CN111827003A - High-temperature-resistant gloss oil for tipping paper and preparation method thereof - Google Patents
High-temperature-resistant gloss oil for tipping paper and preparation method thereof Download PDFInfo
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- CN111827003A CN111827003A CN202010754846.XA CN202010754846A CN111827003A CN 111827003 A CN111827003 A CN 111827003A CN 202010754846 A CN202010754846 A CN 202010754846A CN 111827003 A CN111827003 A CN 111827003A
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- temperature
- gloss oil
- tipping paper
- resistant gloss
- alcohol
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Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/18—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising waxes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
- D21H19/20—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paper (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention relates to high-temperature-resistant gloss oil for tipping paper and a preparation method thereof, wherein the high-temperature-resistant gloss oil for the tipping paper comprises the following components: 10.0-30.0% of nitrocotton, 0.0-15.0% of alcohol-soluble acrylic resin, 0.0-15.0% of maleic acid modified rosin resin, 0.0-1.0% of wax powder, 15-40.0% of ethanol, 30-50.0% of ethyl acetate and 0.0-5.0% of plasticizer.
Description
Technical Field
The invention relates to the technical field of printing ink, in particular to high-temperature-resistant gloss oil for tipping paper and a preparation method thereof.
Background
The tipping paper is special paper for lapping the cigarette and the filter tip, is printed and processed into the tipping paper for the cigarette by adopting transfer paper, and is more and more accepted by the market and has higher and higher occupation ratio due to exquisite printing and bright color. Because the transfer paper is formed by processing a transfer resin layer, a meson layer or an aluminum layer on the base paper of the common tipping paper, the printing ink adhesion of the transfer paper is different from the adhesion of the original base paper through penetration, the resin adhesion is mainly depended on, the resin accumulation and softening lead to the temperature resistance reduction of the tipping paper, the cigarette wrapping and heat sealing process of the product is easy to cause cigarette adhesion due to the softening of the resin with overhigh temperature. The gloss oil in the current market mainly focuses on environmental protection, brightness, wear resistance and the like, the gloss oil basically has no requirement on temperature resistance, and the gloss oil with poor temperature resistance is used on tipping paper, so that the problem of high-temperature adhesion of the transferring tipping paper is difficult to avoid.
Disclosure of Invention
The invention aims to provide high-temperature-resistant gloss oil for tipping paper, which has the advantages of small smell, low viscosity, good stability and temperature resistance of over 130 ℃, is suitable for being applied to a cigarette tipping paper photogravure press, and can effectively avoid the problem of high-temperature adhesion of transfer tipping paper.
The invention also aims to provide a preparation method of the high-temperature-resistant gloss oil for the tipping paper, which has the advantages of simple process and suitability for large-scale production.
The technical scheme of the invention is realized as follows:
a high-temperature resistant gloss oil for tipping paper comprises the following components in percentage by mass: 10.0-30.0% of nitrocotton, 0.0-15.0% of alcohol-soluble acrylic resin, 0.0-15.0% of maleic acid modified rosin resin, 0.0-1.0% of wax powder, 15-40.0% of ethanol, 30-50.0% of ethyl acetate and 0.0-5.0% of plasticizer, wherein the sum of the weight percentages of the components is 100%.
Preferably, the nitrocotton is L-shaped 1/8 sec alcohol-soluble nitrocotton, and the nitrogen content of the nitrocotton is 10-12%.
Preferably, the alcohol-soluble acrylic resin is formed by polymerizing methyl methacrylate and butyl acrylate, the molecular weight of the alcohol-soluble acrylic resin is 10000, and the softening point of the alcohol-soluble acrylic resin is more than 150 ℃.
Preferably, the maleic acid modified rosin resin is prepared by taking gum rosin as a raw material, performing addition reaction with maleic anhydride, and performing esterification polymerization with glycerol or pentaerythritol, and the softening point of the resin is above 130 ℃.
Preferably, the wax powder is micronized polyethylene wax with a drop melting point above 130 ℃.
Preferably, the plasticizer is tributyl citrate or acetyl tributyl citrate.
A preparation method of high-temperature-resistant gloss oil for tipping paper comprises the following steps:
step 1: under the condition of stirring, firstly adding ethyl acetate and ethanol to obtain a mixed solvent a;
step 2: : adding nitrocotton, alcohol-soluble acrylic resin, maleic acid modified rosin resin and a plasticizer into the mixed solvent a obtained in the step 1 according to a ratio, and stirring and fully dissolving the mixture by using a stirrer to obtain a mixed solvent b;
and step 3: adding wax powder into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper;
and 4, step 4: and (4) filtering the tipping paper obtained in the step (3) by using high-temperature resistant gloss oil, and then packaging, detecting and warehousing.
Preferably, the stirring speed of the stirrer in the step 2 is 500-1000 rpm; the time is 60-120 min.
Preferably, the stirring speed of the stirrer in the step 3 is 700-1200 rpm; the time is 20-30 min.
Preferably, the filtration mode in step 4 is 200-mesh filter bags, and the filtration is carried out in bag filters.
In conclusion, the beneficial effects of the invention are as follows:
1. the invention provides high-temperature-resistant gloss oil for tipping paper, which adopts the technical scheme that the wear resistance and the transparency of the gloss oil as a surface layer are considered, the temperature resistance is also fully considered, the temperature resistance is over 130 ℃, the gloss oil is suitable for being applied to a cigarette tipping paper gravure printing machine, the problem of resin softening and adhesion in the tipping paper rolling process can be effectively prevented, and the gloss oil has the advantages of small smell, low viscosity and good stability. In addition, the high-temperature-resistant gloss oil for the tipping paper takes the alcohol-soluble resin as a main body and the ethanol and ethyl ester mixture as a solvent, so that the dosage of the ester solvent is reduced, the high-temperature-resistant gloss oil is volatile, and the high-temperature-resistant gloss oil is suitable for food and tobacco packaging and reduces VOC (volatile organic compounds) emission.
2. The invention provides a preparation method of high-temperature-resistant gloss oil for tipping paper, which has the advantages of simple and convenient process and suitability for large-scale production.
Detailed Description
The following description is only a preferred embodiment of the present invention, and the protection scope is not limited to the embodiment, and any technical solution that falls under the idea of the present invention should fall within the protection scope of the present invention. It should also be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention.
The embodiment of the invention provides high-temperature-resistant gloss oil for tipping paper, which comprises the following components in percentage by mass: 10.0-30.0% of nitrocotton, 0.0-15.0% of alcohol-soluble acrylic resin, 0.0-15.0% of maleic acid modified rosin resin, 0.0-1.0% of wax powder, 15-40.0% of ethanol, 30-50.0% of ethyl acetate and 0.0-5.0% of plasticizer, wherein the sum of the weight percentages of the components is 100%.
Preferably, the nitrocotton is L-shaped 1/8 second alcohol-soluble nitrocotton, the nitrogen content of the nitrocotton is 10-12%, the 1/8 second alcohol-soluble nitrocotton is easily dissolved by alcohol, the smell is low, and a film with thermoplasticity can be formed.
Preferably, the alcohol-soluble acrylic resin is formed by polymerizing methyl methacrylate and butyl acrylate, the molecular weight of the alcohol-soluble acrylic resin is 10000, and the softening point of the alcohol-soluble acrylic resin is more than 150 ℃.
Preferably, the maleic acid modified rosin resin is prepared by taking gum rosin as a raw material, performing addition reaction with maleic anhydride, and performing esterification polymerization with glycerol or pentaerythritol, and has a softening point of over 130 ℃ and good heat resistance.
Preferably, the wax powder is micronized polyethylene wax with a dropping melting point of more than 130 ℃, the main functions of the wax powder are light moistening and light extinction, the flow can be improved, a smooth surface is obtained, the scratch resistance of the gloss oil is increased, the scratch resistance, the wear resistance, the high temperature resistance and the blocking resistance of the gloss oil can be obviously improved by the micronized polyethylene wax with the dropping melting point of more than 130 ℃, and the micronized polyethylene wax can be replaced by the micronized polypropylene wax and can also achieve the same effect.
Preferably, the plasticizer is tributyl citrate, the plasticizer can increase the shaping and adhesive force of the gloss oil, the adopted tributyl citrate has high boiling point and good plasticizing effect, and can endow the gloss oil with good cold resistance, water resistance and mildew resistance, and the tributyl citrate can be replaced by acetyl tributyl citrate to achieve the same effect.
The embodiment of the invention also provides a preparation method of the high-temperature-resistant gloss oil for tipping paper, which comprises the following steps:
step 1: under the condition of stirring, firstly adding ethyl acetate and ethanol to obtain a mixed solvent a;
step 2: adding nitrocotton, alcohol-soluble acrylic resin, maleic acid modified rosin resin and a plasticizer into the mixed solvent a obtained in the step 1 according to a ratio, and stirring and fully dissolving the mixture by using a stirrer to obtain a mixed solvent b;
and step 3: adding wax powder into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper;
and 4, step 4: and (4) filtering the tipping paper obtained in the step (3) by using high-temperature resistant gloss oil, and then packaging, detecting and warehousing.
Preferably, the stirring speed of the stirrer in the step 2 is 500-1000 rpm; the time is 60-120 min.
Preferably, the stirring speed of the stirrer in the step 3 is 700-1200 rpm; the time is 20-30 min.
Preferably, the filtration mode in the step 4 adopts 200-mesh filter bags to carry out filtration in a bag filter.
Example 1
The embodiment of the invention provides high-temperature-resistant gloss oil for tipping paper, which comprises the following components in percentage by mass: 15% of L-type 1/8 second nitro-cotton, 5% of alcohol-soluble acrylic resin, 5% of maleic acid modified rosin resin, 1.0% of polyethylene wax, 5% of tributyl citrate, 30% of ethanol and 39% of ethyl acetate.
The preparation method comprises the following steps:
step 1: under the condition of stirring, firstly adding ethanol and ethyl acetate solvent to obtain a mixed solvent a;
step 2: adding L-type 1/8 second alcohol-soluble nitrocotton, alcohol-soluble acrylic resin, maleic acid modified rosin resin and tributyl citrate into the mixed solvent a obtained in the step 1, and stirring and fully dissolving the mixture by using a stirrer to obtain a mixed solvent b; the dispersion stirring speed of the stirrer is 500 r/min, and the time is 110 min.
And step 3: adding polyethylene wax into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper; the dispersion stirring speed of the stirrer is 1200 r/min, and the time is 20 min.
And 4, step 4: filtering in a bag filter by using a filter bag with 200 meshes, and then packaging, detecting and warehousing.
The gloss oil prepared by the embodiment has the temperature resistance of 140 ℃, namely, the gloss oil can not generate viscosity in the environment of 140 ℃, has small smell and low VOC (volatile organic compounds) emission, and meets the daily production requirement.
Example 2
The embodiment of the invention provides high-temperature-resistant gloss oil for tipping paper, which comprises the following components in percentage by mass: 30% of L-type 1/8 second nitrocotton, 0% of alcohol-soluble acrylic resin, 10% of maleic acid modified rosin resin, 1.0% of polyethylene wax, 5% of tributyl citrate, 20% of ethanol and 34% of ethyl acetate.
The preparation method comprises the following steps:
step 1: under the condition of stirring, firstly adding ethanol and ethyl acetate solvent to obtain a mixed solvent a;
step 2: adding L-shaped 1/8 sec alcohol-soluble nitrocotton, maleic acid modified rosin resin and tributyl citrate into the mixed solvent a obtained in the step (1), and stirring and fully dissolving by using a stirrer to obtain a mixed solvent b; the dispersion stirring speed of the stirrer is 300 r/min, and the time is 120 min.
And step 3: adding polyethylene wax into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper; the dispersion stirring speed of the stirrer is 900 r/min, and the time is 20 min.
And 4, step 4: filtering in a bag filter by using a filter bag with 200 meshes, and then packaging, detecting and warehousing.
The gloss oil prepared by the embodiment has the temperature resistance up to 160 ℃, good temperature resistance effect and high stability.
Example 3
The embodiment of the invention provides high-temperature-resistant gloss oil for tipping paper, which comprises the following components in percentage by mass: 20% of L-type 1/8 second nitrocotton, 10% of alcohol-soluble acrylic resin, 0% of maleic acid modified rosin resin, 1.0% of polyethylene wax, 5% of tributyl citrate, 20% of ethanol and 44% of ethyl acetate.
The preparation method comprises the following steps:
step 1: under the condition of stirring, firstly adding ethanol and ethyl acetate solvent to obtain a mixed solvent a;
step 2: adding the L-type 1/8 sec alcohol-soluble nitrocotton, the alcohol-soluble acrylic resin and the tributyl citrate into the mixed solvent a obtained in the step 1, and stirring and fully dissolving the mixture by using a stirrer to obtain a mixed solvent b; the dispersion stirring speed of the stirrer is 800 r/min, and the time is 70 min.
And step 3: adding polyethylene wax into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper; the dispersion stirring speed of the stirrer is 800 r/min, and the time is 30 min.
And 4, step 4: filtering in a bag filter by using a filter bag with 200 meshes, and then packaging, detecting and warehousing.
The gloss oil prepared by the embodiment has the temperature resistance of 180 ℃, excellent temperature resistance effect, low high-temperature viscocity, good stability and low smell, and is suitable for any high-temperature environment in production.
Table 1 shows the temperature resistance of the gloss oil in the temperature resistance test, and in addition to the gloss oil according to the present invention, the commercially available alcohol-soluble gloss oil, ester-soluble gloss oil, and water-based gloss oil were used for comparison, and the specific results were as follows:
in conclusion, the temperature resistance of the transfer tipping paper is better in example 1, good in example 2 and excellent in example 3, and the examples 1, 2 and 3 can meet the use requirement on temperature in ordinary production and can effectively avoid the problem of high-temperature adhesion of the transfer tipping paper.
Claims (10)
1. The utility model provides a connect dress paper with high temperature resistant gloss oil which characterized in that: the composite material comprises the following components in percentage by mass: 10.0-30.0% of nitrocotton, 0.0-15.0% of alcohol-soluble acrylic resin, 0.0-15.0% of maleic acid modified rosin resin, 0.0-1.0% of wax powder, 15-40.0% of ethanol, 30-50.0% of ethyl acetate and 0.0-5.0% of plasticizer, wherein the sum of the weight percentages of the components is 100%.
2. The high-temperature-resistant gloss oil for tipping paper according to claim 1, characterized in that: the nitrocotton is L-shaped 1/8 sec alcohol-soluble nitrocotton, and the nitrogen content of the nitrocotton is 10-12%.
3. The high-temperature-resistant gloss oil for tipping paper according to claim 1, characterized in that: the alcohol-soluble acrylic resin is formed by polymerizing methyl methacrylate and butyl acrylate, the molecular weight of the alcohol-soluble acrylic resin is 10000, and the softening point of the alcohol-soluble acrylic resin is more than 150 ℃.
4. The high-temperature-resistant gloss oil for tipping paper according to claim 1, characterized in that: the maleic acid modified rosin resin is prepared by taking gum rosin as a raw material, performing addition reaction with maleic anhydride, and performing esterification polymerization with glycerol or pentaerythritol, and the softening point of the resin is above 130 ℃.
5. The high-temperature-resistant gloss oil for tipping paper according to claim 1, characterized in that: the wax powder is micronized polyethylene wax with a dropping melting point above 130 ℃.
6. The high-temperature-resistant gloss oil for tipping paper according to claim 1, characterized in that: the plasticizer is tributyl citrate.
7. The method for preparing the high-temperature-resistant gloss oil for the tipping paper according to claim 1, characterized by comprising the following steps: the preparation method comprises the following steps:
step 1: under the condition of stirring, firstly adding ethyl acetate and ethanol to obtain a mixed solvent a;
step 2: adding nitrocotton, alcohol-soluble acrylic resin, maleic acid modified rosin resin and a plasticizer into the mixed solvent a obtained in the step 1 according to a ratio, and stirring and fully dissolving the mixture by using a stirrer to obtain a mixed solvent b;
and step 3: adding wax powder into the mixed solvent b obtained in the step 2, and stirring and dispersing uniformly by using a stirrer to obtain high-temperature-resistant gloss oil for tipping paper;
and 4, step 4: and (4) filtering the tipping paper obtained in the step (3) by using high-temperature resistant gloss oil, and then packaging, detecting and warehousing.
8. The method for preparing the high-temperature-resistant gloss oil for the tipping paper according to claim 7, characterized by comprising the following steps: the stirring speed of the stirrer in the step 2 is 500-1000 r/min, and the time is 60-120 min.
9. The method for preparing the high-temperature-resistant gloss oil for the tipping paper according to claim 7, characterized by comprising the following steps: the stirring speed of the stirrer in the step 3 is 700-1200 r/min, and the time is 20-30 min.
10. The method for preparing the high-temperature-resistant gloss oil for the tipping paper according to claim 7, characterized by comprising the following steps: the filtration mode in step 4 is 200-mesh filter bag filtration in a bag filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010754846.XA CN111827003A (en) | 2020-07-31 | 2020-07-31 | High-temperature-resistant gloss oil for tipping paper and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010754846.XA CN111827003A (en) | 2020-07-31 | 2020-07-31 | High-temperature-resistant gloss oil for tipping paper and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113278325A (en) * | 2021-05-24 | 2021-08-20 | 江苏卫星新材料股份有限公司 | Flocking ink for printing cigarette tipping paper and preparation method thereof |
| CN113622216A (en) * | 2021-08-11 | 2021-11-09 | 湖北中烟工业有限责任公司 | Tipping paper product based on flavor-changing protein and preparation method thereof |
| CN113773703A (en) * | 2021-10-26 | 2021-12-10 | 湖北中烟工业有限责任公司 | Anti-adhesion gloss oil for cigarette tipping paper and preparation method and application thereof |
| CN113931004A (en) * | 2021-11-19 | 2022-01-14 | 增和包装股份有限公司 | Improved process for softness of ester-soluble ink tipping paper |
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| CN103254687A (en) * | 2013-05-24 | 2013-08-21 | 东莞市锐达涂料有限公司 | High-temperature resistant ester-soluble printing ink |
| CN107043571A (en) * | 2017-02-22 | 2017-08-15 | 长春吉星印务有限责任公司 | A kind of alcohol-soluble intaglio plate Anti-curling gloss oil and preparation method thereof |
| CN110511611A (en) * | 2019-10-17 | 2019-11-29 | 温州立可达印业股份有限公司 | A kind of aqueous tipping paper printing ink |
| CN110862713A (en) * | 2019-12-09 | 2020-03-06 | 江苏泰格油墨有限公司 | Alcohol-soluble nitrocellulose light-variable ink and preparation process thereof |
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| CN101864245A (en) * | 2010-04-30 | 2010-10-20 | 佛山市顺德区乐从镇盛昌油墨有限公司 | Alcohol-soluble printing varnish and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113278325A (en) * | 2021-05-24 | 2021-08-20 | 江苏卫星新材料股份有限公司 | Flocking ink for printing cigarette tipping paper and preparation method thereof |
| CN113622216A (en) * | 2021-08-11 | 2021-11-09 | 湖北中烟工业有限责任公司 | Tipping paper product based on flavor-changing protein and preparation method thereof |
| CN113773703A (en) * | 2021-10-26 | 2021-12-10 | 湖北中烟工业有限责任公司 | Anti-adhesion gloss oil for cigarette tipping paper and preparation method and application thereof |
| CN113931004A (en) * | 2021-11-19 | 2022-01-14 | 增和包装股份有限公司 | Improved process for softness of ester-soluble ink tipping paper |
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