CN111569464A - Salidroside processing extraction element - Google Patents
Salidroside processing extraction element Download PDFInfo
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- CN111569464A CN111569464A CN202010461985.3A CN202010461985A CN111569464A CN 111569464 A CN111569464 A CN 111569464A CN 202010461985 A CN202010461985 A CN 202010461985A CN 111569464 A CN111569464 A CN 111569464A
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- salidroside
- conveying belt
- hot reflux
- tank
- processing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C21/00—Disintegrating plant with or without drying of the material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/08—Separating or sorting of material, associated with crushing or disintegrating
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/18—Acyclic radicals, substituted by carbocyclic rings
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- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
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- Health & Medical Sciences (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
A salidroside processing and extracting device comprises a slicing machine, a dryer, a pulverizer, a vibrating screen, a grinding machine, a water tank, an ethanol tank, a mixing tank, a hot reflux concentration extractor, a centrifugal spray dryer and a powder collecting box. The slicer is connected with the dryer through a conveyer belt. The dryer is connected with the crusher through a conveyer belt. The crusher is connected with the oscillating screen through a conveyer belt. The oscillating screen is connected with the hot reflux concentration extractor through a conveyer belt. The oscillating screen is connected with the grinder through a coarse powder collecting pipe. The hot reflux concentration extractor is provided with a PH value detector. The water tank and the ethanol tank are respectively connected with the mixing tank. The mixing tank is communicated with the hot reflux concentration extractor through a pipeline. The hot reflux concentration extractor is connected with the feed inlet of the centrifugal spray dryer through a conveying pipeline. The centrifugal spray dryer is communicated with the powder collecting box through a conveying belt. The invention can adjust the PH value of the extractant by automatic detection, and can improve the extraction rate of salidroside to the maximum extent.
Description
Technical Field
The invention belongs to the technical field of deep processing of plants, and particularly relates to a salidroside processing and extracting device.
Background
Salidroside has important effects of resisting anoxia, relieving fatigue, resisting aging, preventing radiation, protecting cardiovascular system, inhibiting tumor growth, inhibiting cell cycle, and inducing apoptosis in various cancers (breast cancer, lung cancer, colon cancer, bladder cancer, glioma, etc.). Besides inhibiting the growth of cancer cells, the composition can also inhibit tumor metastasis and reduce the formation of new blood vessels. The salidroside medicine can obviously affect the cardiovascular system of the organism after entering the organism, thereby improving the condition of patients. In recent years, research shows that the traditional Chinese medicine composition has a certain therapeutic effect on various nervous system diseases. The anti-anoxia and anti-fatigue effects can stimulate organism, promote blood circulation, facilitate the combination of hemoglobin and oxygen, enhance the saturation of blood oxygen, reduce oxygen consumption of organism, increase exercise endurance, and resist fatigue.
Rhodiola rosea used for extracting salidroside is a perennial herb or a shrub wild plant, and is rare and precious, so that the salidroside is required to be extracted from rhodiola rosea raw materials as much as possible. However, the existing equipment has low utilization rate of raw materials in the process of extracting salidroside, filtered coarse powder cannot be reused in time, the extraction rate of salidroside is low, the yield is low, and the production efficiency is low.
Disclosure of Invention
Based on the background technology, the invention aims to provide a salidroside processing and extracting device for improving the extraction rate of salidroside.
In order to achieve the purpose, the invention adopts the following technical scheme:
a salidroside processing and extracting device comprises a slicing machine, a dryer, a pulverizer, a vibrating screen, a grinding machine, a water tank, an ethanol tank, a mixing tank, a hot reflux concentration extractor, a centrifugal spray dryer and a powder collecting box.
The discharge gate department of slicer is provided with conveyer belt one, the other end of conveyer belt one links to each other with the feed inlet of drying-machine.
And a second conveying belt is arranged at the outlet of the dryer, and the other end of the second conveying belt is connected with a feed inlet of the pulverizer.
And a third conveying belt is arranged at the outlet of the pulverizer, and the other end of the third conveying belt is connected with a feeding hole of the oscillating screen.
And a fourth conveying belt is arranged at the outlet of the oscillating screen, and the other end of the fourth conveying belt is connected with a feed inlet of the hot reflux concentration extractor.
And a coarse powder collecting pipe is arranged on the oscillating screen, and the other end of the coarse powder collecting pipe is connected with a feeding hole of the grinding mill.
And a first temperature controller and a PH value detector are arranged on the hot reflux concentration extractor.
The water tank and the ethanol tank are respectively connected with the mixing tank through pipelines, and the outlets of the water tank and the ethanol tank are respectively provided with an electromagnetic valve.
The outlet of the mixing tank is communicated with a hot reflux concentration extractor through a pipeline. And a third flowmeter and an electromagnetic valve are arranged at the outlet of the mixing tank.
And a fifth conveying pipeline is arranged at the discharge port of the hot reflux concentration extractor, and the tail end of the fifth conveying pipeline is connected with the feed port of the centrifugal spray dryer.
And a sixth conveying belt is arranged at an outlet of the centrifugal spray dryer, and the tail end of the sixth conveying belt is communicated with the powder collecting box.
Furthermore, a liquid supplementing pipe is arranged on the mixing tank and is communicated with the hot reflux concentration extractor.
Furthermore, a flow meter IV and an electromagnetic valve are arranged on the liquid supplementing pipe.
Furthermore, a timer and a second temperature control device are arranged on the dryer.
Furthermore, a heating plate is arranged below the hot reflux concentration extractor.
Furthermore, an electronic scale is arranged on the fourth conveying belt.
Furthermore, a powder return pipe is arranged at the discharge outlet of the grinding machine, and an outlet at the tail end of the powder return pipe is arranged above the third conveying belt.
Furthermore, an eighty-mesh sieve is arranged in the oscillating sieve.
Further, the mixing tank and the hot reflux concentration extractor are respectively provided with a sampling tube.
Furthermore, flow meters are respectively arranged at the outlets of the water tank and the ethanol tank.
Further, a water pump is arranged at an inlet of the water tank.
The invention has the beneficial effects that: can automatically complete slicing, drying, crushing, filtering, extracting and concentrating of the rhodiola rosea raw material. Can carry out fine grinding to filterable middlings, realize the reuse of middlings, avoid the material extravagant. The pH value of the extractant is detected and adjusted, so that the extraction rate of the salidroside is always maintained at the highest state, more salidroside can be extracted to the greatest extent, and the yield is improved.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic diagram showing the connection state of the mixing tank with the water tank, the ethanol tank and the hot reflux concentration extractor.
Reference numerals: 1-a slicer, 2-a dryer, 3-a pulverizer, 4-a vibrating screen, 5-a grinder, 6-a water tank, 7-an ethanol tank, 8-a mixing tank, 9-a hot reflux concentration extractor, 10-a centrifugal spray dryer, 11-a powder collecting box, 12-a flowmeter I, 13-a flowmeter II, 14-a heating plate, 15-a temperature controller I, 16-a timer, 17-a temperature control II, 18-a conveyer belt I, 19-a conveyer belt II, 20-a conveyer belt III, 21-a powder return pipe, 22-a coarse powder collecting pipe, 23-a conveyer belt IV, 24-a conveyer belt V, 25-a conveyer belt VI, 26-a water pump, 27-a PH value detector, 28-an electromagnetic valve and 29-a sampling pipe I, 30-sampling tube II, 31-flowmeter III, 32-liquid supplementing tube.
Detailed Description
For the convenience of understanding, the technical scheme of the invention is further described in detail by embodiments with reference to the attached drawings:
as shown in fig. 1 and 2, a salidroside processing and extracting device comprises a slicer 1, a dryer 2, a pulverizer 3, a vibrating screen 4, a grinder 5, a water tank 6, an ethanol tank 7, a mixing tank 8, a hot reflux concentration extractor 9, a centrifugal spray dryer 10 and a powder collecting box 11.
A first conveying belt 18 is arranged at the discharge port of the slicing machine 1, and the other end of the first conveying belt 18 is connected with the feed port of the dryer 2.
A second conveying belt 19 is arranged at the outlet of the dryer 2, and the other end of the second conveying belt 19 is connected with the feeding hole of the crusher 3. The dryer 2 is provided with a timer 16 and a second temperature control 17.
And a third conveying belt 20 is arranged at the outlet of the pulverizer 3, and the other end of the third conveying belt 20 is connected with the feeding hole of the oscillating screen 4.
And a fourth conveying belt 23 is arranged at the outlet of the oscillating screen 4, and the other end of the fourth conveying belt 23 is connected with a feed inlet of the hot reflux concentration extractor 9. An electronic scale is arranged on the fourth conveying belt 23.
The oscillating screen 4 is provided with a coarse powder collecting pipe 22, and the other end of the coarse powder collecting pipe 22 is connected with the feeding hole of the grinding mill 5. A powder return pipe 21 is arranged at the discharge port of the grinding machine 5, and the tail end outlet of the powder return pipe 21 is arranged above the third conveying belt 20. Eighty mesh sieves are arranged in the oscillating sieve 4.
The hot reflux concentration extractor 9 is provided with a first temperature controller 15 and a PH value detector 27.
A heating plate 14 is arranged below the hot reflux concentration extractor 9.
The second sampling tube 30 is arranged on the hot reflux concentration extractor 9.
The water tank 6 and the ethanol tank 7 are both connected with the mixing tank 8 through pipelines, and the outlet of the water tank 6 and the outlet of the ethanol tank 7 are respectively provided with a first flowmeter 12 and a second flowmeter 13. The outlets of the water tank 6 and the ethanol tank 7 are provided with electromagnetic valves 28. A water pump 26 is provided at the inlet of the water tank 6.
The outlet of the mixing tank 8 is communicated with a hot reflux concentration extractor 9 through a pipeline. The outlet of the mixing tank 8 is provided with a flow meter III 31 and an electromagnetic valve 28. The mixing tank 8 is provided with a first sampling pipe 29.
The mixing tank 8 is provided with a liquid supplementing pipe 32, and the liquid supplementing pipe 32 is communicated with the hot reflux concentration extractor 9. The liquid replenishing pipe 32 is provided with a flow meter four 33 and an electromagnetic valve 28.
A fifth conveying pipeline 24 is arranged at the discharge port of the hot reflux concentration extractor 9, and the tail end of the fifth conveying pipeline 24 is connected with the feed port of the centrifugal spray dryer 10.
The centrifugal spray dryer 10 is preferably a medicinal centrifugal spray drying apparatus manufactured by Junno drying apparatus, Inc. of Changzhou city, model number LPG-25.
The outlet of the centrifugal spray dryer 10 is provided with a conveying belt six 25, and the tail end of the conveying belt six 25 is communicated with the powder collecting box 11.
When the rhodiola rosea slicing machine is used, prepared rhodiola rosea raw materials are placed at an inlet of the slicing machine 1, the slicing machine 1 slices the rhodiola rosea, the rhodiola rosea raw materials are conveyed into a feeding port of the drying machine 2 through the first conveying belt 18, the drying machine 2 dries the slices at fixed temperature at fixed time, the dried slices are conveyed into the crushing machine 3 through the second conveying belt 19 and crushed into powder by the crushing machine 3, the powder is conveyed into the oscillating screen 4 through the third conveying belt 20 and passes through an eighty-mesh sieve, and the filtered fine powder is conveyed into the hot reflux concentration extracting machine 9 through the fourth conveying belt 23. The oscillating screen 4 conveys the filtered coarse powder into the grinder 5 through the coarse powder collecting pipe 22, the grinder 5 grinds the coarse powder into finer fine powder, and the powder returning pipe 21 is used for conveying the filtered coarse powder onto the conveying belt III 20 again, so that coarse powder grinding and recycling are realized, and the utilization rate of raw materials is improved. The water in the water tank 6 and the ethanol in the ethanol tank 7 are injected into the mixing tank 8 according to the proportion of 1:4 for mixing, and the mixed solution is quantitatively injected into the hot reflux concentration extractor 9. The rhodiola powder is refluxed, extracted and concentrated into an extract by a hot reflux concentration extractor 9, and the extract is dried into fine powder by a centrifugal spray dryer 10 to complete the processing and extraction of the salidroside.
In the process of reflux extraction and concentration, the PH detector 27 monitors the PH value in the hot reflux concentration extractor 9 at any time, and supplements an ethanol mixed solution to the hot reflux concentration extractor 9 through the flow meter three 31 and the electromagnetic valve 28 if necessary, so as to ensure that the PH value in the hot reflux concentration extractor 9 is consistent to PH8.0, so that the extraction rate of salidroside in the hot reflux concentration extractor 9 is always maintained at the highest state, more salidroside can be extracted to the greatest extent, and the yield is improved.
Claims (10)
1. A salidroside processing and extracting device comprises a slicing machine, a dryer, a pulverizer, a vibrating screen, a grinder, a water tank, an ethanol tank, a mixing tank, a hot reflux concentration extractor, a centrifugal spray dryer and a powder collecting box;
a first conveying belt is arranged at the discharge port of the slicing machine, and the other end of the first conveying belt is connected with the feed port of the dryer;
a second conveying belt is arranged at the outlet of the dryer, and the other end of the second conveying belt is connected with a feed inlet of the pulverizer;
a third conveying belt is arranged at the outlet of the pulverizer, and the other end of the third conveying belt is connected with a feeding hole of the oscillating screen;
a fourth conveying belt is arranged at the outlet of the oscillating screen, and the other end of the fourth conveying belt is connected with a feed inlet of the hot reflux concentration extractor;
a coarse powder collecting pipe is arranged on the oscillating screen, and the other end of the coarse powder collecting pipe is connected with a feed inlet of the grinding mill;
the hot reflux concentration extractor is provided with a first temperature controller and a PH value detector;
the water tank and the ethanol tank are respectively connected with the mixing tank through pipelines, and the outlets of the water tank and the ethanol tank are respectively provided with an electromagnetic valve;
an outlet of the mixing tank is communicated with the hot reflux concentration extractor through a pipeline, and a third flowmeter and an electromagnetic valve are arranged at the outlet of the mixing tank;
a fifth conveying pipeline is arranged at the discharge port of the hot reflux concentration extractor, and the tail end of the fifth conveying pipeline is connected with the feed port of the centrifugal spray dryer;
and a sixth conveying belt is arranged at an outlet of the centrifugal spray dryer, and the tail end of the sixth conveying belt is communicated with the powder collecting box.
2. The salidroside processing and extracting device according to claim 1, wherein: and a liquid supplementing pipe is arranged on the mixing tank and is communicated with the hot reflux concentration extractor.
3. The salidroside processing and extracting device according to claim 2, wherein: and a flow meter IV and an electromagnetic valve are arranged on the liquid supplementing pipe.
4. The salidroside processing and extracting device according to claim 3, wherein: and the dryer is provided with a timer and a second temperature control device.
5. The salidroside processing and extracting device according to claim 4, wherein: a heating plate is arranged below the hot reflux concentration extractor.
6. The salidroside processing and extracting device according to claim 5, wherein: and an electronic scale is arranged on the fourth conveying belt.
7. The salidroside processing and extracting device according to claim 6, wherein: and a powder return pipe is arranged at the discharge outlet of the grinding machine, and an outlet at the tail end of the powder return pipe is arranged above the third conveying belt.
8. The salidroside processing and extracting device according to claim 7, wherein: eighty mesh sieves are arranged in the oscillating sieves.
9. The salidroside processing and extracting device according to claim 8, wherein: the mixing tank and the hot reflux concentration extractor are respectively provided with a sampling tube.
10. The salidroside processing and extracting device according to any of claims 1 to 9, wherein: and flow meters are respectively arranged at the outlets of the water tank and the ethanol tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010461985.3A CN111569464A (en) | 2020-05-27 | 2020-05-27 | Salidroside processing extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010461985.3A CN111569464A (en) | 2020-05-27 | 2020-05-27 | Salidroside processing extraction element |
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| Publication Number | Publication Date |
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| CN111569464A true CN111569464A (en) | 2020-08-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202010461985.3A Pending CN111569464A (en) | 2020-05-27 | 2020-05-27 | Salidroside processing extraction element |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842667A (en) * | 2020-09-17 | 2021-12-28 | 湖南食尚康农业股份有限公司 | Sealwort extract product preparation equipment |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1091957A (en) * | 1993-03-05 | 1994-09-14 | 西藏自治区藏医院 | A kind of is the medicinal granule and preparation method thereof of main component with the Radix Rhodiolae extract |
| CN103288896A (en) * | 2013-05-15 | 2013-09-11 | 郁浩东 | Preparation process of salidroside |
| CN106905383A (en) * | 2017-03-31 | 2017-06-30 | 林婷 | A kind of hypoglycemic use glucoside extract and its manufacture method |
| CN109666052A (en) * | 2017-10-13 | 2019-04-23 | 肖梅 | A kind of extracting method of rhodioside |
| CN209866197U (en) * | 2019-04-27 | 2019-12-31 | 山东方舟生物科技有限公司 | A grinder for preparation of baikal skullcap root preparation |
-
2020
- 2020-05-27 CN CN202010461985.3A patent/CN111569464A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1091957A (en) * | 1993-03-05 | 1994-09-14 | 西藏自治区藏医院 | A kind of is the medicinal granule and preparation method thereof of main component with the Radix Rhodiolae extract |
| CN103288896A (en) * | 2013-05-15 | 2013-09-11 | 郁浩东 | Preparation process of salidroside |
| CN106905383A (en) * | 2017-03-31 | 2017-06-30 | 林婷 | A kind of hypoglycemic use glucoside extract and its manufacture method |
| CN109666052A (en) * | 2017-10-13 | 2019-04-23 | 肖梅 | A kind of extracting method of rhodioside |
| CN209866197U (en) * | 2019-04-27 | 2019-12-31 | 山东方舟生物科技有限公司 | A grinder for preparation of baikal skullcap root preparation |
Non-Patent Citations (1)
| Title |
|---|
| 刘桂艳: "单因素分析法优化红景天中红景天苷提取工艺的探究", 《生物化工》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842667A (en) * | 2020-09-17 | 2021-12-28 | 湖南食尚康农业股份有限公司 | Sealwort extract product preparation equipment |
| CN113842667B (en) * | 2020-09-17 | 2023-01-24 | 湖北鄂达生物科技有限公司 | Sealwort extract product preparation equipment |
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Application publication date: 20200825 |