CN111568803A - Solid-state extreme-release mask and preparation method thereof - Google Patents
Solid-state extreme-release mask and preparation method thereof Download PDFInfo
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- CN111568803A CN111568803A CN202010609201.7A CN202010609201A CN111568803A CN 111568803 A CN111568803 A CN 111568803A CN 202010609201 A CN202010609201 A CN 202010609201A CN 111568803 A CN111568803 A CN 111568803A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/0279—Porous; Hollow
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Biophysics (AREA)
- Molecular Biology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a solid polar-release mask and a preparation method thereof, wherein the solid polar-release mask comprises the following raw material components in parts by weight: 0.1-5 parts of hydroxyethyl urea, 0.1-1.5 parts of sodium hyaluronate, 0.1-1.5 parts of glycerol, 0.1-1.5 parts of ceramide, 1-3 parts of first aid, 2-5 parts of second aid and 50-75 parts of water. The activity of the feed liquid is rapidly dormant and freeze-dried in liquid nitrogen at the temperature of-196 ℃, so that an active substance structure attached to a membrane cloth after freeze-drying is not in a common block shape or a powder shape, but forms a net-shaped loose porous structure like a snowflake crystal, and after the feed liquid meets water, the hydrophilic group and the water have a tension effect, so that the whole space is rapidly disintegrated within 1 second, the active substance is extremely rapidly released, the active substance rapidly permeates into the muscle bottom, the component effect is exerted by the inclination force, the permeation is deeper, and the water supplementing, moisturizing and repairing force is more rapidly activated.
Description
Technical Field
The invention relates to the technical field of cosmetic skin care, in particular to a solid extreme-release facial mask and a preparation method thereof.
Background
Beauty and skin care are pursued by each woman, the facial mask is a beauty mode which is most frequently used, the form of the facial mask mainly comprises a mud paste type, a tearing type, a jelly type, a wet tissue and the like, relatively speaking, the wet tissue is the most convenient facial mask, the facial mask is soaked by essence, the use is convenient, the functions are various, but for long-term storage, the wet tissue facial mask is based on an essence soaking production technology, preservatives and other raw materials can be added, and the safety is low;
the added chemical synthetic additives can cause certain irritation to the skin and can cause the skin to generate dependence on the chemical additives, so that a facial mask without preservatives is needed at present, the active ingredients of the facial mask can be guaranteed to the greatest extent, and long-term storage can be realized.
Disclosure of Invention
The invention aims to solve the defects in the prior art, and provides a solid extremely-releasing mask and a preparation method thereof, which can ensure the active ingredients of the mask to the maximum extent, do not need to add preservatives and have high safety.
In order to achieve the purpose, the invention adopts the following technical scheme:
a solid extreme-release mask comprises the following raw materials in parts by weight: 0.1-5 parts of hydroxyethyl urea, 0.1-1.5 parts of sodium hyaluronate, 0.1-1.5 parts of glycerol, 0.1-1.5 parts of ceramide, 0.1-1.5 parts of tremella polysaccharide, 1-3 parts of first aid, 2-5 parts of second aid and 50-75 parts of water.
Preferably, the ceramide is one or a combination of more of ceramide 1, ceramide 2, ceramide 3 and ceramide 4.
Preferably, the first auxiliary agent is one or a combination of more of butanediol, 1, 2-pentanediol, 1, 2-hexanediol, ethylhexyl glycerol or propylene glycol.
Preferably, the second auxiliary agent is one or a combination of more of hydroxyphenylpropionamide benzoic acid, allantoin, ascorbic acid polypeptide and betaine.
The invention also comprises a preparation method of the solid polar-release mask, which comprises the following steps:
(1) mixing hydroxyethyl urea, sodium hyaluronate, glycerol, ceramide, a first aid, a second aid and water, uniformly stirring, and soaking a membrane cloth;
(2) freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth;
(3) and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 10-45Pa, the drying time is 0.5-1h, and finally packaging the dry membrane with the water content of less than 5%.
Compared with the prior art, the invention has the beneficial effects that:
the activity of the feed liquid is rapidly dormant and freeze-dried in liquid nitrogen at the temperature of-196 ℃, so that an active substance structure attached to a membrane cloth after freeze-drying is not in a common block shape or a powder shape, but forms a net-shaped loose porous structure like a snowflake crystal, and after the feed liquid meets water, the hydrophilic group and the water have a tension effect, so that the whole space is rapidly disintegrated within 1 second, the active substance is extremely rapidly released, the active substance rapidly permeates into the muscle bottom, the component effect is exerted by the inclination force, the permeation is deeper, and the water supplementing, moisturizing and repairing force is more rapidly activated.
Detailed Description
The technical solutions of the present invention are described below clearly and completely by using specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A preparation method of a solid state extreme release mask comprises the following steps:
(1) mixing 0.1 part of hydroxyethyl urea, 0.1 part of sodium hyaluronate, 0.1 part of glycerol, 0.1 part of a composition of ceramide 1 and ceramide 2, 1 part of butanediol, 0.1 part of tremella polysaccharide, 2 parts of hydroxyphenylpropionamide benzoic acid and 50 parts of water, uniformly stirring, and soaking a membrane cloth;
(2) freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth;
(3) and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 10Pa, the drying time is 0.5h, and finally packaging the dry membrane with the water content of less than 5%.
Example 2
A preparation method of a solid state extreme release mask comprises the following steps:
(1) 1.5 parts of hydroxyethyl urea, 0.5 part of sodium hyaluronate, 0.6 part of glycerol, 0.5 part of a composition of ceramide 2 and ceramide 4, 2 parts of a composition of 1, 2-pentanediol and 1, 2-hexanediol, 3 parts of ascorbic acid polypeptide and 60 parts of water are mixed, and after the mixture is uniformly stirred, membrane cloth is soaked;
(2) freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth;
(3) and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 20Pa, the drying time is 0.6h, and finally packaging the dry membrane with the water content of less than 5%.
Example 3
A preparation method of a solid state extreme release mask comprises the following steps:
(1) mixing 3 parts of hydroxyethyl urea, 0.9 part of sodium hyaluronate, 0.8 part of glycerol, 0.8 part of a composition of ceramide 3 and ceramide 4, 3 parts of propylene glycol, 4 parts of a composition of allantoin and betaine and 65 parts of water, uniformly stirring, and soaking a membrane cloth;
(2) freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth;
(3) and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 35Pa, the drying time is 0.8h, and finally packaging the dry membrane with the water content of less than 5%.
Example 4
A preparation method of a solid state extreme release mask comprises the following steps:
(1) 5 parts of hydroxyethyl urea, 1.5 parts of sodium hyaluronate, 1.5 parts of glycerol, 1.5 parts of a composition of ceramide 2 and ceramide 4, 3 parts of a composition of ethylhexyl glycerol and propylene glycol, 5 parts of a composition of hydroxyphenylpropionamide benzoic acid, allantoin, ascorbic acid polypeptide and betaine and 75 parts of water are mixed, and after the mixture is uniformly stirred, membrane cloth is soaked;
(2) freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth;
(3) and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 45Pa, the drying time is 1h, and finally packaging the dry membrane with the water content of less than 5%.
The method comprises the steps of utilizing an ultralow temperature environment of liquid nitrogen-196 ℃, enabling liquid freeze-drying adsorbed by membrane cloth to be dormant on the membrane cloth within three seconds, forming a three-dimensional space by an active matter structure adsorbed on the membrane cloth after freeze-drying, enabling the active matter structure to be a net-shaped loose porous structure like snowflake crystals, utilizing a vacuum drying technology to volatilize moisture of the freeze-dried membrane cloth, and finally controlling the moisture content to be below 5% and obtaining a dry membrane containing high-concentration essence, namely a solid extreme-release facial mask;
when the solid-state extreme-release facial mask is used, the solid-state extreme-release facial mask is soaked in water, and after the solid-state extreme-release facial mask meets water, the hydrophilic group and the water act under tension, so that the whole facial mask is rapidly disintegrated within 1 second, an active substance is extremely rapidly released, the active substance rapidly permeates into the bottom of muscles, the efficacy of the ingredients is exerted by the aid of the inclined force, the permeation is deeper, and the moisturizing and repairing force is more rapidly stimulated.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical scope of the present invention and the equivalent alternatives or modifications according to the technical solution and the inventive concept of the present invention within the technical scope of the present invention.
Claims (5)
1. The solid extreme-release mask is characterized by comprising the following raw materials in parts by weight: 0.1-5 parts of hydroxyethyl urea, 0.1-1.5 parts of sodium hyaluronate, 0.1-1.5 parts of glycerol, 0.1-1.5 parts of ceramide, 0.1-1.5 parts of tremella polysaccharide, 1-3 parts of first aid, 2-5 parts of second aid and 50-75 parts of water.
2. The solid polar-release mask according to claim 1, wherein the ceramide is one or a combination of ceramide 1, ceramide 2, ceramide 3 or ceramide 4.
3. The solid immediate release mask as claimed in claim 1, wherein the first auxiliary agent is one or more of butylene glycol, 1, 2-pentanediol, 1, 2-hexanediol, ethylhexylglycerin or propylene glycol.
4. The solid extreme release mask as claimed in claim 1, wherein the second auxiliary agent is one or more of hydroxyphenylpropionamide benzoic acid, allantoin, ascorbic acid polypeptide and betaine.
5. The method for preparing a solid polar-release mask according to any one of claims 1 to 4, comprising the steps of:
mixing hydroxyethyl urea, sodium hyaluronate, glycerol, ceramide, a first aid, a second aid and water, uniformly stirring, and soaking a membrane cloth; freeze-drying the liquid mixture adsorbed by the membrane cloth in liquid nitrogen at-196 ℃ to make the liquid mixture dormant on the membrane cloth; and (3) carrying out vacuum drying treatment on the obtained freeze-dried membrane cloth, wherein the vacuum degree is 10-45Pa, the drying time is 0.5-1h, and finally packaging the dry membrane with the water content of less than 5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010609201.7A CN111568803A (en) | 2020-06-30 | 2020-06-30 | Solid-state extreme-release mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010609201.7A CN111568803A (en) | 2020-06-30 | 2020-06-30 | Solid-state extreme-release mask and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN111568803A true CN111568803A (en) | 2020-08-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010609201.7A Withdrawn CN111568803A (en) | 2020-06-30 | 2020-06-30 | Solid-state extreme-release mask and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114366683A (en) * | 2022-02-14 | 2022-04-19 | 广东巴松那生物科技有限公司 | Long-acting moisturizing composition and preparation method and application thereof |
-
2020
- 2020-06-30 CN CN202010609201.7A patent/CN111568803A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114366683A (en) * | 2022-02-14 | 2022-04-19 | 广东巴松那生物科技有限公司 | Long-acting moisturizing composition and preparation method and application thereof |
| CN114366683B (en) * | 2022-02-14 | 2023-07-14 | 广东巴松那生物科技有限公司 | Long-acting moisturizing composition, preparation method and application |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20200825 |
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| WW01 | Invention patent application withdrawn after publication |