CN111700821A - Milky perfume and preparation method thereof - Google Patents

Milky perfume and preparation method thereof Download PDF

Info

Publication number
CN111700821A
CN111700821A CN202010673765.7A CN202010673765A CN111700821A CN 111700821 A CN111700821 A CN 111700821A CN 202010673765 A CN202010673765 A CN 202010673765A CN 111700821 A CN111700821 A CN 111700821A
Authority
CN
China
Prior art keywords
perfume
acrylate copolymer
styrene acrylate
parts
ethanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202010673765.7A
Other languages
Chinese (zh)
Inventor
李日明
陈志鹏
陈坤祥
罗建彬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangzhou Zuofun Cosmetics Co ltd
Original Assignee
Guangzhou Zuofun Cosmetics Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangzhou Zuofun Cosmetics Co ltd filed Critical Guangzhou Zuofun Cosmetics Co ltd
Priority to CN202010673765.7A priority Critical patent/CN111700821A/en
Publication of CN111700821A publication Critical patent/CN111700821A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A45HAND OR TRAVELLING ARTICLES
    • A45DHAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
    • A45D34/00Containers or accessories specially adapted for handling liquid toiletry or cosmetic substances, e.g. perfumes
    • A45D34/02Scent flasks, e.g. with evaporator
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides milky perfume which comprises a transparent glass bottle and liquid perfume, wherein the liquid perfume is arranged in the transparent glass bottle. The liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer. The texture of the mixture liquid obtained by mixing ethanol, deionized water and styrene acrylate copolymer has a very thick state, giving visually a stronger fragrance, and the liquid perfume obtained in fact can promote a continuous stable state.

Description

Milky perfume and preparation method thereof
Technical Field
The invention relates to the field of perfume, in particular to milky perfume and a preparation method thereof.
Background
The perfume is a cosmetic made of essence, alcohol and deionized water. Most of common perfumes in the market are mainly transparent and mostly solvent-type perfumes, wherein essence or perfume is dissolved in ethanol to form transparent solution, but the solvent-type perfumes use a large amount of ethanol raw materials, so that the defects are brought. The perfume alcohol molecules are carried by perfume molecules to volatilize rapidly due to the high alcohol content, and the perfume molecules are accompanied by strong pungent smell, so that the perfume effect is difficult to keep in a continuous and stable state, and the existing perfume is not thick and heavy enough in texture and difficult to persist in perfume retaining effect.
Disclosure of Invention
The present invention has been made to solve the above problems, and it is an object of the present invention to provide an emulsion perfume and a method for preparing the same, which increase the body feeling of the perfume and also increase the fragrance-remaining time.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the milky perfume comprises a transparent glass bottle and liquid perfume, wherein the liquid perfume is arranged in the transparent glass bottle, and the liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer.
Further, the liquid perfume comprises the following components in parts by weight: essence: 3-15 parts of ethanol: 60-70 parts of deionized water: 25-30 parts of ethylene diamine tetraacetic acid: 0.02-0.05 part of butylated hydroxytoluene, 0.03-0.1 part of styrene acrylate copolymer and 0.08-0.2 part of styrene acrylate copolymer.
Further, the liquid perfume comprises the following components in parts by weight: essence: 3 parts of ethanol: 70 parts of deionized water: 30 parts of disodium ethylene diamine tetraacetate: 0.03 part of butylated hydroxytoluene, 0.05 part of styrene acrylate copolymer and 0.1 part of styrene acrylate copolymer.
A method of preparing an emulsion perfume comprising the steps of:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding essence, ethanol, deionized water, disodium ethylene diamine tetraacetate, butylated hydroxytoluene and styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging to obtain an aged mixture;
and 5: freezing and filtering the aged mixture;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Further, the aging time in step 4 is 24 hours.
Further, the temperature of the freezing in the step 5 is-5 ℃.
Compared with the prior art, the invention has the following advantages:
by adopting the technical scheme, the texture of the mixture liquid obtained by mixing the ethanol, the deionized water and the styrene acrylate copolymer has a very thick and heavy state, the fragrance of people is visually stronger, and the continuous and stable state of the obtained liquid perfume can be actually improved.
Drawings
The invention is further illustrated with reference to the following figures and examples.
Fig. 1 is a process flow diagram of one of the milky perfumes of the present invention.
Detailed Description
The present invention is further described with reference to the following drawings and specific examples so that those skilled in the art can better understand the present invention and can practice the present invention, but the examples are not intended to limit the present invention.
The milky perfume of the present invention includes transparent glass and liquid perfume, and the liquid perfume is set inside the transparent glass bottle. The liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer. The texture of the mixture liquid obtained by mixing ethanol, deionized water and styrene acrylate copolymer has a very thick state, especially in the case of observation through a clear glass bottle, and enables the resulting liquid perfume to be improved in a continuous stable state.
The invention is further described below by way of examples.
Example 1:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid and 0.05g of butylated hydroxytoluene at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 2:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.1g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 3:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.2g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 4:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.3g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
The difference between the 4 examples is whether there is a styrene acrylate copolymer and the styrene acrylate copolymer is present in different amounts, and the perfume model with the styrene acrylate copolymer is visually thicker and heavier, and the perfume is thicker and heavier when the styrene acrylate copolymer is present in a higher amount.
The milky perfume prepared in the 4 examples above was tested.
The test method comprises the following steps: the perfume sample plates obtained in 4 embodiments are sprayed on the wrists of office workers in a daily working environment, testers do not know each other and avoid communication, the fragrance of the wrists is smelled again every 30 minutes until the fragrance is completely volatilized, and the final fragrance remaining time is recorded.
Figure DEST_PATH_IMAGE001
It is known that styrene acrylate copolymers can also affect the length of perfume stay and the skin feel, the higher the styrene acrylate copolymer content the longer the perfume stay and the more sticky the skin feel.
Example 5:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 15g of essence, 60g of ethanol, 25g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.1g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
The difference between the embodiment 5 and the embodiment 2 is that the proportion of the essence, the ethanol and the deionized water is adjusted, the content of the essence is increased, and the content of the ethanol and the deionized water is reduced, because the proportion of the styrene acrylate copolymer to the ethanol and the deionized water is high, the texture of the perfume is slightly thicker and heavier, the fragrance-retaining time of the perfume is slightly increased, the skin-feel viscosity is slightly increased, the proportion of the essence to the ethanol and the deionized water is high, and the fragrance of the perfume is stronger.
The texture, the fragrance-retaining duration and the skin feeling of the perfume are influenced by the proportion of ethanol, deionized water and styrene acrylate copolymer, and the perfume effect of the example 2 is finally seen at present.
As described above, the present invention can be preferably applied to practical production. The above-mentioned embodiments are merely preferred embodiments of the present invention, which are not intended to limit the scope of the present invention, i.e., the present invention is claimed in the appended claims with all equivalent variations and modifications.

Claims (6)

1. An emulsion perfume characterized by: including transparent glass bottle and liquid perfume, liquid perfume is installed in transparent glass bottle, liquid perfume has following component to constitute: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer.
2. The emulsion perfume according to claim 1, characterized in that: the liquid perfume comprises the following components in parts by weight: essence: 3-15 parts of ethanol: 60-70 parts of deionized water: 25-30 parts of ethylene diamine tetraacetic acid: 0.02-0.05 part of butylated hydroxytoluene, 0.03-0.1 part of styrene acrylate copolymer and 0.08-0.2 part of styrene acrylate copolymer.
3. The emulsion perfume according to claim 2, characterized in that: the liquid perfume comprises the following components in parts by weight: essence: 3 parts of ethanol: 70 parts of deionized water: 30 parts of disodium ethylene diamine tetraacetate: 0.03 part of butylated hydroxytoluene, 0.05 part of styrene acrylate copolymer and 0.1 part of styrene acrylate copolymer.
4. A method for preparing an emulsion perfume, comprising the steps of:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding essence, ethanol, deionized water, disodium ethylene diamine tetraacetate, butylated hydroxytoluene and styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging to obtain an aged mixture;
and 5: freezing and filtering the aged mixture;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
5. The process for the preparation of an emulsion perfume according to claim 4, characterized in that the aging time in step 4 is 24 hours.
6. The process for the preparation of an emulsion perfume according to claim 4, characterized in that the temperature of freezing in step 5 is-5 ℃.
CN202010673765.7A 2020-07-14 2020-07-14 Milky perfume and preparation method thereof Pending CN111700821A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202010673765.7A CN111700821A (en) 2020-07-14 2020-07-14 Milky perfume and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202010673765.7A CN111700821A (en) 2020-07-14 2020-07-14 Milky perfume and preparation method thereof

Publications (1)

Publication Number Publication Date
CN111700821A true CN111700821A (en) 2020-09-25

Family

ID=72545825

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202010673765.7A Pending CN111700821A (en) 2020-07-14 2020-07-14 Milky perfume and preparation method thereof

Country Status (1)

Country Link
CN (1) CN111700821A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114601768A (en) * 2022-04-22 2022-06-10 重庆菩璞生物科技有限公司 Antioxidant gold fragrant willow perfume and preparation method thereof

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5547611A (en) * 1978-09-29 1980-04-04 Pola Chem Ind Inc Three-layered perfumery
EP0138635A2 (en) * 1983-09-23 1985-04-24 Societe Eparco S.A. Method of preparing a perfume composition and composition so obtained
JPS62226915A (en) * 1986-03-28 1987-10-05 Pentel Kk Liquid cosmetic
CN101491484A (en) * 2008-12-12 2009-07-29 颜林 Milky perfume and preparation method thereof
WO2013004003A1 (en) * 2011-07-04 2013-01-10 丽华(泰国)香精有限公司 Nano-flavor and preparation method thereof
CN103405357A (en) * 2013-06-08 2013-11-27 吴江市利达上光制品有限公司 Preparation process of long-acting sustained-release perfume
CN107427422A (en) * 2015-02-25 2017-12-01 西姆莱斯股份公司 Fragrant agent dispersion for detergent composition
CN109793676A (en) * 2019-01-25 2019-05-24 上海芬尚生物科技有限公司 A kind of process of preparing of suspension drift sand perfume
CN110237027A (en) * 2019-07-29 2019-09-17 苏州卓纳纳米技术有限公司 A kind of preparation method of the hydrogel for hydrophobic drug carrier

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5547611A (en) * 1978-09-29 1980-04-04 Pola Chem Ind Inc Three-layered perfumery
EP0138635A2 (en) * 1983-09-23 1985-04-24 Societe Eparco S.A. Method of preparing a perfume composition and composition so obtained
JPS62226915A (en) * 1986-03-28 1987-10-05 Pentel Kk Liquid cosmetic
CN101491484A (en) * 2008-12-12 2009-07-29 颜林 Milky perfume and preparation method thereof
WO2013004003A1 (en) * 2011-07-04 2013-01-10 丽华(泰国)香精有限公司 Nano-flavor and preparation method thereof
CN103405357A (en) * 2013-06-08 2013-11-27 吴江市利达上光制品有限公司 Preparation process of long-acting sustained-release perfume
CN107427422A (en) * 2015-02-25 2017-12-01 西姆莱斯股份公司 Fragrant agent dispersion for detergent composition
CN109793676A (en) * 2019-01-25 2019-05-24 上海芬尚生物科技有限公司 A kind of process of preparing of suspension drift sand perfume
CN110237027A (en) * 2019-07-29 2019-09-17 苏州卓纳纳米技术有限公司 A kind of preparation method of the hydrogel for hydrophobic drug carrier

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114601768A (en) * 2022-04-22 2022-06-10 重庆菩璞生物科技有限公司 Antioxidant gold fragrant willow perfume and preparation method thereof

Similar Documents

Publication Publication Date Title
WO2018040414A1 (en) Deep replenishing and moisturizing cream
CN111700821A (en) Milky perfume and preparation method thereof
CN110464682A (en) A kind of peach gum composition, preparation method and application
CN108451789B (en) Emulsion containing carboxymethyl pachyman and preparation method and application thereof
CN113491646A (en) Natural plant essential oil microemulsion as well as preparation method and application thereof
Devina et al. The purity and viscosity of sodium alginate extracted from Sargassum brown seaweed species as a basic ingredient in dental alginate impression material
CN108456513A (en) A kind of fracturing fluid organic aluminum crosslinker, preparation method and application
CN102697701B (en) Skin care composition with skin whitening and moisturizing efficacies as well as preparation method and applications thereof
CN114259440A (en) Compound plant extract with anti-aging effect for skin care products and application thereof
CN109394640A (en) A kind of ferment skin care compositions and its application
CN103308357B (en) A kind of lead oil lacquer coat standard substance and preparation method
CN115990127B (en) Composition with pore shrinking and skin smoothing functions, and preparation method and application thereof
CN110403913B (en) Amantadine hydrochloride soft capsule and preparation method thereof
CN108338950A (en) With stablizing the anti-apolexis composition and application thereof for being adhered effect between epidermis and corium
CN108785116A (en) A kind of mascara and preparation method thereof
CN102018668A (en) Preparation method of aceglutamide
CN112516008A (en) Thickener and application thereof in cosmetics
Shiinoki et al. Viscoelastic behavior of an agar—gelatin mixture gel as a function of its composition
CN110025558A (en) One kind is rich in soybean polyoses amino acid nanometer mildy wash and preparation method thereof
CN108059674A (en) A kind of Yolk antibody extracting method of scale
CN109771307A (en) A kind of low deuterium-oxide light moistens essence film and preparation method thereof
CN114848575B (en) Essence and preparation method thereof
CN110025542A (en) A kind of skin-care product additive and preparation method thereof with anti-blue light
CN109199924A (en) A kind of natural lotion and preparation method thereof
Kawazura et al. Morphology and crystallization behavior of lightly crosslinked natural rubber in blend

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20200925

RJ01 Rejection of invention patent application after publication