CN111732451A - Porous thick polished glaze and preparation method thereof - Google Patents
Porous thick polished glaze and preparation method thereof Download PDFInfo
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- CN111732451A CN111732451A CN202010689380.XA CN202010689380A CN111732451A CN 111732451 A CN111732451 A CN 111732451A CN 202010689380 A CN202010689380 A CN 202010689380A CN 111732451 A CN111732451 A CN 111732451A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Abstract
The invention discloses a porous thick polished glaze and a preparation method thereof, belonging to the technical field of ceramic building materials and mainly comprising the following raw materials in parts by weight: 30-45 parts of plastic clay, 15-30 parts of feldspar powder, 1-3 parts of suspending agent, 0.3-0.9 part of cosolvent, 15-40 parts of foaming material, 30-55 parts of shell powder, 7-13 parts of hygroscopic agent, 20-50 parts of aggregate, 1-8 parts of antifouling agent, 11-23 parts of nano silicon dioxide powder particles, 10-25 parts of magnesia soil and 5-10 parts of roller rod waste. According to the invention, through the designed mutual matching among the feldspar powder, the shell powder, the moisture absorbent, the aggregate, the antifouling agent, the nano silicon dioxide powder particles, the magnesia, the roller rod waste material, the coal dust and the limestone, the inner surfaces of the holes formed on the surface of the glaze-polished layer have certain antifouling effect, and meanwhile, the formed holes are utilized to adjust the indoor humidity, so that the using effect of the glaze-polished ceramic tile can be further improved, and the influence of the holes on the physical properties of the structure of the glaze-polished layer is reduced by enhancing the structural strength of the glaze-polished layer.
Description
Technical Field
The invention belongs to the technical field of ceramic building materials, and particularly relates to a porous thick polished glaze and a preparation method thereof.
Background
The porous thick glaze is a glaze with a special formula which can be used for polishing a glazed surface, is a last glaze applied to an antique brick, is generally a transparent overglaze or a transparent convex glaze, integrates the advantages of the polished brick and the antique brick, is smooth and bright as the polished brick, and has rich patterns, thick colors or gorgeous colors as the antique brick. The glaze material features that the transparent glaze layer and the fancy glaze layer are not covered, only one thin layer of transparent glaze layer is thrown away during glaze throwing, and the transparent convex fancy glaze layer is used as the outstanding whole glaze layer.
Although the porous thick glaze polishing can achieve a special decorative effect indoors, the existing porous thick glaze polishing can gather a large amount of dust, fiber yarns and other pollutants in holes due to the formed holes after long-term use, the decorative effect of the glaze polishing layer is seriously affected, and due to the formation of the holes, the structural strength of the glaze polishing layer is low, cracks are easy to generate, and the glaze polishing layer can be broken seriously, so that the problems are solved urgently in the market at the current stage by the porous thick glaze polishing and the preparation method thereof.
Disclosure of Invention
The invention aims to: the porous thick glaze and the preparation method thereof are provided in order to solve the problems that after long-term use of the existing porous thick glaze, a large amount of dust, fiber yarns and other pollutants are accumulated in the holes, the decoration effect of a glaze polishing layer is seriously influenced, the structural strength of the glaze polishing layer is low due to the formation of the holes, cracks are easy to generate, and the glaze polishing layer can be broken seriously.
In order to achieve the purpose, the invention adopts the following technical scheme:
a porous thick polished glaze is mainly prepared from the following raw materials in parts by weight:
30-45 parts of plastic clay, 15-30 parts of feldspar powder, 1-3 parts of suspending agent, 0.3-0.9 part of cosolvent, 15-40 parts of foaming material, 30-55 parts of shell powder, 7-13 parts of hygroscopic agent, 20-50 parts of aggregate, 1-8 parts of antifouling agent, 11-23 parts of nano silica powder particles, 10-25 parts of magnesia, 5-10 parts of roller rod waste, 15-36 parts of fly ash, 6-19 parts of limestone, 5-7 parts of spodumene and 11-16 parts of calcined talc.
As a further description of the above technical solution:
the plastic clay is formed by mixing strong plastic clay and weak plastic clay, the weight fraction ratio of the strong plastic clay to the weak plastic clay is about 1:7, and the strong plastic clay is selected from one or more of black mud, white mud, bentonite, kaolin, montmorillonite, ball clay or nodular soil.
As a further description of the above technical solution:
the feldspar powder is prepared by mixing potassium feldspar powder, sodium feldspar powder and lithium feldspar powder, the weight percentage of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder is about 3:1:1.2, and the particle size of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder is smaller than 100 meshes.
As a further description of the above technical solution:
the suspending agent comprises one or more of quartz, alumina and calcined kaolin, the cosolvent comprises one or more of zinc oxide, talc and dolomite, and the main components of the magnesia soil comprise 7-13 wt% of MgO, 23-45 wt% of SiO2 and 0.5-5 wt% of Al2O 3.
As a further description of the above technical solution:
the foaming material comprises polishing slag, the polishing slag comprises polishing bricks or waste residues formed in the polishing process of the polishing bricks, and the moisture absorbent is formed by mixing one or four of zeolite molecular sieve, diatomite, sepiolite and lightweight concrete in any proportion.
As a further description of the above technical solution:
the aggregate includes one in useless ceramic tile, the crushed aggregates of stone material, slay, gangue, chain row slag, just useless ceramic tile is including useless polishing brick, useless throwing glazed brick, useless interior wall brick, useless archaize brick in, just the crushed aggregates of stone material includes one in granite, the red quartz of source, quartzy stone, the porcelain stone, just the slay includes one in iron ore sediment, the copper mine sediment.
As a further description of the above technical solution:
the antifouling agent comprises the following raw materials in parts by weight: the antifouling agent is prepared by uniformly stirring the alkoxy modified silicone oil, the hydroxyl silicone oil, the silane coupling agent, the silicon dioxide and the organic tin catalyst according to the formula ratio under the protection of inert gas.
As a further description of the above technical solution:
the roller rod waste material is corundum-mullite roller rod waste material, the content of Al2O3 is 50-80 wt%, the content of Al2O3 in the fly ash is 30-45 wt%, and the content of CaO is 5-15 wt%.
A preparation method of porous thick polished glaze comprises the following operation flows:
step S1: adding plastic clay, feldspar powder, a foaming material, shell powder, aggregate, nano-silica powder particles, magnesia soil, roller stick waste, fly ash, limestone, spodumene and calcined talc in the porous thick glaze-polishing ingredient into a ball mill according to the weight part ratio for ball milling and mixing, then adding a suspending agent, a cosolvent, a hygroscopic agent and an antifouling agent into the mixed slurry according to the ratio, fully and uniformly stirring to form overglaze, and aging for later use;
step S2: sequentially performing ball milling, sieving, iron removal, granulation, press forming, drying, water spraying and ground glaze applying, printing or ink-jet coloring on the brick blank, and then spraying surface glaze;
step S3: and (3) keeping the temperature at the temperature of 1160-1180 ℃ and 1180 ℃ for 8-10 minutes until the total firing time is 50-60 minutes, and then polishing the glaze to obtain the high-hardness and high-wear-resistance fully-polished glaze product.
In summary, due to the adoption of the technical scheme, the invention has the beneficial effects that:
1. according to the invention, through the designed mutual matching among the feldspar powder, the shell powder, the moisture absorbent, the aggregate, the antifouling agent, the nano silicon dioxide powder particles, the magnesia, the roller rod waste material, the coal dust and the limestone, the inner surfaces of the holes formed on the surface of the glaze-polished layer have certain antifouling effect, and meanwhile, the formed holes are utilized to adjust the indoor humidity, so that the using effect of the glaze-polished ceramic tile can be further improved, and the influence of the holes on the physical properties of the structure of the glaze-polished layer is reduced by enhancing the structural strength of the glaze-polished layer.
2. In the invention, the high-plasticity clay and the weak-plasticity clay are mixed for use through the designed plastic clay, the using amount of the high-plasticity clay can be reduced, the firing time of the glaze polishing in an oxidation section is greatly shortened, the unit energy consumption of the glaze polishing surface is greatly reduced through the compound use of the high-plasticity clay and the weak-plasticity clay, the feldspar powder is formed by mixing the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder and is used for reducing the formula temperature to enable the glass gloss to be visible in holes, the lithium feldspar can provide relatively high-temperature viscosity to enable the internal structure of the holes to be more stable, the strength of the inner walls of the holes can be improved, the compactness of the inner walls of the holes can be improved at the same time, the dustproof effect of the holes can be improved to a certain extent, and the foaming materials are more uniformly distributed in the glaze through the designed suspending agent, cosolvent, the foaming, the foaming material and the limestone can form the karst cave effect of imitating natural stone on the surface of the polished glaze in the process of high-temperature heating, and through the designed moisture absorbent and the shell powder, due to the unique structure, the water absorption material has the capability of absorbing water molecules, when the external humidity changes, the moisture absorbent or the shell powder quickly feeds back, the effect of adjusting the indoor humidity is achieved by absorbing or releasing the moisture through the hole body communicated with the air, by the designed aggregate, in the forming process of high-temperature roasting of the aggregate, the glaze is thrown and the edges and corners on the surfaces of the aggregate particles form a low-temperature eutectic body, the edges of the particles become smooth, the gaps among the particles are increased and are more lubricated, therefore, particles or fiber substances in the pollutants are not easy to remain in the holes, and the holes can be further treated by the designed antifouling agent, so that the glossiness of the inner surfaces of the holes is greatly enhanced.
3. According to the invention, the nano-silica powder particles have good binding force and can improve the stability among the antifouling agent, the aggregate and the feldspar powder, the designed magnesia soil, the roller bar waste material and the fly ash are used, the magnesia soil provides Mg, and the Mg can react with the roller bar waste material with high aluminum content and the fly ash to form cordierite, so that the thermal shock resistance of the glaze layer is improved, mullite can be generated in the firing process of the roller bar waste material with high aluminum content and the fly ash, so that the breaking strength and the thermal shock resistance of the glaze layer are improved, and the designed strong plastic clay and the weak plastic clay are used as bentonite, the sand content is lower, and the weak plastic clay is bentonite with relatively higher sand content.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a technical scheme that: a porous thick polished glaze is mainly prepared from the following raw materials in parts by weight:
30-45 parts of plastic clay, 15-30 parts of feldspar powder, 1-3 parts of suspending agent, 0.3-0.9 part of cosolvent, 15-40 parts of foaming material, 30-55 parts of shell powder, 7-13 parts of hygroscopic agent, 20-50 parts of aggregate, 1-8 parts of antifouling agent, 11-23 parts of nano silica powder particles, 10-25 parts of magnesia, 5-10 parts of roller rod waste, 15-36 parts of fly ash, 6-19 parts of limestone, 5-7 parts of spodumene and 11-16 parts of calcined talc.
Specifically, the plastic clay is formed by mixing strong plastic clay and weak plastic clay, the weight ratio of the strong plastic clay to the weak plastic clay is about 1:7, and the strong plastic clay is selected from one or more of black clay, white clay, bentonite, kaolin, montmorillonite, ball clay or nodular soil.
The feldspar powder is prepared by mixing potassium feldspar powder, sodium feldspar powder and lithium feldspar powder, the weight percentage of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder is about 3:1:1.2, and the particle size of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder is smaller than 100 meshes.
Specifically, the suspending agent comprises one or more of quartz, alumina and calcined kaolin, the cosolvent comprises one or more of zinc oxide, talc and dolomite, and the main components of the magnesia comprise 7-13 wt% of MgO, 23-45 wt% of SiO2 and 0.5-5 wt% of Al2O 3.
Specifically, the foaming material comprises polishing slag, the polishing slag comprises polishing brick or waste slag formed in the polishing process of the polishing brick, and the moisture absorbent is formed by mixing one or four of zeolite molecular sieve, diatomite, sepiolite and lightweight concrete in any proportion.
Specifically, the aggregate comprises one of waste ceramic tiles, crushed stone materials, slag, coal gangue and chain-row slag, the waste ceramic tiles comprise one of waste polished tiles, waste glazed tiles, waste inner wall tiles and waste archaized tiles, the crushed stone materials comprise one of granite, red Roots, quartz stones and porcelain stones, and the slag comprises one of iron slag and copper slag.
Specifically, the antifouling agent comprises the following raw materials in parts by weight: 40-80 parts of alkoxy modified silicone oil, 10-25 parts of hydroxyl silicone oil, 10-20 parts of silane coupling agent, 4-9 parts of silicon dioxide and 1-2 parts of organic tin catalyst, wherein the antifouling agent is prepared by uniformly stirring the alkoxy modified silicone oil, the hydroxyl silicone oil, the silane coupling agent, the silicon dioxide and the organic tin catalyst under the protection of inert gas according to the formula ratio.
Specifically, the roller bar waste is corundum-mullite roller bar waste, the content of Al2O3 is 50-80 wt%, the content of Al2O3 in the fly ash is 30-45 wt%, and the content of CaO is 5-15 wt%.
A preparation method of porous thick polished glaze comprises the following operation flows:
step S1: adding plastic clay, feldspar powder, a foaming material, shell powder, aggregate, nano-silica powder particles, magnesia soil, roller stick waste, fly ash, limestone, spodumene and calcined talc in the porous thick glaze-polishing ingredient into a ball mill according to the weight part ratio for ball milling and mixing, then adding a suspending agent, a cosolvent, a hygroscopic agent and an antifouling agent into the mixed slurry according to the ratio, fully and uniformly stirring to form overglaze, and aging for later use;
step S2: sequentially performing ball milling, sieving, iron removal, granulation, press forming, drying, water spraying and ground glaze applying, printing or ink-jet coloring on the brick blank, and then spraying surface glaze;
step S3: and (3) keeping the temperature at the temperature of 1160-1180 ℃ and 1180 ℃ for 8-10 minutes until the total firing time is 50-60 minutes, and then polishing the glaze to obtain the high-hardness and high-wear-resistance fully-polished glaze product.
The working principle is as follows: when in use, the plastic clay, feldspar powder, foaming material, shell powder, aggregate, nano-silica powder, magnesia soil, roller rod waste, fly ash, limestone, spodumene and burnt talc in the porous thick glaze-polished ingredient are added into a ball mill according to the weight part ratio for ball milling and mixing, then suspending agent, cosolvent, hygroscopic agent and antifouling agent are added into the mixed slurry according to the ratio, the mixture is fully and uniformly stirred into glaze, the glaze is aged for standby, the brick blank is sequentially subjected to ball milling, sieving, iron removal, granulation, press molding, drying, water spraying, base glaze bottom glaze application, printing or ink jet coloring, surface glaze is sprayed, the highest temperature is kept for 8-10 minutes at the temperature of 1160-1180 ℃, the total time of firing is 50-60 minutes, then glaze polishing is carried out, a high-hardness high-wear-resistance full-polished glaze product is obtained, the glazed porcelain brick after glaze polishing is attached indoors, the moisture absorbent and the shell powder have the capacity of absorbing water molecules due to the unique structures, when the external humidity changes, the moisture absorbent or the shell powder quickly feeds back, and the hole body communicated with the air absorbs or releases the moisture, so that the effect of adjusting the indoor humidity is achieved.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. The porous thick polished glaze is characterized by being mainly prepared from the following raw materials in parts by weight:
30-45 parts of plastic clay, 15-30 parts of feldspar powder, 1-3 parts of suspending agent, 0.3-0.9 part of cosolvent, 15-40 parts of foaming material, 30-55 parts of shell powder, 7-13 parts of hygroscopic agent, 20-50 parts of aggregate, 1-8 parts of antifouling agent, 11-23 parts of nano silica powder particles, 10-25 parts of magnesia, 5-10 parts of roller rod waste, 15-36 parts of fly ash, 6-19 parts of limestone, 5-7 parts of spodumene and 11-16 parts of calcined talc.
2. A porous thick glaze according to claim 1, wherein the plastic clay is formed by mixing a strong plastic clay and a weak plastic clay, the weight ratio of the strong plastic clay to the weak plastic clay is about 1:7, and the strong plastic clay is selected from one or more of black clay, white clay, bentonite, kaolin, montmorillonite, ball clay or nodular soil.
3. The perforated thick polished glaze according to claim 1, wherein the feldspar powder is prepared by mixing potassium feldspar powder, sodium feldspar powder and lithium feldspar powder, the weight ratio of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder is about 3:1:1.2, and the particle sizes of the potassium feldspar powder, the sodium feldspar powder and the lithium feldspar powder are smaller than 100 meshes.
4. A porous thick glaze according to claim 1, wherein the suspending agent comprises one or more of quartz, alumina and calcined kaolin, the cosolvent comprises one or more of zinc oxide, talc and dolomite, the MgO content in the main component of the magnesia is 7-13 wt%, the SiO2 content is 23-45 wt%, and the Al2O3 content is 0.5-5 wt%.
5. A porous thick glaze according to claim 1, wherein the foaming material is composed of polishing slag, the polishing slag comprises polishing brick or waste slag formed in the polishing process of the polishing brick, and the moisture absorbent is composed of one or four of zeolite molecular sieve, diatomite, sepiolite and lightweight concrete in any proportion.
6. A perforated thick glaze according to claim 1, wherein said aggregate comprises one of waste ceramic tile, crushed stone material, slag, coal gangue, chain-link slag, and said waste ceramic tile comprises one of waste polished tile, waste glazed tile, waste interior wall tile, waste antique tile, and said crushed stone material comprises one of granite, rosewood, quartz stone, and porcelain stone, and said slag comprises one of iron slag, copper slag.
7. The perforated thick polished glaze according to claim 1, wherein the antifouling agent comprises the following raw materials in parts by weight: the antifouling agent is prepared by uniformly stirring the alkoxy modified silicone oil, the hydroxyl silicone oil, the silane coupling agent, the silicon dioxide and the organic tin catalyst according to the formula ratio under the protection of inert gas.
8. A porous thick glaze polish according to claim 1, wherein said roller bar waste is corundum mullite roller bar waste, Al2O3 content is 50-80 wt%, Al2O3 content in said fly ash is 30-45 wt%, CaO content is 5-15 wt%.
9. The method for preparing the perforated thick polished glaze according to claim 1, wherein the method comprises the following operation procedures:
step S1: adding plastic clay, feldspar powder, a foaming material, shell powder, aggregate, nano-silica powder particles, magnesia soil, roller stick waste, fly ash, limestone, spodumene and calcined talc in the porous thick glaze-polishing ingredient into a ball mill according to the weight part ratio for ball milling and mixing, then adding a suspending agent, a cosolvent, a hygroscopic agent and an antifouling agent into the mixed slurry according to the ratio, fully and uniformly stirring to form overglaze, and aging for later use;
step S2: sequentially performing ball milling, sieving, iron removal, granulation, press forming, drying, water spraying and ground glaze applying, printing or ink-jet coloring on the brick blank, and then spraying surface glaze;
step S3: and (3) keeping the temperature at the temperature of 1160-1180 ℃ and 1180 ℃ for 8-10 minutes until the total firing time is 50-60 minutes, and then polishing the glaze to obtain the high-hardness and high-wear-resistance fully-polished glaze product.
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| CN112939566A (en) * | 2021-03-31 | 2021-06-11 | 亚细亚建筑材料股份有限公司 | Porcelain blank material and preparation method of high-strength porcelain blank |
| CN112979271A (en) * | 2021-03-24 | 2021-06-18 | 江西金唯冠建材有限公司 | Preparation method of light high-strength pure-color glazed brick |
| CN113321534A (en) * | 2021-05-27 | 2021-08-31 | 湖南银和瓷业有限公司 | Glazing method and device for ceramic special-shaped product |
| CN114105607A (en) * | 2021-11-30 | 2022-03-01 | 王武 | High-whiteness and high-strength ceramic blank, ceramic product and preparation method thereof |
| CN115611518A (en) * | 2022-10-31 | 2023-01-17 | 安徽昆仑新材料科技有限公司 | Environment-friendly ceramic glaze with anti-freezing and anti-cracking effects and preparation method thereof |
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