CN111840206A - Wormwood massage cream and preparation method thereof - Google Patents
Wormwood massage cream and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a wormwood massage cream, which belongs to the technical field of skin care health products, and comprises a phase A, a phase B, a phase C and a phase D; the phase A comprises the following components: glycerin, propylene glycol, erythritol, carbomer, allantoin, dipotassium glycyrrhizinate, methylparaben, xanthan gum, sodium hyaluronate and water; the phase B comprises the following components: squalane, isohexadecane, ethylhexyl palmitate, cetearyl alcohol, cetearyl glucoside, tocopherol; the phase C comprises the following components: menthol, mugwort leaf oil, pubescent angelica root extract, purslane extract, centella asiatica extract, giant knotweed rhizome root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract, rosemary leaf extract, bacillus/soybean fermentation product extract, ginger root oil; the phase D comprises the following components: caprylhydroxamic acid, glyceryl caprylate. The wormwood massage cream can relieve massage and improve the softness of skin.
Description
Technical Field
The invention belongs to the technical field of skin care health products, and particularly relates to a wormwood massage cream and a preparation method thereof.
Background
With the development of economy, the living standard of people is improved, the living pressure is increased, people are inevitably tired in body and mind under high pressure, the body and mind need to be relieved at this time, the massage cream can not only protect the skin, but also relieve the pressure, and therefore the market is opened.
Disclosure of Invention
The invention aims to provide a wormwood massage cream and a preparation method thereof.
The technical purpose of the invention is realized by the following technical scheme:
a wormwood massage cream, which comprises a phase A, a phase B, a phase C and a phase D;
the phase A comprises the following components: glycerin, propylene glycol, erythritol, carbomer, allantoin, dipotassium glycyrrhizinate, methylparaben, xanthan gum, sodium hyaluronate and water;
the phase B comprises the following components: squalane, isohexadecane, ethylhexyl palmitate, cetearyl alcohol, cetearyl glucoside, tocopherol;
the phase C comprises the following components: menthol, mugwort leaf oil, pubescent angelica root extract, purslane extract, centella asiatica extract, giant knotweed rhizome root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract, rosemary leaf extract, bacillus/soybean fermentation product extract, ginger root oil;
the phase D comprises the following components: caprylhydroxamic acid, glyceryl caprylate.
Preferably, the massage cream comprises a phase A, a phase B, a phase C and a phase D;
the phase A comprises the following components in percentage by weight in the massage cream: 2% of glycerol, 2% of propylene glycol, 1% of erythritol, 0.1% of carbomer, 0.2% of allantoin, 0.1% of dipotassium glycyrrhizinate, 0.1% of methylparaben, 0.1% of xanthan gum, 0.1% of sodium hyaluronate and the balance of water;
the B phase comprises the following components in percentage by weight in the massage cream: 2% squalane, 2% isohexadecane, 2% ethylhexyl palmitate, 1% cetearyl alcohol, 1% cetearyl glucoside, 0.3% tocopherol;
the C phase comprises the following components in percentage by weight in the massage cream: 0.1% menthol, 2% argyi leaf oil, 2% pubescent angelica root extract, 2% purslane extract, 2% centella asiatica extract, 2% polygonum cuspidatum root extract, 2% scutellaria baicalensis root extract, 2% tea leaf extract, 2% glycyrrhiza glabra root extract, 2% chamomile flower extract, 2% rosemary leaf extract, 0.5% bacillus/soybean fermentation product extract, 0.1% ginger root oil;
the phase D comprises the following components: 0.1% caprylhydroxamic acid, 0.1% glyceryl caprylate.
The preparation method of the blumea oil comprises the following steps: taking 100 g of naturally dried folium artemisiae argyi, grinding, placing in a 1000ML round-bottom flask, adding 700ML distilled water, carrying out cold soaking for 2h, then carrying out heating extraction according to a steam distillation method, refluxing for 4h, separating out volatile oil, adding anhydrous sodium sulfate, and drying to obtain folium artemisiae argyi oil; has effects in dispelling cold, relieving pain, and relieving skin allergy.
The preparation method of the radix angelicae pubescentis extract comprises the following steps: pulverizing radix Angelicae Pubescentis powder, filtering, and reflux-extracting with 4 times of methanol for three times, each time for 2 hr; it has effects in expelling pathogenic wind, removing dampness, relieving arthralgia, and relieving pain.
The preparation method of the purslane extract comprises the following steps: extracting from stem and leaf of herba Portulacae with low temperature method to obtain bioactive extract, and dissolving in butanediol solution; it can relieve skin and inhibit skin pruritus caused by dryness.
The preparation method of the centella asiatica extract comprises the following steps: using ethanol solution as solvent, and performing crude extraction on centella asiatica by using an ultrasonic extraction method; separating out effective components by using an AB-8 resin separation column and using an ethanol solution as an eluent, wherein the target component eluted by 30-50% of ethanol and 51-75% of the ethanol solution is the centella asiatica extract; has the effects of clearing away heat, promoting diuresis, removing toxic substances and relieving swelling.
The preparation method of the giant knotweed root extract comprises the following steps: pulverizing rhizoma Polygoni Cuspidati, refluxing with 95% ethanol for 2 times, each for 2 hr, mixing extractive solutions, recovering ethanol under reduced pressure until no alcohol smell exists, extracting with ethyl acetate, recovering ethyl acetate under reduced pressure to obtain stilbene, hydrolyzing water layer with acid, performing Soxhlet extraction with diethyl ether until colorless, extracting diethyl ether layer with 5% sodium hydroxide solution, acidifying to obtain anthraquinones, and mixing stilbene type anthraquinone to obtain rhizoma Polygoni Cuspidati extract; resveratrol and emodin are main functional components in giant knotweed rhizome, and resveratrol is helpful for relieving pain, clearing heat and eliminating dampness, and emodin has anti-inflammation effect.
The preparation method of the scutellaria baicalensis root extract comprises the following steps: decocting Scutellariae radix with water, mixing decoctions, concentrating, adjusting pH to 1.0-2.0 with hydrochloric acid, keeping the temperature at 80 deg.C, standing, filtering, adding appropriate amount of water into precipitate, stirring, adjusting pH to 7.0 with 40% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.0-2.0 with hydrochloric acid, standing at 60 deg.C for 30 min, washing precipitate with water and ethanol sequentially until pH is 7.0, volatilizing ethanol, and drying under reduced pressure to obtain the final product; has effects of clearing away heat and toxic materials, and inhibiting bacteria and inflammation.
The preparation method of the tea extract comprises the following steps: treating raw tea leaves by steaming, collecting water vapor containing tea leaf aroma components generated from the raw tea leaves, and cooling the collected water vapor to obtain an extract containing the tea leaf aroma components; the tea extract contains tea polyphenols, catechin, epigallocatechin gallate and small amount of caffeine as main active components, and has antioxidant and antibacterial effects.
The preparation method of the glycyrrhiza glabra root extract comprises the following steps: smashing glabrous greenbrier rhizome powder, then adding the glabrous greenbrier rhizome powder into liquid resin extracting solution, leaching for 24 hours, filtering, leaching again, filtering and combining the extracting solution, wherein the mass ratio of the glabrous greenbrier rhizome to the liquid resin extracting solution is 1: 5-10, adding the extracting solution into a calcium chloride solution until the calcium concentration is 0.02-0.006mol/L, standing until a precipitate is separated out, filtering, adding an ethyl acetate aqueous solution into the precipitate, adding acid to adjust the pH value of the solution to 2.0, extracting, dissolving, standing for layering, taking an ethyl acetate layer, carrying out reduced pressure concentration on the ethyl acetate layer solution, and then carrying out vacuum drying; has antibacterial, antiinflammatory, and antioxidant effects.
The preparation method of the chamomile flower extract comprises the following steps: decocting flos Chrysanthemi in water for 1-2 hr, filtering to obtain flos Chrysanthemi solution, decocting flos Chrysanthemi residue in water for 0.5-1 hr, filtering to obtain flos Chrysanthemi solution, discarding flos Chrysanthemi residue, mixing decoctions, concentrating to density below 60 deg.C of 1.05-1.2, and cooling to room temperature to obtain decoction; it has effects in relieving skin, resisting skin sensitivity, resisting inflammation, resisting bacteria, and resisting oxidation.
The preparation method of the rosemary leaf extract comprises the following steps: putting 40-mesh rosemary powder into a 150mL triangular flask with a plug, adding an ethanol water solution, sealing, uniformly mixing, putting into an ultrasonic cleaner, carrying out ultrasonic treatment at normal temperature for 15min, taking out the triangular flask, carrying out suction filtration, and rotatably steaming the filtrate to be dry. Rosemary is a highly effective natural antioxidant.
A preparation method of wormwood massage cream comprises the following steps:
1) adding the phase A into an emulsifying pot, heating to 85 ℃, homogenizing and uniformly stirring, and stirring for 30 minutes at the constant temperature for later use;
2) putting the phase B into an oil phase pot, heating to 80 ℃ to ensure complete dissolution, and stirring for 30 minutes at the constant temperature for later use;
3) homogenizing A, B at 80 deg.C, stirring, homogenizing, and stirring for 15 min;
4) cooling to 45 ℃, adding the phase C, and stirring uniformly;
5) adding phase D, and stirring.
Compared with the prior art, the invention has the following advantages:
the wormwood massage cream disclosed by the invention can relieve massage and improve the softness of skin, is safe and environment-friendly in components, and has good health care and use effects.
Detailed Description
A wormwood massage cream, which comprises a phase A, a phase B, a phase C and a phase D;
the phase A comprises the following components in percentage by weight in the massage cream: 2% of glycerol, 2% of propylene glycol, 1% of erythritol, 0.1% of carbomer, 0.2% of allantoin, 0.1% of dipotassium glycyrrhizinate, 0.1% of methylparaben, 0.1% of xanthan gum, 0.1% of sodium hyaluronate and the balance of water;
the B phase comprises the following components in percentage by weight in the massage cream: 2% squalane, 2% isohexadecane, 2% ethylhexyl palmitate, 1% cetearyl alcohol, 1% cetearyl glucoside, 0.3% tocopherol;
the C phase comprises the following components in percentage by weight in the massage cream: 0.1% menthol, 2% argyi leaf oil, 2% pubescent angelica root extract, 2% purslane extract, 2% centella asiatica extract, 2% polygonum cuspidatum root extract, 2% scutellaria baicalensis root extract, 2% tea leaf extract, 2% glycyrrhiza glabra root extract, 2% chamomile flower extract, 2% rosemary leaf extract, 0.5% bacillus/soybean fermentation product extract, 0.1% ginger root oil;
the phase D comprises the following components: 0.1% caprylhydroxamic acid, 0.1% glyceryl caprylate.
The preparation method of the blumea oil comprises the following steps: taking 100 g of naturally dried folium artemisiae argyi, grinding, placing in a 1000ML round-bottom flask, adding 700ML distilled water, carrying out cold soaking for 2h, then carrying out heating extraction according to a steam distillation method, refluxing for 4h, separating out volatile oil, adding anhydrous sodium sulfate, and drying to obtain folium artemisiae argyi oil;
the preparation method of the radix angelicae pubescentis extract comprises the following steps: pulverizing radix Angelicae Pubescentis powder, filtering, and reflux-extracting with 4 times of methanol for three times, each time for 2 hr;
the preparation method of the purslane extract comprises the following steps: extracting from stem and leaf of herba Portulacae with low temperature method to obtain bioactive extract, and dissolving in butanediol solution;
the preparation method of the centella asiatica extract comprises the following steps: using ethanol solution as solvent, and performing crude extraction on centella asiatica by using an ultrasonic extraction method; separating out effective components by using an AB-8 resin separation column and using an ethanol solution as an eluent, wherein the target component eluted by 30-50% of ethanol and 51-75% of the ethanol solution is the centella asiatica extract;
the preparation method of the giant knotweed root extract comprises the following steps: pulverizing rhizoma Polygoni Cuspidati, refluxing with 95% ethanol for 2 times, each for 2 hr, mixing extractive solutions, recovering ethanol under reduced pressure until no alcohol smell exists, extracting with ethyl acetate, recovering ethyl acetate under reduced pressure to obtain stilbene, hydrolyzing water layer with acid, performing Soxhlet extraction with diethyl ether until colorless, extracting diethyl ether layer with 5% sodium hydroxide solution, acidifying to obtain anthraquinones, and mixing stilbene type anthraquinone to obtain rhizoma Polygoni Cuspidati extract;
the preparation method of the scutellaria baicalensis root extract comprises the following steps: decocting Scutellariae radix with water, mixing decoctions, concentrating, adjusting pH to 1.0-2.0 with hydrochloric acid, keeping the temperature at 80 deg.C, standing, filtering, adding appropriate amount of water into precipitate, stirring, adjusting pH to 7.0 with 40% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.0-2.0 with hydrochloric acid, standing at 60 deg.C for 30 min, washing precipitate with water and ethanol sequentially until pH is 7.0, volatilizing ethanol, and drying under reduced pressure to obtain the final product;
the preparation method of the tea extract comprises the following steps: treating raw tea leaves by steaming, collecting water vapor containing tea leaf aroma components generated from the raw tea leaves, and cooling the collected water vapor to obtain an extract containing the tea leaf aroma components;
the preparation method of the glycyrrhiza glabra root extract comprises the following steps: smashing glabrous greenbrier rhizome powder, then adding the glabrous greenbrier rhizome powder into liquid resin extracting solution, leaching for 24 hours, filtering, leaching again, filtering and combining the extracting solution, wherein the mass ratio of the glabrous greenbrier rhizome to the liquid resin extracting solution is 1: 5-10, adding the extracting solution into a calcium chloride solution until the calcium concentration is 0.02-0.006mol/L, standing until a precipitate is separated out, filtering, adding an ethyl acetate aqueous solution into the precipitate, adding acid to adjust the pH value of the solution to 2.0, extracting, dissolving, standing for layering, taking an ethyl acetate layer, carrying out reduced pressure concentration on the ethyl acetate layer solution, and then carrying out vacuum drying;
the preparation method of the chamomile flower extract comprises the following steps: decocting flos Chrysanthemi in water for 1-2 hr, filtering to obtain flos Chrysanthemi solution, decocting flos Chrysanthemi residue in water for 0.5-1 hr, filtering to obtain flos Chrysanthemi solution, discarding flos Chrysanthemi residue, mixing decoctions, concentrating to density below 60 deg.C of 1.05-1.2, and cooling to room temperature to obtain decoction;
the preparation method of the rosemary leaf extract comprises the following steps: putting 40-mesh rosemary powder into a 150mL triangular flask with a plug, adding an ethanol water solution, sealing, uniformly mixing, putting into an ultrasonic cleaner, carrying out ultrasonic treatment at normal temperature for 15min, taking out the triangular flask, carrying out suction filtration, and rotatably steaming the filtrate to be dry.
A preparation method of wormwood massage cream comprises the following steps:
1) adding the phase A into an emulsifying pot, heating to 85 ℃, homogenizing and uniformly stirring, and stirring for 30 minutes at the constant temperature for later use;
2) putting the phase B into an oil phase pot, heating to 80 ℃ to ensure complete dissolution, and stirring for 30 minutes at the constant temperature for later use;
3) homogenizing A, B at 80 deg.C, stirring, homogenizing, and stirring for 15 min;
4) cooling to 45 ℃, adding the phase C, and stirring uniformly;
5) adding phase D, and stirring.
Claims (4)
1. The wormwood massage cream is characterized by comprising a phase A, a phase B, a phase C and a phase D;
the phase A comprises the following components: glycerin, propylene glycol, erythritol, carbomer, allantoin, dipotassium glycyrrhizinate, methylparaben, xanthan gum, sodium hyaluronate and water;
the phase B comprises the following components: squalane, isohexadecane, ethylhexyl palmitate, cetearyl alcohol, cetearyl glucoside, tocopherol;
the phase C comprises the following components: menthol, mugwort leaf oil, pubescent angelica root extract, purslane extract, centella asiatica extract, giant knotweed rhizome root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract, rosemary leaf extract, bacillus/soybean fermentation product extract, ginger root oil;
the phase D comprises the following components: caprylhydroxamic acid, glyceryl caprylate.
2. The wormwood massage cream according to claim 1, wherein the massage cream comprises a phase A, a phase B, a phase C and a phase D;
the phase A comprises the following components in percentage by weight in the massage cream: 2% of glycerol, 2% of propylene glycol, 1% of erythritol, 0.1% of carbomer, 0.2% of allantoin, 0.1% of dipotassium glycyrrhizinate, 0.1% of methylparaben, 0.1% of xanthan gum, 0.1% of sodium hyaluronate and the balance of water;
the B phase comprises the following components in percentage by weight in the massage cream: 2% squalane, 2% isohexadecane, 2% ethylhexyl palmitate, 1% cetearyl alcohol, 1% cetearyl glucoside, 0.3% tocopherol;
the C phase comprises the following components in percentage by weight in the massage cream: 0.1% menthol, 2% argyi leaf oil, 2% pubescent angelica root extract, 2% purslane extract, 2% centella asiatica extract, 2% polygonum cuspidatum root extract, 2% scutellaria baicalensis root extract, 2% tea leaf extract, 2% glycyrrhiza glabra root extract, 2% chamomile flower extract, 2% rosemary leaf extract, 0.5% bacillus/soybean fermentation product extract, 0.1% ginger root oil;
the phase D comprises the following components: 0.1% caprylhydroxamic acid, 0.1% glyceryl caprylate.
3. The wormwood massage cream according to claim 2, wherein the preparation method of the wormwood oil comprises the following steps: taking 100 g of naturally dried folium artemisiae argyi, grinding, placing in a 1000ML round-bottom flask, adding 700ML distilled water, carrying out cold soaking for 2h, then carrying out heating extraction according to a steam distillation method, refluxing for 4h, separating out volatile oil, adding anhydrous sodium sulfate, and drying to obtain folium artemisiae argyi oil;
the preparation method of the radix angelicae pubescentis extract comprises the following steps: pulverizing radix Angelicae Pubescentis powder, filtering, and reflux-extracting with 4 times of methanol for three times, each time for 2 hr;
the preparation method of the purslane extract comprises the following steps: extracting from stem and leaf of herba Portulacae with low temperature method to obtain bioactive extract, and dissolving in butanediol solution;
the preparation method of the centella asiatica extract comprises the following steps: using ethanol solution as solvent, and performing crude extraction on centella asiatica by using an ultrasonic extraction method; separating out effective components by using an AB-8 resin separation column and using an ethanol solution as an eluent, wherein the target component eluted by 30-50% of ethanol and 51-75% of the ethanol solution is the centella asiatica extract;
the preparation method of the giant knotweed root extract comprises the following steps: pulverizing rhizoma Polygoni Cuspidati, refluxing with 95% ethanol for 2 times, each for 2 hr, mixing extractive solutions, recovering ethanol under reduced pressure until no alcohol smell exists, extracting with ethyl acetate, recovering ethyl acetate under reduced pressure to obtain stilbene, hydrolyzing water layer with acid, performing Soxhlet extraction with diethyl ether until colorless, extracting diethyl ether layer with 5% sodium hydroxide solution, acidifying to obtain anthraquinones, and mixing stilbene type anthraquinone to obtain rhizoma Polygoni Cuspidati extract;
the preparation method of the scutellaria baicalensis root extract comprises the following steps: decocting Scutellariae radix with water, mixing decoctions, concentrating, adjusting pH to 1.0-2.0 with hydrochloric acid, keeping the temperature at 80 deg.C, standing, filtering, adding appropriate amount of water into precipitate, stirring, adjusting pH to 7.0 with 40% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.0-2.0 with hydrochloric acid, standing at 60 deg.C for 30 min, washing precipitate with water and ethanol sequentially until pH is 7.0, volatilizing ethanol, and drying under reduced pressure to obtain the final product;
the preparation method of the tea extract comprises the following steps: treating raw tea leaves by steaming, collecting water vapor containing tea leaf aroma components generated from the raw tea leaves, and cooling the collected water vapor to obtain an extract containing the tea leaf aroma components;
the preparation method of the glycyrrhiza glabra root extract comprises the following steps: smashing glabrous greenbrier rhizome powder, then adding the glabrous greenbrier rhizome powder into liquid resin extracting solution, leaching for 24 hours, filtering, leaching again, filtering and combining the extracting solution, wherein the mass ratio of the glabrous greenbrier rhizome to the liquid resin extracting solution is 1: 5-10, adding the extracting solution into a calcium chloride solution until the calcium concentration is 0.02-0.006mol/L, standing until a precipitate is separated out, filtering, adding an ethyl acetate aqueous solution into the precipitate, adding acid to adjust the pH value of the solution to 2.0, extracting, dissolving, standing for layering, taking an ethyl acetate layer, carrying out reduced pressure concentration on the ethyl acetate layer solution, and then carrying out vacuum drying;
the preparation method of the chamomile flower extract comprises the following steps: decocting flos Chrysanthemi in water for 1-2 hr, filtering to obtain flos Chrysanthemi solution, decocting flos Chrysanthemi residue in water for 0.5-1 hr, filtering to obtain flos Chrysanthemi solution, discarding flos Chrysanthemi residue, mixing decoctions, concentrating to density below 60 deg.C of 1.05-1.2, and cooling to room temperature to obtain decoction;
the preparation method of the rosemary leaf extract comprises the following steps: putting 40-mesh rosemary powder into a 150mL triangular flask with a plug, adding an ethanol water solution, sealing, uniformly mixing, putting into an ultrasonic cleaner, carrying out ultrasonic treatment at normal temperature for 15min, taking out the triangular flask, carrying out suction filtration, and rotatably steaming the filtrate to be dry.
4. The preparation method of the wormwood massage cream is characterized by comprising the following steps:
1) adding the phase A into an emulsifying pot, heating to 85 ℃, homogenizing and uniformly stirring, and stirring for 30 minutes at the constant temperature for later use;
2) putting the phase B into an oil phase pot, heating to 80 ℃ to ensure complete dissolution, and stirring for 30 minutes at the constant temperature for later use;
3) homogenizing A, B at 80 deg.C, stirring, homogenizing, and stirring for 15 min;
4) cooling to 45 ℃, adding the phase C, and stirring uniformly;
5) adding phase D, and stirring.
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Cited By (1)
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CN114652620A (en) * | 2020-12-23 | 2022-06-24 | 天津拂瑞雅生物科技有限公司 | Private gel and preparation method thereof |
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CN106389162A (en) * | 2016-09-29 | 2017-02-15 | 广州暨南生物医药研究开发基地有限公司 | Massage oil emulsion containing argy wormwood leaf essential oil and preparation method of massage oil emulsion |
CN108524837A (en) * | 2018-06-12 | 2018-09-14 | 湖南金领玮业现代家庭服务产业联盟管理有限公司 | Warm clever moxibustion frost of one kind and preparation method thereof |
CN109568246A (en) * | 2018-12-24 | 2019-04-05 | 广州欧盛化妆品有限公司 | A kind of crease-resistant moisturiser and preparation method thereof |
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CN106389162A (en) * | 2016-09-29 | 2017-02-15 | 广州暨南生物医药研究开发基地有限公司 | Massage oil emulsion containing argy wormwood leaf essential oil and preparation method of massage oil emulsion |
CN108524837A (en) * | 2018-06-12 | 2018-09-14 | 湖南金领玮业现代家庭服务产业联盟管理有限公司 | Warm clever moxibustion frost of one kind and preparation method thereof |
CN109568246A (en) * | 2018-12-24 | 2019-04-05 | 广州欧盛化妆品有限公司 | A kind of crease-resistant moisturiser and preparation method thereof |
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CN114652620A (en) * | 2020-12-23 | 2022-06-24 | 天津拂瑞雅生物科技有限公司 | Private gel and preparation method thereof |
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