymes for 15-20 min respectively, drying at 55-65 ℃, crushing and sieving with a 60-80-mesh sieve.
7. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: the water removing time of the agilawood leaves is 5-10 min, and the water removing time of the partridge tea is 4-8 min.
8. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: in the step (4), the filter membrane filtration diameter is 30-50 μm; in the step (5), the filter diameter of the filter membrane is 0.65-1.5 μm.
9. The preparation method of the compound agilawood leaf concentrated powder for relaxing bowel according to claim 1, wherein the preparation method comprises the following steps: in the step (6), the spray drying is carried out at the air inlet temperature of 140-180 ℃, the air outlet temperature of 80-95 ℃, the rotation speed of an atomizer of 260-280 r/s and the air inlet amount of 0.30-0.35 m3And preparing the concentrated extract into compound agilawood leaf concentrated powder at the min condition.
10. The compound agilawood leaf concentrated powder for relaxing bowel, prepared by the preparation method according to any one of claims 1 to 9.
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