CN111568839A - Hot compress steam microcapsule dry facial mask and preparation method thereof - Google Patents

Hot compress steam microcapsule dry facial mask and preparation method thereof Download PDF

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Publication number
CN111568839A
CN111568839A CN202010336052.1A CN202010336052A CN111568839A CN 111568839 A CN111568839 A CN 111568839A CN 202010336052 A CN202010336052 A CN 202010336052A CN 111568839 A CN111568839 A CN 111568839A
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parts
microcapsule
mask
steam
hot compress
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代学忠
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Jiangsu Yuebisheng Medical Equipment Co ltd
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Jiangsu Yuebisheng Medical Equipment Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
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    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F7/00Heating or cooling appliances for medical or therapeutic treatment of the human body
    • A61F7/02Compresses or poultices for effecting heating or cooling
    • A61F7/03Compresses or poultices for effecting heating or cooling thermophore, i.e. self-heating, e.g. using a chemical reaction
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    • A61F2007/0203Cataplasms, poultices or compresses, characterised by their contents; Bags therefor
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    • A61FFILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
    • A61F7/00Heating or cooling appliances for medical or therapeutic treatment of the human body
    • A61F7/02Compresses or poultices for effecting heating or cooling
    • A61F7/03Compresses or poultices for effecting heating or cooling thermophore, i.e. self-heating, e.g. using a chemical reaction
    • A61F7/032Compresses or poultices for effecting heating or cooling thermophore, i.e. self-heating, e.g. using a chemical reaction using oxygen from the air, e.g. pocket-stoves
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    • A61F2007/036Fuels
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    • A61H2201/00Characteristics of apparatus not provided for in the preceding codes
    • A61H2201/10Characteristics of apparatus not provided for in the preceding codes with further special therapeutic means, e.g. electrotherapy, magneto therapy or radiation therapy, chromo therapy, infrared or ultraviolet therapy
    • A61H2201/105Characteristics of apparatus not provided for in the preceding codes with further special therapeutic means, e.g. electrotherapy, magneto therapy or radiation therapy, chromo therapy, infrared or ultraviolet therapy with means for delivering media, e.g. drugs or cosmetics
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    • A61M2037/0007Other apparatus for introducing media into the body; Percutany, i.e. introducing medicines into the body by diffusion through the skin having means for enhancing the permeation of substances through the epidermis, e.g. using suction or depression, electric or magnetic fields, sound waves or chemical agents
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Abstract

The invention discloses a hot compress steam microcapsule dry facial mask and a preparation method thereof, relates to the technical field of cosmetic facial masks, and solves the problem that the transdermal absorption capacity of the human face to effective components in the facial mask is greatly reduced due to the cold stimulation effect on the human face skin when the facial mask is used in winter or cold winter, wherein the hot compress steam microcapsule dry facial mask comprises the following components in parts by weight: 3-4 parts of a microcapsule skin-care repair core material; 2-3 parts of microcapsule wall material; 60-80 parts of mask cloth; 40-50 parts of self-heating warm patch; 0.8-2 parts of adhesive. The hot compress steam microcapsule dry facial mask can effectively promote the transdermal absorption of effective components in the facial mask, and has good overall applicability.

Description

Hot compress steam microcapsule dry facial mask and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetic masks, in particular to a hot compress steam microcapsule dry mask and a preparation method thereof.
Background
The facial mask is a category of skin care products, is a carrier of the beauty care products, and is applied on the face for beauty functions such as moisturizing, whitening, anti-aging, grease balancing and the like.
The Chinese invention patent application with publication number CN108143702A discloses an efficient whitening and moisturizing mask liquid, a mask and a preparation method thereof, wherein the efficient whitening and moisturizing mask liquid at least comprises the following components in parts by weight: 100 parts of deionized water, 6-13 parts of a humectant and 3-9 parts of a skin conditioner; the skin conditioner at least comprises the following components in parts by weight: 3-7 parts of allantoin, 1-5 parts of ceramide, 35-44 parts of beta-glucan, 36-42 parts of Gentiana ruditapes root and grape seed extracts, and 16-23 parts of Aequorea victoria and rice extracts.
In the above application documents, the main active ingredients are all natural ingredient extracts, which do not stimulate the skin, and can stimulate the activity of skin cells, and enhance the immune protection function of the skin itself, but the existing facial mask is mostly water-based, and has a cold stimulation effect on the skin of the human face when used in winter or cold winter, which results in greatly reduced transdermal absorption capacity of the human face to the active ingredients in the facial mask, although the facial mask can be heated before use, so as to reduce the cold stimulation effect and promote the absorption of the active ingredients, but is difficult to preserve heat in a longer use process, the absorption effect of the skin of the human face to the active ingredients can be gradually reduced in the use process, so that the effect of the facial mask is greatly reduced, and further the application effect of the facial mask in cold winter is greatly reduced, therefore, a new scheme needs to be provided to solve the above problems.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a hot compress steam microcapsule dry facial mask to solve the technical problems, and when the hot compress steam microcapsule dry facial mask is applied in cold winter, the percutaneous absorption of effective components in the facial mask can be effectively promoted, and the overall applicability is good.
In order to achieve the first purpose, the invention provides the following technical scheme:
a hot compress steam microcapsule dry facial mask comprises the following components in parts by weight:
3-4 parts of a microcapsule skin-care repair core material;
2-3 parts of microcapsule wall material;
60-80 parts of mask cloth;
40-50 parts of self-heating warm patch;
0.8-2 parts of adhesive.
By adopting the technical scheme, the microcapsule skin-care repair core material and the microcapsule wall material are prepared into microcapsule particles, the microcapsule particles are attached to the surface of the mask cloth, and then the heating sheet is attached to the surface of the mask cloth, the heating sheet is directly attached to the targeted skin, the self-heating warm patch can act with oxygen in the air to generate an exothermic reaction in the use process, the wall material of the microcapsule particles is dissolved and releases effective components in the core material when the temperature reaches 45-55 ℃, and the effects of medicine treatment and thermotherapy and the effect of external treatment of internal diseases can be achieved. Meanwhile, the heat energy generated by the self-heating warm patch can greatly reduce the cold stimulation effect of the mask on the facial skin when the mask is applied in cold winter, and further can effectively promote the transdermal absorption of effective components in the mask. Moreover, the application of the microcapsule and the dry mask greatly prolongs the service cycle of the hot compress steam microcapsule dry mask on the premise of not adding corrosion resistance, and the application is safer and has good overall application effect.
Further preferably, the microcapsule skin care repair core material comprises the following components in parts by weight:
0.1-0.5 part of hydrolyzed sodium hyaluronate;
0.3-0.9 part of sodium hyaluronate;
5-10 parts of traditional Chinese medicine extract;
0.5-1.5 parts of 1, 2-pentanediol;
10-30 parts of trehalose;
0.5-2 parts of betaine;
1-3 parts of small molecule tripeptide;
2-3 parts of hydroxyethyl cellulose;
4-8 parts of deionized water.
By adopting the technical scheme, the small-molecule tripeptide is uniquely ordered, can simulate the mechanism of a human body to generate collagen through TGF-beta, not only can obviously increase the collagen and improve the skin plumpness, but also can protect the collagen from being degraded and reduce various types of wrinkles. The sodium hyaluronate and the sodium hyaluronate are good moisturizing agents and are beneficial to keeping skin moist and glossy. The betaine has strong moisture absorption performance, can play a good cleaning role, does not hurt skin, has good compatibility and has excellent decontamination and sterilization effects. Trehalose has low hygroscopicity and high moisture-retaining function. The 1, 2-pentanediol can improve the moisturizing effect of the formula and enable the face of a human body to have smooth skin feeling. The traditional Chinese medicine extract has a natural preservative effect, can provide cell activity, and has a certain anti-aging effect. The hydroxyethyl cellulose is beneficial to keeping the good and stable mixed state of the microcapsule skin-care repair core material. Therefore, the microcapsule skin care repair core material obtained by mixing the components has good moisturizing and tightening effects on facial skin of a human body.
More preferably, the microcapsule wall material is any one of acacia, gelatin, ethyl cellulose and paraffin.
By adopting the technical scheme, the microcapsule wall material prepared from the Arabic gum, the gelatin, the ethyl cellulose or the paraffin wax has a good sealing effect on the microcapsule core material, can effectively inhibit the volatilization loss of the microcapsule core material, improves the storage and use stability of the microcapsule core material, has the capabilities of resisting oxygen, light and heat, enables the microcapsule core material to have a slow release function, and further ensures the stability of the hot compress steam microcapsule dry mask.
Further preferably, the mask cloth is made of any one of non-woven fabric material, silk film cloth, fruit fiber film cloth, biological fiber film cloth and tencel film cloth.
Through adopting above-mentioned technical scheme, non-woven fabrics material membrane cloth, silk membrane cloth, fruit fine membrane cloth, biological fiber membrane cloth and tencel membrane cloth are good mask cloth, have good associativity between it and the microcapsule core, and the gas permeability is good, bearing capacity is strong to have fine obedience ability, make hot compress steam microcapsule dry facial mask have good quality.
Further preferably, the self-heating warm patch comprises an outer bag, a breathable membrane and a self-heating mixed material, wherein the self-heating mixed material comprises the following raw materials in parts by weight:
10-15 parts of activated carbon;
0.5-1 part of sodium chloride;
50-55 parts of iron powder;
8-10 parts of vermiculite.
By adopting the technical scheme, the outer bag is attached to the breathable film, so that the outer bag has the function of isolating the outside air and can be torn off when in use; the breathable membrane plays a role in shaping and fixing the self-heating mixed material, and can enable oxygen in the air to permeate through the breathable membrane to further react with the self-heating mixed material to generate heat; the active carbon has the function of adsorbing moisture in the air and ensuring the smooth oxidation process; sodium chloride is a catalyst for promoting the corrosion of iron powder; vermiculite can expand when being heated, has strong self water absorption capacity, disperses iron powder together with activated carbon, can avoid burning skin due to too fast heating of self-heating warm patches, and further improves the stability of the hot compress steam microcapsule dry mask when in application.
Further preferably, the self-heating mixed material is distributed on the breathable film in a dotted manner.
By adopting the technical scheme, the self-heating mixed materials are distributed in a dotted manner on the breathable film, so that the hot compress steam microcapsule dry facial mask is convenient to fold, keeps soft and comfortable, can uniformly supply heat to the skin of the human body, and can effectively promote the transdermal absorption of effective components in the facial mask.
More preferably, the adhesive is selected from any one of vinyl acetate resin and acrylic resin.
By adopting the technical scheme, the vinyl acetate resin and the acrylic resin are both emulsion type curing agents and have good light resistance and ageing resistance, so that the hot compress steam microcapsule dry mask keeps good stability in the storage process. Meanwhile, when the self-heating warm patch emits a large amount of heat, the adhesive is not easy to discolor and turn yellow, and the hot compress steam microcapsule dry mask can exert good and stable efficacy.
More preferably, the adhesive is doped with high thermal conductive filler accounting for 2-5% of the adhesive by weight.
More preferably, the high-thermal-conductivity filler is any one or a mixture of more than one of boron nitride, aluminum nitride and silicon carbide, and the particle size of the high-thermal-conductivity filler is 7-10 μm.
By adopting the technical scheme, the boron nitride, the aluminum nitride and the silicon carbide are good high-thermal-conductivity fillers, have high thermal conductivity, can enable heat emitted by the self-heating warm patch to quickly penetrate through the bonding layer formed by the adhesive, enable microcapsule ions on the mask cloth to be damaged, and quickly release effective ingredients. Meanwhile, the high-heat-conduction filler can also effectively avoid dissipation of heat emitted by the self-heating warm patch, so that more heat can be applied to the skin of the face of a human body, the overall application effect of the hot-compress steam microcapsule dry facial mask is further improved, the particle size of the high-heat-conduction filler is 7-10 microns, the high-heat-conduction filler can be uniformly distributed, and the comfort level of the hot-compress steam microcapsule dry facial mask in an application mode is guaranteed.
The second purpose of the invention is to provide a preparation method of the hot compress steam microcapsule dry facial mask, and the hot compress steam microcapsule dry facial mask prepared by the method can effectively promote the transdermal absorption of effective components in the facial mask when applied in cold winter, and has good overall applicability.
In order to achieve the second purpose, the invention provides the following technical scheme, and the preparation method of the hot compress steam microcapsule dry mask comprises the following steps:
step one, mixing microcapsule skin care repair core materials and microcapsule wall materials in corresponding parts by weight, heating to 35-40 ℃, and stirring for 5-10min at 20-30rpm to obtain an encapsulated initial solution;
step two, spraying and freezing the encapsulated initial solution at-40 to-45 ℃, and carrying out vacuum drying in a frozen state to obtain microcapsule particles;
and step three, attaching the microcapsule particles obtained in the step two to the mask cloth by utilizing a microparticle attachment technology, coating an adhesive on the surface of the mask cloth, and attaching the self-heating warm patch and the mask cloth together to obtain the hot compress steam microcapsule dry mask.
By adopting the technical scheme, the microcapsule particle prepared by the spray freezing method is generally 5-200 mu m, the shape is mostly spherical, the wall thickness of the microcapsule is 0.2-8 mu m, the microcapsule has good storage stability, and after the microcapsule is heated and reaches a certain temperature, the wall of the microcapsule can be quickly damaged, so that the microcapsule can be stably released to protect and repair the core material, and the stability of the hot compress steam microcapsule dry facial mask in application is ensured. Meanwhile, the preparation method is simple to operate, and the obtained hot compress steam microcapsule dry facial mask is good and stable in quality, high in production efficiency and good in overall application.
In summary, compared with the prior art, the invention has the following beneficial effects:
(1) the heat energy generated by the self-heating warm patch can greatly reduce the cold stimulation effect of the mask on the facial skin when the mask is applied in cold winter, so that the transdermal absorption of active ingredients in the mask can be effectively promoted, the application of the microcapsule and the dry mask is utilized, the service cycle of the hot compress steam microcapsule dry mask is greatly prolonged on the premise of not adding corrosion resistance, and the mask is safer and has good integral application effect;
(2) the self-heating mixed materials are distributed on the breathable film in a dotted manner, so that the hot compress steam microcapsule dry mask is convenient to fold, soft and comfortable, heat can be uniformly supplied to the skin of the human body, and the transdermal absorption of effective components in the mask can be effectively promoted;
(3) the high-heat-conductivity filler can enable heat emitted from the self-heating warm patch to quickly penetrate through the adhesive layer formed by the adhesive, and enable microcapsule ions on the mask cloth to be damaged, so that effective ingredients can be quickly released. Meanwhile, the high-thermal-conductivity filler can also effectively avoid dissipation of heat emitted by the self-heating warm patch, so that more heat can be applied to the facial skin of a human body, and the overall application effect of the hot-compress steam microcapsule dry facial mask is further improved.
Drawings
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
The invention is described in detail below with reference to the figures and examples.
Example 1: the hot compress steam microcapsule dry mask comprises the components and corresponding parts by weight shown in table 1, and is prepared by the following steps:
step one, mixing microcapsule skin care repair core materials and microcapsule wall materials in corresponding parts by weight, heating to 37.5 ℃, and stirring at 25rpm for 7.5min to obtain an encapsulated initial solution;
step two, spraying and freezing the encapsulated initial solution at the temperature of-42.5 ℃, and carrying out vacuum drying in a frozen state to obtain microcapsule particles;
and step three, attaching the microcapsule particles obtained in the step two to the mask cloth by utilizing a microparticle attachment technology, coating an adhesive on the surface of the mask cloth, and attaching the self-heating warm patch and the mask cloth together to obtain the hot compress steam microcapsule dry mask.
Note: in the above steps, the microcapsule wall material is Arabic gum. The mask cloth is made of non-woven fabric. The microcapsule skin care repair core material comprises the following components in parts by weight: 0.3 part of hydrolyzed sodium hyaluronate; 0.6 part of sodium hyaluronate; 7.5 parts of traditional Chinese medicine extract; 1 part of 1, 2-pentanediol; 20 parts of trehalose; 1.25 parts of betaine; 2 parts of small-molecule tripeptide; 2.5 parts of hydroxyethyl cellulose; 4 parts of deionized water, and uniformly stirring and mixing by adopting a conventional technology to obtain the traditional Chinese medicine extract, wherein the traditional Chinese medicine extract is a coix seed extract and is purchased from Guangzhou Kafen biotechnology limited company. The self-heating warm patch comprises an outer bag, a breathable membrane and a self-heating mixed material, wherein the self-heating mixed material comprises the following raw materials in parts by weight: 12.5 parts of activated carbon; 0.75 part of sodium chloride; 52.5 parts of iron powder; 9 parts of vermiculite, wherein the self-heating mixed material is distributed on the breathable membrane in a dotted manner, the outer bag is made of gelatin, and the breathable membrane is made of non-woven fabric. The adhesive is vinyl acetate resin which is purchased from high stand chemical industry Co., Ltd, Dongguan and is of film grade EVA U.S. DuPont 770. The ion content of the microcapsule in the mask cloth is 250 g/piece.
Example 2: a steam microcapsule hot compress dry pack, which is different from example 1 in that it is prepared by the following steps:
step one, mixing microcapsule skin care repair core materials and microcapsule wall materials in corresponding parts by weight, heating to 35 ℃, and stirring at 30rpm for 5min to obtain an encapsulated initial solution;
step two, spraying and freezing the encapsulated initial solution at the temperature of minus 40 ℃, and carrying out vacuum drying in a frozen state to obtain microcapsule particles;
and step three, attaching the microcapsule particles obtained in the step two to the mask cloth by utilizing a microparticle attachment technology, coating an adhesive on the surface of the mask cloth, and attaching the self-heating warm patch and the mask cloth together to obtain the hot compress steam microcapsule dry mask.
Example 3: a steam microcapsule hot compress dry pack, which is different from example 1 in that it is prepared by the following steps:
step one, mixing microcapsule skin care repair core materials and microcapsule wall materials in corresponding parts by weight, heating to 0 ℃, and stirring at 20rpm for 10min to obtain an encapsulated initial solution;
step two, spraying and freezing the encapsulated initial solution at the temperature of minus 45 ℃, and carrying out vacuum drying in a frozen state to obtain microcapsule particles;
and step three, attaching the microcapsule particles obtained in the step two to the mask cloth by utilizing a microparticle attachment technology, coating an adhesive on the surface of the mask cloth, and attaching the self-heating warm patch and the mask cloth together to obtain the hot compress steam microcapsule dry mask.
Examples 4 to 5: a steam microcapsule dry pack for hot compress, which is different from example 1 in that each component and corresponding parts by weight are shown in Table 1.
TABLE 1 Components and parts by weight of examples 1-5
Figure BDA0002466652890000061
Example 6: a steam microcapsule dry facial mask for hot compress is different from the embodiment 1 in that in the step one, the wall material of the microcapsule is gelatin.
Example 7: a steam microcapsule dry pack for hot compress, which is different from the dry pack of embodiment 1, is characterized in that in the first step, the microcapsule wall material is ethyl cellulose.
Example 8: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the step two, the mask cloth is silk film cloth.
Example 9: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the step two, the mask cloth is fruit fiber film cloth.
Example 10: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the step one, the microcapsule skin care repair core material comprises the following components in parts by weight: 0.1 part of hydrolyzed sodium hyaluronate; 0.3 part of sodium hyaluronate; 5 parts of traditional Chinese medicine extract; 0.5 part of 1, 2-pentanediol; 10 parts of trehalose; 0.5 part of betaine; 1 part of small molecule tripeptide; 2 parts of hydroxyethyl cellulose and 6 parts of deionized water.
Example 11: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the step one, the microcapsule skin care repair core material comprises the following components in parts by weight: 0.5 part of hydrolyzed sodium hyaluronate; 0.9 part of sodium hyaluronate; 10 parts of traditional Chinese medicine extract; 1.5 parts of 1, 2-pentanediol; 30 parts of trehalose; 2 parts of betaine; 3 parts of small molecule tripeptide; 3 parts of hydroxyethyl cellulose and 8 parts of deionized water.
Example 12: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the third step, the self-heating mixed material in the self-heating warm patch comprises the following raw materials in parts by weight: 10 parts of activated carbon; 0.5 part of sodium chloride; 50 parts of iron powder; 8 parts of vermiculite.
Example 13: the difference between the hot compress steam microcapsule dry mask and the embodiment 1 is that in the third step, the self-heating mixed material in the self-heating warm patch comprises the following raw materials in parts by weight: 15 parts of activated carbon; 1 part of sodium chloride; 55 parts of iron powder; 10 parts of vermiculite.
Example 14: a hot compress steam microcapsule dry facial mask is different from the embodiment 1 in that in the third step, the adhesive is acrylic resin, namely the Yingchuangdegusan PM 612.
Example 15: a hot compress steam microcapsule dry facial mask is different from the embodiment 1 in that in the third step, a high heat conduction filler accounting for 3.5 percent of the self weight percentage is doped in a binding agent, the high heat conduction filler is boron nitride, and the particle size of the boron nitride is 8.5 mu m.
Example 16: a hot compress steam microcapsule dry facial mask is different from the embodiment 1 in that in the third step, a high heat conduction filler accounting for 2% of the self weight percentage is doped in a bonding agent, the high heat conduction filler is aluminum nitride, and the particle size of the aluminum nitride is 7 mu m.
Example 17: a hot compress steam microcapsule dry facial mask is different from the embodiment 1 in that in the third step, a high heat conduction filler accounting for 5 percent of the self weight is doped in an adhesive, the high heat conduction filler is silicon carbide, and the grain diameter of the silicon carbide is 10 mu m.
Comparative example 1: the difference between the conventional mask and the embodiment 1 is that the mask liquid comprises the following components in parts by weight: 0.3 part of hydrolyzed sodium hyaluronate; 0.6 part of sodium hyaluronate; 7.5 parts of traditional Chinese medicine extract; 1 part of 1, 2-pentanediol; 20 parts of trehalose; 1.25 parts of betaine; 2 parts of small-molecule tripeptide; 2.5 parts of hydroxyethyl cellulose; 4 parts of deionized water; the mask cloth is made of non-woven fabric; and the content of the mask liquid in the mask cloth is 250 mL/piece.
Comparative example 2: a hot compress steam microcapsule dry facial mask, which is different from the embodiment 15 in that a binder is doped with a high thermal conductive filler accounting for 3.5 percent of the self weight percentage, the high thermal conductive filler is boron nitride, and the particle size of the boron nitride is 6 μm.
Comparative example 3: a hot compress steam microcapsule dry facial mask, which is different from the embodiment 15 in that a binder is doped with a high thermal conductive filler accounting for 3.5 percent of the self weight percentage, the high thermal conductive filler is boron nitride, and the particle size of the boron nitride is 11 μm.
Performance testing
Test samples: the steam-microcapsule heat-application dry facial masks obtained in examples 1 to 17 were used as test samples 1 to 17, and the conventional facial masks and the steam-microcapsule heat-application dry facial masks obtained in comparative examples 1 to 3 were used as control samples 1 to 3.
The test method comprises the following steps: according to the requirements of the trade standard QB/T4256-; detecting the moisture content of the stratum corneum of each group of volunteers after 4 hours of use at the ambient temperature of 5 ℃ and the relative humidity of 50%; then the skin tightening effect is evaluated by application, 10 points represent the best effect, and 1 point represents the worst effect.
And (3) test results: the test results of the test samples 1 to 17 and the control samples 1 to 3 are shown in Table 2. As can be seen from table 2, compared with the conventional facial mask, the hot compress steam microcapsule dry facial mask has better moisturizing and water locking effects after being used, better and excellent skin tightening effects and good overall application effect, and can be obtained by comparing the test results of the test samples 1 to 5 with the test result of the control sample 1. The test results of the test samples 15-17 and the test sample 1 are compared, and the high-thermal-conductivity filler can be applied to the adhesive, so that the overall moisture-preserving and water-locking effect and the skin tightening effect of the hot-compress steam microcapsule dry mask can be improved, and the application effect of the hot-compress steam microcapsule dry mask can be greatly improved. The test results of the test sample 15 and the control samples 2-3 are compared, and the high-thermal-conductivity filler with the particle size of 7-10 microns is selected, so that the hot-compress steam microcapsule dry mask has the best moisture-preserving and water-locking effect and the best skin tightening effect when being applied.
TABLE 2 test results of test samples 1-17 and control samples 1-3
Figure BDA0002466652890000081
Figure BDA0002466652890000091
The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims (10)

1. The hot compress steam microcapsule dry mask is characterized by comprising the following components in parts by weight:
3-4 parts of a microcapsule skin-care repair core material;
2-3 parts of microcapsule wall material;
60-80 parts of mask cloth;
40-50 parts of self-heating warm patch;
0.8-2 parts of adhesive.
2. The steam-on-heat microcapsule dry mask as claimed in claim 1, wherein the microcapsule skin-care repair core material comprises the following components in parts by weight:
0.1-0.5 part of hydrolyzed sodium hyaluronate;
0.3-0.9 part of sodium hyaluronate;
5-10 parts of traditional Chinese medicine extract;
0.5-1.5 parts of 1, 2-pentanediol;
10-30 parts of trehalose;
0.5-2 parts of betaine;
1-3 parts of small molecule tripeptide;
2-3 parts of hydroxyethyl cellulose;
4-8 parts of deionized water.
3. The steam-encapsulated dry mask pack according to claim 1, wherein the wall material of the microcapsules is selected from any one of gum arabic, gelatin, ethylcellulose and paraffin.
4. The dry mask with steam heat packs and microcapsules of claim 1, wherein the mask cloth is selected from one of non-woven fabric, silk, fruit fiber, biological fiber and tencel.
5. The steam microcapsule hot compress dry mask as claimed in claim 1, wherein the self-heating warm patch comprises an outer bag, an air permeable membrane and a self-heating mix, and the self-heating mix comprises the following raw materials in parts by weight:
10-15 parts of activated carbon;
0.5-1 part of sodium chloride;
50-55 parts of iron powder;
8-10 parts of vermiculite.
6. The steam-on-hot microcapsule dry pack as claimed in claim 5, wherein the self-heating mixture is distributed in a dotted pattern on the air-permeable film.
7. The steam microcapsule dry pack for hot compress of claim 1, wherein the binder is selected from any one of vinyl acetate resin and acrylic resin.
8. The steam-on-heat microcapsule dry pack as set forth in claim 1, wherein the binder is doped with the high thermal conductive filler in an amount of 2 to 5% by weight thereof.
9. The steam-heated microcapsule dry pack as claimed in claim 8, wherein the high thermal conductive filler is one or more selected from the group consisting of boron nitride, aluminum nitride and silicon carbide, and has a particle size of 7 to 10 μm.
10. A method of preparing a steam encapsulated dry pack for hot compress according to claim 1, comprising the steps of:
step one, mixing microcapsule skin care repair core materials and microcapsule wall materials in corresponding parts by weight, heating to 35-40 ℃, and stirring for 5-10min at 20-30rpm to obtain an encapsulated initial solution;
step two, spraying and freezing the encapsulated initial solution at-40 to-45 ℃, and carrying out vacuum drying in a frozen state to obtain microcapsule particles;
and step three, attaching the microcapsule particles obtained in the step two to the mask cloth by utilizing a microparticle attachment technology, coating an adhesive on the surface of the mask cloth, and attaching the self-heating warm patch and the mask cloth together to obtain the hot compress steam microcapsule dry mask.
CN202010336052.1A 2020-04-25 2020-04-25 Hot compress steam microcapsule dry facial mask and preparation method thereof Withdrawn CN111568839A (en)

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CN113304081A (en) * 2021-06-10 2021-08-27 龙青容 Degradable moisturizing self-heating polyester-based dry facial mask
CN116650379A (en) * 2023-06-19 2023-08-29 淄博金藏新材料科技有限公司 Preparation process and application of novel heating adhesive powder

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CN110302086A (en) * 2019-06-15 2019-10-08 上海优康化妆品有限公司 A kind of multiple-effect maintenance essence and its preparation process

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Publication number Priority date Publication date Assignee Title
CN101547667A (en) * 2006-12-15 2009-09-30 金伯利-克拉克环球有限公司 Self warming mask
CN106420156A (en) * 2016-10-21 2017-02-22 广州市科能化妆品科研有限公司 Self-heating paster
CN109722912A (en) * 2018-12-11 2019-05-07 代学忠 A kind of microcapsule essence composite material and its preparation process for self-heating product
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113304081A (en) * 2021-06-10 2021-08-27 龙青容 Degradable moisturizing self-heating polyester-based dry facial mask
CN113304081B (en) * 2021-06-10 2023-08-18 菲诗倾城(广州)生物科技有限公司 Degradable moisturizing self-heating polyester-based dry mask
CN116650379A (en) * 2023-06-19 2023-08-29 淄博金藏新材料科技有限公司 Preparation process and application of novel heating adhesive powder

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Application publication date: 20200825