CN109199924A - A kind of natural lotion and preparation method thereof - Google Patents

A kind of natural lotion and preparation method thereof Download PDF

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Publication number
CN109199924A
CN109199924A CN201811195548.0A CN201811195548A CN109199924A CN 109199924 A CN109199924 A CN 109199924A CN 201811195548 A CN201811195548 A CN 201811195548A CN 109199924 A CN109199924 A CN 109199924A
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oil
natural
lotion
preparation
content
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杨枝沅
盛虹
赵玉莲
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Shanghai And Sheng Cosmetics Co Ltd
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Shanghai And Sheng Cosmetics Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10General cosmetic use
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of natural lotions and preparation method thereof, including following component: hydrolecithin, Wild soybean sterols, Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil, glycerol, 1,3-PD, dipotassium glycyrrhizinate, Sodium Hyaluronate, xanthan gum, tremella polysaccharides, glycine betaine, raspberry ketone and water.Natural lotion of the invention is mildly non-stimulated, pure natural, skin is not given to increase any burden, and product is cold-resistant and heat resistance is good;Meanwhile the preparation method of natural lotion of the invention is simple, it is easy to spread.

Description

A kind of natural lotion and preparation method thereof
Technical field
The present invention relates to field of fine chemical, especially a kind of natural skin care product lotion and preparation method thereof.
Background technique
With being constantly progressive for social economy and enriching constantly for material life, skin care item are more and more extensive to be applied to women Consumer, skin care item on the market mainly include facial mask, eye cream, face cream, essence, mildy wash, stoste, toner, cream at present The products such as liquid, hydrosol, skin cream, sun screen, BB frost, CC frost, suncream.
But lotion and cream kind skin care item at present on the market nearly all contains a certain amount of emulsifier, dormant oil, silicone oil, prevents Rotten agent etc..Though many products declare naturally, can not accomplish it is real pure natural no added, compared to other non-natural prods For, their difference is only that be improved on additive amount and the mildness in emulsifier and grease, but emulsifier and The use of silicone oil, even content are few, certain burden can be also generated to our skin, particularly with the people of sensibility skin Group, be badly in need of it is a kind of it is mild it is non-stimulated, pure natural, to skin do not increase natural lotion of any burden and preparation method thereof to solve Above-mentioned technical problem.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of natural lotion and preparation method thereof, days of the invention Right lotion is mildly non-stimulated, pure natural, does not give skin to increase any burden;The preparation method of natural lotion of the invention is simple, It is easy to spread.
The present invention is to solve above-mentioned technical problem by following technical solution:
There is provided a kind of natural lotions for one of technical solution of the present invention, by mass percentage include following component: 0 ~1% hydrolecithin, 0~1% Wild soybean sterols, 5~10% Butyrospermum parkii fruit rouge, 3~5% sunflower seed Oil, 0~1% rosemary leaf oil, 3~5% olive oil, 2~5% grape seed oil, 1~5% glycerol, 5~ 10% 1,3- propylene glycol, 0~1% dipotassium glycyrrhizinate, 0~1% Sodium Hyaluronate, 0~1% xanthan gum, 0~1% Tremella polysaccharides, 1~3% glycine betaine, 1~3% raspberry ketone and the water for complementing to 100%, wherein the hydrogenation lecithin The content of rouge does not include 0 and 1%, and the content of the Wild soybean sterols does not include 0 and 1%, the content of the rosemary leaf oil Not comprising 0 and 1%, the content of the dipotassium glycyrrhizinate does not include 0 and 1%, and the content of the Sodium Hyaluronate does not include 0 He 1%, the content of the xanthan gum does not include 0 and 1%, and the content of the tremella polysaccharides does not include 0 and 1%.
In the present invention, the hydrolecithin is moisturizer commonly used in the art, molecular formula C42H84NO8P is big Beans are as obtained by extraction;The index of the hydrolecithin are as follows: arsenic < 2.0ppm, water < 5.0%, heavy metal < 2.0ppm;
Preferably, the content of the hydrolecithin is 0.5%.
In the present invention, the Wild soybean sterols is emollients commonly used in the art, is obtained by Wild soybean oil extract It arrives;The index of the Wild soybean sterols are as follows: arsenic < 2.0ppm, water < 5.0%, heavy metal < 2.0ppm;
Preferably, the content of the Wild soybean sterols is 0.3%.
In the present invention, grease of the Butyrospermum parkii fruit rouge in butter fruit fruit stone contains a large amount of phytosterol And vitamin E etc. is not saponified ingredient;The index of the Butyrospermum parkii fruit rouge are as follows: acid value < 1mgKOH/g, peroxide value < 10meq O2/kg;
Preferably, the content of the Butyrospermum parkii fruit rouge is 10%.
In the present invention, the sunflower seed oil is a vegetable fat obtained by sunflower seeds cold rolling, contains a large amount of sub- oil The substances such as acid, vitamin E, vitamin B3, protein, potassium, phosphorus, iron, magnesium, sterol, linoleic acid;The index of the sunflower seed oil Are as follows: acid value < 1mg KOH/g, peroxide value < 10meq O2/kg;
Preferably, the content of the sunflower seed oil is 2%.
In the present invention, the rosemary leaf oil is the extract of rosemary leave, has stronger inoxidizability;The fan changes The index of geranium oil are as follows: acid value < 1mg KOH/g, peroxide value < 10meq O2/kg;
Preferably, the content of the rosemary leaf oil is 0.2%.
In the present invention, the olive oil derives from olive fruit, gives birth to containing higher unsaturated fatty acid, dimension abundant Plain A, vitamin D and vitamin E;The index of the olive oil are as follows: acid value < 1mgKOH/g, peroxide value < 10meq O2/kg;
Preferably, the content of the olive oil is 5%.
In the present invention, the grape seed oil is the vegetable fat of grape pip squeezing, is rich in linoleic acid and a variety of dimensions abundant Raw element;The index of the grape seed oil are as follows: acid value < 0.5mg KOH/g, peroxide value < 10meqO2/kg;
Preferably, the content of the grape seed oil is 2%.
In the present invention, the glycerol is the by-product in vegetable fat extractive process, also known as natural glycerin;The glycerol Index are as follows: glycerol content be greater than 99.5%, diethylene glycol (DEG) is without detection;
Preferably, the content of the glycerol is 5%,
In the present invention, the 1,3-PD is to purify to generate by corn fermentation, molecular formula C3H8O2, Ke Yifa Raw oxidation, esterification;The index of the 1,3-PD are as follows: 1,3-PD content is greater than 99.8%, and content of beary metal is small In 5.0ppm;
Preferably, the content of the 1,3-PD is 6%.
In the present invention, the dipotassium glycyrrhizinate is that white or off-white color fine powder, purity have special sweet taste, water up to 99% It is solvent, mouthfeel is pure, the dipotassium glycyrrhizinate using Radix Glycyrrhizae as raw material be made;The index of the dipotassium glycyrrhizinate are as follows: heavy metal < 10ppm, chloride < 0.014%;
Preferably, the content of the dipotassium glycyrrhizinate is 0.1%.
In the present invention, the Sodium Hyaluronate is the substance extracted from cockscomb, can also be fermented and is made by Lactococcus, For white or off-white color particle or powder, odorless;The index of the Sodium Hyaluronate are as follows: when dry, Sodium Hyaluronate >= 91%, heavy metal < 10ppm, glucuronic acid content are 37.0%-51.0%;
Preferably, the content of the Sodium Hyaluronate is 0.1%.
In the present invention, the xanthan gum is also known as yellow glue, xanthan gum, is a kind of monospore generated by pseudo xanthomonas fermentation Polysaccharide, by cabbage black rot xanthomonas campestris using carbohydrate as primary raw material, through aerobic fermentation biotechnology, 1,6- glycosidic bond is cut off, is macromolecular in a kind of acidic extracellular heteroglycan of acidity for being bonded to straight chain composition by Isosorbide-5-Nitrae-after opening branch Film forming agent and stabilizer;The index of the xanthan gum are as follows: viscosity (1%KCl) 1200-1600mpa.s, total number of bacteria < 1000;
Preferably, the content of the xanthan gum is 0.4%.
In the present invention, the tremella polysaccharides are a kind of acid heteroglycans, are obtained from Tremella fructification, and backbone structure is By the mannosan of α-(1 → 3) glucosides key connection, branch is made of glucuronic acid and xylose;The index of the tremella polysaccharides Are as follows: molecular weight >=1000000D, nitrogen content < 0.5%, glucuronic acid 13.0-30.0%;
Preferably, the content of the tremella polysaccharides is 0.08%.
In the present invention, the glycine betaine is the extract of beet root, and scientific name is trimethylglycine, for white squamous or rib Shape crystalline powder has slight characteristic odor;The index of the glycine betaine are as follows: content > 99.0%, chloride content (in terms of Cl) < 0.03%, arsenic < 2ppm;
Preferably, the content of the glycine betaine is 2%.
In the present invention, the raspberry ketone Chinese nickname is 4- (4- hydroxy phenyl) -2- butanone, and the raspberry ketone is day Right ingredient is mainly reflected in the fragrance component for being included in Strawberry Tree;The index of the raspberry ketone are as follows: 1% aqueous solution pH is 5.0-7.0, specific gravity (d20/20) are 1.02-1.08g/cm3
Preferably, the content of the raspberry ketone is 3%.
In the present invention, the water is aqueous solution commonly used in the art, generally deionized water, is present in as water phase In the lotion;
Preferably, the content of the water is 63.32%.
In the present invention, the natural lotion includes following component by mass percentage: 0.5% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% Olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% It Sodium Hyaluronate, 0.4% xanthan gum, 0.08% tremella polysaccharides, 2% glycine betaine, 3% raspberry ketone and complements to 100% water.
In the present invention, the component of the preferably natural lotion of an example is by mass percentage are as follows: 0.5% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% Olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% xanthan gum, 0.08% tremella polysaccharides, 2% glycine betaine, 3% raspberry ketone and 63.32% Water.
There is provided a kind of preparation methods of natural lotion described above for another technical solution of the invention:
In the present invention, the natural lotion can be prepared by the method for this field routine.
Preferably, the preparation method of the natural lotion includes the following steps:
S1, hydrolecithin, Wild soybean sterols and glycerol are mixed, is warming up to 78~82 DEG C, 1,3-PD is added After stir evenly, obtain emulsifying material A;
S2, Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil are mixed, heating To 70~75 DEG C, oil phase material B is obtained;
S3, Jiang Shui, Sodium Hyaluronate, xanthan gum, tremella polysaccharides mixing, are warming up to 78~82 DEG C, obtain water phase material C;
S4, oil phase material B is added in emulsifying material A, first time 12~18min of homogeneous;Water phase material C is added, Second of 6~10min of homogeneous, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 9~11min at 78~82 DEG C, is cooled to 43~47 DEG C, dipotassium glycyrrhizinate is added And raspberry ketone, it stirs evenly;
Wherein, described S1, S2 and S3 in no particular order sequence.
More preferably, the S1 is carried out in emulsion pot;
More preferably, the S2 is carried out in oily phase pot;
More preferably, the S3 is carried out in water phase pot;
More preferably, in the S1, the temperature of heating is 80 DEG C;
More preferably, in the S3, the temperature of heating is 80 DEG C;
More preferably, in the S4, the time of first time homogeneous is 15min, and the time of second of homogeneous is 8min;
More preferably, in the S5, the time of heat preservation is 10min, and the temperature after cooling is 45 DEG C;
It more preferably, further include S6 after the S5, the S6 are as follows: the product feeding inspection for obtaining S5 after mixing evenly, Qualified filtering and discharging.
In the present invention, related raw material is commercially available.
The advantages and beneficial effects of the present invention are: natural lotion of the invention passes through the coordinated of each component and each The stringent screening of constituent content realizes the excellent effect of product, and natural lotion of the invention is mildly non-stimulated, pure natural, does not give Skin increases any burden.Meanwhile applicant has finally determined the system of natural lotion of the invention by many experiments and research Preparation Method, the fine quality that ensure that product of the product being worth by this method, product is cold-resistant and heat resistance is good, and method Simply, easy to spread.
Specific embodiment
With reference to embodiment, the specific embodiment of the present invention is further described.Following embodiment is only used for more Add and clearly demonstrate technical solution of the present invention, and not intended to limit the protection scope of the present invention.
The raw material arrived used in following embodiment and comparative example is commercially available.
Embodiment 1
A kind of natural lotion is present embodiments provided, by mass percentage raw material components are as follows: 0.5% hydrogenation lecithin Rouge, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% xanthan gum, 0.08% tremella polysaccharides, 2% glycine betaine, 3% raspberry ketone and 63.32% water.
The natural lotion of the present embodiment the preparation method comprises the following steps:
S1, hydrolecithin, Wild soybean sterols and glycerol mixed in emulsion pot, is warming up to 80 DEG C, is added 1,3- It is stirred evenly after propylene glycol, obtains emulsifying material A;
S2, in oily phase pot by Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil Mixing, is warming up to 70~75 DEG C, obtains oil phase material B;
S3, in water phase pot by water, Sodium Hyaluronate, xanthan gum, tremella polysaccharides mix, be warming up to 80 DEG C, obtain aqueous-phase material Expect C;
S4, oil phase material B is added in emulsifying material A, first time homogeneous 15min;Add water phase material C, second Secondary homogeneous 8min, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 10min at 80 DEG C, is cooled to 45 DEG C, dipotassium glycyrrhizinate and raspberry ketone is added, It stirs evenly;
S6, the product feeding inspection for obtaining S5 after mixing evenly, qualified filtering and discharging.
The product that the present embodiment is obtained is tested for the property, as a result as shown in table 1 below:
The performance indicator of 1 embodiment of table, 1 product
Comparative example 1
This comparative example provides a kind of lotion, by mass percentage raw material components are as follows: 0.3% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% Olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.2% xanthan gum, 0.08% tremella polysaccharides, 2% glycine betaine, 3% raspberry ketone and 63.72% Water.
The lotion of this comparative example the preparation method comprises the following steps:
S1, hydrolecithin, Wild soybean sterols and glycerol mixed in emulsion pot, is warming up to 80 DEG C, is added 1,3- It is stirred evenly after propylene glycol, obtains emulsifying material A;
S2, in oily phase pot by Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil Mixing, is warming up to 70~75 DEG C, obtains oil phase material B;
S3, in water phase pot by water, Sodium Hyaluronate, xanthan gum, tremella polysaccharides mix, be warming up to 80 DEG C, obtain aqueous-phase material Expect C;
S4, oil phase material B is added in emulsifying material A, first time homogeneous 15min;Add water phase material C, second Secondary homogeneous 8min, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 10min at 80 DEG C, is cooled to 45 DEG C, dipotassium glycyrrhizinate and raspberry ketone is added, It stirs evenly;
S6, the product feeding inspection for obtaining S5 after mixing evenly, qualified filtering and discharging.
The product of this comparative example is tested for the property, wherein standard is not achieved in the centrifugation test of product.
Comparative example 2
This comparative example provides a kind of lotion, by mass percentage raw material components are as follows: 0.5% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% Olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% carbomer, 0.08% tremella polysaccharides, 2% glycine betaine, 3% raspberry ketone and 63.32% Water.
The lotion of this comparative example the preparation method comprises the following steps:
S1, hydrolecithin, Wild soybean sterols and glycerol mixed in emulsion pot, is warming up to 80 DEG C, is added 1,3- It is stirred evenly after propylene glycol, obtains emulsifying material A;
S2, in oily phase pot by Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil Mixing, is warming up to 70~75 DEG C, obtains oil phase material B;
S3, in water phase pot by water, Sodium Hyaluronate, carbomer, tremella polysaccharides mix, be warming up to 80 DEG C, obtain aqueous-phase material Expect C;
S4, oil phase material B is added in emulsifying material A, first time homogeneous 15min;Add water phase material C, second Secondary homogeneous 8min, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 10min at 80 DEG C, is cooled to 45 DEG C, dipotassium glycyrrhizinate and raspberry ketone is added, It stirs evenly;
S6, the product feeding inspection for obtaining S5 after mixing evenly, qualified filtering and discharging.
The product of this comparative example is tested for the property, product system is relatively stable, and every Testing index all meets country It is required that but the carbomer in raw material components is synthetic macromolecule, so the component of the formula is not belonging to 100% natural origin.
Comparative example 3
This comparative example provides a kind of lotion, by mass percentage raw material components are as follows: 0.8% PEG-100 stearic acid Ester, 0.6% stearine, 1.0% cetostearyl alcohol, 8% Butyrospermum parkii fruit rouge, 2% sunflower seed oil, 0.2% rosemary leaf oil, 5% olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% carbomer, 0.08% tremella polysaccharides, 2% beet Alkali, 3% raspberry ketone and 63.72% water.
The lotion of this comparative example the preparation method comprises the following steps:
S1, PEG-100 stearate, the pure and mild glycerol of stearine, cetearyl alcohol mixed in emulsion pot, heating To 80 DEG C, is stirred evenly after 1,3-PD is added, obtain emulsifying material A;
S2, in oily phase pot by Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil Mixing, is warming up to 70~75 DEG C, obtains oil phase material B;
S3, in water phase pot by water, Sodium Hyaluronate, carbomer, tremella polysaccharides mix, be warming up to 80 DEG C, obtain aqueous-phase material Expect C;
S4, oil phase material B is added in emulsifying material A, first time homogeneous 15min;Add water phase material C, second Secondary homogeneous 8min, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 10min at 80 DEG C, is cooled to 45 DEG C, dipotassium glycyrrhizinate and raspberry ketone is added, It stirs evenly;
S6, the product feeding inspection for obtaining S5 after mixing evenly, qualified filtering and discharging.
The product of this comparative example is tested for the property, product system is relatively stable, and indices are all in national requirements model In enclosing, but emulsifier and thickener are not belonging to existing for nature, cannot declare 100% natural origin.
Change the type or content meeting of a certain formula of the application it can be seen from the effect of above-described embodiment and comparative example The effect of product is produced a very large impact;Meanwhile even if existing certain emulsion formulations can reach with lotion phase of the invention The very few performance of difference, but it is difficult to pure natural, can more or less have a negative impact to human skin.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (10)

1. a kind of natural lotion, which is characterized in that by mass percentage include following component: 0~1% hydrolecithin, 0 ~1% Wild soybean sterols, 5~10% Butyrospermum parkii fruit rouge, 3~5% sunflower seed oil, 0~1% rosemary leave Oil, 3~5% olive oil, 2~5% grape seed oil, 1~5% glycerol, 5~10% 1,3- propylene glycol, 0~ 1% dipotassium glycyrrhizinate, 0~1% Sodium Hyaluronate, 0~1% xanthan gum, 0~1% tremella polysaccharides, 1~3% sweet tea Dish alkali, 1~3% raspberry ketone and complement to 100% water, wherein the content of the hydrolecithin do not include 0 and 1%, The content of the Wild soybean sterols does not include 0 and 1%, and the content of the rosemary leaf oil does not include 0 and 1%, the Radix Glycyrrhizae The content of sour dipotassium does not include 0 and 1%, and the content of the Sodium Hyaluronate does not include 0 and 1%, and the content of the xanthan gum is not Comprising 0 and 1%, the content of the tremella polysaccharides does not include 0 and 1%.
2. natural lotion as described in claim 1, which is characterized in that the natural lotion includes such as by mass percentage Lower component: 0.5% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed Oil, 0.2% rosemary leaf oil, 5% olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% xanthan gum, 0.08% tremella polysaccharides, 2% beet Alkali, 3% raspberry ketone and complement to 100% water.
3. natural lotion as described in claim 1, which is characterized in that by mass percentage, the group of the natural lotion It is divided into: 0.5% hydrolecithin, 0.3% Wild soybean sterols, 10% Butyrospermum parkii fruit rouge, 2% sunflower seed Oil, 0.2% rosemary leaf oil, 5% olive oil, 2% grape seed oil, 5% glycerol, 6% 1,3 propylene glycol, 0.1% dipotassium glycyrrhizinate, 0.1% Sodium Hyaluronate, 0.4% xanthan gum, 0.08% tremella polysaccharides, 2% beet Alkali, 3% raspberry ketone and 63.32% water.
4. a kind of preparation method of natural lotion as claimed in any one of claims 1 to 3, which is characterized in that described is natural The preparation method of lotion includes the following steps:
S1, hydrolecithin, Wild soybean sterols and glycerol are mixed, is warming up to 78~82 DEG C, stirred after 1,3-PD is added It mixes uniformly, obtains emulsifying material A;
S2, Butyrospermum parkii fruit rouge, sunflower seed oil, rosemary leaf oil, olive oil, grape seed oil are mixed, is warming up to 70 ~75 DEG C, obtain oil phase material B;
S3, Jiang Shui, Sodium Hyaluronate, xanthan gum, tremella polysaccharides mixing, are warming up to 78~82 DEG C, obtain water phase material C;
S4, oil phase material B is added in emulsifying material A, first time 12~18min of homogeneous;Add water phase material C, second Secondary 6~10min of homogeneous, obtains homogenous mass D;
S5, homogenous mass D kept the temperature into 9~11min at 78~82 DEG C, is cooled to 43~47 DEG C, dipotassium glycyrrhizinate is added and covers Basin ketone, stirs evenly;
Wherein, described S1, S2 and S3 in no particular order sequence.
5. the preparation method of natural lotion as claimed in claim 4, which is characterized in that the S1 is carried out in emulsion pot;
And/or the S2 is carried out in oily phase pot;
And/or the S3 is carried out in water phase pot.
6. the preparation method of natural lotion as claimed in claim 4, which is characterized in that in the S1, the temperature of heating is 80 ℃。
7. the preparation method of natural lotion as claimed in claim 4, which is characterized in that in the S3, the temperature of heating is 80 ℃。
8. the preparation method of lotion as claimed in claim 4 natural, which is characterized in that in the S4, first time homogeneous when Between be 15min, time of second of homogeneous is 8min.
9. the preparation method of natural lotion as claimed in claim 4, which is characterized in that in the S5, the time of heat preservation is 10min, the temperature after cooling are 45 DEG C.
10. the preparation method of lotion as claimed in claim 4 natural, which is characterized in that it after the S5 further include S6, it is described S6 are as follows: the product feeding inspection for obtaining S5 after mixing evenly, qualified filtering and discharging.
CN201811195548.0A 2018-10-15 2018-10-15 A kind of natural lotion and preparation method thereof Pending CN109199924A (en)

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CN114617811A (en) * 2021-09-01 2022-06-14 中山中研化妆品有限公司 Natural organic emulsion and preparation method thereof
CN114617811B (en) * 2021-09-01 2023-09-15 中山中研化妆品有限公司 Natural organic emulsion and preparation method thereof

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Application publication date: 20190115