CN111574741A - 一种果实运输用epe珍珠棉的制备方法 - Google Patents

一种果实运输用epe珍珠棉的制备方法 Download PDF

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CN111574741A
CN111574741A CN202010527816.5A CN202010527816A CN111574741A CN 111574741 A CN111574741 A CN 111574741A CN 202010527816 A CN202010527816 A CN 202010527816A CN 111574741 A CN111574741 A CN 111574741A
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epe pearl
essential oil
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徐笑笑
李烨
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Hefei Xingye Packing Material Co ltd
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Abstract

本发明公开了一种果实运输用EPE珍珠棉的制备方法,包括以下操作步骤:(1)将肉桂精油、甘油混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉混合搅拌均匀后,制得抗菌醋酸酯淀粉;(2)将硅藻土、混晶二氧化钛加入至球磨机中,进行球磨处理后,制得成核剂;(3)将低密度聚乙烯、聚乙烯蜡、抗收缩剂、抗菌醋酸酯淀粉、成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入发泡剂,然后进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。本发明制得的EPE珍珠棉,具有优异的透气性能和抗菌效果,极大地延长了内部水果的保存时间。

Description

一种果实运输用EPE珍珠棉的制备方法
技术领域
本发明涉及包装材料制备的技术领域,具体涉及一种果实运输用EPE珍珠棉的制备方法。
背景技术
由于EPE珍珠棉发泡材料是一种新型的环保包装、填充材料。它的优越特性,越来越被人们认识,因此它的使用将不断扩大和创新。特别是在包装和其它工业用材方面,它比传统的用材性能更好,成本更低,档次更高,美观大方,效果更佳。另外它在农副产品包装用材领域也得到了较为广阔的应用。
但是现有的EPE珍珠棉作为一些水果的包装用材时,由于其透气性较差,并且不具有任何抗菌的效果,导致水果的保质期较短,经常的会发生水果在EPE珍珠棉包装材料内发生病虫害等腐烂的现象。
发明内容
为了解决上述存在的技术问题,延长水果在EPE珍珠棉包装材料内的保鲜时间,本发明提供一种果实运输用EPE珍珠棉的制备方法。
本发明是通过以下技术方案实现的:
一种果实运输用EPE珍珠棉的制备方法,包括以下操作步骤:
(1)将肉桂精油、甘油混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉混合搅拌均匀后,制得抗菌醋酸酯淀粉;
(2)将硅藻土、混晶二氧化钛加入至球磨机中,进行球磨处理后,制得成核剂;
(3)按重量份计,将180-200份低密度聚乙烯、30-40份聚乙烯蜡、1-5份抗收缩剂、3-6份抗菌醋酸酯淀粉、2-8份成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入15-20份发泡剂,发泡完成后,进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。
具体地,上述步骤(1)中,肉桂精油与甘油的质量比为1:5-8。
具体地,上述步骤(1)中,肉桂精油溶液与醋酸酯淀粉的质量比为1:15-20。
具体地,上述步骤(2)中,硅藻土与混晶二氧化钛的质量比为1:3-6。
具体地,上述步骤(2)中,球磨处理时,球磨介质为质量分数为75%的乙醇水溶液。
具体地,上述步骤(3)中,抗收缩剂为聚氧乙烯烷基醇酰胺。
由以上的技术方案可知,本发明的有益效果是:
本发明制得的EPE珍珠棉,加工性能优异,便于裁剪、加工成各种形状的包装材料,同时具有优异的透气性能和抗菌效果,极大地延长了内部水果的保存时间。其中,本发明制得的抗菌醋酸酯淀粉,无毒环保,并且在自然界中易于降解,尤其是具有优异的抗菌效果,能显著的抑制病菌在其表面繁衍生殖,进而有效的降低了包装材料内部水果被病虫害侵害的概率;同时本发明制得的抗菌醋酸酯淀粉,还能有效的提升EPE珍珠棉的白度,进而有效的提升了EPE珍珠棉包装材料的外观,提升了其品质;本发明制得的成核剂,能有效的提升EPE珍珠棉内部气泡分布的均匀性,同时能提升EPE珍珠棉的透氧性,保证包装材料内部具有一定的氧气和较高浓度的二氧化碳,使得果蔬能在包装材料内部保持较低的呼吸作用,进而有效的提升了果蔬的保鲜效果。
具体实施方式
下面将结合实施例对本发明的实施方案进行详细描述,但是本领域技术人员将会理解,下列实施例仅用于说明本发明,而不应视为限制本发明的范围。实施例中未注明具体条件者,按照常规条件或制造商建议的条件进行。所用试剂或仪器未注明生产厂商者,均为可以通过市售购买获得的常规产品。
实施例1
一种果实运输用EPE珍珠棉的制备方法,包括以下操作步骤:
(1)将肉桂精油、甘油按照质量比为1:5的比例混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉按照质量比为1:15的比例混合搅拌均匀后,制得抗菌醋酸酯淀粉;
(2)将硅藻土、混晶二氧化钛按照质量比为1:3的比例加入至球磨机中,进行球磨处理后,制得成核剂,其中球磨介质为质量分数为75%的乙醇水溶液;
(3)按重量份计,将180份低密度聚乙烯、30份聚乙烯蜡、1份聚氧乙烯烷基醇酰胺、3份抗菌醋酸酯淀粉、2份成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入15份发泡剂,发泡完成后,进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。
实施例2
一种果实运输用EPE珍珠棉的制备方法,包括以下操作步骤:
(1)将肉桂精油、甘油按照质量比为1:7的比例混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉按照质量比为1:18的比例混合搅拌均匀后,制得抗菌醋酸酯淀粉;
(2)将硅藻土、混晶二氧化钛按照质量比为1:5的比例加入至球磨机中,进行球磨处理后,制得成核剂,其中球磨介质为质量分数为75%的乙醇水溶液;
(3)按重量份计,将190份低密度聚乙烯、35份聚乙烯蜡、3份聚氧乙烯烷基醇酰胺、4份抗菌醋酸酯淀粉、4份成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入18份发泡剂,发泡完成后,进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。
实施例3
一种果实运输用EPE珍珠棉的制备方法,包括以下操作步骤:
(1)将肉桂精油、甘油按照质量比为1:8的比例混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉按照质量比为1:20的比例混合搅拌均匀后,制得抗菌醋酸酯淀粉;
(2)将硅藻土、混晶二氧化钛按照质量比为1:6的比例加入至球磨机中,进行球磨处理后,制得成核剂,其中球磨介质为质量分数为75%的乙醇水溶液;
(3)按重量份计,将200份低密度聚乙烯、40份聚乙烯蜡、5份聚氧乙烯烷基醇酰胺、6份抗菌醋酸酯淀粉、8份成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入20份发泡剂,发泡完成后,进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。
对比例1
步骤(3)中不添加抗菌醋酸酯淀粉,其余操作步骤与实施例1完全相同。
对比例2
将步骤(3)中的成核剂替换为等量的滑石粉,其余操作步骤与实施例2完全相同。
实验:
分别用各实施例和对比例的方法制得EPE珍珠棉,然后将制成包装箱,再将刚采摘下来的樱桃均匀的摆放在包装箱内,每箱放置一层樱桃,每箱放置1kg,将EPE珍珠棉包装箱至于室内环境中,每隔7天取果,并对果实的品质进行分析,其中果实硬度采用日本FHM-1果实硬度计测定;可溶性固形物(%)采用PAL-1手持数字式折光糖度仪测定;果皮褐变指数共分5级:0级无褐变;1级果皮褐变面积<1/4;2级果皮褐变面积为1/4~1/2;3级果皮褐变面积为1/2~3/4;四级果皮褐变面积>3/4,
果皮褐变指数=Σ(级别×该级别果数)/(最高级别×调查果数)×100%,实验结果如表1所示:
表1樱桃品质测定结果
Figure BDA0002534280590000041
其中,樱桃的硬度越高,可溶性固形物的含量越高,褐变指数越低,樱桃越新鲜。
由表1中实施例1和对比例1的数据可知,本发明制得的抗菌醋酸酯淀粉,能显著的抑制病菌在其表面繁衍生殖,进而有效的降低了包装材料内部水果被病虫害侵害的概率;由表1中实施例2和对比例2的数据可知,本发明制得的成核剂,能有效的提升EPE珍珠棉内部气泡分布的均匀性,同时能提升EPE珍珠棉的透氧性,保证包装材料内部具有一定的氧气和较高浓度的二氧化碳,使得果蔬能在包装材料内部保持较低的呼吸作用,进而有效的提升了果蔬的保鲜效果。
以上所描述的实施例是本发明一部分实施例,而不是全部的实施例。本发明的实施例的详细描述并非旨在限制要求保护的本发明的范围,而是仅仅表示本发明的选定实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。

Claims (6)

1.一种果实运输用EPE珍珠棉的制备方法,其特征在于,包括以下操作步骤:
(1)将肉桂精油、甘油混合均匀后,制得肉桂精油溶液,将肉桂精油溶液与醋酸酯淀粉混合搅拌均匀后,制得抗菌醋酸酯淀粉;
(2)将硅藻土、混晶二氧化钛加入至球磨机中,进行球磨处理后,制得成核剂;
(3)按重量份计,将180-200份低密度聚乙烯、30-40份聚乙烯蜡、1-5份抗收缩剂、3-6份抗菌醋酸酯淀粉、2-8份成核剂混合均匀后,加入至发泡机中,加热至低密度聚乙烯完全融化后,向其中加入15-20份发泡剂,发泡完成后,进行牵引定型、冷却、延展、收卷处理后,得到果实运输用EPE珍珠棉。
2.根据权利要求1所述的一种果实运输用EPE珍珠棉的制备方法,其特征在于,上述步骤(1)中,肉桂精油与甘油的质量比为1:5-8。
3.根据权利要求2所述的一种果实运输用EPE珍珠棉的制备方法,其特征在于,上述步骤(1)中,肉桂精油溶液与醋酸酯淀粉的质量比为1:15-20。
4.根据权利要求1所述的一种果实运输用EPE珍珠棉的制备方法,其特征在于,上述步骤(2)中,硅藻土与混晶二氧化钛的质量比为1:3-6。
5.根据权利要求1所述的一种果实运输用EPE珍珠棉的制备方法,其特征在于,上述步骤(2)中,球磨处理时,球磨介质为质量分数为75%的乙醇水溶液。
6.根据权利要求1所述的一种果实运输用EPE珍珠棉的制备方法,其特征在于,上述步骤(3)中,抗收缩剂为聚氧乙烯烷基醇酰胺。
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090285886A1 (en) * 2008-05-14 2009-11-19 Van Beek Ronald R Enhanced antimicrobial activity of plant essential oils
CN108442178A (zh) * 2018-05-07 2018-08-24 句容市兴武包装有限公司 一种高效抗菌生活用纸及其制备方法
CN109181071A (zh) * 2018-09-06 2019-01-11 安徽英美达新材料科技有限公司 一种epe珍珠棉及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090285886A1 (en) * 2008-05-14 2009-11-19 Van Beek Ronald R Enhanced antimicrobial activity of plant essential oils
CN108442178A (zh) * 2018-05-07 2018-08-24 句容市兴武包装有限公司 一种高效抗菌生活用纸及其制备方法
CN109181071A (zh) * 2018-09-06 2019-01-11 安徽英美达新材料科技有限公司 一种epe珍珠棉及其制备方法

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