CN111958734A - Antique treatment method for antique wicker-woven artware - Google Patents

Antique treatment method for antique wicker-woven artware Download PDF

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Publication number
CN111958734A
CN111958734A CN202010600389.9A CN202010600389A CN111958734A CN 111958734 A CN111958734 A CN 111958734A CN 202010600389 A CN202010600389 A CN 202010600389A CN 111958734 A CN111958734 A CN 111958734A
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Prior art keywords
parts
willow
wicker
dried
clear water
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Chinese (zh)
Inventor
徐蓝天
徐艳云
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Anhui Sanhe Crafts Co ltd
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Anhui Sanhe Crafts Co ltd
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Priority to CN202010600389.9A priority Critical patent/CN111958734A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27MWORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M1/00Working of wood not provided for in subclasses B27B - B27L, e.g. by stretching
    • B27M1/08Working of wood not provided for in subclasses B27B - B27L, e.g. by stretching by multi-step processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27JMECHANICAL WORKING OF CANE, CORK, OR SIMILAR MATERIALS
    • B27J1/00Mechanical working of cane or the like
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/34Organic impregnating agents
    • B27K3/36Aliphatic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/0015Treating of wood not provided for in groups B27K1/00, B27K3/00 by electric means
    • B27K5/002Electric discharges, plasma
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/04Combined bleaching or impregnating and drying of wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/002Cane, bamboo
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27MWORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M1/00Working of wood not provided for in subclasses B27B - B27L, e.g. by stretching
    • B27M1/06Working of wood not provided for in subclasses B27B - B27L, e.g. by stretching by burning or charring, e.g. cutting with hot wire

Abstract

The invention discloses an antique treatment method of an antique wicker-woven handicraft, which comprises the following steps: removing branches, leaves and peels of willow stems, naturally ventilating and airing, and then placing in a reaction kettle for reaction; taking out willow rattan, placing in a drying oven, and drying, wherein irregular scratches and grooves are formed on the surface of the willow rattan through a file, a scraper and a cutter; the willow rattan is hung in a plasma treatment box and subjected to low-temperature plasma treatment; taking out willow rattan from the plasma treatment box, and placing the willow rattan in a fermentation tank for fermentation; weaving willow rattans into a willow-woven artwork; cleaning the wicker handicraft with clear water, drying the wicker handicraft in a drying box, and then dyeing the wicker handicraft in a dyeing tank; taking out the wickerwork from the dyeing tank, draining, and burning the surface of the wickerwork by flame; after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying box for drying, and then put into a warehouse after surface grinding, varnish coating, polishing and waxing. The wicker handicraft treated by the method can permanently emit light plant fragrance, and has the advantages of long service life and good antique effect.

Description

Antique treatment method for antique wicker-woven artware
Technical Field
The invention belongs to the technical field of wicker processes, and particularly relates to an antique treatment method of an antique wicker handicraft.
Background
Wickerwork is one of the traditional handicraft articles in China, and is only used as a common daily practical article in ancient times, and the wickerwork is gradually made up until decades after the 20 th century and also gradually becomes an export-earning project in parts of China. The wicker is soft and easy to bend, uniform in thickness and elegant in color, and various simple, natural, attractive in appearance, light and durable practical artworks can be woven through a novel design. The wicker products are handcrafts widely distributed among China, and due to wide raw material sources, the wicker products are abundant around the country, and the processing technology of the wicker products is stricter and stricter along with the increase of market demands.
The wicker handicraft is mostly used for household decoration handicrafts, the existing handicrafts often have the defect of poor color, so that the wicker handicraft is not attractive in appearance and cannot play a role in decoration, and the most fundamental reason of the problems is that the wicker is not treated sufficiently, so that the color of the wicker is monotonous, and the overall appearance of the handicraft is influenced. Meanwhile, the existing artware has no fragrance, and if the artware can emit fragrance, the artware can be certainly favored by the market.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides an antique treatment method of an antique wicker handicraft.
The invention is realized by the following technical scheme:
an antique treatment method of antique wicker artware is characterized in that: the method comprises the following steps:
1) removing branches, leaves and peels of willow stems, naturally ventilating and airing for 1-3 days, airing and then placing in a reaction kettle, containing a soaking solution, and reacting for 1-2 hours at the temperature of 160-180 ℃;
2) taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 25-30%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 400-500W, wherein the duration of each time of plasma generation of the plasma generating device is 3-5s, the interval between two times of plasma generation is 2-4s, and the total plasma processing time is 10-15 times;
4) taking out willow rattan from the plasma treatment box, placing into a fermentation tank, placing fermentation material in the fermentation tank, burying willow rattan in the fermentation material, controlling the temperature of the fermentation tank at 35-45 deg.C, fermenting for 10-15 days, taking out, and naturally drying;
5) step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 6-8%, placing the dried wicker handicraft in a dyeing tank for dyeing, placing dye in the dyeing tank, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing tank for 10-15 h;
7) taking out the wicker handicraft from the dyeing pool, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 150-;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 13-15%, and then put into a warehouse after surface grinding, varnish coating, polishing and waxing.
Preferably, in the step 1), the soak solution is prepared from ethanol, acetone, sulfuric acid and clear water, and is prepared by mixing, stirring and placing 6-8 parts of ethanol, 2-7 parts of acetone, 1-2 parts of sulfuric acid and 100 parts of clear water in a reaction kettle, then pouring clear water into the reaction kettle for stirring, and finally slowly adding sulfuric acid for stirring until the mixture is uniformly stirred.
Preferably, in the step 4), the fermentation material is prepared from pond bottom sludge, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the pond bottom sludge is 70-80 parts, the biogas residues are 20-25 parts, the dried pine needles are 5-8 parts, the dried chestnut shells are 6-10 parts, the dried lychee shells are 3-6 parts, the dried lotus leaves are 5-8 parts, the clear water is 100 parts, and the water content of the pond bottom sludge is 60-70%;
the preparation process of the fermentation material comprises the following steps: pulverizing dried folium Pini, dried chestnut shell, dried litchi shell, and dried folium Nelumbinis, sieving with 80-100 mesh sieve, mixing with sludge and biogas residue at the bottom of pond, adding clear water, stirring, and standing for 1-2 hr.
Preferably, in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, litchi shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by weight, wherein 3-6 parts of carbon powder, 6-8 parts of bronze powder, 2-6 parts of chestnut shells, 3-5 parts of litchi shells, 5-7 parts of orange peels, 2-4 parts of iron oxide yellow, 3-5 parts of iron oxide red, 1-2 parts of sodium bicarbonate, 0.5-0.8 part of titanium dioxide, 6-8 parts of acetone, 2-4 parts of acetic acid, 10-13 parts of ethanol and clear water, the carbon powder, bronze powder, chestnut shells, litchi shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate and titanium dioxide are mixed, stirred and put into a ball mill for ball milling, sieving with 160-fold 200-mesh sieve to obtain dyeing powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyeing powder, mixing and stirring until the mixture is uniformly stirred to obtain the dye.
The working principle of the invention is as follows:
1) the invention adopts the soak solution to treat the surface of the willow rattan, thereby generating micropores on the surface of the willow rattan;
2) irregular scratches and grooves are formed on the surfaces of the willow rattans by a file, a scraper and a cutter, and black scars are left on the scratches and the grooves after treatment, so that the purpose of archaizing is achieved, and the primitive and primitive odour of the willow rattans is increased;
3) performing low-temperature plasma treatment to enable willow rattans to form a black carbon layer with an irregular shape and increase primitive odour of the willow rattans;
4) during fermentation, materials with deep color and certain fragrance are added, so that the wicker handicraft can emit fragrance in the later use process.
5) Through dyeing, the wicker handicraft is finally reddish brown, and the antique effect is achieved.
Compared with the prior art, the invention has the beneficial effects that:
1) when the wicker handicraft processed by the method is used at home, the wicker handicraft can permanently emit light plant fragrance;
2) after fermentation treatment, the internal structure of the willow rattan can be effectively improved, so that the willow woven handicraft is firm in structure and long in service life;
3) the wicker handicraft treated by the method has thick primitive and simple flavor and achieves the effect of antiquing.
Detailed Description
An antique treatment method of antique wicker artware is characterized in that: the method comprises the following steps:
1) removing branches, leaves and peels of willow stems, naturally ventilating and airing for 1-3 days, airing and then placing in a reaction kettle, containing a soaking solution, and reacting for 1-2 hours at the temperature of 160-180 ℃;
2) taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 25-30%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 400-500W, wherein the duration of each time of plasma generation of the plasma generating device is 3-5s, the interval between two times of plasma generation is 2-4s, and the total plasma processing time is 10-15 times;
4) taking out willow rattan from the plasma treatment box, placing into a fermentation tank, placing fermentation material in the fermentation tank, burying willow rattan in the fermentation material, controlling the temperature of the fermentation tank at 35-45 deg.C, fermenting for 10-15 days, taking out, and naturally drying;
5) step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 6-8%, placing the dried wicker handicraft in a dyeing tank for dyeing, placing dye in the dyeing tank, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing tank for 10-15 h;
7) taking out the wicker handicraft from the dyeing pool, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 150-;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 13-15%, and then put into a warehouse after surface grinding, varnish coating, polishing and waxing.
Preferably, in the step 1), the soak solution is prepared from ethanol, acetone, sulfuric acid and clear water, and is prepared by mixing, stirring and placing 6-8 parts of ethanol, 2-7 parts of acetone, 1-2 parts of sulfuric acid and 100 parts of clear water in a reaction kettle, then pouring clear water into the reaction kettle for stirring, and finally slowly adding sulfuric acid for stirring until the mixture is uniformly stirred.
Preferably, in the step 4), the fermentation material is prepared from pond bottom sludge, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the pond bottom sludge is 70-80 parts, the biogas residues are 20-25 parts, the dried pine needles are 5-8 parts, the dried chestnut shells are 6-10 parts, the dried lychee shells are 3-6 parts, the dried lotus leaves are 5-8 parts, the clear water is 100 parts, and the water content of the pond bottom sludge is 60-70%;
the preparation process of the fermentation material comprises the following steps: pulverizing dried folium Pini, dried chestnut shell, dried litchi shell, and dried folium Nelumbinis, sieving with 80-100 mesh sieve, mixing with sludge and biogas residue at the bottom of pond, adding clear water, stirring, and standing for 1-2 hr.
Preferably, in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, litchi shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by weight, wherein 3-6 parts of carbon powder, 6-8 parts of bronze powder, 2-6 parts of chestnut shells, 3-5 parts of litchi shells, 5-7 parts of orange peels, 2-4 parts of iron oxide yellow, 3-5 parts of iron oxide red, 1-2 parts of sodium bicarbonate, 0.5-0.8 part of titanium dioxide, 6-8 parts of acetone, 2-4 parts of acetic acid, 10-13 parts of ethanol and clear water, the carbon powder, bronze powder, chestnut shells, litchi shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate and titanium dioxide are mixed, stirred and put into a ball mill for ball milling, sieving with 160-fold 200-mesh sieve to obtain dyeing powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyeing powder, mixing and stirring until the mixture is uniformly stirred to obtain the dye.
Example 1
1) Removing branches, leaves and peels of willow stems, naturally ventilating and airing for 1 day, airing, putting the aired willow stems into a reaction kettle, containing a soaking solution in the reaction kettle, and reacting for 1-2 hours at the temperature of 160 ℃;
in the step 1), the soak solution is prepared from 6 parts by weight of ethanol, 2 parts by weight of acetone, 1 part by weight of sulfuric acid and 100 parts by weight of clear water, and the ethanol and the acetone are mixed, stirred, placed in a reaction kettle and stirred, then poured with the clear water and stirred, and finally the sulfuric acid is slowly added and stirred until the mixture is uniformly stirred.
2) Taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 25%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 400W, enabling the plasma generating device to generate plasma for 3s each time, enabling the interval between two times of generation of plasma to be 2s, and enabling the total plasma processing times to be 10;
4) taking out willow rattan from the plasma treatment box, placing the willow rattan in a fermentation tank, placing a fermentation material in the fermentation tank, burying the willow rattan in the fermentation material, controlling the temperature of the fermentation tank at 35 ℃, taking out the willow rattan after fermenting for 10 days, and naturally drying the willow rattan;
in the step 4), the fermentation material is prepared from pond bottom sludge, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the pond bottom sludge comprises 70 parts, the biogas residues comprise 20 parts, 5 parts of the dried pine needles, 6 parts of the dried chestnut shells, 3 parts of the dried lychee shells, 5 parts of the dried lotus leaves and 100 parts of the clear water, and the water content of the pond bottom sludge is 60%;
the preparation process of the fermentation material comprises the following steps: crushing the dried pine needles, the dried chestnut shells, the dried lychee shells and the dried lotus leaves by a crusher, sieving by a 80-mesh sieve, uniformly mixing with sludge and biogas residues at the bottom of a pond, finally adding clear water, uniformly stirring, and standing for 1 h.
5) Step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 6%, placing the dried wicker handicraft in a dyeing pool for dyeing, placing dye in the dyeing pool, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing pool for 10 hours;
in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, lychee shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by mass, the preparation method comprises the steps of mixing and stirring carbon powder, bronze powder, chestnut shell, sodium bicarbonate 1 part, titanium dioxide 0.5 part, acetone 6 part, acetic acid 2 part, ethanol 10 part and clear water part, putting the mixture into a ball mill for ball milling, sieving by a 160-mesh sieve to obtain dyeing powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyeing powder, mixing and stirring until the mixture is uniform, and obtaining the dye.
7) Taking out the wicker handicraft from the dyeing tank, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 150 ℃, and burning for 10 min;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 13%, and then the wicker handicraft is put into a warehouse after surface grinding, varnish coating, polishing and waxing.
The wicker handicraft processed by the method is dark reddish brown, bright in color and simple, black strip-shaped and spot-shaped traces are distributed on the wicker handicraft, the bending resistance reaches 152N, the appearance is attractive, and the craft cabinet can emit heavy fragrance for a long time.
Example 2
1) Removing branches, leaves and peels of willow stems, naturally ventilating and airing for 3 days, airing, placing in a reaction kettle, containing a soaking solution, and reacting for 2 hours at the temperature of 180 ℃;
in the step 1), the soak solution is prepared from 8 parts by weight of ethanol, 7 parts by weight of acetone, 2 parts by weight of sulfuric acid and 100 parts by weight of clear water, and the ethanol and the acetone are mixed, stirred, placed in a reaction kettle, poured with the clear water and stirred, and finally slowly added with the sulfuric acid and stirred until the mixture is uniformly stirred.
2) Taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 30%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 500W, enabling the plasma generating device to generate plasma for 5s each time, enabling the interval between two times of generation of plasma to be 4s, and enabling the total number of times of plasma processing to be 15;
4) taking out willow rattans from the plasma treatment box, placing the willow rattans in a fermentation tank, placing a fermentation material in the fermentation tank, burying the willow rattans in the fermentation material, controlling the temperature of the fermentation tank at 45 ℃, taking out the willow rattans after fermenting for 15 days, and naturally drying the willow rattans;
in the step 4), the fermentation material is prepared from sludge at the bottom of the pond, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the sludge at the bottom of the pond is 80 parts, the biogas residues are 25 parts, the dried pine needles are 8 parts, the dried chestnut shells are 10 parts, the dried lychee shells are 6 parts, the dried lotus leaves are 8 parts and the clear water is 100 parts, and the water content of the sludge at the bottom of the pond is 70%;
the preparation process of the fermentation material comprises the following steps: crushing the dried pine needles, the dried chestnut shells, the dried lychee shells and the dried lotus leaves by a crusher, sieving by a 100-mesh sieve, uniformly mixing with sludge and biogas residues at the bottom of a pond, finally adding clear water, uniformly stirring, and standing for 2 hours.
5) Step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 8%, placing the dried wicker handicraft in a dyeing pool for dyeing, placing dye in the dyeing pool, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing pool for 15 hours;
in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, lychee shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by mass, the preparation method comprises the following steps of mixing and stirring carbon powder, bronze powder, chestnut shell, sodium bicarbonate, 0.8 part of titanium dioxide, 8 parts of acetone, 4 parts of acetic acid, 13 parts of ethanol and clear water, putting the mixture into a ball mill for ball milling, sieving by a 200-mesh sieve to obtain dyeing powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyeing powder, mixing and stirring until the mixture is uniform, and obtaining the dye.
7) Taking out the wicker handicraft from the dyeing tank, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 180 ℃, and burning for 15 min;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 15%, and then the wicker handicraft is put into a warehouse after surface grinding, varnish coating, polishing and waxing.
The wicker handicraft processed by the method is dark reddish brown, bright in color and simple, black strip-shaped and spot-shaped traces are distributed on the wicker handicraft, the bending resistance reaches 144N, the appearance is attractive, and the craft cabinet can emit strong fragrance for a long time.
Example 3
1) Removing branches, leaves and peels of willow stems, naturally ventilating and airing for 2 days, airing, placing in a reaction kettle, containing a soaking solution, and reacting at the temperature of 170 ℃ for 1.5 hours;
in the step 1), the soak solution is prepared from 7 parts by weight of ethanol, 4.5 parts by weight of acetone, 1.5 parts by weight of sulfuric acid and 100 parts by weight of clear water, and the ethanol and the acetone are mixed and stirred in a reaction kettle, then the clear water is poured in the reaction kettle for stirring, and finally the sulfuric acid is slowly added in the reaction kettle for stirring until the mixture is uniformly stirred.
2) Taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 27.5%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 450W, enabling the plasma generating device to generate plasmas for 4s each time, enabling the interval between two times of generation of plasmas to be 3s, and enabling the total number of times of plasma processing to be 13;
4) taking out willow rattans from the plasma treatment box, placing the willow rattans in a fermentation tank, placing a fermentation material in the fermentation tank, burying the willow rattans in the fermentation material, controlling the temperature of the fermentation tank at 40 ℃, taking out the willow rattans after fermenting for 13 days, and naturally drying the willow rattans;
in the step 4), the fermentation material is prepared from pond bottom sludge, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the pond bottom sludge is 75 parts, the biogas residues are 23 parts, the dried pine needles are 6.5 parts, the dried chestnut shells are 8 parts, the dried lychee shells are 4.5 parts, the dried lotus leaves are 6.5 parts and the clear water is 100 parts, and the water content of the pond bottom sludge is 65%;
the preparation process of the fermentation material comprises the following steps: crushing the dried pine needles, the dried chestnut shells, the dried lychee shells and the dried lotus leaves by a crusher, sieving by a 90-mesh sieve, uniformly mixing with sludge and biogas residues at the bottom of a pond, finally adding clear water, uniformly stirring, and standing for 1.5 hours.
5) Step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 7%, placing the dried wicker handicraft in a dyeing pool for dyeing, placing dye in the dyeing pool, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing pool for 12.5 hours;
in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, lychee shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by mass, the preparation method comprises the following steps of mixing and stirring carbon powder, bronze powder, chestnut shell, litchi shell, 3 parts of orange peel, 3 parts of iron oxide yellow, 4 parts of iron oxide red, 1.5 parts of sodium bicarbonate, 0.6 part of titanium dioxide, 7 parts of acetone, 3 parts of acetic acid, 11.5 parts of ethanol and clear water, putting the mixture into a ball mill for ball milling, sieving by a 180-mesh sieve to obtain dyed powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyed powder, mixing and stirring until the mixture is uniformly stirred to obtain the dye.
7) Taking out the wicker handicraft from the dyeing tank, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 165 ℃ and the burning time to be 12.5 min;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 14%, and then the wicker handicraft is put into a warehouse after surface grinding, varnish coating, polishing and waxing.
The wicker handicraft processed by the method is dark reddish brown, bright in color and simple, black strip-shaped and spot-shaped traces are distributed on the wicker handicraft, the bending resistance reaches 132N, the appearance is attractive, and the craft cabinet can emit heavy fragrance for a long time.
The technical solution of the present invention is only exemplary described, and it is obvious that the specific implementation of the present invention is not limited by the above-mentioned manner, and it is within the protection scope of the present invention as long as various insubstantial modifications are made by using the method concept and technical solution of the present invention, or the inventive concept and technical solution are directly applied to other occasions without modifications.

Claims (4)

1. An antique treatment method of antique wicker artware is characterized in that: the method comprises the following steps:
1) removing branches, leaves and peels of willow stems, naturally ventilating and airing for 1-3 days, airing and then placing in a reaction kettle, containing a soaking solution, and reacting for 1-2 hours at the temperature of 160-180 ℃;
2) taking out willow rattans from the reaction kettle, placing the willow rattans in a drying box, drying until the water content is 25-30%, taking out the willow rattans, and forming irregular scratches and grooves on the surfaces of the willow rattans through a file, a scraper and a cutter;
3) suspending the willow rattan processed in the step 2) in a plasma processing box, adjusting the power of a low-temperature plasma generating device to 400-500W, wherein the duration of each time of plasma generation of the plasma generating device is 3-5s, the interval between two times of plasma generation is 2-4s, and the total plasma processing time is 10-15 times;
4) taking out willow rattan from the plasma treatment box, placing into a fermentation tank, placing fermentation material in the fermentation tank, burying willow rattan in the fermentation material, controlling the temperature of the fermentation tank at 35-45 deg.C, fermenting for 10-15 days, taking out, and naturally drying;
5) step 4), weaving the willow rattans into a willow woven artwork after the treatment;
6) cleaning the wicker handicraft with clear water, placing the wicker handicraft in a drying box, drying the wicker handicraft until the water content is 6-8%, placing the dried wicker handicraft in a dyeing tank for dyeing, placing dye in the dyeing tank, continuously stirring the dye in the dyeing process, and soaking the dye in the dyeing tank for 10-15 h;
7) taking out the wicker handicraft from the dyeing pool, draining, burning the surface of the wicker handicraft by flame, controlling the surface temperature of the wicker handicraft to be 150-;
8) after the firing is finished, the wicker handicraft is soaked in clear water, washed, placed in a drying oven to be dried until the water content is 13-15%, and then put into a warehouse after surface grinding, varnish coating, polishing and waxing.
2. The antique treatment method of the antique wicker-woven artware as claimed in claim 1, characterized in that: in the step 1), the soak solution is prepared from 6-8 parts by weight of ethanol, 2-7 parts by weight of acetone, 1-2 parts by weight of sulfuric acid and 100 parts by weight of clear water, and the ethanol and the acetone are mixed and stirred in a reaction kettle, then the clear water is poured in the reaction kettle for stirring, and finally the sulfuric acid is slowly added in the reaction kettle for stirring until the mixture is uniformly stirred.
3. The antique treatment method of the antique wicker-woven artware as claimed in claim 1, characterized in that: in the step 4), the fermentation material is prepared from pond bottom sludge, biogas residues, dried pine needles, dried chestnut shells, dried lychee shells, dried lotus leaves and clear water, and is prepared according to the mass parts during preparation, wherein the pond bottom sludge is 70-80 parts, the biogas residues are 20-25 parts, the dried pine needles are 5-8 parts, the dried chestnut shells are 6-10 parts, the dried lychee shells are 3-6 parts, the dried lotus leaves are 5-8 parts, the clear water is 100 parts, and the water content of the pond bottom sludge is 60-70%;
the preparation process of the fermentation material comprises the following steps: pulverizing dried folium Pini, dried chestnut shell, dried litchi shell, and dried folium Nelumbinis, sieving with 80-100 mesh sieve, mixing with sludge and biogas residue at the bottom of pond, adding clear water, stirring, and standing for 1-2 hr.
4. The antique treatment method of the antique wicker-woven artware as claimed in claim 1, characterized in that: in the step 6), the dye is prepared from carbon powder, bronze powder, chestnut shells, litchi shells, orange peels, iron oxide yellow, iron oxide red, sodium bicarbonate, titanium dioxide, acetone, acetic acid, ethanol and clear water in parts by mass, wherein 3-6 parts of carbon powder, 6-8 parts of bronze powder, 2-6 parts of chestnut shells, 3-5 parts of litchi shells, 5-7 parts of orange peels, 2-4 parts of iron oxide yellow, 3-5 parts of iron oxide red, 1-2 parts of sodium bicarbonate, 0.5-0.8 part of titanium dioxide, 6-8 parts of acetone, 2-4 parts of acetic acid, 10-13 parts of ethanol and clear water in parts by mass, and the carbon powder, the bronze powder, the chestnut shells, the litchi shells, the orange peels, the iron oxide yellow, the iron oxide red, the sodium bicarbonate and the titanium dioxide are mixed, stirred and put into a ball mill for ball milling, sieving with 160-fold 200-mesh sieve to obtain dyeing powder, uniformly mixing acetone, acetic acid, ethanol and clear water, pouring the dyeing powder, mixing and stirring until the mixture is uniformly stirred to obtain the dye.
CN202010600389.9A 2020-06-28 2020-06-28 Antique treatment method for antique wicker-woven artware Pending CN111958734A (en)

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CN101733802A (en) * 2010-02-04 2010-06-16 苏州市职业大学 Antique dyeing formula and dyeing method for pit carvings
KR101404216B1 (en) * 2013-12-27 2014-06-05 주식회사 죽산 The method of manufacturing unevenness forming carbonic wood
CN104149150A (en) * 2014-07-17 2014-11-19 嘉丰木业(苏州)有限公司 Archaizing floorboard manufacturing method
CN106078995A (en) * 2016-06-03 2016-11-09 阜南县黄岗利达工艺品有限公司 A kind of wicker products dry treatment process of Ramulus et Folium Tamaricis branch
CN106182241A (en) * 2016-07-22 2016-12-07 阜南县永盛工艺品有限公司 A kind of wicker for braiding does old antique imitation process
CN107553649A (en) * 2017-09-12 2018-01-09 阜南县永兴工艺品有限公司 A kind of antique-imitation processing method of wicker plaiting article
CN108000656A (en) * 2017-11-09 2018-05-08 当涂县瑞龙果树种植专业合作社 A kind of willow-plaited process product antique treatment method
CN109049230A (en) * 2018-06-29 2018-12-21 广西浙缘农业科技有限公司 A kind of processing method of bamboo rattan

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101733802A (en) * 2010-02-04 2010-06-16 苏州市职业大学 Antique dyeing formula and dyeing method for pit carvings
KR101404216B1 (en) * 2013-12-27 2014-06-05 주식회사 죽산 The method of manufacturing unevenness forming carbonic wood
CN104149150A (en) * 2014-07-17 2014-11-19 嘉丰木业(苏州)有限公司 Archaizing floorboard manufacturing method
CN106078995A (en) * 2016-06-03 2016-11-09 阜南县黄岗利达工艺品有限公司 A kind of wicker products dry treatment process of Ramulus et Folium Tamaricis branch
CN106182241A (en) * 2016-07-22 2016-12-07 阜南县永盛工艺品有限公司 A kind of wicker for braiding does old antique imitation process
CN107553649A (en) * 2017-09-12 2018-01-09 阜南县永兴工艺品有限公司 A kind of antique-imitation processing method of wicker plaiting article
CN108000656A (en) * 2017-11-09 2018-05-08 当涂县瑞龙果树种植专业合作社 A kind of willow-plaited process product antique treatment method
CN109049230A (en) * 2018-06-29 2018-12-21 广西浙缘农业科技有限公司 A kind of processing method of bamboo rattan

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Application publication date: 20201120