CN111533604A - Liquid nitrogen fertilizer for improving crop planting and preparation method thereof - Google Patents

Liquid nitrogen fertilizer for improving crop planting and preparation method thereof Download PDF

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Publication number
CN111533604A
CN111533604A CN202010390420.0A CN202010390420A CN111533604A CN 111533604 A CN111533604 A CN 111533604A CN 202010390420 A CN202010390420 A CN 202010390420A CN 111533604 A CN111533604 A CN 111533604A
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parts
water
liquid nitrogen
nitrogen fertilizer
pepper leaves
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张博
王宏
段建锋
杨蓉蓉
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Gansu Fangyangwa Agricultural Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/20Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers
    • C05G5/27Dispersions, e.g. suspensions or emulsions
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Dispersion Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a liquid nitrogen fertilizer for improving crop planting and a preparation method thereof, and belongs to the technical field of agricultural fertilizer preparation. The liquid nitrogen fertilizer of the invention is composed of the following raw materials: decomposed pig manure, urea, monopotassium phosphate, a water-soluble isolating agent, aloe powder, silicone oil emulsion, pepper leaves, magnesium oxide, hydrotalcite, microbial powder, water-soluble calcium oxide, boric acid, ferrous sulfate and zinc sulfate. The liquid nitrogen fertilizer can obviously improve the yield of crops, obviously relieve the seedling burning phenomenon, improve the utilization rate of the fertilizer and supplement the deficiency of nutrient absorption of roots. The yield per mu of the corn is 622.63-627.72 kg/mu, the seedling burning rate is 1.2-1.4%, the yield per mu of the rape is 216.96-218.87 kg/mu, the seedling burning rate is 1.3-1.5%, the yield per mu of the wheat is 514.69-519.42 kg/mu, the seedling burning rate is 1.2-1.5%, the incidence rate of plant diseases and insect pests of each crop is obviously reduced, and the economic benefit is obvious.

Description

Liquid nitrogen fertilizer for improving crop planting and preparation method thereof
Technical Field
The invention belongs to the technical field of agricultural fertilizer preparation, and particularly relates to a liquid nitrogen fertilizer for improving crop planting and a preparation method thereof.
Background
Liquid fertilizers, also known as fluid fertilizers, include clear liquid, suspended, and slurry types. The liquid fertilizer has the following advantages: dust and smoke can not appear in the production, application and transportation, and the pollution is less; the product has no problems of moisture absorption and caking; can be mixed with pesticide, bactericide and herbicide and can be mixed uniformly; the quality is not different like the segregation of solid fertilizers in storage and transportation; the application method is various, can be sprayed on the leaf surface, can be applied along with water, can also be used for sprinkling irrigation, drip irrigation or irrigation, and has the advantages of convenient use, cost saving and quick effect. Therefore, liquid fertilizers are one of the trends in the development of the fertilizer industry in the world today. In the 90 s of the 20 th century, the liquid fertilizer consumed in the United states each year accounts for more than 38% of the total fertilizer consumption. In recent years, liquid fertilizers have been rapidly developed due to the application of foliar fertilizers and irrigation techniques, particularly drip irrigation techniques.
The liquid slow-release nitrogen fertilizer adopts an advanced polymethylene urea slow-release technology and combines American active small molecular carbon, the traditional striking root fertilizer can be replaced by spraying the liquid slow-release nitrogen fertilizer on a seedbed before rice transplanting, the striking root speed is extremely high, the seedling reviving process is almost not generated, and the spraying method is labor-saving; the fertilizer can be used on corn to replace topdressing, and can be used as spike fertilizer in the later period, and the yield increasing effect is particularly obvious when the fertilizer is used before soybean pod setting. The liquid slow-release nitrogen fertilizer is very safe for spraying rice seedlings, and because the salt index of the liquid slow-release nitrogen fertilizer product is extremely low and is within 0.5, and the urea height is up to 70, the seedling burning phenomenon can be caused by spraying after the common urea is converted into water. Therefore, the adoption of the liquid nitrogen fertilizer can greatly promote the increase of the crop yield and reduce the occurrence probability of plant diseases and insect pests.
Disclosure of Invention
The invention aims to provide a liquid nitrogen fertilizer for improving crop planting, which reduces seedling burning, reduces the occurrence probability of plant diseases and insect pests and improves crop yield, and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a liquid nitrogen fertilizer for improving crop planting comprises the following raw materials in parts by weight: 80-90 parts of decomposed pig manure, 60-72 parts of urea, 15-25 parts of monopotassium phosphate, 5-10 parts of water-soluble isolating agent, 4-12 parts of aloe powder, 6-8 parts of silicone oil emulsion, 30-40 parts of pepper leaves, 7-10 parts of magnesium oxide, 6-10 parts of hydrotalcite, 3-7 parts of microbial powder, 1-4 parts of water-soluble calcium oxide, 0.8-1.6 parts of boric acid, 0.7-0.9 part of ferrous sulfate and 0.05-0.09 part of zinc sulfate.
Further, the liquid nitrogen fertilizer for improving crop planting is composed of the following raw materials in parts by weight: 85 parts of decomposed pig manure, 66 parts of urea, 20 parts of monopotassium phosphate, 8 parts of water-soluble separant, 8 parts of aloe powder, 7 parts of silicone oil emulsion, 35 parts of pepper leaves, 9 parts of magnesium oxide, 8 parts of hydrotalcite, 5 parts of microbial powder, 3 parts of water-soluble calcium oxide, 1.2 parts of boric acid, 0.8 part of ferrous sulfate and 0.07 part of zinc sulfate.
The preparation method of the liquid nitrogen fertilizer for improving crop planting comprises the following steps:
1) adding deionized water into a reaction kettle, introducing water vapor into the reaction kettle, controlling the temperature to be 45-48 ℃, adding urea, monopotassium phosphate and aloe powder into the reaction kettle, uniformly stirring to obtain a stirred material, and drying until the water content is 10-15% for later use;
2) spraying cattle and sheep urine on the pepper leaves until the leaves are thoroughly wetted, then drying the pepper leaves adsorbed with the cattle and sheep urine in the sun, diluting a silicone oil emulsion to 300-500 times of liquid, spraying the liquid on the pepper leaves in a spraying manner, fully and uniformly stirring the pepper leaves and decomposed pig manure, stacking for fermentation for 15-20 days, turning over once every 5-6 days, adding microbial powder into the mixture for secondary stacking fermentation, reducing the temperature to 25-28 ℃, and fermenting for 7-10 days to obtain a fermented product for later use;
3) and (2) performing filter pressing and drying on the stirred material and the fermented material, granulating by using a granulator, adding a water-soluble isolating agent, shaking uniformly for 30-50 min, standing for 10-20 min, then mixing and stirring with other raw materials, adding 50-60 parts of water, uniformly mixing, keeping the temperature at 30-40 ℃, stirring for reacting for 50min, and cooling to obtain the liquid nitrogen fertilizer.
Further, the temperature in the step 2) before adding the microbial powder is 40-50 ℃.
Compared with the prior art, the invention has the beneficial effects that:
1) the liquid nitrogen fertilizer can obviously improve the yield of crops, obviously relieve the seedling burning phenomenon, improve the utilization rate of the fertilizer and supplement the deficiency of nutrient absorption of roots.
2) The liquid separant, the silicone oil emulsion and the pepper leaves are matched, so that the bacteria colony and the insecticide are isolated to carry out intermolecular isolation, and the phenomenon that the insecticide kills the bacteria colony in the transportation and storage processes is avoided.
3) The yield per mu of the corn is 622.63-627.72 kg/mu, the seedling burning rate is 1.2-1.4%, the yield per mu of the rape is 216.96-218.87 kg/mu, the seedling burning rate is 1.3-1.5%, the yield per mu of the wheat is 514.69-519.42 kg/mu, the seedling burning rate is 1.2-1.5%, the incidence rate of plant diseases and insect pests of each crop is obviously reduced, and the economic benefit is obvious.
Detailed Description
The following examples further describe in detail specific embodiments of the present invention. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
Example 1
A liquid nitrogen fertilizer for improving crop planting comprises the following raw materials in parts by weight: 80 parts of decomposed pig manure, 60 parts of urea, 15 parts of monopotassium phosphate, 5 parts of water-soluble separant, 4 parts of aloe powder, 6 parts of silicone oil emulsion, 30 parts of pepper leaves, 7 parts of magnesium oxide, 6 parts of hydrotalcite, 3 parts of microbial powder, 1 part of water-soluble calcium oxide, 0.8 part of boric acid, 0.7 part of ferrous sulfate and 0.05 part of zinc sulfate.
The preparation method of the liquid nitrogen fertilizer for improving crop planting comprises the following steps:
1) adding deionized water into a reaction kettle, introducing water vapor, controlling the temperature at 45 ℃, adding urea, potassium dihydrogen phosphate and aloe powder into the reaction kettle, uniformly stirring to obtain a stirred substance, and drying until the water content is 10% for later use;
2) spraying cattle and sheep urine on the pepper leaves until the leaves are thoroughly wetted, then drying the pepper leaves adsorbed with the cattle and sheep urine in the sun, diluting a silicone oil emulsion to 300 times of liquid, spraying the silicone oil emulsion on the pepper leaves in a spraying manner, fully and uniformly stirring the pepper leaves and decomposed pig manure, stacking the pepper leaves for 15 days of fermentation, turning over the pepper leaves once every 5 days at the fermentation temperature of 40 ℃, adding microbial powder into the pepper leaves for secondary stacking fermentation, reducing the temperature to 25 ℃, and fermenting for 7 days to obtain a fermented product for later use after the fermentation is finished;
3) and (3) carrying out filter pressing and drying on the stirred material and the fermented material, granulating by using a granulator, adding a water-soluble isolating agent, shaking uniformly for 30min, standing for 10min, then mixing and stirring with other raw materials, adding 50 parts of water, uniformly mixing, keeping the temperature at 30 ℃, stirring for reacting for 50min, and cooling to obtain the liquid nitrogen fertilizer.
Example 2
A liquid nitrogen fertilizer for improving crop planting comprises the following raw materials in parts by weight: 85 parts of decomposed pig manure, 66 parts of urea, 20 parts of monopotassium phosphate, 8 parts of water-soluble separant, 8 parts of aloe powder, 7 parts of silicone oil emulsion, 35 parts of pepper leaves, 9 parts of magnesium oxide, 8 parts of hydrotalcite, 5 parts of microbial powder, 3 parts of water-soluble calcium oxide, 1.2 parts of boric acid, 0.8 part of ferrous sulfate and 0.07 part of zinc sulfate.
The preparation method of the liquid nitrogen fertilizer for improving crop planting comprises the following steps:
1) adding deionized water into a reaction kettle, introducing water vapor into the reaction kettle, controlling the temperature at 46 ℃, adding urea, potassium dihydrogen phosphate and aloe powder into the reaction kettle, uniformly stirring to obtain a stirred material, and drying until the moisture content is 12% for later use;
2) spraying cattle and sheep urine on the pepper leaves until the leaves are thoroughly wetted, then drying the pepper leaves adsorbed with the cattle and sheep urine in the sun, diluting a silicone oil emulsion to 400 times of the emulsion, spraying the silicone oil emulsion on the pepper leaves in a spraying manner, fully and uniformly stirring the pepper leaves and decomposed pig manure, stacking the pepper leaves for 18 days of fermentation, wherein the fermentation temperature is 45 ℃, turning over the pepper leaves once every 5 days, adding microbial powder into the pepper leaves for secondary stacking fermentation, reducing the temperature to 27 ℃, and fermenting for 8 days to obtain a fermented product for later use after the fermentation is finished;
3) and (3) carrying out filter pressing and drying on the stirred material and the fermented material, granulating by using a granulator, adding a water-soluble isolating agent, shaking uniformly for 40min, standing for 15min, then mixing and stirring with other raw materials, adding 55 parts of water, uniformly mixing, keeping the temperature at 35 ℃, stirring for reacting for 50min, and cooling to obtain the liquid nitrogen fertilizer.
Example 3
A liquid nitrogen fertilizer for improving crop planting comprises the following raw materials in parts by weight: 90 parts of decomposed pig manure, 72 parts of urea, 25 parts of monopotassium phosphate, 10 parts of water-soluble separant, 12 parts of aloe powder, 8 parts of silicone oil emulsion, 40 parts of pepper leaves, 10 parts of magnesium oxide, 10 parts of hydrotalcite, 7 parts of microbial powder, 4 parts of water-soluble calcium oxide, 1.6 parts of boric acid, 0.9 part of ferrous sulfate and 0.09 part of zinc sulfate.
The preparation method of the liquid nitrogen fertilizer for improving crop planting comprises the following steps:
1) adding deionized water into a reaction kettle, introducing water vapor into the reaction kettle, controlling the temperature at 48 ℃, adding urea, monopotassium phosphate and aloe powder into the reaction kettle, uniformly stirring to obtain a stirred material, and drying until the moisture content is 10% -15% for later use;
2) spraying cattle and sheep urine on the pepper leaves until the leaves are thoroughly wetted, then drying the pepper leaves adsorbed with the cattle and sheep urine in the sun, diluting a silicone oil emulsion to 500 times of liquid, spraying the liquid on the pepper leaves in a spraying manner, fully and uniformly stirring the pepper leaves and decomposed pig manure, stacking the pepper leaves for 20 days of fermentation, turning over the pepper leaves once every 6 days at the fermentation temperature of 50 ℃, adding microbial powder into the pepper leaves for secondary stacking fermentation, reducing the temperature to 28 ℃, and fermenting for 10 days to obtain a fermented product for later use;
3) and (3) carrying out filter pressing and drying on the stirred material and the fermented material, granulating by using a granulator, adding a water-soluble isolating agent, shaking uniformly for 50min, standing for 20min, then mixing and stirring with other raw materials, adding 60 parts of water, uniformly mixing, keeping the temperature at 40 ℃, stirring for reacting for 50min, and cooling to obtain the liquid nitrogen fertilizer.
Examples of the experiments
Rape, corn and wheat are respectively selected as experimental objects in the calm and cool areas of Gansu to apply liquid nitrogen fertilizer, and the growth conditions of crops are observed after a period of time, which is specifically shown in Table 1:
Figure DEST_PATH_IMAGE001
as can be seen from Table 1, the yield per mu of corn is 622.63-627.72 kg/mu, the seedling burning rate is 1.2-1.4%, the yield per mu of rape is 216.96-218.87 kg/mu, the seedling burning rate is 1.3-1.5%, the yield per mu of wheat is 514.69-519.42 kg/mu, the seedling burning rate is 1.2-1.5%, the incidence of plant diseases and insect pests of each crop is obviously reduced, and the economic benefit is obvious.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.

Claims (4)

1. A liquid nitrogen fertilizer for improving crop planting is characterized by comprising the following raw materials in parts by weight: 80-90 parts of decomposed pig manure, 60-72 parts of urea, 15-25 parts of monopotassium phosphate, 5-10 parts of water-soluble isolating agent, 4-12 parts of aloe powder, 6-8 parts of silicone oil emulsion, 30-40 parts of pepper leaves, 7-10 parts of magnesium oxide, 6-10 parts of hydrotalcite, 3-7 parts of microbial powder, 1-4 parts of water-soluble calcium oxide, 0.8-1.6 parts of boric acid, 0.7-0.9 part of ferrous sulfate and 0.05-0.09 part of zinc sulfate.
2. The liquid nitrogen fertilizer for improving crop planting according to claim 1, characterized by comprising the following raw materials in parts by weight: 85 parts of decomposed pig manure, 66 parts of urea, 20 parts of monopotassium phosphate, 8 parts of water-soluble separant, 8 parts of aloe powder, 7 parts of silicone oil emulsion, 35 parts of pepper leaves, 9 parts of magnesium oxide, 8 parts of hydrotalcite, 5 parts of microbial powder, 3 parts of water-soluble calcium oxide, 1.2 parts of boric acid, 0.8 part of ferrous sulfate and 0.07 part of zinc sulfate.
3. A method of preparing a liquid nitrogen fertilizer for improving crop planting according to claim 1, characterized by comprising the steps of:
1) adding deionized water into a reaction kettle, introducing water vapor into the reaction kettle, controlling the temperature to be 45-48 ℃, adding urea, monopotassium phosphate and aloe powder into the reaction kettle, uniformly stirring to obtain a stirred material, and drying until the water content is 10-15% for later use;
2) spraying cattle and sheep urine on the pepper leaves until the leaves are thoroughly wetted, then drying the pepper leaves adsorbed with the cattle and sheep urine in the sun, diluting a silicone oil emulsion to 300-500 times of liquid, spraying the liquid on the pepper leaves in a spraying manner, fully and uniformly stirring the pepper leaves and decomposed pig manure, stacking for fermentation for 15-20 days, turning over once every 5-6 days, adding microbial powder into the mixture for secondary stacking fermentation, reducing the temperature to 25-28 ℃, and fermenting for 7-10 days to obtain a fermented product for later use;
3) and (2) performing filter pressing and drying on the stirred material and the fermented material, granulating by using a granulator, adding a water-soluble isolating agent, shaking uniformly for 30-50 min, standing for 10-20 min, then mixing and stirring with other raw materials, adding 50-60 parts of water, uniformly mixing, keeping the temperature at 30-40 ℃, stirring for reacting for 50min, and cooling to obtain the liquid nitrogen fertilizer.
4. The liquid nitrogen fertilizer for improving crop planting according to claim 3, wherein the temperature of the step 2) before adding the microbial powder is 40-50 ℃.
CN202010390420.0A 2020-05-11 2020-05-11 Liquid nitrogen fertilizer for improving crop planting and preparation method thereof Pending CN111533604A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114369345A (en) * 2022-02-07 2022-04-19 万华化学(四川)有限公司 High-barrier full-biodegradable mulching film with fertilizer effect and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA200601419A1 (en) * 2006-07-06 2008-02-28 Научно-Исследовательское Республиканское Унитарное Предприятие "Институт Почвоведения И Агрохимии Нан Беларуси" LIQUID NITROGEN FERTILIZER WITH BIOLOGICALLY ACTIVE ADDITIVE AND MICRO ELEMENTS
CN103833472A (en) * 2014-03-21 2014-06-04 润禾泰华生物科技(北京)有限公司 Special liquid pesticide fertilizer for increasing yield and killing pests of corn and preparation method thereof
CN104030804A (en) * 2014-05-29 2014-09-10 陈凯 Multiple-effect biological pesticide fertilizer and preparation method thereof
CN105622283A (en) * 2014-11-08 2016-06-01 青岛蓝农谷农产品研究开发有限公司 Trace element liquid fertilizer for soybean planting, and production method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EA200601419A1 (en) * 2006-07-06 2008-02-28 Научно-Исследовательское Республиканское Унитарное Предприятие "Институт Почвоведения И Агрохимии Нан Беларуси" LIQUID NITROGEN FERTILIZER WITH BIOLOGICALLY ACTIVE ADDITIVE AND MICRO ELEMENTS
CN103833472A (en) * 2014-03-21 2014-06-04 润禾泰华生物科技(北京)有限公司 Special liquid pesticide fertilizer for increasing yield and killing pests of corn and preparation method thereof
CN104030804A (en) * 2014-05-29 2014-09-10 陈凯 Multiple-effect biological pesticide fertilizer and preparation method thereof
CN105622283A (en) * 2014-11-08 2016-06-01 青岛蓝农谷农产品研究开发有限公司 Trace element liquid fertilizer for soybean planting, and production method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114369345A (en) * 2022-02-07 2022-04-19 万华化学(四川)有限公司 High-barrier full-biodegradable mulching film with fertilizer effect and preparation method thereof
CN114369345B (en) * 2022-02-07 2023-09-19 万华化学(四川)有限公司 High-barrier full-biodegradable mulching film with fertilizer effect and preparation method thereof

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