CN111939111A - A Chinese herbal shampoo prepared from Chinese herbal extract, and its preparation method - Google Patents
A Chinese herbal shampoo prepared from Chinese herbal extract, and its preparation method Download PDFInfo
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- CN111939111A CN111939111A CN202010918850.5A CN202010918850A CN111939111A CN 111939111 A CN111939111 A CN 111939111A CN 202010918850 A CN202010918850 A CN 202010918850A CN 111939111 A CN111939111 A CN 111939111A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a Chinese herbal medicine shampoo prepared from Chinese herbal medicine leachate and a preparation method thereof, and is characterized in that: the raw materials are as follows by weight: 60 parts of purslane, 20 parts of old ginger, 10 parts of fleece-flower root, 10 parts of mint and 200 parts of water. The shampoo is prepared from pure natural Chinese herbal medicines, and can thoroughly solve the problems of dandruff and oily pruritus. The shampoo does not contain harmful chemical synthetic substances, is natural and safe, has no side effect, is easy to obtain raw materials, and has moderate price, thereby solving the defects in the preparation of other traditional Chinese herbal medicine shampoos.
Description
Technical Field
The invention relates to the technical field of shampoo, in particular to Chinese herbal medicine shampoo prepared from Chinese herbal medicine leachate and a preparation method thereof.
Background
The shampoo is a common sanitary product for removing dandruff and cleaning hair. The shampoo provided by the invention mainly comprises the components of purslane and old ginger in a compatibility manner, and is supplemented with polygonum multiflorum and mint.
The invention for preparing the shampoo by adopting the Chinese herbal medicines is more, but most of the shampoo adopts the conventional boiling water leaching method, the effective components cannot be extracted to the maximum extent, and the space for improving the shampoo is greatly provided.
Purslane is a common medicinal and edible Chinese herbal medicine, and is recorded in the Kaibao Chinese herbal medicine of Liu Han in Song Dynasty, that is, the purslane can prevent hair and beard from whitening after being taken for a long time. According to the traditional Chinese medicine literature, the purslane has the effects of relieving swelling, detoxifying, promoting the production of body fluid to quench thirst, diminishing inflammation and promoting urination. The components of purslane can increase the secretion and activity of melanocytes, thereby blackening hair. Meanwhile, purslane is cold in nature and has the effects of clearing heat and relieving itching, sebum secretion is vigorous in summer, red rashes and pustules easily grow on the scalp, and scalp itching and red swelling symptoms can be improved by washing hair with purslane. Is an effective medicinal plant for keeping hair and scalp clean and healthy.
Purslane is a common natural plant for washing and protecting hair in folk, is nontoxic and harmless, but is mostly used independently. In the experimental process, the purslane dandruff-removing and hair-protecting effect is more remarkable after the purslane is matched with the old ginger. Meanwhile, according to the literature, a small amount of polygonum multiflorum is added to increase the hair nourishing effect, and mint is added to increase the hair washing comfort, so that a better hair washing and protecting effect is expected.
The raw materials used in the invention are all pure natural Chinese herbal medicines. Purslane: moistening scalp, eliminating sore, relieving itching, invigorating kidney yin, strengthening body resistance, consolidating constitution, nourishing yin, and promoting hair growth; the old ginger has the obvious effect of inhibiting dermatophytes and can treat various carbuncle swelling sore toxins. Polygoni Multiflori radix with effects of nourishing liver and kidney, replenishing essence and blood, blackening beard and hair, strengthening tendons and bones, eliminating turbid pathogen and reducing blood lipid, and can be used for treating blood deficiency sallow complexion, giddiness tinnitus, early white beard and hair, soreness of waist and knees, limbs anesthesia, and hyperlipidemia; herba Menthae is pungent and cool, and has effects of inducing sweat and clearing heat, and can be used for treating influenza, headache, conjunctival congestion, fever, laryngopharynx, and gum swelling and pain, and for treating neuralgia, skin pruritus, erythra and eczema, etc. by topical application, herba Menthae is usually used for replacing tea, and has effects of clearing heart fire and improving eyesight; the mint contains menthol, and the substance can refresh breath, has various medicinal properties, and also has the effects of antisepsis and sterilization, diuresis, phlegm reduction, stomach strengthening, digestion assistance and the like; the shampoo prepared by the process and the components has no chemical synthetic components, is environment-friendly, has no pollution to the environment after use, has no stimulation to the scalp of a human body, has the effects of washing hair, brightening hair, removing dandruff, relieving itching, growing hair and blackening hair after use, and is a pure natural Chinese herbal medicine shampoo.
Therefore, according to the experimental result, the invention particularly adopts the method of firstly mixing the purslane and the polygonum multiflorum and heating and pressurizing: extracting effective components to the maximum extent under the pressure of 0.04-0.05Mpa and the temperature of 110 ℃, adding old ginger and mint under normal temperature and pressure to continue leaching, preparing the Chinese herbal medicine leachate and preparing the Chinese herbal medicine shampoo.
With the improvement of living standard of people, the requirements on the hair washing function effect and the like of the shampoo are higher and higher, the most basic requirements on hair washing and cleaning are met, meanwhile, the care on the hair quality and the scalp is more emphasized, the effects of hair washing, dandruff removing and the like are required, and the effects of environmental protection, health care, safety, no damage and the like are required.
At present, other shampoo sold in the market and not prepared from Chinese herbal medicines is generally prepared by mixing chemical synthetic substances, has strong hair washing and hairdressing effects, but cannot fundamentally solve the problems of dandruff increase and oil generation and itching, has more chemical components, possibly has certain side effect on human bodies after long-term use, and causes certain pollution and damage to the environment in the manufacturing and using processes. Other traditional Chinese herbal medicine shampoos in the market are from the perspective of nutrition and hair blackening, are not the same as the shampoo of the invention, and solve the problem on the basis of the medicinal efficacy of clearing heat and relieving itching by considering the pathological reasons of scurf and pruritus.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a Chinese herbal medicine shampoo prepared from Chinese herbal medicine leachate and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a Chinese herbal shampoo prepared from Chinese herbal medicine leachate comprises the following raw materials in parts by weight: 60 parts of purslane, 20 parts of old ginger, 10 parts of fleece-flower root, 10 parts of mint and 200 parts of water.
The invention also provides a preparation method of the Chinese herbal medicine shampoo prepared from the Chinese herbal medicine leachate, which is characterized by comprising the following steps of: the method comprises the following steps:
the method comprises the following steps: the materials are cleaned and aired, and the weight parts of purslane: 60 parts, old ginger: 20 parts, polygonum multiflorum: 10 parts, mint: 10 parts of the raw materials are weighed, cut and ground into powder respectively, the powder is sieved by a 100-mesh sieve to serve as raw material powder, and the powder which is not sieved is ground again;
step two: adding 60 parts of purslane and 10 parts of polygonum multiflorum powder in the step one into a sealed stainless steel reaction kettle, adding sufficient parts of purified water obtained by a reverse osmosis device into the reaction kettle, sealing the reaction kettle, heating the reaction kettle to the pressure of 0.04-0.05Mpa, the temperature of 110 ℃, the stirring speed of 30 r/min, cooling and depressurizing after one hour, reducing the pressure to normal pressure, reducing and maintaining the temperature at 65-70 ℃, and keeping constant temperature heating for 4 hours;
step three: after heating at constant temperature for 2 hours, adding 20 parts of old ginger powder into the reaction kettle for continuous constant temperature heating;
step four: heating at constant temperature for 3 hours, adding 10 parts of mint powder into a reaction kettle until the constant temperature heating is finished, cooling to room temperature, filtering by using a cloth bag machine, adding 0.2 mass percent of commercially available shampoo natural thickening agent into the filtrate after antisepsis and disinfection, uniformly mixing and canning to obtain the Chinese herbal medicine shampoo.
Preferably, the step one comprises the following raw materials: the purslane, the old ginger, the tuber fleeceflower root and the mint are dry products and are ground and sieved by a 100-mesh sieve, and the mass ratio of the components is 6: 2: 1.
Preferably, in the second step, the effective components of the purslane and the polygonum multiflorum are leached by heating and pressurizing a 316 stainless steel closed reaction kettle, and the amount of the added reverse osmosis water is 2 times of the mass of all the raw materials. The heating temperature is 110 ℃, the pressure is 0.04-0.05Mpa, the stirring speed is 30 r/min, and the time is 1 hour.
Preferably, the ginger and the mint powder in the third step are added under the conditions of constant pressure and temperature of 65-70 ℃ for 2 hours and 3 hours respectively.
Preferably, the leachate obtained in the fourth step is filtered by a cloth bag, and then is subjected to conventional antisepsis and disinfection, and then 0.5% of commercial shampoo natural thickener in mass ratio is added, mixed uniformly and canned to obtain the Chinese herbal medicine shampoo.
The invention adopts an advanced heating and pressurizing method: the pressure is 0.04-0.05Mpa, the temperature is 110 deg.C, and the effective components in the Chinese herbal medicine are extracted to the maximum extent. The shampoo is prepared from pure natural Chinese herbal medicines, and can thoroughly solve the problems of dandruff and oily pruritus. The shampoo does not contain harmful chemical synthetic substances, is natural and safe, has no side effect, is easy to obtain raw materials, and has moderate price, thereby solving the defects in the preparation of other traditional Chinese herbal medicine shampoos.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
A Chinese herbal medicine liquid shampoo prepared by a heating and pressurizing process adopts Chinese herbal medicine leaching liquor prepared by the heating and pressurizing process and prepares pure natural Chinese herbal medicine liquid shampoo, wherein the Chinese herbal medicine leaching liquor comprises the following raw materials in parts by mass:
purslane: 60 parts; old ginger: 20 parts of (1); polygonum multiflorum: 10 parts of (A); mint: 10 parts of (A); water: 200 parts of (a) a mixture of (b),
wherein the mass ratio of the purslane, the old ginger, the tuber fleeceflower root and the mint is 6: 2: 1;
the preparation method of the Chinese herbal medicine leaching liquor comprises the following steps:
the method comprises the following steps: the preparation method comprises the following steps of (1) cleaning and airing the materials in parts by mass: purslane: 60 parts, old ginger: 20 parts, polygonum multiflorum: 10 parts, mint: 10 parts of the raw materials are respectively weighed, cut and ground into powder of 100 meshes, so that the heating and leaching are sufficient, and the effective components are not wasted.
Step two: and (3) adding the purslane and polygonum multiflorum powder in the step one into a sealed stainless steel reaction kettle, adding 200 parts of RO water into the reaction kettle, and heating the reaction kettle to the pressure of 0.04-0.05Mpa, the temperature of 110 ℃, and the stirring speed of 30 revolutions per minute. After one hour, reducing the temperature and the pressure, and keeping the temperature at 65-70 ℃ and normal pressure for 4 hours to heat at constant temperature; the production water is RO reverse osmosis pure water, so that the quality and sanitation of the Chinese herbal medicine leaching liquor are ensured. It needs to be further explained here that the closed reaction kettle comprises a shell with a cover, a stirrer and a heating pipe, wherein the heating pipe is arranged outside the container and is provided with a heat insulation protective shell. The high-pressure heating and stirring are helpful for fully dissolving out the effective components of the Chinese herbal medicines, and the temperature is kept at 110 ℃ without damaging the organic components. As will be appreciated by those skilled in the art.
Step three: after heating at constant temperature for 1 hour, reducing the temperature and the pressure, keeping the temperature at 60-70 ℃ and the pressure at normal pressure, adding 20 parts of old ginger into the reaction kettle, and continuously heating and stirring at constant temperature for 2 hours; the old ginger is added in the time period for leaching, the volatility of the dissolved substance of the old ginger is mainly considered, and the old ginger is not suitable for heating, so that the effective components of the ginger are kept as far as possible.
Step four: after heating at constant temperature and normal pressure for 3 hours, 5-10 parts of mint are added into the reaction kettle until the constant temperature heating is finished. Also, since menthol contained in mint is easily volatilized by heating, the medicinal efficacy of mint can be maximally secured by such an operation. The cloth bag filtration is adopted for filtration, so that the active ingredients are completely leached out with water to the maximum extent, and the medicine residues are completely removed. Other processes such as preservation, disinfection, thickening, etc. are modern and common processes, as will be understood by those skilled in the art.
For normal production yield requirement, the volume of each closed reaction kettle is 4000L, and the Chinese herbal medicine leaching liquor product obtained through the four steps is 2000kg by mass, namely 2000L;
the shampoo application method comprises the following steps:
and (3) performing antisepsis, disinfection and thickening on the Chinese herbal medicine filtrate obtained by filtering to obtain the Chinese herbal medicine shampoo. The shampoo can be directly used for washing hair. The hair is completely moistened by the shampoo, and the hair is gently massaged and scrubbed for 5 to 10 minutes so as to remove hair dirt and dandruff. Finally, washing for 2-3 times by using clear water, finishing the hair washing process after the hair washing is cleaned, and repeating the operation if necessary. The method of washing hair can be performed according to the instruction of the use of the existing commercially available shampoo, and should not be limited thereto.
To confirm the effectiveness of the present invention, the following group experiments of leaching under different temperature conditions were carried out:
example 2, the same as example 1, in that purslane: 60 parts, old ginger: 20 parts, polygonum multiflorum: 10 parts, mint: 10 parts of water: 200 parts.
The preparation method of the Chinese herbal medicine leaching liquor in the embodiment is different from the heating and pressurizing method in the embodiment 1, but adopts most of the Chinese herbal medicine leaching methods: namely heating to 100 ℃ under normal pressure, leaching for 5 hours, and then obtaining the leaching solution by a cloth bag filtration method. The Chinese herbal medicine leaching liquor prepared by the components and the process is 2000L, and the shampoo is prepared according to the method of the embodiment 1.
In addition, a comparative test is also carried out on the promotion effect of the ginger on the hair growth and itching relieving effect of the purslane.
Example 3, which differs from example 1 in that purslane: 80 parts, old ginger: 0 part, polygonum multiflorum: 10 parts, mint: 10 parts of water: 200 parts of (a) a mixture of (b),
in example 3, the preparation method and preparation method of the Chinese herbal medicine leaching liquor are the same as those in example 1, and the Chinese herbal medicine leaching liquor prepared by the mass parts is 2000L. The shampoo was prepared as in example 1.
Clinical study: in order to explain the using effect of the shampoo under the conditions of the preparation method and different formulas in detail, 100 (half of men and women) users who suffer from scalp itch, much dandruff, dry hair and alopecia and are 30-40 years old are selected and divided into two experimental groups and two control groups to be tested, and each group is 25.
Test protocol:
the first experimental group washed hair with the herbal shampoo of the present invention prepared in example 1 for 1 month; the second experimental group washed hair with the herbal shampoo of the present invention prepared in example 1 for 2 months; the first control group was shampooed using the shampoo prepared in example 2 for 2 months; the second control group was washed with the shampoo prepared in example 3 for 2 months;
the experimental group and the control group have the same hair washing frequency, the hair washing frequency is based on that the ordinary people wash hair for 1 time every 1-2 days, and frequent hair washing easily causes damage to hair and hair, and is not beneficial to hair maintenance and nursing.
And (3) judging the use effect: the hair blackening cream has no effect on dandruff, oily and itching, relieves, obviously improves and blackens the hair effect, and the softness and the allergic condition are evaluated by experimenters.
As is apparent from the above table, in the experimental group, the experimental group 2 using the shampoo for 2 months was significantly improved more than the experimental group 1 using the shampoo for one month, and the symptoms of most users were improved after 2 months. Therefore, the obvious effects of relieving itching and blackening hair can be obtained by insisting on using the Chinese herbal medicine shampoo for more than 2 months.
The results of the first control group example 2 show that the effects of the same Chinese herbal medicine composition and the same using method are greatly different by adopting the heating and pressurizing leaching, and the heating and pressurizing leaching is proved to play a great role in the exertion of the efficacy of the Chinese herbal medicine;
the experiment of example 3 in the second control group also showed a significant difference from the experiment group 2, indicating that the effect of the shampoo was somewhat diminished without the compatibility of old ginger. Therefore, the compatibility of the purslane and the old ginger is another reason for the obvious improvement of the treatment effect of the invention.
By using the natural Chinese herbal medicine shampoo extracted by heating and pressurizing, the feedback effective rate after the shampoo is used by a user in an experiment reaches over 90 percent, and the situations of allergy and frizzy hair are avoided, so that the effects of nourishing black hair, removing dandruff, relieving itching, controlling oil and inhibiting bacteria are achieved, and the effective effect is obtained in the practical use of the shampoo.
In conclusion, the invention is prepared by leaching pure natural Chinese herbal medicines by heating and pressurizing, and the process is effective and reliable. The shampoo is composed of Chinese herbal medicines without any chemical synthesis components, and has remarkable effect. Meanwhile, the production process is environment-friendly and pollution-free, and the hair is not damaged after the hair conditioner is used. The ginger is added, so that the hair is maintained, and more importantly, the dandruff removing and itching relieving effects of the purslane are improved. The experimental result shows that the Chinese herbal medicine shampoo prepared by the heating and pressurizing preparation process is safe and effective and is suitable for long-term use by consumers.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. A Chinese herbal shampoo prepared from Chinese herbal medicine leachate is characterized in that: the raw materials are as follows by weight: 60 parts of purslane, 20 parts of old ginger, 10 parts of fleece-flower root, 10 parts of mint and 200 parts of water.
2. A method of preparing a herbal shampoo from the leachate of herbal medicine of claim 1, comprising: the method comprises the following steps:
the method comprises the following steps: the materials are cleaned and aired, and the weight parts of purslane: 60 parts, old ginger: 20 parts, polygonum multiflorum: 10 parts, mint: 10 parts of the raw materials are weighed, cut and ground into powder respectively, the powder is sieved by a 100-mesh sieve to serve as raw material powder, and the powder which is not sieved is ground again;
step two: adding 60 parts of purslane and 10 parts of polygonum multiflorum powder in the step one into a sealed stainless steel reaction kettle, adding sufficient parts of purified water obtained by a reverse osmosis device into the reaction kettle, sealing the reaction kettle, heating the reaction kettle to the pressure of 0.04-0.05Mpa, the temperature of 110 ℃, the stirring speed of 30 r/min, cooling and depressurizing after one hour, reducing the pressure to normal pressure, reducing and maintaining the temperature at 65-70 ℃, and keeping constant temperature heating for 4 hours;
step three: after heating at constant temperature for 2 hours, adding 20 parts of old ginger powder into the reaction kettle for continuous constant temperature heating;
step four: heating at constant temperature for 3 hours, adding 10 parts of mint powder into a reaction kettle until the constant temperature heating is finished, cooling to room temperature, filtering by using a cloth bag machine, adding 0.2 mass percent of commercially available shampoo natural thickening agent into the filtrate after antisepsis and disinfection, uniformly mixing and canning to obtain the Chinese herbal medicine shampoo.
3. The method according to claim 2, wherein the shampoo is prepared from a herbal extract, the method comprising: the first step comprises the following raw materials: the purslane, the old ginger, the tuber fleeceflower root and the mint are dry products and are ground and sieved by a 100-mesh sieve, and the mass ratio of the components is 6: 2: 1.
4. The method according to claim 2, wherein the shampoo is prepared from a herbal extract, the method comprising: and in the second step, the effective components of the purslane and the polygonum multiflorum are leached by heating and pressurizing a 316 stainless steel closed reaction kettle, the amount of the added reverse osmosis water is 2 times of the mass of all the raw materials, the heating temperature is 110 ℃, the pressure is 0.04-0.05Mpa, the stirring speed is 30 r/min, and the time is 1 hour.
5. The method according to claim 2, wherein the shampoo is prepared from a herbal extract, the method comprising: the ginger and the mint powder in the third step are respectively added after 2 hours and 3 hours under the conditions of normal pressure and constant temperature of 65-70 ℃.
6. The method according to claim 2, wherein the shampoo is prepared from a herbal extract, the method comprising: and filtering the leachate in the fourth step by using a cloth bag, adding 0.5 mass percent of commercially available shampoo natural thickening agent after conventional corrosion prevention and disinfection, uniformly mixing and canning to obtain the Chinese herbal medicine shampoo.
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Cited By (1)
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