CN111793517A - 一种新型润滑材料及其制作工艺 - Google Patents
一种新型润滑材料及其制作工艺 Download PDFInfo
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- CN111793517A CN111793517A CN202010706542.6A CN202010706542A CN111793517A CN 111793517 A CN111793517 A CN 111793517A CN 202010706542 A CN202010706542 A CN 202010706542A CN 111793517 A CN111793517 A CN 111793517A
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- 230000001050 lubricating effect Effects 0.000 title claims abstract description 28
- 239000000463 material Substances 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 34
- YUTUUOJFXIMELV-UHFFFAOYSA-N 2-Hydroxy-2-(2-methoxy-2-oxoethyl)butanedioic acid Chemical compound COC(=O)CC(O)(C(O)=O)CC(O)=O YUTUUOJFXIMELV-UHFFFAOYSA-N 0.000 claims abstract description 26
- KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical compound O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 claims abstract description 26
- -1 polyoxyethylene Polymers 0.000 claims abstract description 21
- 239000003921 oil Substances 0.000 claims abstract description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 13
- HCVBQXINVUFVCE-UHFFFAOYSA-N Citronensaeure-beta-methylester Natural products COC(=O)C(O)(CC(O)=O)CC(O)=O HCVBQXINVUFVCE-UHFFFAOYSA-N 0.000 claims abstract description 13
- BWXDHBQGBNPJMN-UHFFFAOYSA-N Lupeol palmitate Natural products C12CCC3C4C(C(C)=C)CCC4(C)CCC3(C)C1(C)CCC1C2(C)CCC(OC(=O)CCCCCCCCCCCCCCC)C1(C)C BWXDHBQGBNPJMN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims abstract description 13
- BWXDHBQGBNPJMN-VBHWJLTNSA-N [(1r,3ar,5ar,5br,7ar,9s,11ar,11br,13ar,13br)-3a,5a,5b,8,8,11a-hexamethyl-1-prop-1-en-2-yl-1,2,3,4,5,6,7,7a,9,10,11,11b,12,13,13a,13b-hexadecahydrocyclopenta[a]chrysen-9-yl] hexadecanoate Chemical compound C([C@@]1(C)CC[C@H]([C@@H]1[C@H]1CC[C@H]23)C(C)=C)C[C@@]1(C)[C@]3(C)CC[C@@H]1[C@]2(C)CC[C@H](OC(=O)CCCCCCCCCCCCCCC)C1(C)C BWXDHBQGBNPJMN-VBHWJLTNSA-N 0.000 claims abstract description 13
- 235000014121 butter Nutrition 0.000 claims abstract description 13
- 239000004359 castor oil Substances 0.000 claims abstract description 13
- 235000019438 castor oil Nutrition 0.000 claims abstract description 13
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 13
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 13
- 239000010439 graphite Substances 0.000 claims abstract description 13
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 13
- 239000012188 paraffin wax Substances 0.000 claims abstract description 13
- 239000000344 soap Substances 0.000 claims abstract description 13
- 229960002317 succinimide Drugs 0.000 claims abstract description 13
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 9
- QNUYJANMNWBLBH-UHFFFAOYSA-N C1(CCC(N1OC(C(CC(=O)O)S(=O)(=O)O)=O)=O)=O Chemical compound C1(CCC(N1OC(C(CC(=O)O)S(=O)(=O)O)=O)=O)=O QNUYJANMNWBLBH-UHFFFAOYSA-N 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 150000007970 thio esters Chemical class 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- 230000009347 mechanical transmission Effects 0.000 abstract description 5
- 230000007246 mechanism Effects 0.000 abstract description 5
- 238000005299 abrasion Methods 0.000 abstract description 2
- 239000000853 adhesive Substances 0.000 abstract description 2
- 230000001070 adhesive effect Effects 0.000 abstract description 2
- 239000002184 metal Substances 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000000314 lubricant Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 239000004519 grease Substances 0.000 description 3
- 238000005461 lubrication Methods 0.000 description 3
- QXZGLTYKKZKGLN-UHFFFAOYSA-N 4-(2,5-dioxopyrrolidin-1-yl)oxy-4-oxobutanoic acid Chemical compound OC(=O)CCC(=O)ON1C(=O)CCC1=O QXZGLTYKKZKGLN-UHFFFAOYSA-N 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/10—Compounds containing silicon
- C10M2201/102—Silicates
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/106—Naphthenic fractions
- C10M2203/1065—Naphthenic fractions used as base material
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/287—Partial esters
- C10M2207/289—Partial esters containing free hydroxy groups
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/109—Polyethers, i.e. containing di- or higher polyoxyalkylene groups esterified
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/09—Heterocyclic compounds containing no sulfur, selenium or tellurium compounds in the ring
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- Chemical & Material Sciences (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
本发明公开了一种新型润滑材料及其制作工艺，由黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油、枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯、滑石粉、石墨、石腊基、脂肪皂、聚烯基琥珀酰亚胺制成。本发明润滑剂的浓稠度较低，从而降低了机械传动机构的阻力，降低机械运转的负载，此外，本发明润滑材料的附着力大，容易附着到金属表面，从而附着到机械传动机构上，使得机械传动机构顺畅运行，进一步降低阻力，还能够保护机械结构，降低磨损，具有推广应用的价值。
Description
技术领域
本发明涉及一种润滑材料，尤其涉及一种新型润滑材料及其制作工艺。
背景技术
机械中许多相对运动表面之间都必须润滑，以减少摩擦、磨损和粘滞。在机械运作中，如发动机润滑系统发生故障,主轴和齿轮可能在瞬间烧结、咬住乃至折断，发动机的机械结构没有良好的润滑会很快被烧坏；齿轮传动机构无良好的润滑工作会不正常。润滑材料按物理状态和特性分为润滑油、润滑脂和固体润滑剂三类。现有技术中，对于机械齿轮润滑的润滑剂，但现有的润滑剂产生的阻力较大，使得机械运转同时负载增大，因此，需要不断的改进与创新。
发明内容
本发明的目的就在于为了解决上述问题而提供一种新型润滑材料及其制作工艺。
本发明通过以下技术方案来实现上述目的：
本发明一种新型润滑材料，由黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油、枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯、滑石粉、石墨、石腊基、脂肪皂、聚烯基琥珀酰亚胺制成。
进一步，按重量比，每份含所述黄油40-50％、所述环烷油5-10％、所述甘油10-20％、所述聚氧乙烯氢化蓖麻油3-6％、所述枸橼酸甲酯2-3％、所述柠檬酸单甲酯1-3％、所述羽扇醇棕榈酸酯1-2％、所述丁二酰亚胺丁二酸酯基硫代酯3-5％、所述滑石粉2-5％、所述石墨5-10％、所述石腊基3-6％、所述脂肪皂2-5％、所述聚烯基琥珀酰亚胺1-3％。
优选的，按重量比，每份含所述黄油45％、所述环烷油7％、所述甘油15％、所述聚氧乙烯氢化蓖麻油5％、所述枸橼酸甲酯2％、所述柠檬酸单甲酯2％、所述羽扇醇棕榈酸酯1％、所述丁二酰亚胺丁二酸酯基硫代酯4％、所述滑石粉3％、所述石墨8％、所述石腊基4％、所述脂肪皂3％、所述聚烯基琥珀酰亚胺1％。
本发明一种新型润滑材料制作工艺，包括以下步骤：
S1：黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油按比例称取后，放入搅拌机中2000r/min转速搅拌20min；
S2：加入枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯，继续搅拌均匀；
S3：继续加入滑石粉、石墨、石腊基、脂肪皂搅拌均匀；
S4：将搅拌均匀的混混合物升温至120摄氏度后与加入聚烯基琥珀酰亚胺混合，冷却后即得成品。
本发明的有益效果在于：
本发明是一种新型润滑材料及其制作工艺，与现有技术相比，本发明润滑剂的浓稠度较低，从而降低了机械传动机构的阻力，降低机械运转的负载，此外，本发明润滑材料的附着力大，容易附着到金属表面，从而附着到机械传动机构上，使得机械传动机构顺畅运行，进一步降低阻力，还能够保护机械结构，降低磨损，具有推广应用的价值。
具体实施方式
下面对本发明作进一步说明：
本发明一种新型润滑材料，由黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油、枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯、滑石粉、石墨、石腊基、脂肪皂、聚烯基琥珀酰亚胺制成。
进一步，按重量比，每份含所述黄油40-50％、所述环烷油5-10％、所述甘油10-20％、所述聚氧乙烯氢化蓖麻油3-6％、所述枸橼酸甲酯2-3％、所述柠檬酸单甲酯1-3％、所述羽扇醇棕榈酸酯1-2％、所述丁二酰亚胺丁二酸酯基硫代酯3-5％、所述滑石粉2-5％、所述石墨5-10％、所述石腊基3-6％、所述脂肪皂2-5％、所述聚烯基琥珀酰亚胺1-3％。
优选的，按重量比，每份含所述黄油45％、所述环烷油7％、所述甘油15％、所述聚氧乙烯氢化蓖麻油5％、所述枸橼酸甲酯2％、所述柠檬酸单甲酯2％、所述羽扇醇棕榈酸酯1％、所述丁二酰亚胺丁二酸酯基硫代酯4％、所述滑石粉3％、所述石墨8％、所述石腊基4％、所述脂肪皂3％、所述聚烯基琥珀酰亚胺1％。
本发明一种新型润滑材料制作工艺，包括以下步骤：
S1：黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油按比例称取后，放入搅拌机中2000r/min转速搅拌20min；
S2：加入枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯，继续搅拌均匀；
S3：继续加入滑石粉、石墨、石腊基、脂肪皂搅拌均匀；
S4：将搅拌均匀的混混合物升温至120摄氏度后与加入聚烯基琥珀酰亚胺混合，冷却后即得成品。
试验测试：依照GB/T 392标准进行压力分油测定，润滑脂的分油率为6.42％，表明新型润滑材料的安定性稳定。介电常数测试：测得介电常数和国内常硅润滑剂下降了22％。将本发明样品放在200℃的烘箱中12h，测定发现其前后的质量几乎无变化。测得本发明样品氧化率很小。低温测试：在-60℃时通过滚珠轴承润滑脂低温转矩测定，其起动转矩和运转转矩都很小。摩擦系数测试：依照SH/T 0072-91标准对润滑脂进行摩擦系数测定，测得摩擦系数和国内常用润滑剂下降了25％，说明润滑性能有很大的提高。
以上显示和描述了本发明的基本原理和主要特征及本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。
Claims (4)
1.一种新型润滑材料，其特征在于：由黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油、枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯、滑石粉、石墨、石腊基、脂肪皂、聚烯基琥珀酰亚胺制成。
2.根据权利要求1所述的新型润滑材料，其特征在于：按重量比，每份含所述黄油40-50％、所述环烷油5-10％、所述甘油10-20％、所述聚氧乙烯氢化蓖麻油3-6％、所述枸橼酸甲酯2-3％、所述柠檬酸单甲酯1-3％、所述羽扇醇棕榈酸酯1-2％、所述丁二酰亚胺丁二酸酯基硫代酯3-5％、所述滑石粉2-5％、所述石墨5-10％、所述石腊基3-6％、所述脂肪皂2-5％、所述聚烯基琥珀酰亚胺1-3％。
3.根据权利要求2所述的新型润滑材料，其特征在于：按重量比，每份含所述黄油45％、所述环烷油7％、所述甘油15％、所述聚氧乙烯氢化蓖麻油5％、所述枸橼酸甲酯2％、所述柠檬酸单甲酯2％、所述羽扇醇棕榈酸酯1％、所述丁二酰亚胺丁二酸酯基硫代酯4％、所述滑石粉3％、所述石墨8％、所述石腊基4％、所述脂肪皂3％、所述聚烯基琥珀酰亚胺1％。
4.一种新型润滑材料制作工艺，其特征在于：包括以下步骤：
S1：黄油、环烷油、甘油、聚氧乙烯氢化蓖麻油按比例称取后，放入搅拌机中2000r/min转速搅拌20min；
S2：加入枸橼酸甲酯、柠檬酸单甲酯、羽扇醇棕榈酸酯、丁二酰亚胺丁二酸酯基硫代酯，继续搅拌均匀；
S3：继续加入滑石粉、石墨、石腊基、脂肪皂搅拌均匀；
S4：将搅拌均匀的混混合物升温至120摄氏度后与加入聚烯基琥珀酰亚胺混合，冷却后即得成品。
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| CN106635323A (zh) * | 2016-11-17 | 2017-05-10 | 淮阴工学院 | 一种机械齿轮专用润滑油 |
| CN106906034A (zh) * | 2017-04-17 | 2017-06-30 | 龙岩学院 | 一种沼气发动机专用润滑油及制备方法 |
| CN107353972A (zh) * | 2017-07-25 | 2017-11-17 | 淮阴工学院 | 一种轴承专用润滑膏 |
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| CN106635323A (zh) * | 2016-11-17 | 2017-05-10 | 淮阴工学院 | 一种机械齿轮专用润滑油 |
| CN106906034A (zh) * | 2017-04-17 | 2017-06-30 | 龙岩学院 | 一种沼气发动机专用润滑油及制备方法 |
| CN107353972A (zh) * | 2017-07-25 | 2017-11-17 | 淮阴工学院 | 一种轴承专用润滑膏 |
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