CN111700821A - Milky perfume and preparation method thereof - Google Patents
Milky perfume and preparation method thereof Download PDFInfo
- Publication number
- CN111700821A CN111700821A CN202010673765.7A CN202010673765A CN111700821A CN 111700821 A CN111700821 A CN 111700821A CN 202010673765 A CN202010673765 A CN 202010673765A CN 111700821 A CN111700821 A CN 111700821A
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- Prior art keywords
- perfume
- acrylate copolymer
- styrene acrylate
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- ethanol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D34/00—Containers or accessories specially adapted for handling liquid toiletry or cosmetic substances, e.g. perfumes
- A45D34/02—Scent flasks, e.g. with evaporator
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention provides milky perfume which comprises a transparent glass bottle and liquid perfume, wherein the liquid perfume is arranged in the transparent glass bottle. The liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer. The texture of the mixture liquid obtained by mixing ethanol, deionized water and styrene acrylate copolymer has a very thick state, giving visually a stronger fragrance, and the liquid perfume obtained in fact can promote a continuous stable state.
Description
Technical Field
The invention relates to the field of perfume, in particular to milky perfume and a preparation method thereof.
Background
The perfume is a cosmetic made of essence, alcohol and deionized water. Most of common perfumes in the market are mainly transparent and mostly solvent-type perfumes, wherein essence or perfume is dissolved in ethanol to form transparent solution, but the solvent-type perfumes use a large amount of ethanol raw materials, so that the defects are brought. The perfume alcohol molecules are carried by perfume molecules to volatilize rapidly due to the high alcohol content, and the perfume molecules are accompanied by strong pungent smell, so that the perfume effect is difficult to keep in a continuous and stable state, and the existing perfume is not thick and heavy enough in texture and difficult to persist in perfume retaining effect.
Disclosure of Invention
The present invention has been made to solve the above problems, and it is an object of the present invention to provide an emulsion perfume and a method for preparing the same, which increase the body feeling of the perfume and also increase the fragrance-remaining time.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the milky perfume comprises a transparent glass bottle and liquid perfume, wherein the liquid perfume is arranged in the transparent glass bottle, and the liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer.
Further, the liquid perfume comprises the following components in parts by weight: essence: 3-15 parts of ethanol: 60-70 parts of deionized water: 25-30 parts of ethylene diamine tetraacetic acid: 0.02-0.05 part of butylated hydroxytoluene, 0.03-0.1 part of styrene acrylate copolymer and 0.08-0.2 part of styrene acrylate copolymer.
Further, the liquid perfume comprises the following components in parts by weight: essence: 3 parts of ethanol: 70 parts of deionized water: 30 parts of disodium ethylene diamine tetraacetate: 0.03 part of butylated hydroxytoluene, 0.05 part of styrene acrylate copolymer and 0.1 part of styrene acrylate copolymer.
A method of preparing an emulsion perfume comprising the steps of:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding essence, ethanol, deionized water, disodium ethylene diamine tetraacetate, butylated hydroxytoluene and styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging to obtain an aged mixture;
and 5: freezing and filtering the aged mixture;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Further, the aging time in step 4 is 24 hours.
Further, the temperature of the freezing in the step 5 is-5 ℃.
Compared with the prior art, the invention has the following advantages:
by adopting the technical scheme, the texture of the mixture liquid obtained by mixing the ethanol, the deionized water and the styrene acrylate copolymer has a very thick and heavy state, the fragrance of people is visually stronger, and the continuous and stable state of the obtained liquid perfume can be actually improved.
Drawings
The invention is further illustrated with reference to the following figures and examples.
Fig. 1 is a process flow diagram of one of the milky perfumes of the present invention.
Detailed Description
The present invention is further described with reference to the following drawings and specific examples so that those skilled in the art can better understand the present invention and can practice the present invention, but the examples are not intended to limit the present invention.
The milky perfume of the present invention includes transparent glass and liquid perfume, and the liquid perfume is set inside the transparent glass bottle. The liquid perfume comprises the following components: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer. The texture of the mixture liquid obtained by mixing ethanol, deionized water and styrene acrylate copolymer has a very thick state, especially in the case of observation through a clear glass bottle, and enables the resulting liquid perfume to be improved in a continuous stable state.
The invention is further described below by way of examples.
Example 1:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid and 0.05g of butylated hydroxytoluene at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 2:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.1g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 3:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.2g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
Example 4:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 3g of essence, 70g of ethanol, 30g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.3g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
The difference between the 4 examples is whether there is a styrene acrylate copolymer and the styrene acrylate copolymer is present in different amounts, and the perfume model with the styrene acrylate copolymer is visually thicker and heavier, and the perfume is thicker and heavier when the styrene acrylate copolymer is present in a higher amount.
The milky perfume prepared in the 4 examples above was tested.
The test method comprises the following steps: the perfume sample plates obtained in 4 embodiments are sprayed on the wrists of office workers in a daily working environment, testers do not know each other and avoid communication, the fragrance of the wrists is smelled again every 30 minutes until the fragrance is completely volatilized, and the final fragrance remaining time is recorded.
It is known that styrene acrylate copolymers can also affect the length of perfume stay and the skin feel, the higher the styrene acrylate copolymer content the longer the perfume stay and the more sticky the skin feel.
Example 5:
this example was prepared using the following steps:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding 15g of essence, 60g of ethanol, 25g of deionized water, 0.03g of disodium ethylenediamine tetraacetic acid, 0.05g of butylated hydroxytoluene and 0.1g of styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a liquid perfume mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging for 24 hours to obtain an aged mixture;
and 5: freezing the aged mixture at-5 deg.C, and vacuum filtering;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
The difference between the embodiment 5 and the embodiment 2 is that the proportion of the essence, the ethanol and the deionized water is adjusted, the content of the essence is increased, and the content of the ethanol and the deionized water is reduced, because the proportion of the styrene acrylate copolymer to the ethanol and the deionized water is high, the texture of the perfume is slightly thicker and heavier, the fragrance-retaining time of the perfume is slightly increased, the skin-feel viscosity is slightly increased, the proportion of the essence to the ethanol and the deionized water is high, and the fragrance of the perfume is stronger.
The texture, the fragrance-retaining duration and the skin feeling of the perfume are influenced by the proportion of ethanol, deionized water and styrene acrylate copolymer, and the perfume effect of the example 2 is finally seen at present.
As described above, the present invention can be preferably applied to practical production. The above-mentioned embodiments are merely preferred embodiments of the present invention, which are not intended to limit the scope of the present invention, i.e., the present invention is claimed in the appended claims with all equivalent variations and modifications.
Claims (6)
1. An emulsion perfume characterized by: including transparent glass bottle and liquid perfume, liquid perfume is installed in transparent glass bottle, liquid perfume has following component to constitute: essence, ethanol, deionized water, ethylene diamine tetraacetic acid disodium, butylated hydroxytoluene and styrene acrylate copolymer.
2. The emulsion perfume according to claim 1, characterized in that: the liquid perfume comprises the following components in parts by weight: essence: 3-15 parts of ethanol: 60-70 parts of deionized water: 25-30 parts of ethylene diamine tetraacetic acid: 0.02-0.05 part of butylated hydroxytoluene, 0.03-0.1 part of styrene acrylate copolymer and 0.08-0.2 part of styrene acrylate copolymer.
3. The emulsion perfume according to claim 2, characterized in that: the liquid perfume comprises the following components in parts by weight: essence: 3 parts of ethanol: 70 parts of deionized water: 30 parts of disodium ethylene diamine tetraacetate: 0.03 part of butylated hydroxytoluene, 0.05 part of styrene acrylate copolymer and 0.1 part of styrene acrylate copolymer.
4. A method for preparing an emulsion perfume, comprising the steps of:
step 1: detecting the used raw materials;
step 2: weighing qualified raw materials according to a formula, rechecking and then feeding;
and step 3: adding essence, ethanol, deionized water, disodium ethylene diamine tetraacetate, butylated hydroxytoluene and styrene acrylate copolymer at normal temperature, and mixing and stirring uniformly to obtain a mixture;
and 4, step 4: uniformly stirring the mixture obtained in the step 3, and then aging to obtain an aged mixture;
and 5: freezing and filtering the aged mixture;
step 6: returning to normal temperature for inspection after the suction filtration is finished;
and 7: and after the liquid perfume is qualified, adding the liquid perfume into a transparent container.
5. The process for the preparation of an emulsion perfume according to claim 4, characterized in that the aging time in step 4 is 24 hours.
6. The process for the preparation of an emulsion perfume according to claim 4, characterized in that the temperature of freezing in step 5 is-5 ℃.
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CN202010673765.7A CN111700821A (en) | 2020-07-14 | 2020-07-14 | Milky perfume and preparation method thereof |
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CN202010673765.7A CN111700821A (en) | 2020-07-14 | 2020-07-14 | Milky perfume and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114601768A (en) * | 2022-04-22 | 2022-06-10 | 重庆菩璞生物科技有限公司 | Antioxidant gold fragrant willow perfume and preparation method thereof |
Citations (9)
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JPS5547611A (en) * | 1978-09-29 | 1980-04-04 | Pola Chem Ind Inc | Three-layered perfumery |
EP0138635A2 (en) * | 1983-09-23 | 1985-04-24 | Societe Eparco S.A. | Method of preparing a perfume composition and composition so obtained |
JPS62226915A (en) * | 1986-03-28 | 1987-10-05 | Pentel Kk | Liquid cosmetic |
CN101491484A (en) * | 2008-12-12 | 2009-07-29 | 颜林 | Milky perfume and preparation method thereof |
WO2013004003A1 (en) * | 2011-07-04 | 2013-01-10 | 丽华(泰国)香精有限公司 | Nano-flavor and preparation method thereof |
CN103405357A (en) * | 2013-06-08 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation process of long-acting sustained-release perfume |
CN107427422A (en) * | 2015-02-25 | 2017-12-01 | 西姆莱斯股份公司 | Fragrant agent dispersion for detergent composition |
CN109793676A (en) * | 2019-01-25 | 2019-05-24 | 上海芬尚生物科技有限公司 | A kind of process of preparing of suspension drift sand perfume |
CN110237027A (en) * | 2019-07-29 | 2019-09-17 | 苏州卓纳纳米技术有限公司 | A kind of preparation method of the hydrogel for hydrophobic drug carrier |
-
2020
- 2020-07-14 CN CN202010673765.7A patent/CN111700821A/en active Pending
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5547611A (en) * | 1978-09-29 | 1980-04-04 | Pola Chem Ind Inc | Three-layered perfumery |
EP0138635A2 (en) * | 1983-09-23 | 1985-04-24 | Societe Eparco S.A. | Method of preparing a perfume composition and composition so obtained |
JPS62226915A (en) * | 1986-03-28 | 1987-10-05 | Pentel Kk | Liquid cosmetic |
CN101491484A (en) * | 2008-12-12 | 2009-07-29 | 颜林 | Milky perfume and preparation method thereof |
WO2013004003A1 (en) * | 2011-07-04 | 2013-01-10 | 丽华(泰国)香精有限公司 | Nano-flavor and preparation method thereof |
CN103405357A (en) * | 2013-06-08 | 2013-11-27 | 吴江市利达上光制品有限公司 | Preparation process of long-acting sustained-release perfume |
CN107427422A (en) * | 2015-02-25 | 2017-12-01 | 西姆莱斯股份公司 | Fragrant agent dispersion for detergent composition |
CN109793676A (en) * | 2019-01-25 | 2019-05-24 | 上海芬尚生物科技有限公司 | A kind of process of preparing of suspension drift sand perfume |
CN110237027A (en) * | 2019-07-29 | 2019-09-17 | 苏州卓纳纳米技术有限公司 | A kind of preparation method of the hydrogel for hydrophobic drug carrier |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114601768A (en) * | 2022-04-22 | 2022-06-10 | 重庆菩璞生物科技有限公司 | Antioxidant gold fragrant willow perfume and preparation method thereof |
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