CN111826994A - Preparation method of cigar-flavor cigarette paper - Google Patents
Preparation method of cigar-flavor cigarette paper Download PDFInfo
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- CN111826994A CN111826994A CN202010670391.3A CN202010670391A CN111826994A CN 111826994 A CN111826994 A CN 111826994A CN 202010670391 A CN202010670391 A CN 202010670391A CN 111826994 A CN111826994 A CN 111826994A
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- cigar
- cigarette paper
- bacterial cellulose
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/10—Coatings without pigments
- D21H19/14—Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/14—Carboxylic acids; Derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
- D21H17/25—Cellulose
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H23/00—Processes or apparatus for adding material to the pulp or to the paper
- D21H23/02—Processes or apparatus for adding material to the pulp or to the paper characterised by the manner in which substances are added
- D21H23/22—Addition to the formed paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H25/00—After-treatment of paper not provided for in groups D21H17/00 - D21H23/00
- D21H25/04—Physical treatment, e.g. heating, irradiating
- D21H25/06—Physical treatment, e.g. heating, irradiating of impregnated or coated paper
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- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to a preparation method of cigar flavor cigarette paper, which comprises the steps of uniformly dip-coating a bacterial cellulose dispersion liquid on a coating machine to the cigarette paper during the production of the cigarette paper, and drying the cigarette paper by a quick low-temperature drying cylinder, so that the bacterial cellulose dispersion liquid and the cigarette paper are tightly combined together and are uniformly distributed. Along with the burning and smoking of the cigarette, the cigarette can be endowed with rich cigar aroma, the aroma is rich and full, the aftertaste is natural and comfortable, the active effects of improving the sweet and moist feeling, the thick feeling and the richness of the cigarette smoke, reducing the smoke irritation and covering the miscellaneous gas are achieved, and the style characteristics of the cigar type cigarette can be stabilized and enhanced.
Description
Technical Field
The invention belongs to the technical field of cigarettes, and particularly relates to a preparation method of cigar flavor cigarette paper.
Background
The cigar-type cigarette integrates the advantages and characteristics of cigar and flue-cured tobacco, and has the flavor characteristics of rich and rich cigar and pure and comfortable flue-cured tobacco. In recent years, the output and sales of cigar-type cigarettes in China are remarkably increased, the consumer groups are continuously expanded, and meanwhile, the problem of serious shortage of high-quality cigar tobacco raw materials is faced.
Compared with imported raw materials, the domestic cigar tobacco leaves have the characteristics of weaker fragrance, insufficient fragrance concentration, larger strength, obvious miscellaneous gas, and heavier bitter taste and astringent taste. Under the existing situation, it is urgent to strengthen the cigar flavor characteristics of cigar-type cigarettes, meet and adapt to the requirements of consumers on the quality and taste of cigarettes, and further effectively improve the market competitiveness of cigar-type cigarettes.
Disclosure of Invention
The invention aims to provide a preparation method of cigar flavor cigarette paper, which aims to solve the problems that high-quality cigar tobacco raw materials are seriously short or essence or spice is directly added into cigarette filters or tobacco shreds, so that the essence and spice are not uniformly released or the release amount of harmful components is increased, and the like.
The invention is realized by the following technical scheme:
a preparation method of cigar flavor cigarette paper comprises the following steps:
s1, extracting the cigar powder with water to obtain a uniform and transparent solution, and removing water to obtain a cigar extracting solution;
s2, adjusting the obtained cigar extract to be weakly acidic, subpackaging and sterilizing, inoculating the activated cellulose-producing flora into the solution according to the set inoculation amount, and culturing at constant temperature for 2-3 weeks to obtain a bacterial cellulose membrane;
s3, taking out the bacterial cellulose membrane, and performing homogenization treatment by adopting a mechanical method to obtain uniformly dispersed bacterial cellulose slurry;
s4, adding the combustion improver into the bacterial cellulose slurry according to a set proportion to obtain a cigarette paper sizing solution;
s5, uniformly coating the cigarette paper sizing solution on the cigarette paper through a coating machine, and then quickly drying for 5-10S at 70-100 ℃ to obtain the cigar flavor cigarette paper.
Preferably, the mass ratio of the cigar powder to the water in the water extraction of the cigar powder in the step S1 is 1: 5-1: 10, soaking for 2-5 hours, and heating and extracting for 2-6 hours.
Preferably, water is removed by distillation under reduced pressure in step S1.
Preferably, the cellulose-producing flora in step S2 includes, but is not limited to, gluconacetobacter xylinus, acetobacter xylinus, or black tea fungus.
Preferably, in step S2, the pH of the cigar extract is adjusted to 5-6.5 using diluted acetic acid.
Preferably, in step S2, the sterilization temperature is 120 ℃, the sterilization time is 10-30 min, and the inoculation amount is 2-6% of the weight of the packaged and sterilized cigar extract.
Preferably, in step S3, the mass concentration of the bacterial cellulose in the bacterial cellulose slurry is 0.1% to 0.5%.
Preferably, in step S4, the combustion improver is potassium citrate or sodium citrate, and the mass concentration of the combustion improver in the cigarette paper sizing solution is 12-20%.
Preferably, the addition amount of the bacterial cellulose accounts for 2-6% of the weight of the cigarette paper, and the addition amount of the combustion improver accounts for 0.7-3% of the weight of the cigarette paper.
The invention has the beneficial effects that:
according to the technical scheme, the cigarette paper sizing agent is uniformly dip-coated on the back surface of the cigarette paper on a coating machine during the production of the cigarette paper, and then the cigarette paper is dried by a low-temperature drying cylinder, so that on one hand, the fragrance components are embedded by bacterial cellulose to reduce the loss of the fragrance components, on the other hand, new hydrogen bonds are formed between the exposed hydroxyl on the surface of the bacterial fibers and the hydroxyl on the surface of the plant fibers, and a space network structure formed by the bacterial fibers plays a bridging role well among the fibers, so that the bonding force among the fibers can be increased, and the physical strength of the finished.
The aroma components can reduce the generation of harmful components under the combustion condition of low temperature and oxygen enrichment, the release is relatively uniform and stable, and the difference in mouth-to-mouth suction can be reduced.
Detailed Description
The following embodiments are merely exemplary, and can be used to explain and illustrate the technical solution of the present invention, but not be construed as limiting the technical solution of the present invention.
According to the technical scheme, cigar powder collected in a tobacco shred making workshop is used as a raw material, a cigar extracting solution is prepared through water leaching and concentrated, the cigar concentrated solution is used as a culture medium to prepare bacterial cellulose, the bacterial cellulose is homogenized and is mixed with a combustion improver to be subjected to new technologies of coating in a machine, drying in a low-temperature drying cylinder and the like in the production of cigarette paper, the adding uniformity and the retention performance of spices on the cigarette paper are ensured, and the purpose of stabilizing and strengthening the style characteristics of cigar type cigarettes is achieved.
Example 1
Weighing 5.0kg cigar powder, adding 50.0kg water, soaking for 2 hr, heating under mechanical stirring to boil, keeping slightly boiling state for 2 hr, cooling to room temperature, filtering under reduced pressure to collect filtrate, and distilling under reduced pressure to remove about 1/4 vol water to obtain cigar extractive solution.
Adjusting pH of the cigar extractive solution to 5 with 10% diluted acetic acid, packaging into conical bottle with plug, sealing with sealing film, and sterilizing at 120 deg.C for 20 min.
Inoculating the black tea strain into the sterilizing solution in an inoculation amount of 6 wt% of the cigar extracting solution in the conical flask with the plug, fully shaking, and standing and culturing at the constant temperature of 30 ℃ for 2 weeks. After 2 weeks, the resulting brown bacterial cellulose membrane floated on the surface of the solution.
The brown cellulose membrane was removed and homogenized in a standard fluffer to give a slurry having a concentration of about 0.3%.
2.4kg of potassium citrate is weighed and dissolved in 20.0kg of the serous fluid, so that the mass concentration of the combustion improver is 12 percent, and the cigarette paper sizing fluid is obtained.
Preparing cigarette paper according to the cigarette paper production and manufacturing process: defibering, pulping, proportioning long and short fibers, adding a filler and a functional auxiliary agent, dehydrating, forming paper, squeezing, drying and reeling. Weighing 50kg of newly prepared cigarette paper, spraying bacterial cellulose slurry on the back of the cigarette paper in an off-line manner by adopting an off-line coating machine, drying by using a low-temperature drying cylinder at the temperature of 70 ℃ until the bacterial cellulose slurry is completely dried, and finally cutting to obtain the cigar flavor cigarette paper A, wherein the bacterial cellulose accounts for about 3% of the weight of the cigarette paper, and the combustion improver accounts for 1.2%.
Example 2
Weighing 5.0kg cigar powder, adding 50.0kg water, soaking for 3 hr, heating to boil under mechanical stirring, maintaining slightly boiling state for 3 hr, cooling to room temperature, filtering under reduced pressure to collect filtrate, and distilling under reduced pressure to remove about 1/5 vol water to obtain cigar extractive solution.
Adjusting pH of the cigar extractive solution to 6 with 10% diluted acetic acid, packaging into conical bottle with plug, sealing with sealing film, and sterilizing at 120 deg.C for 30 min.
Inoculating the strain of the gluconacetobacter xylinus into the sterilizing solution in an inoculation amount of 4% by weight of the cigar extract in the conical flask with the plug, sufficiently shaking, and then standing and culturing at constant temperature of 30 ℃ for 2 weeks. After 2 weeks, the resulting brown bacterial cellulose membrane floated on the surface of the solution.
The brown cellulose membrane was removed and homogenized in a standard fluffer to give a slurry having a concentration of about 0.2%.
4.0kg of potassium citrate was weighed out and dissolved in 20.0kg of the above slurry so that the concentration percentage of the combustion improver was 20%.
Preparing cigarette paper according to the cigarette paper production and manufacturing process: defibering, pulping, proportioning long and short fibers, adding a filler and a functional auxiliary agent, dehydrating, forming paper, squeezing, drying and reeling. Weighing 50kg of newly prepared cigarette paper, spraying bacterial cellulose slurry on the back of the cigarette paper in an off-line manner by adopting an off-line coating machine, drying by using a low-temperature drying cylinder at the temperature of 80 ℃ until the bacterial cellulose slurry is completely dried, and finally cutting to obtain the cigar flavor cigarette paper B, wherein the bacterial cellulose accounts for 2 percent of the weight of the cigarette paper, and the combustion improver accounts for 2.0 percent.
Example 3
Weighing 5.0kg cigar powder, adding 48.0kg water, soaking for 2 hr, heating to boil under mechanical stirring, maintaining slightly boiling state for 2 hr, cooling to room temperature, filtering under reduced pressure to collect filtrate, and distilling under reduced pressure to remove about 1/3 vol water to obtain cigar extractive solution.
Adjusting pH of the cigar extractive solution to 5.6 with 10% diluted acetic acid, packaging into conical bottle with plug, sealing with sealing film, and sterilizing in 120 deg.C sterilizing pan for 20 min.
Inoculating acetobacter xylinum strain into the sterilized solution in an inoculation amount of 3% of the weight of the cigar extract in the conical flask with the plug, fully shaking, and standing and culturing at constant temperature of 30 ℃ for 2 weeks. After 2 weeks, the resulting brown bacterial cellulose membrane floated on the surface of the solution.
Taking out the brown cellulose membrane, and homogenizing in a standard fluffer to obtain a slurry with bacterial cellulose concentration of about 0.5%.
3.0kg of potassium citrate was weighed out and dissolved in 20.0kg of the above slurry so that the concentration percentage of the combustion improver was 15%.
Preparing cigarette paper according to the cigarette paper production and manufacturing process: defibering, pulping, proportioning long and short fibers, adding a filler and a functional auxiliary agent, dehydrating, forming paper, squeezing, drying and reeling. Weighing 50kg of newly prepared cigarette paper, spraying bacterial cellulose slurry on the back of the cigarette paper in an off-line manner by adopting an off-line coating machine, drying by using a low-temperature drying cylinder at the temperature of 90 ℃ until the bacterial cellulose slurry is completely dried, and finally cutting to obtain the cigar flavor cigarette paper C, wherein the bacterial cellulose accounts for 5% of the weight of the cigarette paper, and the combustion improver accounts for 1.5%.
The prepared cigar flavor cigarette paper and common cigarette paper with the same quantitative index, air permeability index, ash content index and other indexes are respectively rolled into cigarette samples by adopting the same cut tobacco, the cigarette samples are respectively marked as sample cigarettes (A-C) and blank cigarettes, the blank cigarettes are used as comparative examples, and cigarette sensory quality evaluation is carried out on the prepared sample cigarettes according to the standard of GB5606.4-2005 'fourth part sensory technical requirements of cigarettes', and the results are shown in Table 1.
TABLE 1 cigarette sensory quality evaluation
As can be seen from the table 1, when the cigar flavor cigarette paper prepared by the invention is used in cigarettes, the fragrance score of the cigarettes is increased compared with that of a comparison sample, the cigar flavor cigarette paper has obvious cigar flavor notes, the effects of inhibiting irritation, covering offensive odor, improving aftertaste and the like can be achieved, the sensory quality is overall good, and the cigar flavor cigarette paper has a certain application prospect.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. A preparation method of cigar flavor cigarette paper is characterized by comprising the following steps:
s1, extracting the cigar powder with water to obtain a uniform and transparent solution, and removing water to obtain a cigar extracting solution;
s2, adjusting the obtained cigar extract to be weakly acidic, subpackaging and sterilizing, inoculating the activated cellulose-producing flora into the solution according to the set inoculation amount, and culturing at constant temperature for 2-3 weeks to obtain a bacterial cellulose membrane;
s3, taking out the bacterial cellulose membrane, and performing homogenization treatment by adopting a mechanical method to obtain uniformly dispersed bacterial cellulose slurry;
s4, adding the combustion improver into the bacterial cellulose slurry according to a set proportion to obtain a cigarette paper sizing solution;
s5, uniformly coating the cigarette paper sizing solution on the cigarette paper through a coating machine, and then quickly drying for 5-10S at 70-100 ℃ to obtain the cigar flavor cigarette paper.
2. The preparation method of the cigar-flavor cigarette paper as claimed in claim 1, wherein the water extraction of the cigar powder in the step S1 has a cigar powder to water mass ratio of 1: 5-1: 10, soaking for 2-5 hours, and heating and extracting for 2-6 hours.
3. The method for preparing cigar-flavor cigarette paper according to claim 1, wherein the water is removed by distillation under reduced pressure in step S1.
4. The method of making a cigar-flavored cigarette paper according to claim 1, wherein the cellulose-producing flora in step S2 includes, but is not limited to, gluconacetobacter xylinus, acetobacter xylinus, or black tea fungus.
5. The method of preparing cigar-flavor cigarette paper as claimed in claim 1, wherein in step S2, the pH of the cigar extract is adjusted to 5-6.5 using diluted acetic acid.
6. The preparation method of the cigar-flavor cigarette paper as claimed in claim 1, wherein in the step S2, the sterilization temperature is 120 ℃, the sterilization time is 10-30 min, and the inoculation amount is 2-6% of the weight of the packaged and sterilized cigar extract.
7. The preparation method of the cigar flavor cigarette paper as claimed in claim 1, wherein in the step S3, the mass concentration of the bacterial cellulose in the bacterial cellulose slurry is 0.1-0.5%.
8. The preparation method of the cigar-flavor cigarette paper as claimed in claim 1, wherein in the step S4, the combustion improver is potassium citrate or sodium citrate, and the mass concentration of the combustion improver in the cigarette paper sizing solution is 12-20%.
9. The preparation method of the cigar-flavor cigarette paper as claimed in claim 1, wherein the addition amount of the bacterial cellulose accounts for 2-6% of the weight of the cigarette paper, and the addition amount of the combustion improver accounts for 0.7-3% of the weight of the cigarette paper.
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| CN202010670391.3A CN111826994B (en) | 2020-07-13 | 2020-07-13 | Preparation method of cigar-flavor cigarette paper |
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| CN202010670391.3A CN111826994B (en) | 2020-07-13 | 2020-07-13 | Preparation method of cigar-flavor cigarette paper |
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| CN111826994A true CN111826994A (en) | 2020-10-27 |
| CN111826994B CN111826994B (en) | 2022-05-24 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113403878A (en) * | 2021-06-16 | 2021-09-17 | 河南中烟工业有限责任公司 | Preparation method of tobacco fragrant cigarette paper with moisture retention function |
| CN113424981A (en) * | 2021-06-16 | 2021-09-24 | 河南中烟工业有限责任公司 | Preparation method of tobacco sheets of heated cigarettes |
| CN113463437A (en) * | 2021-06-16 | 2021-10-01 | 河南中烟工业有限责任公司 | Preparation method of fragrance slow-release wrap paper |
| CN113519882A (en) * | 2021-06-16 | 2021-10-22 | 河南中烟工业有限责任公司 | Method for preparing sour-flavor tobacco extract by using acetobacter gluconicum |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113403878A (en) * | 2021-06-16 | 2021-09-17 | 河南中烟工业有限责任公司 | Preparation method of tobacco fragrant cigarette paper with moisture retention function |
| CN113424981A (en) * | 2021-06-16 | 2021-09-24 | 河南中烟工业有限责任公司 | Preparation method of tobacco sheets of heated cigarettes |
| CN113463437A (en) * | 2021-06-16 | 2021-10-01 | 河南中烟工业有限责任公司 | Preparation method of fragrance slow-release wrap paper |
| CN113519882A (en) * | 2021-06-16 | 2021-10-22 | 河南中烟工业有限责任公司 | Method for preparing sour-flavor tobacco extract by using acetobacter gluconicum |
| CN113424981B (en) * | 2021-06-16 | 2022-10-25 | 河南中烟工业有限责任公司 | Preparation method of tobacco sheets of heated cigarettes |
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| CN111826994B (en) | 2022-05-24 |
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