CN111759789A - Hair care serum formula and preparation method thereof - Google Patents
Hair care serum formula and preparation method thereof Download PDFInfo
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- CN111759789A CN111759789A CN202010747652.7A CN202010747652A CN111759789A CN 111759789 A CN111759789 A CN 111759789A CN 202010747652 A CN202010747652 A CN 202010747652A CN 111759789 A CN111759789 A CN 111759789A
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- 210000002966 serum Anatomy 0.000 title claims abstract description 18
- 238000009472 formulation Methods 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 45
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 42
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 42
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 32
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000203 mixture Substances 0.000 claims abstract description 27
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000011780 sodium chloride Substances 0.000 claims abstract description 16
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 claims abstract description 15
- FMRHJJZUHUTGKE-UHFFFAOYSA-N Ethylhexyl salicylate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1O FMRHJJZUHUTGKE-UHFFFAOYSA-N 0.000 claims abstract description 15
- 235000018597 common camellia Nutrition 0.000 claims abstract description 15
- 229940086555 cyclomethicone Drugs 0.000 claims abstract description 15
- 229940068171 ethyl hexyl salicylate Drugs 0.000 claims abstract description 15
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 15
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229960003415 propylparaben Drugs 0.000 claims abstract description 15
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 15
- 235000019445 benzyl alcohol Nutrition 0.000 claims abstract description 9
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 9
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims abstract description 9
- 229960002216 methylparaben Drugs 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims description 82
- 238000010438 heat treatment Methods 0.000 claims description 17
- 238000000265 homogenisation Methods 0.000 claims description 16
- 238000007599 discharging Methods 0.000 claims description 6
- 230000001804 emulsifying effect Effects 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 6
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 241000209507 Camellia Species 0.000 claims 3
- 239000002002 slurry Substances 0.000 claims 2
- 240000001548 Camellia japonica Species 0.000 abstract description 12
- 239000000341 volatile oil Substances 0.000 abstract description 6
- 238000005406 washing Methods 0.000 abstract description 6
- 239000002932 luster Substances 0.000 abstract description 3
- 239000003921 oil Substances 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract description 2
- 235000019198 oils Nutrition 0.000 abstract description 2
- 230000008569 process Effects 0.000 abstract description 2
- 230000014759 maintenance of location Effects 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000013589 supplement Substances 0.000 abstract 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 32
- 229940008099 dimethicone Drugs 0.000 description 8
- 238000009960 carding Methods 0.000 description 3
- 210000004761 scalp Anatomy 0.000 description 3
- 239000002453 shampoo Substances 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000003766 combability Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000003676 hair preparation Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Abstract
The invention relates to a hair care serum formula which comprises the following components in parts by weight: 10-70 parts of a polydimethylsiloxane/dimethiconol mixture; 10-40 parts of water; 2-30 parts of cyclomethicone; 1-15 parts of polydimethylsiloxane; 4-20 parts of isopropyl palmitate; PPG-5-cetyl polyether-202-30 parts; 1-10 parts of glycerol; 0.1-2 parts of essence; 0.01-1.0 part of hydrolyzed silk; 0.1-0.5 part of benzyl alcohol; 0.05-0.3 part of methylparaben; 0.05-0.12 part of propyl hydroxybenzoate; 0.05-1.0 part of camellia seed oil; 0.1-0.4 parts of ethylhexyl salicylate; 0.05-0.5 part of sodium chloride; its preparing process is also disclosed. The invention has the advantages that: the product can be used for caring hair, and has the advantages of softness, long smoothness, good luster, smoothness without knotting during hair washing, good safety compared with oil-rich essential oil, and moisture retention and water supplement effects to prevent hair from drying.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a hair care serum formula and a preparation method thereof.
Background
Hair lotions, also known as shampoos, shampoos or hair creams, are the most widely used hair washing products and are also one of the most commonly used hair cosmetics. It can be used for cleaning human body secreted oil, sweat scale, cells detached from scalp, foreign dust, microorganism, and residue and unpleasant odor of styling product, etc. attached to scalp and hair, and keeping scalp and hair clean and beautiful.
After the existing shampoo is used, the hair is not soft enough, the smoothness is poor, the glossiness is darker, the hair is easy to be knotted during washing, the safety is poor, and the hair is easy to dry after washing and protecting.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a hair care serum formula and a preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
the hair care size formula comprises the following components in parts by weight:
10-70 parts of a polydimethylsiloxane/dimethiconol mixture; 10-40 parts of water; 2-30 parts of cyclomethicone; 1-15 parts of polydimethylsiloxane; 4-20 parts of isopropyl palmitate; PPG-5-cetyl polyether-202-30 parts; 1-10 parts of glycerol; 0.1-2 parts of essence; 0.01-1.0 part of hydrolyzed silk; 0.1-0.5 part of benzyl alcohol; 0.05-0.3 part of methylparaben; 0.05-0.12 part of propyl hydroxybenzoate; 0.05-1.0 part of camellia seed oil; 0.1-0.4 parts of ethylhexyl salicylate; 0.05-0.5 part of sodium chloride.
Further, the hair care size formula comprises the following components in parts by weight:
40 parts of a polydimethylsiloxane/dimethiconol mixture; 25 parts of water; 16 parts of cyclomethicone; 8 parts of polydimethylsiloxane; 12 parts of isopropyl palmitate; PPG-5-cetyl polyether-2016 parts; 5 parts of glycerol; 1 part of essence; 0.5 part of hydrolyzed silk; 0.3 part of benzyl alcohol; 0.16 part of methylparaben; 0.08 part of propyl hydroxybenzoate; 0.6 part of camellia seed oil; 0.25 part of ethylhexyl salicylate; 0.25 part of sodium chloride.
Further, the ratio of the polydimethylsiloxane to the dimethiconol in the polydimethylsiloxane/dimethiconol mixture is 1-6: 1.
Further, the water is pure water.
A preparation method of hair care size comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 in proportion, and stirring and dissolving completely to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 60-70 ℃, stirring and dissolving completely, and keeping the temperature to obtain a phase C;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
Further, in step S2, the stirring speed is 20-40 rpm and the stirring time is 20-30 min.
Further, in step S3, the stirring speed is 40-60 rpm and the stirring time is 30-40 min.
Further, in step S3, the temperature rise rate is 2-4 ℃/min during heating.
Further, during stirring, a forward and reverse rotation stirring method is adopted for stirring, and the forward and reverse alternating time interval is 1-2 min.
Further, in step S5, the homogenization parameters of the homogenization step are as follows: the temperature of the primary homogenization is 50-60 ℃, the pressure is 12-15 Mpa, the temperature of the secondary homogenization is 50-60 ℃, and the pressure is 8-10 Mpa.
The invention has the following advantages:
1. the product of the invention has the advantages of soft hair care, lasting smoothness, better gloss, smoothness without knotting during hair washing, better safety than full-oil essential oil, and capability of moisturizing and moisturizing to prevent hair from drying.
2. The method has the advantages of simple process, easy operation and production cost reduction.
Detailed Description
The invention is further described below with reference to examples, but the scope of the invention is not limited to the following.
[ example 1 ]
The hair care size formula comprises the following components in parts by weight:
10 parts of a polydimethylsiloxane/dimethiconol mixture; 40 parts of water; 2 parts of cyclomethicone; 15 parts of polydimethylsiloxane; 4 parts of isopropyl palmitate; PPG-5-cetyl polyether-2030 parts; 1 part of glycerol; 2 parts of essence; 0.05 part of hydrolyzed silk; 0.5 part of benzyl alcohol; 0.05 part of methylparaben; 0.12 part of propyl hydroxybenzoate; 0.05 part of camellia seed oil; 0.4 part of ethylhexyl salicylate; 0.05 part of sodium chloride.
Further, the ratio of dimethicone to dimethiconol in the dimethicone/dimethiconol mixture is 1: 1.
Further, the water is pure water.
A preparation method of hair care size comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 according to the proportion, stirring and dissolving completely, wherein the stirring speed is 40rpm and the stirring time is 20min during stirring to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 70 ℃, wherein the heating speed is 2 ℃/min during heating, stirring for dissolving completely, the stirring speed is 60rpm during stirring, the stirring time is 30min, and keeping the temperature to obtain a phase C;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly, wherein the homogenizing parameters in the homogenizing step are as follows: the temperature of the primary homogenization is 60 ℃, the pressure is 12Mpa, the temperature of the secondary homogenization is 60 ℃, and the pressure is 8 Mpa;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
During stirring, the stirring is carried out by adopting a forward and reverse rotation stirring method, and the forward and reverse alternation time interval is 2 min.
[ example 2 ]
The hair care size formula comprises the following components in parts by weight:
40 parts of a polydimethylsiloxane/dimethiconol mixture; 25 parts of water; 16 parts of cyclomethicone; 8 parts of polydimethylsiloxane; 12 parts of isopropyl palmitate; PPG-5-cetyl polyether-2016 parts; 5 parts of glycerol; 1 part of essence; 0.5 part of hydrolyzed silk; 0.3 part of benzyl alcohol; 0.16 part of methylparaben; 0.08 part of propyl hydroxybenzoate; 0.6 part of camellia seed oil; 0.25 part of ethylhexyl salicylate; 0.25 part of sodium chloride.
Further, the ratio of dimethicone to dimethiconol in the dimethicone/dimethiconol mixture is 3: 1.
Further, the water is pure water.
A preparation method of hair care size comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 according to the proportion, stirring and dissolving completely, wherein the stirring speed is 30rpm and the stirring time is 25min during stirring to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 65 ℃, wherein the heating speed is 3 ℃/min during heating, stirring for dissolving completely, the stirring speed is 50rpm during stirring, the stirring time is 35min, and keeping the temperature to obtain a phase C;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly, wherein the homogenizing parameters in the homogenizing step are as follows: the temperature of the primary homogenization is 55 ℃, the pressure is 13.5Mpa, the temperature of the secondary homogenization is 55 ℃, and the pressure is 9 Mpa;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
During stirring, the stirring is carried out by adopting a forward and reverse rotation stirring method, and the forward and reverse alternation time interval is 1.5 min.
This embodiment is the most preferred embodiment.
[ example 3 ]
The hair care size formula comprises the following components in parts by weight:
50 parts of a polydimethylsiloxane/dimethiconol mixture; 20 parts of water; 10 parts of cyclomethicone; 10 parts of polydimethylsiloxane; 15 parts of isopropyl palmitate; PPG-5-cetyl polyether-2020 parts; 8 parts of glycerol; 0.9 part of essence; 0.5 part of hydrolyzed silk; 0.3 part of benzyl alcohol; 0.15 part of methylparaben; 0.09 part of propyl hydroxybenzoate; 0.5 part of camellia seed oil; 0.25 part of ethylhexyl salicylate; 0.3 part of sodium chloride.
Further, the ratio of dimethicone to dimethiconol in the dimethicone/dimethiconol mixture is 4: 1.
Further, the water is pure water.
A preparation method of hair care size comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 according to the proportion, stirring and dissolving completely, wherein the stirring speed is 30rpm and the stirring time is 22min during stirring to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 67 ℃, wherein the heating speed is 3 ℃/min during heating, stirring for dissolving completely, the stirring speed is 55rpm during stirring, the stirring time is 33min, and keeping the temperature to obtain a C phase;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly, wherein the homogenizing parameters in the homogenizing step are as follows: the temperature of the primary homogenization is 53 ℃, the pressure is 14Mpa, the temperature of the secondary homogenization is 56 ℃, and the pressure is 8 Mpa;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
During stirring, the stirring is carried out by adopting a forward and reverse rotation stirring method, and the forward and reverse alternation time interval is 1 min.
[ example 4 ]
The hair care size formula comprises the following components in parts by weight:
70 parts of a polydimethylsiloxane/dimethiconol mixture; 10 parts of water; 30 parts of cyclomethicone; 1 part of polydimethylsiloxane; 20 parts of isopropyl palmitate; PPG-5-cetyl polyether-202 parts; 10 parts of glycerol; 0.1 part of essence; 1.0 part of hydrolyzed silk; 0.1 part of benzyl alcohol; 0.3 part of methylparaben; 0.05 part of propyl hydroxybenzoate; 1.0 part of camellia seed oil; 0.1 part of ethylhexyl salicylate; 0.5 part of sodium chloride.
Further, the ratio of dimethicone to dimethiconol in the dimethicone/dimethiconol mixture is 6: 1.
Further, the water is pure water.
A preparation method of hair care size comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 according to the proportion, stirring and dissolving completely, wherein the stirring speed is 20rpm and the stirring time is 30min during stirring to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 60 ℃, wherein the heating speed is 4 ℃/min during heating, stirring for dissolving completely, the stirring speed is 40rpm during stirring, the stirring time is 40min, and keeping the temperature to obtain a phase C;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly, wherein the homogenizing parameters in the homogenizing step are as follows: the temperature of the primary homogenization is 50 ℃, the pressure is 15Mpa, the temperature of the secondary homogenization is 50 ℃, and the pressure is 10 Mpa;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
During stirring, the stirring is carried out by adopting a forward and reverse rotation stirring method, and the forward and reverse alternation time interval is 1 min.
Comparative tests were carried out with the product obtained in example 2 of the invention:
1. light brightness
The same large bundle of bleached and dyed hair is divided into three bundles of a, b and c which are respectively uniform.
Applying 3 to 5 drops: hair care serum No. a, commercial essential oil No. b, No. c do not smear (blank), observe the bright intensity under the natural light: a > b > c.
2. Durable luster
The same large bundle of bleached and dyed hair is divided into three bundles of No. a, No. b and No. c which are respectively and uniformly coated with 3 to 5 drops: hair care serum No. a, commercial essential oil No. b and No. c are not smeared (blank), and the luster is observed to be lasting after hanging and airing under natural light:
30 minutes: a > b > c;
and (5) 60 minutes: a > b > c;
and (3) 90 minutes: a > b > c;
120 minutes: the a number is larger than the b number and is approximately equal to the c number.
3. Smoothness and smoothness of the surface
The same large bundle of bleached and dyed hair is divided into three bundles of No. a, No. b and No. c which are respectively and uniformly coated with 3 to 5 drops: hair care serum A, commercial essential oil B and c are not smeared (blank) and naturally hung and dried for 5 minutes.
3.1 test of dry combing:
carding work: a < b < c.
3.2 test of Wet combability: the same large bundle of bleached and dyed hair is divided into three bundles of No. a, No. b and No. c which are respectively and uniformly coated with 3 to 5 drops: hair care serum A, commercial essential oil B and c are not smeared (blank) and naturally hung and dried for 30 minutes.
3.2.1 washing with tap water at room temperature
Carding work: a < b < c.
3.2.2 soaking in 0.5% NaCl solution for 30min
Carding work: a < b < c.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. The hair care slurry formula is characterized in that: the composition comprises the following components in parts by weight:
10-70 parts of a polydimethylsiloxane/dimethiconol mixture; 10-40 parts of water; 2-30 parts of cyclomethicone; 1-15 parts of polydimethylsiloxane; 4-20 parts of isopropyl palmitate; PPG-5-cetyl polyether-202-30 parts; 1-10 parts of glycerol; 0.1-2 parts of essence; 0.01-1.0 part of hydrolyzed silk; 0.1-0.5 part of benzyl alcohol; 0.05-0.3 part of methylparaben; 0.05-0.12 part of propyl hydroxybenzoate; 0.05-1.0 part of camellia seed oil; 0.1-0.4 parts of ethylhexyl salicylate; 0.05-0.5 part of sodium chloride.
2. The hair care slurry formulation according to claim 1, wherein: the composition comprises the following components in parts by weight:
40 parts of a polydimethylsiloxane/dimethiconol mixture; 25 parts of water; 16 parts of cyclomethicone; 8 parts of polydimethylsiloxane; 12 parts of isopropyl palmitate; PPG-5-cetyl polyether-2016 parts; 5 parts of glycerol; 1 part of essence; 0.5 part of hydrolyzed silk; 0.3 part of benzyl alcohol; 0.16 part of methylparaben; 0.08 part of propyl hydroxybenzoate; 0.6 part of camellia seed oil; 0.25 part of ethylhexyl salicylate; 0.25 part of sodium chloride.
3. A hair care serum formulation according to claim 1 or 2, characterized in that: the ratio of the polydimethylsiloxane to the dimethiconol in the polydimethylsiloxane/dimethiconol mixture is 1-6: 1.
4. A hair care serum formulation according to claim 1 or 2, characterized in that: the water is pure water.
5. A method for preparing a hair care serum by using the hair care serum formulation of any one of claims 1 to 4, which is characterized in that: the method comprises the following operation steps:
s1, weighing water in a proportional amount for later use;
s2, adding the glycerol, the hydrolyzed silk and the sodium chloride into the water obtained in the step S1 in proportion, and stirring and dissolving completely to obtain a phase A;
s3, heating methyl hydroxybenzoate, propyl hydroxybenzoate and isopropyl palmitate to 60-70 ℃, stirring and dissolving completely, and keeping the temperature to obtain a phase C;
s4, mixing and stirring polydimethylsiloxane, a mixture of dimethiconol and cyclomethicone and polydimethylsiloxane uniformly according to a proportion, adding the preheated and dissolved C phase, camellia seed oil, PPG-5-cetyl polyether-20, essence, ethylhexyl salicylate and benzyl alcohol, and stirring uniformly to obtain a mixed phase;
s5, adding the phase A into the mixed phase in the step S4, stirring, homogenizing and emulsifying uniformly;
s6, checking to be qualified, discharging and standing;
and S7, filling and packaging to obtain the finished product.
6. The method of preparing a hair care serum according to claim 5, wherein: in step S2, the stirring speed is 20-40 rpm and the stirring time is 20-30 min during stirring.
7. The method of preparing a hair care serum according to claim 5, wherein: in step S3, the stirring speed is 40-60 rpm and the stirring time is 30-40 min during stirring.
8. The method of preparing a hair care serum according to claim 5, wherein: in step S3, the heating rate is 2-4 ℃/min during heating.
9. A process for preparing a hair care serum according to claim 6 or 7, characterized in that: during stirring, a forward and reverse rotation stirring method is adopted for stirring, and the forward and reverse alternation time interval is 1-2 min.
10. The method of preparing a hair care serum according to claim 5, wherein: in step S5, the homogenization parameters in the homogenization step are as follows: the temperature of the primary homogenization is 50-60 ℃, the pressure is 12-15 Mpa, the temperature of the secondary homogenization is 50-60 ℃, and the pressure is 8-10 Mpa.
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| CN202010747652.7A CN111759789A (en) | 2020-07-30 | 2020-07-30 | Hair care serum formula and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812252A (en) * | 2019-12-06 | 2020-02-21 | 广州环亚化妆品科技有限公司 | Three-layer hair care composition and preparation method and application thereof |
| CN110974732A (en) * | 2019-12-10 | 2020-04-10 | 上海绿瑞生物科技有限公司 | Hair composition with color protecting effect and preparation method thereof |
| CN111388344A (en) * | 2020-04-08 | 2020-07-10 | 广州骐源生物科技有限公司 | Hair care and nourishing composition containing fibroin and preparation method thereof |
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2020
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812252A (en) * | 2019-12-06 | 2020-02-21 | 广州环亚化妆品科技有限公司 | Three-layer hair care composition and preparation method and application thereof |
| CN110974732A (en) * | 2019-12-10 | 2020-04-10 | 上海绿瑞生物科技有限公司 | Hair composition with color protecting effect and preparation method thereof |
| CN111388344A (en) * | 2020-04-08 | 2020-07-10 | 广州骐源生物科技有限公司 | Hair care and nourishing composition containing fibroin and preparation method thereof |
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Application publication date: 20201013 |