CN111685999A - Preparation method of paperless, sterile and binderless moxibustion consumable - Google Patents
Preparation method of paperless, sterile and binderless moxibustion consumable Download PDFInfo
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- CN111685999A CN111685999A CN202010528502.7A CN202010528502A CN111685999A CN 111685999 A CN111685999 A CN 111685999A CN 202010528502 A CN202010528502 A CN 202010528502A CN 111685999 A CN111685999 A CN 111685999A
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- moxa
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
- A61H39/00—Devices for locating or stimulating specific reflex points of the body for physical therapy, e.g. acupuncture
- A61H39/06—Devices for heating or cooling such points within cell-life limits
Abstract
The invention provides a preparation method of a paperless, sterile and binderless moxibustion consumable, which only consists of a moxa material and moxa micro-nano fiber essence and can be prepared into moxa sticks, moxa columns and moxa cakes; the paper rolling process technology of moxibustion consumables since Ming dynasty is changed, the wrapping paper is removed, the new era of the clean mould pressing process of micro-nano molecular materials of the moxibustion consumables is opened, the prepared moxibustion consumables keep or are superior to the main combustion function of the traditional moxibustion consumables by combining infrared high-temperature sterilization treatment, and are clean and sterile and accord with the standards of medical and health supplies; compared with the traditional moxibustion consumables, the moxibustion consumables prepared by the process have the advantages of obvious appearance difference, 100 percent of moxa content, high effective active ingredient content, moderate density, good plasticity and high added value, and can be used for industrial cleaning and manufacturing production of novel moxibustion consumables with various types and specifications.
Description
Technical Field
The invention belongs to the field of medical and health consumables for moxibustion, and particularly relates to a preparation method of a paperless sterile adhesive-free moxibustion consumable.
Background
The moxibustion consumables mainly comprise moxa sticks/moxa columns/cakes and the like with various specifications, and the quality of the moxa sticks/moxa columns/cakes is the primary basic substance for ensuring the clinical effect of moxibustion. In the last 600 years, the moxa-moxibustion consumables are basically manufactured by simply crushing and screening the moxa raw fibers, wrapping the moxa raw fibers with brocade paper, rice paper or mulberry paper, and sealing the moxa raw fibers with an adhesive. For example, chinese patent CN206463215U discloses a paper tube moxa cone, which is composed of moxa cone, spacer, moxa layer and ignition twist. Wherein the moxa cone is formed by rolling moxa with paper and adhering the moxa with adhesive sticker; chinese patent CN108814952A discloses a rolled moxa column with a hole at the center, which is composed of moxa, leatheroid and flame-retardant film, and the moxa column is also made by wrapping the moxa with paper.
The moxa cone prepared by the method reduces the proportion of moxa content because paper is used as a package; and the addition of an adhesive to bond the paper causes the moxa column to generate pollutants when burned and has a polluting effect on moxibustion, indoor air and the like. In addition, moxa keeps the identity of agricultural products, the processing level of moxa is difficult to carry out dust-free and disinfection treatment, clear hygienic quality standards are lacked, basic hygienic and healthy requirements after health literacy promotion and consumption upgrade are not met, basic specifications of medical hygienic behaviors are not met, and the use of moxibustion consumable products is greatly limited.
2017.09.05 patent publication No. CN206463215U entitled "paper tube moxa cone", which discloses a paper tube moxa cone, consisting of moxa cone, spacer, moxa layer and ignition twist. The moxa cone adheres to the upper portion of the spacer, the bottom of the spacer is coated with a non-setting adhesive coating, the ignition is twisted on the upper and lower through arrangement inside the moxa cone, a plurality of layers of mutually parallel moxa oil layers are sequentially arranged in the moxa cone from top to bottom at intervals, a mesh cover with uniformly distributed meshes on the surface is covered outside the moxa cone, and a polymer gel layer is arranged between the spacer and the non-setting adhesive coating. However, the paper tube moxa cone has the advantages of large using amount of packing paper, more adhesive sticker components, more unpleasant and strong burnt paper smell generated in the combustion process, large smoke, heavy smell and more interference to infrared rays. Particularly, the built moxa oil layer has strong combustion heat, is the component which is abandoned after the traditional moxibustion is aged for three years, is the biggest change of the temperature and the heat of maturity of the folium artemisiae argyi, and has the purpose of adding the moxa oil to overcome the inheritable essence of the moxibustion for thousands of years. High quality moxa itself has excellent ignition and smoldering stability, and the use of ignition twists requires the use of other flammable substances, much like this and the potential for increased contamination.
2018.11.16 patent publication No. CN108814952A entitled "rolled moxa column with hole at center and manufacturing process thereof", discloses a rolled moxa column with hole at center, which comprises moxa column, paper skin and flame-retardant film. The moxa column is wrapped by the leatheroid, and one end of the moxa column is wrapped by the flame-retardant film; the moxa column wraps the end face of one end of the flame-retardant film, and a hole extending inwards along the axial direction of the moxa column is formed in the end face. The problem that the rolled moxa column cannot be drilled due to the fact that the material is soft and easy to deform is solved, the production process is claimed to be low-carbon, environment-friendly, free of additive and free of harmful substances generated by combustion is solved, and accordingly moxibustion treatment effect is improved. But the cost performance of the drilling machining process is very low, dust pollution is difficult to avoid, and the implementation possibility is low.
In a word, the traditional moxibustion consumables still have a plurality of pain points at present, still keep the characteristics and the identity of agricultural products so far, need urgently to wait for the industrial evolution and the upgrade: firstly, the packaging paper weight of the traditional moxibustion consumables is about 1.5-3.5%, and the moxa content is extruded; secondly, the packaging paper does not contain plant active ingredients basically, and the packaging materials, the adhesive and the like also aggravate smoke pollution; thirdly, the moxa is difficult to carry out dust-free and disinfection treatment compared with the original processing level mainly based on the manual operation of agricultural products, the sanitation quality standard is lost for a long time, and the moxa does not accord with the basic sanitation and health requirements after the promotion of health literacy and the upgrade of consumption, and also does not accord with the basic standard of medical sanitation behaviors;
in recent years, innovative moxa-carbon smokeless moxibustion consumables, moxa powder pressing consumables and high-temperature and high-pressure forming consumables are tried, although paper packing materials are removed in appearance. However, the moxibustion material has obvious structural defects of large change of infrared spectrum and combustion performance, excessive addition, great reduction of heated active substances and the like, cannot keep the basic physicochemical characteristics of the traditional moxibustion material, and cannot be accepted and recognized by the industry and the market.
Disclosure of Invention
In order to solve the problems in the prior art and further optimize the prior art, the invention provides a preparation method of a paperless sterile binderless moxibustion consumable, which aims to realize the following purposes:
1. the clean mould pressing technology replaces the traditional rolling technology, so that the standardization degree and the automatic manufacturing process of the manufacturing of the paperless sterile moxibustion consumables are improved, and the density of the consumables is improved;
2. the content of moxa and plant active ingredients is improved;
3. the method is low in carbon and environment-friendly, and harmful substances generated by combustion are reduced;
4. sterilizing at high temperature to meet medical and health standards;
in order to solve the technical problems, the invention adopts the following technical scheme:
a preparation method of a paperless, sterile and binderless moxibustion consumable material is characterized by comprising the steps of stirring and mixing, hot extrusion molding, drying and sterilizing in a mold and demolding;
the moxibustion consumable consists of a primary moxa fiber material and moxa micro-nano fiber essence;
the mixing and mixing are carried out, the mixing mass ratio of the primary moxa fiber material to the moxa micro-nano fiber essence to the water is 1: 1-5: 8-15 parts of;
stirring and mixing at the temperature of 20-25 ℃;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has a solid content of 1-4%, a pH value of 7.0-9.0, an average length of 50-100 microns and a length-diameter ratio of 10-20;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the Chinese mugwort produced in the Chinese spring and meets the quality standard of Chinese patent medicine Qingai strip;
the hot extrusion molding is carried out, and the compression ratio before and after molding is 1: 2-4;
the hot extrusion molding is carried out, and the temperature is 20-25 ℃;
the hot extrusion molding is carried out by adopting a screw to push a hot press or a three-D printing hot press, the die is a regular or irregular cylindrical hollow tube, and the wall thickness is 1-2 mm;
drying and sterilizing in the mold, wherein the peak value of the temperature is 160-170 ℃, and the drying time is 2-4 h; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 6 to 8 hours;
demoulding, cooling and packaging under aseptic condition, cooling to 20-30 ℃, and packaging in an aseptic bag;
the moxibustion consumables comprise, but are not limited to, moxa sticks, moxa columns and moxa cakes.
The invention provides a preparation method of a paperless sterile adhesive-free moxibustion consumable column, which is characterized by comprising the following steps: firstly, moxa and micro-nano fiber essence and water are fully dispersed and mixed according to a certain proportion, then, the moxa is extruded and molded through a mold, then, the sterilization and drying treatment are carried out on the moxa, demolding is carried out after a certain time to obtain various specifications of paperless, sterile and binderless moxa-moxibustion consumable material columns, the moxa-moxibustion consumable material obtained through the process has the characteristics of obvious appearance difference, 100 percent of moxa content, high content of effective active ingredients, good hardness, good plasticity, high added value and the like compared with the traditional moxa-moxibustion consumable material, and can be used for industrial cleaning and manufacturing production of novel moxa-moxibustion consumable materials of various types and specifications.
By adopting the technical scheme, the invention has the beneficial effects that:
1. by adopting the preparation method of the paperless sterile binderless moxibustion consumable, the prepared paperless moxa cone/moxa stick has the diameter of 9-30mm and the length of 1-20cm, has higher strength and hardness compared with paper moxa sticks, and has the density of 0.37-0.48g/cm3；
2. By adopting the preparation method of the paperless sterile binderless moxibustion consumable, the paperless moxa cone has high content of plant active ingredients, is composed of moxa and moxa nanocellulose, has no other additives, contains 100% of moxa components, and has high additional value;
3. the preparation method of the paperless, sterile and binderless moxibustion material has the advantages of simple process, greenness, no pollution, no addition of any chemical, and no generation of harmful substances during combustion;
4. the paperless sterile adhesive-free moxibustion consumable prepared by the invention has the burning speed of 2.5-3.2mm/min, the burning point of 180-;
5. the standardized highly-intelligent manufacturing production line can be adopted for continuous flow cleaning and intelligent manufacturing, manpower is greatly saved, manual or semi-manual operation is thoroughly distinguished, and subversive high-quality and higher cost performance are also provided compared with the current automatic strip rolling machine and the like.
The specific implementation mode is as follows:
the present invention will be described with reference to specific embodiments, wherein moxa is provided by the great name ancient moxa technologies ltd in hubei, and the moxa micro-nano fiber essence is provided by the shengquan group in jenan.
Example 1 preparation of a paperless, sterile, binderless moxibustion consumable
The preparation method comprises the following steps:
(1) stirring and mixing
Mixing moxa, moxa micro-nano fiber essence and water in a ratio of 1: 10 at 23 ℃ until the three are uniformly mixed together to obtain a moxa/micro-nano fiber essence aqueous solution mixed raw material;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has a solid content of 1.5%, a pH value of 7.0, an average length of 55 microns and a length-diameter ratio of 10;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the moxa produced in the spring and meets the moxa quality standard of Chinese patent medicine moxa stick;
(2) hot extrusion molding
Adding the mixed raw materials into a die, and forming by using common screw equipment in an extrusion mode, wherein the temperature is 23 ℃, the compression ratio before and after forming is 1: 2, and the wall thickness of the die is 2 mm;
(3) in-mold drying and sterilization
Putting the raw materials subjected to hot extrusion molding together with a mold into an oven for infrared high-temperature drying and sterilization treatment, wherein the peak temperature is 160 ℃, and the drying time is 2 hours; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 8 hours;
(4) demoulding
And (3) demoulding the dried product to obtain a paper-free sterile adhesive-free moxa cone finished product, and then cooling the paper-free sterile adhesive-free moxa cone finished product to 30 ℃ under a sterile condition for packaging.
Example 2
(1) Stirring and mixing
Mixing moxa, moxa micro-nano fiber essence and water in a ratio of 1: 3: 12 at the temperature of 20 ℃ until the three are completely and uniformly mixed together to obtain a moxa/micro-nano fiber essence mixed liquid raw material;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has a solid content of 1.0%, a pH value of 7.6, an average length of 64 microns and a length-diameter ratio of 10;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the Chinese mugwort produced in the Chinese spring and meets the quality standard of Chinese patent medicine Qingai strip;
(2) hot extrusion molding
Adding the mixed raw materials into a mould, and forming by using a three-D printing hot press device in an extrusion mode, wherein the temperature is 20 ℃, the compression ratio before and after forming is 1: 3, and the wall thickness of the mould is 2 mm;
(3) in-mold drying and sterilization
Putting the raw materials subjected to hot extrusion molding together with a mold into an oven for infrared high-temperature drying and sterilization treatment, wherein the peak temperature is 170 ℃, and the drying time is 2 hours; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 6 hours;
(4) demoulding
And (3) demoulding the dried product to obtain a paper-free sterile adhesive-free moxa cone finished product, and then packaging the paper-free sterile adhesive-free moxa cone finished product after the paper-free sterile adhesive-free moxa cone finished product is cooled to 25 ℃ under a sterile condition.
Example 3
(1) Stirring and mixing
Mixing moxa, moxa micro-nano fiber essence and water in a ratio of 1: 5: 8, stirring and mixing at 20 ℃ until the three are uniformly mixed together to obtain a moxa/micro-nano fiber essence mixed liquid raw material;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has the solid content of 3.0 percent, the pH value of 8.2, the average length of 80 microns and the length-diameter ratio of 15;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the Chinese mugwort produced in the Chinese spring and meets the quality standard of Chinese patent medicine Qingai strip;
(2) hot extrusion molding
Adding the mixed raw materials into a die, and forming by using common screw equipment in an extrusion mode, wherein the temperature is 20 ℃, the compression ratio before and after forming is 1: 4, and the wall thickness of the die is 2 mm;
(3) in-mold drying and sterilization
Putting the raw materials subjected to hot extrusion molding together with a mold into an oven for infrared high-temperature drying and sterilization treatment, wherein the peak temperature is 170 ℃, and the drying time is 4 hours; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 6 hours;
(4) demoulding
And (3) demoulding the dried product to obtain a paper-free sterile adhesive-free moxa cone finished product, and then packaging the paper-free sterile adhesive-free moxa cone finished product after the paper-free sterile adhesive-free moxa cone finished product is cooled to 25 ℃ under a sterile condition.
Example 4
(1) Stirring and mixing
Mixing moxa, moxa micro-nano fiber essence and water in a ratio of 1: 4: 12 at 25 ℃, fully stirring, dispersing and mixing to obtain a moxa/micro-nano fiber essence mixed liquid raw material;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has a solid content of 4.0%, a pH value of 8.9, an average length of 100 microns and a length-diameter ratio of 20;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the Chinese mugwort produced in the Chinese spring and meets the quality standard of Chinese patent medicine Qingai strip;
(2) hot extrusion molding
Adding the mixed raw materials into a mould, and carrying out hot press molding by using a three-D printing hot press device in an extrusion mode, wherein the temperature is 65 ℃, the compression ratio before and after molding is 1: 2, and the wall thickness of the mould is 2 mm;
(3) in-mold drying
Putting the raw materials subjected to hot extrusion molding together with a mold into an oven for infrared high-temperature drying and sterilization treatment, wherein the peak temperature is 170 ℃, and the drying time is 2 hours; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 6 hours;
(4) demoulding
And (3) demoulding the dried product to obtain a paper-free sterile adhesive-free moxa cone finished product, and then cooling the paper-free sterile adhesive-free moxa cone finished product to 30 ℃ under a sterile condition to perform packaging treatment.
Example 5
(1) Stirring and mixing
Mixing moxa and moxa micro-nano fiber essence with water in a ratio of 1: 3: 15 at 22 ℃, fully stirring, dispersing and mixing to obtain a moxa/micro-nano fiber essence liquid mixed raw material;
the moxa micro-nano fiber essence consists of moxa nano fibers and water, is in a green-brown paste shape, has the solid content of 3.8 percent, the pH value of 9.0, the average length of 85 microns and the length-diameter ratio of 18;
the moxa is primary pure moxa fiber which is primary proportion moxa fiber of the Chinese mugwort produced in the Chinese spring and meets the quality standard of Chinese patent medicine Qingai strip;
(2) hot extrusion molding
Adding the mixed raw materials into a die, and forming by using common screw equipment in an extrusion mode, wherein the temperature is 22 ℃, the compression ratio before and after forming is 1: 3, and the wall thickness of the die is 2 mm;
(3) in-mold drying and sterilization
Putting the raw materials subjected to hot extrusion molding together with a mold into an oven for infrared high-temperature drying and sterilization treatment, wherein the peak temperature is 170 ℃, and the drying time is 4 hours; subsequently, the temperature is reduced to 130 ℃, and the drying is continued for 8 hours;
(4) demoulding
And (3) demoulding the dried product to obtain a paper-free sterile adhesive-free moxa cone finished product, and then cooling the paper-free sterile adhesive-free moxa cone finished product to 50 ℃ under a sterile condition to perform packaging treatment.
The samples obtained in examples 1 to 5 were measured for density of moxa cone using a solid densitometer, for combustion rate of moxa cone using a stopwatch, and for combustion temperature of moxa cone using an infrared thermal imager, and the results were as follows:
TABLE 1 Density, burning velocity, ignition point and core temperature at burning of the samples of the examples
Therefore, the paperless moxa cone prepared by the process technology has the advantages of higher density, high combustion speed, high content of effective components, high added value, no addition of any chemical, and no generation of harmful substances during combustion.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art will understand that various changes, modifications and substitutions can be made without departing from the spirit and scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. A preparation method of a paperless, sterile and binderless moxibustion consumable material is characterized by comprising the steps of stirring and mixing, hot extrusion molding, drying and sterilizing in a mold; the moxibustion consumable consists of a primary moxa fiber material and moxa micro-nano fiber essence.
2. The preparation method according to claim 1, wherein the stirring and mixing are carried out, and the mixing mass ratio of the primary moxa fiber material to the moxa micro-nano fiber essence to the water is 1: 1-5: 8-15.
3. The preparation method of claim 2, wherein the moxa micro-nanofiber essence is composed of moxa nanofibers and water, is in a turquoise paste shape, has a solid content of 1% -4%, a pH value of 7.0-9.0, an average length of 50-100 μm, and an aspect ratio of 10-20.
4. The production method according to claim 1, wherein the hot extrusion molding is performed with a compression ratio of 1: 2-4.
5. The preparation method as claimed in claim 1, wherein the mold is dried and sterilized at a peak temperature of 160-170 ℃ for 2-4 h; then the temperature is reduced to 130 ℃, and the drying is continued for 6 to 8 hours.
6. The method of claim 4, wherein the hot extrusion is carried out at a temperature of 20 to 65 ℃.
7. The preparation method according to claim 4, wherein the hot extrusion molding is performed by using a screw-driven hot press or a three-D printing hot press, the die is a regular or irregular cylindrical hollow tube, and the wall thickness is 1-2 mm.
8. The method of claim 1, wherein the mixing is carried out with stirring at a temperature of 20 to 25 ℃.
9. The method of claim 1, further comprising a step of demolding, cooling and packaging under aseptic conditions, cooling to 20-30 ℃, and packaging in a sterile bag.
10. The preparation method of claims 1-9, wherein the moxibustion consumables comprise but are not limited to moxa sticks, moxa cones and moxa cakes.
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| CN114272117A (en) * | 2021-12-31 | 2022-04-05 | 华南理工大学 | Functional moxibustion tablet and preparation method thereof |
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