CN107802519A - A kind of herbal essences solid perfume based on complex enzyme hydrolysis technology and preparation method thereof - Google Patents
A kind of herbal essences solid perfume based on complex enzyme hydrolysis technology and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
Maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch are weighed as cyst material the invention discloses a kind of herbal essences solid perfume based on complex enzyme hydrolysis technology and preparation method thereof, during preparation；Nai Ruoli neroli oils, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil are weighed as core materials；Cyst material is added to the water and dissolved by heating at 50~60 DEG C, obtains capsule wall solution；Core materials are added into capsule wall solution to be well mixed, and 3~6min of homogenization under 30~50MPa, obtain mixed liquor；Mixed liquor is spray-dried, essence microcapsule is made；Take lanolin, Jojoba wax, mink oil, saualane and lecithin to be well mixed, obtain substrate, essence microcapsule is added in basad thing, obtain the solid perfume.Solid perfume of the present invention have be convenient for carrying benefit wipe, fragrance release persistently, interior generation fragrance will not be disappeared or the characteristics of thin out situation during storage.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of herbal essences solid based on complex enzyme hydrolysis technology is fragrant
Water and preparation method thereof.
Background technology
Perfume is that the one kind for being combined together to form a variety of spices carries peat-reek, for making object (logical
Often is human body) possess lasting and happy people smell liquid.Traditional fragrance liquid is because being in liquid condition, it has not been convenient to carries with
Carry out mending the problem of wiping, and the defects of certain be present, thus on the basis of traditional liquid perfume, solid perfume is arisen at the historic moment.
Solid perfume is that essence is dissolved or adsorbed in curing agent, is divided into bar-shaped and granular solids perfume, solid perfume
Product form have essence, solvent and a curing agent, solid perfume have it is handy to carry about mend the characteristics of wiping, but solid
Perfume is there is also certain weak point, and the fragrance release of one side solid perfume is fast, and fragrance persistence is not so good as fragrance liquid
It is quiet and tastefully laid out and long, perfume ingredient in another aspect solid perfume is readily volatilized during storage to be dispersed, and causes to store for a long time
The problem of fragrance disappears or is thin out afterwards, thus there is also area for improvement.
The content of the invention
For deficiencies of the prior art, the present invention provides a kind of herbal essences based on complex enzyme hydrolysis technology and consolidated
Body note water and preparation method thereof, make to have using solid perfume made from this method to be convenient for carrying and mend wiping, fragrance release persistently, no
Understand interior the characteristics of fragrance disappearance or thin out situation occurs during storage.
To achieve these goals, the technical solution adopted by the present invention is as follows：A kind of draft based on complex enzyme hydrolysis technology
Elite solid perfume preparation method, comprises the following steps：
1) maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch are weighed as cyst material；Weigh how
If sharp neroli oil, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil are as core materials；
2) cyst material for weighing step 1) and water are according to 1g：20~30mL mass volume ratio mixing, 50~60
Dissolved by heating at DEG C, obtain capsule wall solution；
3) capsule wall solution that the core materials for weighing step 1) obtain with step 2) is according to 1g：5~10mL is well mixed,
3~6min of homogenization under 30~50MPa, obtains mixed liquor；
4) mixed liquor is spray-dried, essence microcapsule is made；
5) take lanolin, Jojoba wax, mink oil, saualane and lecithin to be well mixed, substrate is obtained, to the base
The essence microcapsule made from adding step 4) in substrate, obtains the solid perfume.
In order to which easily loss of aroma or thin out, the present invention use microcapsules skill during solving the storage of prior art solid perfume
Art, it is wrapped in perfume ingredient as capsule-core inside microcapsules, perfume ingredient is protected by cyst material, is effectively ensured
During storage interior essence do not allow it is volatile, cannot be easily caused loss of aroma, also ensure perfume ingredient not by external interference factor
Harmful effect, avoid the generation of essence deterioration problem.Fragrant unabiding problem is held in order to solve solid perfume in the prior art,
The present invention is using cassava porous-starch as wall material so that after microcapsules are destroyed by rubbing, the essence essential oil in capsule-core is immersed in
Inside porous-starch aperture, the effect of slowly discharging is played, existing solid perfume is solved and holds fragrant unabiding problem, make this hair
Bright solid perfume can effectively hold fragrant 20h, aroma-keeping time length after use is smeared, and be remained holding its fragrance in fragrant period
Unanimously, unlike existing traditional perfume products hold the front half section aromatic flavour in fragrant period, second half section fragrance is boring.
Further, in step 1) by maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch with 15~
25：10~14：10~12：8~12 mass ratio mixing is used as cyst material.Cyst wall material is used as using the mixing of such mass ratio
Material, it is ensured that the embedding rates of microcapsules is high, and it is complete to be effectively ensured microcapsules, ensure content during storage in do not reveal,
Microcapsule product quality is more stable.
Further, by Nai Ruoli neroli oils, fragrant iris caul-fat, Lavender, refined jasmine oil and peppermint essence in step 1)
Oil is according to 5~7：4~5：3~5：2~3：1~2 mass ratio mixing is used as core materials.From the perfume (or spice) of such mass ratio compounding
Essential oil, obtained fragrance fragrant is pleasant, and the fusion degree of fragrance is higher.
Further, cassava porous-starch described in step 1) is made with the following method：By tapioca and pH6.8
PBS is according to 1g：30~50mL mass volume ratio mixing, obtains farinaceous size；By complex enzyme and the farinaceous size
According to 1g：2000~3000mL mass volume ratio mixing, the enzyme deactivation after 1~3h of heating enzymolysis at 50~55 DEG C, to enzymolysis liquid
Centrifuged, take precipitation washing, dry, the cassava porous-starch is made；Wherein, the complex enzyme is by alpha-amylase and saccharification
Enzyme compounding composition.Obtained cassava porous-starch in such a way is adopted, specific surface area is big, and internal void is more, there can be essence
Effect is adsorbed onto inside porous-starch, more preferable to the slow releasing effect of essence, can make the aroma-keeping time of solid perfume of the present invention
It is longer.
As optimization, the mass ratio of alpha-amylase and carbohydrase is 1 in the complex enzyme：2~4.Using what is so compounded
Complex enzyme digests to tapioca, and tapioca can be effectively ensured and neither crushed by all enzymolysis, ensure enzymolysis system again
The starch internal void obtained is more, advantages of good adsorption effect.
As optimization, the condition of spray drying is 160~175 DEG C of EAT in step 4), 85~95 DEG C of leaving air temp,
Feed rate is 2.8~3.6mL/min.Using such spray drying condition, obtained microencapsulated forms can be made more preferable, no
It is easily broken leakage content.
As another optimization, taken in step 5) lanolin, Jojoba wax, mink oil, saualane and lecithin according to 20~
30：10~13：3~4：1~3：0.5~1 mass ratio is well mixed, and obtains substrate.Obtained substrate is so prepared to apply
It is good to smear ductility, facilitates consumer to be taken and smeared, is also convenient for assisting microcapsules broken by rubbing.
As an improvement the mass ratio of mode, the substrate and the essence microcapsule is 10：1~3.
Compared with prior art, the present invention has the advantages that：
1st, in order to which easily loss of aroma or thin out, the present invention use during solving the problems, such as the storage of prior art solid perfume
Microcapsules technology is wrapped in perfume ingredient as capsule-core inside microcapsules, and perfume ingredient is protected by cyst material,
During storage is effectively ensured interior essence do not allow it is volatile, cannot be easily caused loss of aroma, also ensure that perfume ingredient is not dry by the external world
The harmful effect of factor is disturbed, avoids the generation of essence deterioration problem.Experiment proves that solid perfume of the present invention places 1 year still
There is not the problem of fragrance is thin out.
2nd, fragrant unabiding problem is held in order to solve solid perfume in the prior art, the present invention is made using cassava porous-starch
For wall material so that after microcapsules are destroyed by rubbing, the essence essential oil in capsule-core is immersed in inside porous-starch aperture, is played slow
The effect of release, solve existing solid perfume and hold fragrant unabiding problem, make solid perfume of the present invention can after use is smeared
Effectively to hold fragrant 20h, aroma-keeping time length, and it is always consistent holding its fragrance in fragrant period, unlike existing traditional perfume
Product holds the front half section aromatic flavour in fragrant period, and second half section fragrance is boring.
3rd, solid perfume of the present invention is convenient for carrying use, facilitates consumer to carry out benefit wiping, takes a small amount of present invention solid during use
For body note water in needing gently to rub at smearing, microcapsules can be made within 5s by rubbing, and make core materials release and and cyst wall
Material is well mixed, easy to use.
Embodiment
The present invention is described in further detail with reference to specific embodiment.
Embodiment 1
A kind of herbal essences solid perfume preparation method based on complex enzyme hydrolysis technology, comprises the following steps：
1) by maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch with 15：10：10：8 mass ratio
Mixing is used as cyst material；By Nai Ruoli neroli oils, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil according to
5：4：3：2：1 mass ratio mixing is used as core materials；
Wherein, the cassava porous-starch is made with the following method：Tapioca and pH6.8 PBS are pressed
According to 1g：30mL mass volume ratio mixing, obtains farinaceous size；By complex enzyme and the farinaceous size according to 1g：2000mL's
Mass volume ratio is mixed, and enzyme deactivation after heating enzymolysis 1h, is centrifuged to enzymolysis liquid at 50 DEG C, is taken precipitation washing, is dried, is made
The cassava porous-starch；Wherein, the complex enzyme is made up of alpha-amylase and carbohydrase compounding, alpha-amylase and carbohydrase
Mass ratio is 1：2；
2) cyst material for weighing step 1) and water are according to 1g：20mL mass volume ratio mixing, is heated at 50 DEG C
Dissolving, obtains capsule wall solution；
3) capsule wall solution that the core materials for weighing step 1) obtain with step 2) is according to 1g：5mL is well mixed, in
Homogenization 3min under 30MPa, obtains mixed liquor；
4) mixed liquor is spray-dried, essence microcapsule is made；The condition of spray drying is 160 DEG C of EAT,
85 DEG C of leaving air temp, feed rate 2.8mL/min；
5) lanolin, Jojoba wax, mink oil, saualane and lecithin are taken according to 20：10：3：1：0.5 mass ratio mixes
Close uniformly, obtain substrate, the essence microcapsule made from addition step 4), it is fragrant to obtain the solid into the substrate
Water；The mass ratio of the substrate and the essence microcapsule is 10：1.
The present embodiment solid perfume takes when in use to be applied on skin on a small quantity, gently rubs 5s, you can so that microcapsules
Cyst wall rupture, capsule-core essence essential oil overflow simultaneously is blended with cyst material, capsule-core essence immerse cassava porous-starch inside, hair
Wave the slow release action of essence, experiment proves that fragrance still has after smearing the present embodiment solid perfume 10h, and fragrance with just
Difference is little during smearing, and what is had holds fragrant effect.Contrasted with solid perfume caused by company's one day of Shanghai, the present invention is solid
Fragrance is still consistent with what is just produced after body note water is deposited 1 year, and fragrance does not subtract light, and existing commercial solid perfume is put
Just make fragrance substantially thin out after 6 months, it is seen that the present embodiment solid perfume interior generation fragrance will not disappear or become during storage
The characteristics of light situation, property are stable.
Embodiment 2
A kind of herbal essences solid perfume preparation method based on complex enzyme hydrolysis technology, comprises the following steps：
1) by maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch with 20：12：11：10 mass ratio
Mixing is used as cyst material；By Nai Ruoli neroli oils, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil according to
6：4：4：2：1 mass ratio mixing is used as core materials；
Wherein, the cassava porous-starch is made with the following method：Tapioca and pH6.8 PBS are pressed
According to 1g：40mL mass volume ratio mixing, obtains farinaceous size；By complex enzyme and the farinaceous size according to 1g：2500mL's
Mass volume ratio is mixed, and enzyme deactivation after heating enzymolysis 2h, is centrifuged to enzymolysis liquid at 53 DEG C, is taken precipitation washing, is dried, is made
The cassava porous-starch；Wherein, the complex enzyme is made up of alpha-amylase and carbohydrase compounding, alpha-amylase and carbohydrase
Mass ratio is 1：3；
2) cyst material for weighing step 1) and water are according to 1g：25mL mass volume ratio mixing, is heated at 55 DEG C
Dissolving, obtains capsule wall solution；
3) capsule wall solution that the core materials for weighing step 1) obtain with step 2) is according to 1g：8mL is well mixed, in
Homogenization 5min under 40MPa, obtains mixed liquor；
4) mixed liquor is spray-dried, essence microcapsule is made；The condition of spray drying is 170 DEG C of EAT,
90 DEG C of leaving air temp, feed rate 3mL/min；
5) lanolin, Jojoba wax, mink oil, saualane and lecithin are taken according to 25：12：3：2：1 mass ratio mixing
Uniformly, substrate is obtained, the essence microcapsule made from addition step 4), it is fragrant to obtain the solid into the substrate
Water；The mass ratio of the substrate and the essence microcapsule is 10：2.
The present embodiment solid perfume takes when in use to be applied on skin on a small quantity, gently rubs 6s, you can so that microcapsules
Cyst wall rupture, capsule-core essence essential oil overflow simultaneously is blended with cyst material, capsule-core essence immerse cassava porous-starch inside, hair
Wave the slow release action of essence, experiment proves that fragrance still has after smearing the present embodiment solid perfume 9h, and fragrance with just
Difference is little during smearing, and what is had holds fragrant effect.Contrasted with solid perfume caused by the daily use chemicals company of Jiangsu, the present invention is solid
Fragrance is still consistent with what is just produced after body note water is deposited 13 months, and fragrance does not subtract light, and existing commercial solid perfume
Just make fragrance substantially thin out after putting 4 months, it is seen that the present embodiment solid perfume interior generation fragrance will not disappear during storage
Or the characteristics of thin out situation, property are stable.
Embodiment 3
A kind of herbal essences solid perfume preparation method based on complex enzyme hydrolysis technology, comprises the following steps：
1) by maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch with 25：14：12：10 mass ratio
Mixing is used as cyst material；By Nai Ruoli neroli oils, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil according to
7：5：5：3：2 mass ratio mixing is used as core materials；
Wherein, the cassava porous-starch is made with the following method：Tapioca and pH6.8 PBS are pressed
According to 1g：50mL mass volume ratio mixing, obtains farinaceous size；By complex enzyme and the farinaceous size according to 1g：3000mL's
Mass volume ratio is mixed, and enzyme deactivation after heating enzymolysis 3h, is centrifuged to enzymolysis liquid at 55 DEG C, is taken precipitation washing, is dried, is made
The cassava porous-starch；Wherein, the complex enzyme is made up of alpha-amylase and carbohydrase compounding, alpha-amylase and carbohydrase
Mass ratio is 1：4；
2) cyst material for weighing step 1) and water are according to 1g：30mL mass volume ratio mixing, is heated at 60 DEG C
Dissolving, obtains capsule wall solution；
3) capsule wall solution that the core materials for weighing step 1) obtain with step 2) is according to 1g：10mL is well mixed, in
Homogenization 6min under 50MPa, obtains mixed liquor；
4) mixed liquor is spray-dried, essence microcapsule is made；The condition of spray drying is 175 DEG C of EAT,
95 DEG C of leaving air temp, feed rate 3.6mL/min；
5) lanolin, Jojoba wax, mink oil, saualane and lecithin are taken according to 30：13：4：3：1 mass ratio mixing
Uniformly, substrate is obtained, the essence microcapsule made from addition step 4), it is fragrant to obtain the solid into the substrate
Water；The mass ratio of the substrate and the essence microcapsule is 10：3.
The present embodiment solid perfume takes when in use to be applied on skin on a small quantity, gently rubs 8s, you can so that microcapsules
Cyst wall rupture, capsule-core essence essential oil overflow simultaneously is blended with cyst material, capsule-core essence immerse cassava porous-starch inside, hair
Wave the slow release action of essence, experiment proves that fragrance still has after smearing the present embodiment solid perfume 12h, and fragrance with just
Difference is little during smearing, and what is had holds fragrant effect.Contrasted with solid perfume caused by company's one day of Shanghai, the present invention is solid
Fragrance is still consistent with what is just produced after body note water is deposited 16 months, and fragrance does not subtract light, and existing commercial solid perfume
Just make fragrance substantially thin out after putting 7 months, it is seen that the present embodiment solid perfume interior generation fragrance will not disappear during storage
Or the characteristics of thin out situation, property are stable.
The above embodiment of the present invention is only example to illustrate the invention, and is not the implementation to the present invention
The restriction of mode.For those of ordinary skill in the field, other can also be made not on the basis of the above description
With the change and variation of form.Here all embodiments can not be exhaustive.It is every to belong to technical scheme
Row of the obvious changes or variations amplified out still in protection scope of the present invention.
Claims (7)
1. a kind of herbal essences solid perfume preparation method based on complex enzyme hydrolysis technology, it is characterised in that comprise the following steps：
1) maltodextrin, Arabic gum, sodium carboxymethylcellulose pyce and cassava porous-starch are weighed as cyst material；Weigh Nai Ruoli
Neroli oil, fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil are as core materials, the cassava porous-starch
It is made with the following method：By tapioca and pH6.8 PBS according to 1g：30~50mL mass volume ratio mixing,
Obtain farinaceous size；By complex enzyme and the farinaceous size according to 1g：2000~3000mL mass volume ratio mixing, in 50~
Enzyme deactivation after 1~3h of heating enzymolysis, is centrifuged to enzymolysis liquid at 55 DEG C, is taken precipitation washing, is dried, the porous shallow lake of cassava is made
Powder；Wherein, the complex enzyme is made up of alpha-amylase and carbohydrase compounding；
2) cyst material for weighing step 1) and water are according to 1g：20~30mL mass volume ratio mixing, at 50~60 DEG C
Dissolve by heating, obtain capsule wall solution；
3) capsule wall solution that the core materials for weighing step 1) obtain with step 2) is according to 1g：5~10mL is well mixed, in 30
3~6min of homogenization, obtains mixed liquor under~50MPa；
4) mixed liquor is spray-dried, essence microcapsule is made；
5) take lanolin, Jojoba wax, mink oil, saualane and lecithin to be well mixed, substrate is obtained, to the substrate
The essence microcapsule made from middle addition step 4), obtains the solid perfume.
2. the preparation method of solid perfume according to claim 1, it is characterised in that in step 1) by maltodextrin, I
Primary glue, sodium carboxymethylcellulose pyce and cassava porous-starch are with 15~25：10~14：10~12：8~12 mass ratio mixing is used as capsule
Wall material.
3. the preparation method of solid perfume according to claim 1, it is characterised in that in step 1) by Nai Ruoli neroli oils,
Fragrant iris caul-fat, Lavender, refined jasmine oil and Peppermint essential oil are according to 5~7：4~5：3~5：2~3：1~2 mass ratio
Mixing is used as core materials.
4. the preparation method of solid perfume according to claim 4, it is characterised in that alpha-amylase and sugar in the complex enzyme
The mass ratio for changing enzyme is 1：2~4.
5. the preparation method of solid perfume according to claim 1, it is characterised in that the condition of spray drying is in step 4)
160~175 DEG C of EAT, 85~95 DEG C of leaving air temp, feed rate are 2.8~3.6mL/min.
6. the preparation method of solid perfume according to claim 1, it is characterised in that lanolin, Jojoba are taken in step 5)
Wax, mink oil, saualane and lecithin are according to 20~30：10~13：3~4：1~3：0.5~1 mass ratio is well mixed, and is obtained
To substrate.
7. the preparation method of solid perfume according to claim 1, it is characterised in that the substrate and the micro- glue of the essence
The mass ratio of capsule is 10：1~3.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112915048A (en) * | 2021-01-19 | 2021-06-08 | 江西丰兰香精香料有限公司 | Composite essence and preparation method and application thereof |
| CN113502190A (en) * | 2021-07-13 | 2021-10-15 | 广州芬豪香精有限公司 | Manufacturing method of slow-volatilization fragrance-retaining essence |
Citations (3)
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| CN113502190A (en) * | 2021-07-13 | 2021-10-15 | 广州芬豪香精有限公司 | Manufacturing method of slow-volatilization fragrance-retaining essence |
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