CN108789700B - Preparation method of ceramic white salix integra wicker - Google Patents
Preparation method of ceramic white salix integra wicker Download PDFInfo
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- CN108789700B CN108789700B CN201810363270.7A CN201810363270A CN108789700B CN 108789700 B CN108789700 B CN 108789700B CN 201810363270 A CN201810363270 A CN 201810363270A CN 108789700 B CN108789700 B CN 108789700B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27J—MECHANICAL WORKING OF CANE, CORK, OR SIMILAR MATERIALS
- B27J3/00—Peeling osier rods
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/02—Staining or dyeing wood; Bleaching wood
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/04—Combined bleaching or impregnating and drying of wood
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27L—REMOVING BARK OR VESTIGES OF BRANCHES; SPLITTING WOOD; MANUFACTURE OF VENEER, WOODEN STICKS, WOOD SHAVINGS, WOOD FIBRES OR WOOD POWDER
- B27L3/00—Debarking by chemical treatment
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D15/00—Woodstains
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Silicon Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a preparation method of a ceramic white salix integra wicker, which comprises the following operation steps: (1) harvesting Salix integra in autumn, naturally drying in the sun for 5-7 days, adding Salix integra into the soaking solution, boiling, decocting with slow fire for 30-40min, taking out, and peeling; (2) drying the peeled wicker until the water content is 7-9%, putting the wicker into a color-changing solution, soaking for 3-4 hours, taking out, putting into an oven, and drying until the water content is 12-16%; (3) and (3) uniformly spraying color fixing liquid on the surface of the wicker treated in the step (2), and drying the wicker in an oven after 3-4 hours to obtain the ceramic white salix integra wicker. The wicker prepared by the method has ceramic white color, the texture of the prepared wicker product is effectively improved, the ornamental value of the product is increased, meanwhile, the ceramic white color fixation is strong, and the phenomenon of color fading is not easy to occur in the using process.
Description
Technical Field
The invention belongs to the technical field of wicker treatment, and particularly relates to a preparation method of a ceramic white salix integra wicker.
Background
The invented wicker is a kind of willow which can be used as raw material for weaving, and various living and handicraft articles and small-sized furniture made up by using wicker are light and beautiful, and can be sold in domestic and foreign markets, so that it is an important export trade product. In China, a large number of willow varieties can be utilized as wickerwork, but at present, salix integra is generally adopted as a weaving raw material in production, and wickers obtained by peeling salix integra are generally white, single in color and poor in ornamental value.
Disclosure of Invention
In order to solve the technical problems, the invention provides a preparation method of a ceramic white salix integra wicker.
The invention is realized by the following technical scheme.
A preparation method of a ceramic white salix integra wicker comprises the following operation steps:
(1) harvesting salix integra in autumn, naturally drying for 5-7 days, putting the salix integra in a soaking solution, boiling the soaking solution, continuously decocting with slow fire for 30-40min, taking out, and peeling, wherein the soaking solution is prepared from the following components in parts by weight: 5-9 parts of N-octyl diamino ethyl glycine hydrochloride, 10-13 parts of dipotassium sebacate, 15-19 parts of ethylene diamino propane sodium sulfonate, 22-26 parts of sodium polyacrylate and 400 parts of water 350-;
(2) drying the peeled wicker until the water content is 7-9%, putting the wicker into a color-changing solution, soaking for 3-4 hours, taking out the wicker, putting the wicker into an oven, and drying until the water content is 12-16%, wherein the color-changing solution is prepared from the following components in parts by weight: 11-15 parts of gas-phase silicon dioxide, 1-3 parts of 4,4' -bis (2-sodium sulfonate styryl) biphenyl, 18-20 parts of nano zinc oxide, 4-7 parts of hydrolyzed polymaleic anhydride, 0.4-0.6 part of ammonium thiocyanate and 200 parts of water 160-activated carbon;
(3) uniformly spraying color fixing liquid on the surface of the wicker treated in the step (2), and after 3-4 hours, putting the wicker into an oven for drying treatment to prepare the ceramic white salix integra wicker, wherein the color fixing liquid is prepared from the following components in parts by weight: 23-28 parts of urea, 4-6 parts of ethylenediamine propanesulfonic acid sodium, 0.1-0.5 part of o-aminobenzenesulfonic acid and 290 parts of water.
Specifically, the color-changing liquid in the step (2) is prepared by the following method: adding fumed silica, nano zinc oxide and hydrolyzed polymaleic anhydride into water, continuously stirring for 30min at a rotating speed of 400r/min, sequentially adding 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and continuously stirring for 20min at a rotating speed of 300r/min to prepare the color-changing liquid.
Specifically, in the step (2), the temperature of the modifying solution is 45 to 50 ℃ during the soaking treatment of the modifying solution.
Specifically, in the step (3), the temperature at the time of the drying treatment in the oven is 65 to 70 ℃.
According to the technical scheme, the beneficial effects of the invention are as follows:
the preparation method of the ceramic white salix integra wicker provided by the invention is environment-friendly and low in cost, the prepared wicker has ceramic white color, the texture of the prepared wicker product is effectively improved, the ornamental value of the product is increased, meanwhile, the ceramic white color fixation is strong, and the phenomenon of color fading is not easy to occur in the using process. The soaking solution provided in the step (1) can effectively improve the peeling effect of the wickers, improve the toughness of the peeled wickers and enhance the weaving effect of the wickers; the color-changing liquid in the step (2) can permeate into the wickers after the synergistic action of the fumed silica and the nano zinc oxide, and can enable the wickers to present ceramic white color after the synergistic action of the fumed silica and the nano zinc oxide with the original color of the wickers, so that the quality of the wickers is effectively improved; 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate can enhance the permeability of fumed silica and nano zinc oxide in wicker, thereby enhancing the dyeing effect of the wicker; the color fixing solution provided by the invention can effectively improve the color fixing performance of wicker, close the pores of cell tissues on the surface of the wicker and effectively avoid the phenomenon of color loss of the wicker.
Detailed Description
The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention. The conditions used in the examples may be further adjusted according to the manufacturer's conditions, and the unexplained conditions are generally conventional experimental conditions.
Example 1
A preparation method of a ceramic white salix integra wicker comprises the following operation steps:
(1) harvesting salix integra in autumn, naturally drying for 5 days, putting the salix integra in a soaking solution, boiling the soaking solution, continuously decocting with slow fire for 30min, taking out, and peeling, wherein the soaking solution is prepared from the following components in parts by weight: 5 parts of N-octyl diamino ethyl glycine hydrochloride, 10 parts of sebacic acid dipotassium salt, 15 parts of ethylene diamino propane sodium sulfonate, 22 parts of sodium polyacrylate and 350 parts of water;
(2) drying the peeled wicker until the water content is 7%, putting the wicker into a color modifying solution, soaking for 3 hours, taking out, putting the wicker into an oven, and drying until the water content is 12%, wherein the color modifying solution is prepared from the following components in parts by weight: 11 parts of fumed silica, 1 part of 4,4' -bis (2-sodium sulfonate styryl) biphenyl, 18 parts of nano zinc oxide, 4 parts of hydrolyzed polymaleic anhydride, 0.4 part of ammonium thiocyanate and 160 parts of water;
(3) uniformly spraying a color fixing solution on the surface of the wicker treated in the step (2), and after 3 hours, putting the wicker into an oven for drying treatment to prepare the ceramic white salix integra wicker, wherein the color fixing solution is prepared from the following components in parts by weight: 23 parts of urea, 4 parts of ethylene diamine propane sodium sulfonate, 0.1 part of o-aminobenzene sulfonic acid and 250 parts of water.
Specifically, the color-changing liquid in the step (2) is prepared by the following method: adding fumed silica, nano zinc oxide and hydrolyzed polymaleic anhydride into water, continuously stirring for 30min at a rotating speed of 400r/min, sequentially adding 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and continuously stirring for 20min at a rotating speed of 300r/min to prepare the color-changing liquid.
Specifically, in the step (2), the temperature of the modifying solution is 45 ℃ during the immersion treatment of the modifying solution.
Specifically, in the step (3), the temperature at the time of the drying treatment in the oven was 65 ℃.
Example 2
A preparation method of a ceramic white salix integra wicker comprises the following operation steps:
(1) harvesting salix integra in autumn, naturally drying for 6 days, putting the salix integra in a soaking solution, boiling the soaking solution, continuously decocting with slow fire for 35min, taking out, and peeling, wherein the soaking solution is prepared from the following components in parts by weight: 7 parts of N-octyl diamino ethyl glycine hydrochloride, 12 parts of sebacic acid dipotassium salt, 17 parts of ethylene diamino propane sodium sulfonate, 24 parts of sodium polyacrylate and 380 parts of water;
(2) drying the peeled wicker until the water content is 8%, putting the wicker into a color-changing solution, soaking for 3.5 hours, taking out, putting the wicker into an oven, and drying until the water content is 14%, wherein the color-changing solution is prepared from the following components in parts by weight: 13 parts of fumed silica, 2 parts of 4,4' -bis (2-sodium sulfonate styryl) biphenyl, 19 parts of nano zinc oxide, 6 parts of hydrolyzed polymaleic anhydride, 0.5 part of ammonium thiocyanate and 180 parts of water;
(3) uniformly spraying a color fixing solution on the surface of the wicker treated in the step (2), and after 3.5 hours, putting the wicker into an oven for drying treatment to prepare the ceramic white salix integra wicker, wherein the color fixing solution is prepared from the following components in parts by weight: 25 parts of urea, 5 parts of ethylene diamine propane sodium sulfonate, 0.3 part of o-aminobenzene sulfonic acid and 270 parts of water.
Specifically, the color-changing liquid in the step (2) is prepared by the following method: adding fumed silica, nano zinc oxide and hydrolyzed polymaleic anhydride into water, continuously stirring for 30min at a rotating speed of 400r/min, sequentially adding 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and continuously stirring for 20min at a rotating speed of 300r/min to prepare the color-changing liquid.
Specifically, in the step (2), the temperature of the modifying solution is 48 ℃ during the immersion treatment of the modifying solution.
Specifically, in the step (3), the temperature at the time of the drying treatment in the oven was 68 ℃.
Example 3
A preparation method of a ceramic white salix integra wicker comprises the following operation steps:
(1) harvesting salix integra in autumn, naturally drying for 7 days, putting the salix integra in a soaking solution, boiling the soaking solution, continuously decocting with slow fire for 40min, taking out, and peeling, wherein the soaking solution is prepared from the following components in parts by weight: 9 parts of N-octyl diamino ethyl glycine hydrochloride, 13 parts of sebacic acid dipotassium salt, 19 parts of ethylene diamino propane sodium sulfonate, 26 parts of sodium polyacrylate and 400 parts of water;
(2) drying the peeled wicker until the water content is 9%, putting the wicker into a color-changing solution, soaking for 4 hours, taking out, putting the wicker into an oven, and drying until the water content is 16%, wherein the color-changing solution is prepared from the following components in parts by weight: 15 parts of gas-phase silicon dioxide, 3 parts of 4,4' -bis (2-sodium sulfonate styryl) biphenyl, 20 parts of nano zinc oxide, 7 parts of hydrolyzed polymaleic anhydride, 0.6 part of ammonium thiocyanate and 200 parts of water;
(3) uniformly spraying a color fixing solution on the surface of the wicker treated in the step (2), and after 4 hours, putting the wicker into an oven for drying treatment to prepare the ceramic white salix integra wicker, wherein the color fixing solution is prepared from the following components in parts by weight: 28 parts of urea, 6 parts of ethylene diamine propane sulfonic acid sodium salt, 0.5 part of o-aminobenzene sulfonic acid and 290 parts of water.
Specifically, the color-changing liquid in the step (2) is prepared by the following method: adding fumed silica, nano zinc oxide and hydrolyzed polymaleic anhydride into water, continuously stirring for 30min at a rotating speed of 400r/min, sequentially adding 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and continuously stirring for 20min at a rotating speed of 300r/min to prepare the color-changing liquid.
Specifically, in the step (2), the temperature of the modifying solution is 50 ℃ during the immersion treatment of the modifying solution.
Specifically, in the step (3), the temperature at the time of the drying treatment in the oven was 70 ℃.
Comparative example 1
The color-changing solution of the step (2) does not contain 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and the rest of the operation steps are completely the same as those of the example 1.
Comparative example 2
And (3) replacing the color fixing solution in the step (3) with clear water, and completely performing the same operation steps as the example 2.
The ceramic white wicker was prepared by the methods of examples and comparative examples, respectively, and the preparation methods were identical except for the above-described preparation conditions, and the dyeing effects of the prepared wickers are shown in table 1:
TABLE 1 ceramic whitening effect of wickers
| Item | Color and luster of wicker | Soaking in water for 48 hr |
| Example 1 | Uniform and bright color and ceramic white effect | No decolorization occurs |
| Comparative example 1 | Dark color and uneven color distribution | Slight decolorization |
| Example 2 | Uniform and bright color and ceramic white effect | No decolorization occurs |
| Comparative example 2 | Uniform and bright color, and remarkable ceramic white effect | The discoloration phenomenon is serious |
| Example 3 | Uniform and bright color and ceramic white effect | No decolorization occurs |
It should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and are not limited. Although the present invention has been described in detail with reference to the preferred embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted without departing from the scope of the present invention.
Claims (4)
1. The preparation method of the ceramic white salix integra wicker is characterized by comprising the following operation steps:
(1) harvesting salix integra in autumn, naturally drying for 5-7 days, putting the salix integra in a soaking solution, boiling the soaking solution, continuously decocting with slow fire for 30-40min, taking out, and peeling, wherein the soaking solution is prepared from the following components in parts by weight: 5-9 parts of N-octyl diamino ethyl glycine hydrochloride, 10-13 parts of dipotassium sebacate, 15-19 parts of ethylene diamino propane sodium sulfonate, 22-26 parts of sodium polyacrylate and 400 parts of water 350-;
(2) drying the peeled wicker until the water content is 7-9%, putting the wicker into a color-changing solution, soaking for 3-4 hours, taking out the wicker, putting the wicker into an oven, and drying until the water content is 12-16%, wherein the color-changing solution is prepared from the following components in parts by weight: 11-15 parts of gas-phase silicon dioxide, 1-3 parts of 4,4' -bis (2-sodium sulfonate styryl) biphenyl, 18-20 parts of nano zinc oxide, 4-7 parts of hydrolyzed polymaleic anhydride, 0.4-0.6 part of ammonium thiocyanate and 200 parts of water 160-activated carbon;
(3) uniformly spraying color fixing liquid on the surface of the wicker treated in the step (2), and after 3-4 hours, putting the wicker into an oven for drying treatment to prepare the ceramic white salix integra wicker, wherein the color fixing liquid is prepared from the following components in parts by weight: 23-28 parts of urea, 4-6 parts of ethylenediamine propanesulfonic acid sodium, 0.1-0.5 part of o-aminobenzenesulfonic acid and 290 parts of water.
2. The method for preparing the white salix integra wicker with the ceramic according to claim 1, wherein the color-changing liquid in the step (2) is prepared by the following method: adding fumed silica, nano zinc oxide and hydrolyzed polymaleic anhydride into water, continuously stirring for 30min at a rotating speed of 400r/min, sequentially adding 4,4' -bis (2-sodium sulfonate styryl) biphenyl and ammonium thiocyanate, and continuously stirring for 20min at a rotating speed of 300r/min to prepare the color-changing liquid.
3. The method according to claim 1, wherein the temperature of the modifying solution is 45-50 ℃ during the soaking treatment of the color modifying solution in the step (2).
4. The method for preparing the salix integra wicker with ceramic according to claim 1, wherein in the step (3), the temperature of the drying treatment in the oven is 65-70 ℃.
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| JPH11179705A (en) * | 1997-12-18 | 1999-07-06 | Kamei Chikugei Kogyosho:Kk | Manufacture of rattan product |
| CN105965647A (en) * | 2016-07-21 | 2016-09-28 | 阜南佳利工艺品有限公司 | Softening and color fixation treatment solution for straw and willow braided salix integra and preparation method thereof |
| CN106182246A (en) * | 2016-07-21 | 2016-12-07 | 阜南佳利工艺品有限公司 | A kind of processing method of Pericarpium Citri Reticulatae Viride purple willow baskets craft |
| CN106965283A (en) * | 2017-04-10 | 2017-07-21 | 阜南佳利工艺品有限公司 | The colouring method of color stability on a kind of raising wicker |
| CN107186846A (en) * | 2017-06-03 | 2017-09-22 | 阜南县猛发工艺品有限公司 | A kind of processing method of wicker plaiting article raw material wicker |
| CN107253249A (en) * | 2017-07-04 | 2017-10-17 | 阜南县宏达工艺品厂 | A kind of method of natural indigo pigment wicker plaiting article dyeing |
-
2018
- 2018-04-21 CN CN201810363270.7A patent/CN108789700B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11179705A (en) * | 1997-12-18 | 1999-07-06 | Kamei Chikugei Kogyosho:Kk | Manufacture of rattan product |
| CN105965647A (en) * | 2016-07-21 | 2016-09-28 | 阜南佳利工艺品有限公司 | Softening and color fixation treatment solution for straw and willow braided salix integra and preparation method thereof |
| CN106182246A (en) * | 2016-07-21 | 2016-12-07 | 阜南佳利工艺品有限公司 | A kind of processing method of Pericarpium Citri Reticulatae Viride purple willow baskets craft |
| CN106965283A (en) * | 2017-04-10 | 2017-07-21 | 阜南佳利工艺品有限公司 | The colouring method of color stability on a kind of raising wicker |
| CN107186846A (en) * | 2017-06-03 | 2017-09-22 | 阜南县猛发工艺品有限公司 | A kind of processing method of wicker plaiting article raw material wicker |
| CN107253249A (en) * | 2017-07-04 | 2017-10-17 | 阜南县宏达工艺品厂 | A kind of method of natural indigo pigment wicker plaiting article dyeing |
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