CN111529443A - Traditional Chinese medicine shampoo and preparation method thereof - Google Patents
Traditional Chinese medicine shampoo and preparation method thereof Download PDFInfo
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- CN111529443A CN111529443A CN202010410713.0A CN202010410713A CN111529443A CN 111529443 A CN111529443 A CN 111529443A CN 202010410713 A CN202010410713 A CN 202010410713A CN 111529443 A CN111529443 A CN 111529443A
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- shampoo
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- traditional chinese
- chinese medicine
- soapberry
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- 239000002453 shampoo Substances 0.000 title claims abstract description 90
- 239000003814 drug Substances 0.000 title claims abstract description 64
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
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- 235000018324 Shepherdia canadensis Nutrition 0.000 claims abstract description 27
- 239000004094 surface-active agent Substances 0.000 claims abstract description 26
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- 239000003906 humectant Substances 0.000 claims abstract description 19
- 240000005001 Paeonia suffruticosa Species 0.000 claims abstract description 18
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims abstract description 18
- 241000244355 Ligusticum Species 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 6
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 5
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- MYSWGUAQZAJSOK-UHFFFAOYSA-N ciprofloxacin Chemical compound C12=CC(N3CCNCC3)=C(F)C=C2C(=O)C(C(=O)O)=CN1C1CC1 MYSWGUAQZAJSOK-UHFFFAOYSA-N 0.000 description 2
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- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 description 1
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- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-N methyl undecanoic acid Natural products CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/14—Drugs for dermatological disorders for baldness or alopecia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a traditional Chinese medicine shampoo and a preparation method thereof, wherein the traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 1-4 parts of saponin, 1-4 parts of soapberry, 1-2 parts of tree peony bark, 1-2 parts of cacumen biotae, 1-2 parts of ligusticum and 1-2 parts of radix angelicae; the traditional Chinese medicine shampoo further comprises a thickening agent, a surfactant and a humectant, wherein the thickening agent, the surfactant and the humectant respectively account for 4-6%, 10-20% and 0.1-0.5% of the total weight of the shampoo. The invention also provides a preparation method of the traditional Chinese medicine shampoo. The shampoo provided by the invention mainly comprises Chinese herbal medicine components, only a few necessary chemical components are added, the stimulation to scalp is greatly reduced, the effect of the Chinese herbal medicine components is fully exerted by adopting a water extraction method, and the problems of stimulating effect to scalp, poor using effect, environmental pollution and the like are effectively solved.
Description
Technical Field
The invention relates to shampoo and the technical field of preparation thereof, in particular to traditional Chinese medicine shampoo and a preparation method thereof.
Background
The shampoo is also called shampoo, is a hair care product with the functions of removing dandruff, treating oil, dyeing hair and the like, is the most common hair cosmetic, and belongs to one of the earliest and fastest-developed products in the personal care market. The shampoo generally contains a plurality of chemical components, and the mixed salt of triethanolamine of fatty alcohol sulfate and amine hydroxide, lauric acid isopropyl alcohol amide, formaldehyde, polyoxyethylene, lanolin, perfume, pigment and water are mostly adopted as raw materials. The purpose of shampoo used by most people is to clean hair and scalp, and the solution to the beauty of hair and the health of scalp is an increasing choice for many people at present. The traditional Chinese medicine is trusted and loved by people due to natural safety, and the traditional Chinese medicine is also used in health care and daily life in the aspect of medicine. Many washing and caring products are added with Chinese herbal medicine components, but mainly contain chemical components, the Chinese herbal medicine components are added very little, effective dosage cannot be reached, the shampoo has a stimulating effect on scalp, certain damage is generated, the problem that part of people are allergic or uncomfortable to the shampoo is not solved essentially, the effects on the problems that part of hair is greasy, easy to lose hair, scalp is allergic and the like are not good enough, the shampoo is poor in using effect, and the aims of resisting inflammation, removing oil and nourishing hair roots cannot be reached. For the preparation of shampoo, the traditional Chinese medicine water extraction method is almost rarely used in the market, most of the cold preparation methods are adopted, the effective components of the shampoo raw materials cannot be effectively obtained, the effective functions of the pure traditional Chinese medicines are difficult to be fully exerted, and a large amount of pollution is caused to the environment due to the need of pollution discharge.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides the traditional Chinese medicine shampoo and the preparation method thereof, the shampoo mainly comprises Chinese herbal medicine components, only a few necessary chemical components are added, the stimulation to the scalp is greatly reduced, the shampoo is prepared by adopting a water extraction method, the effects of the Chinese herbal medicine components are fully exerted, and the problems of stimulating the scalp, poor using effect, environmental pollution and the like are effectively solved.
In order to achieve the purpose, the technical scheme adopted by the invention for solving the technical problems is as follows: the traditional Chinese medicine shampoo is provided and comprises the following raw materials in parts by weight: 1-4 parts of saponin, 1-4 parts of soapberry, 1-2 parts of tree peony bark, 1-2 parts of cacumen biotae, 1-2 parts of ligusticum and 1-2 parts of radix angelicae.
Further, the traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae, 1 part of ligusticum and 1 part of angelica dahurica.
Further, the traditional Chinese medicine shampoo also comprises a thickening agent, a surfactant and a humectant, wherein the thickening agent, the surfactant and the humectant respectively account for 4-6%, 10-20% and 0.1-0.5% of the total weight of the shampoo.
Further, the thickening agent, the surfactant and the humectant respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
Further, the thickener is methyl glucoside polyoxyethylene (120) ether dioleate, the surfactant is N-lauroyl sodium sarcosinate, and the humectant is ethylhexyl glycerol.
Wherein, the Chinese honeylocust is a natural raw material of medical food, health products, cosmetics and washing products; has repercussive, toxic materials clearing away, pus discharge promoting, and parasite killing effects; meanwhile, the surfactant is used as an excellent natural surfactant and is applied to a certain degree in the washing and caring market.
The triterpene saponin rich in the peel of soapberry has excellent surface activity and physiological effect, and the substance has excellent surface activity and pharmacological effects of sterilization, inflammation diminishing, oxidation resistance, tumor resistance and the like. It can be used together with fructus Gleditsiae Abnormalis to enhance surface activity, and is used as basic material for shampoo.
The book Shen nong Ben Cao Jing records that peony, pyrola and mouse are listed. Flavor: pungent and cold. Mainly has the functions of treating cold and heat, apoplexy, convulsion, spasm, convulsion, pathogenic qi, removing symptom and hardness, retaining blood stasis in intestines and stomach, calming five internal organs and treating carbuncle and wound. Modern researches find that the derivative has better antibacterial activity on staphylococcus aureus and escherichia coli, the derivative with the best activity has better inhibitory action on staphylococcus aureus than ciprofloxacin, and the tree peony bark has the effects of easing pain, resisting inflammation, relieving fever and inhibiting allergic reaction, and not only can inhibit the growth of hair bacteria, but also can relieve itching.
The record of Ben Cao gang mu states that the Chinese arborvitae twig is not growing hair, dried in the shade and made into powder, and coated with sesame oil, and suggests that the Chinese arborvitae twig can be used for growing hair externally; in addition, it is proposed from Lei Gong processing herb Property analysis that Ce Bai Ye can blacken beard and hair. Meanwhile, modern researches find that the cacumen biotae not only has the hair growth effect, but also has antibacterial activity and can inhibit the growth of scalp bacteria. Ligusticum sinense, radix Angelicae sinensis, rhizoma Ligustici, is used as guiding drug to direct the herbs upward.
Compendium of materia Medica: radix angelicae is white and pungent in flavor, and can play a role in improving hand yangming; warmth in nature and thick qi, sufficient yang-yin to clear up; fragrant, ascending and entering the lung meridian of Taiyin. Modern researches show that the radix angelicae has a strong antibacterial effect and has an inhibiting effect on bacteria such as escherichia coli, dysentery bacillus, typhoid bacillus, pseudomonas aeruginosa, gram-positive bacteria and human tubercle bacillus, the radix angelicae methanol extract 1g/kg is injected in the abdominal cavity 5 minutes before X-ray irradiation, the skin damage of mice is protected, and the radix angelicae has an anti-radiation effect on scalp and hair, so that the radix angelicae is added to increase the protection on hair.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) weighing Chinese honeylocust fruit, soapberry, tree peony bark, cacumen biotae, ligusticum and radix angelicae, soaking the Chinese honeylocust fruit and the soapberry in clear water for 20-30 h, heating the Chinese honeylocust fruit and the soapberry in 8-10 times of water to 90-100 ℃, preserving heat for 120-150 min, finally adding the tree peony bark, the cacumen biotae, the ligusticum and the radix angelicae into the water, heating for 30-50 min at 90-100 ℃, and filtering to obtain medicine juice;
(2) and (2) cooling the medicinal juice obtained in the step (1) in air to 70-80 ℃, adding a thickening agent into the medicinal juice, then stirring in vacuum for 1-3 min, then adding a surfactant, stirring in vacuum for 1-3 min, cooling in air to below 40 ℃, adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Further, in the step (1), soaking the Chinese honeylocust fruits and the soapberry fruits for 24 hours in clear water, heating the Chinese honeylocust fruits and the soapberry fruits to 100 ℃ in 9 times of water, preserving the heat for 140 minutes, finally adding the tree peony bark, the Chinese arborvitae twig, the Chinese ligusticum rhizome and the dahurian angelica root into the water, and heating again for 40 minutes at the temperature of 100 ℃.
Further, in the step (2), cooling the medicine juice to 75 ℃ in air, adding the thickening agent into the medicine juice, then stirring for 1min in vacuum, then adding the surfactant, then stirring for 1min in vacuum, and cooling to below 40 ℃ in air.
In summary, the invention has the following advantages:
1. the shampoo disclosed by the invention takes Chinese herbal medicine components such as Chinese honeylocust fruits and soapberry fruits as main components, only a few necessary chemical components are added, the stimulation effect of the chemical components on scalp is greatly reduced, no harm is caused to scalp, the possibility of allergy or discomfort of a user to the shampoo is also reduced, the problems of greasy hair, easiness in hair loss and scalp allergy can be solved, the using effect is good, and the shampoo has the effects of resisting inflammation, removing oil and nourishing hair roots; the shampoo is prepared by adopting a water extraction method instead of a cold preparation method, so that the effective components of the Chinese herbal medicines can be effectively obtained, the effects of the Chinese herbal medicines are fully exerted, a large amount of sewage is not generated in the preparation process, the shampoo is environment-friendly, and the problems of irritation to scalp, poor use effect, environmental pollution and the like are effectively solved.
2. The shampoo raw material contains saponin which has the functions of detumescence, pus discharge, insect disinfestation and the like and does not damage scalp, and is a natural surfactant; the soapberry is rich in triterpenoid saponin, has the effects of sterilizing, diminishing inflammation, resisting oxidation and resisting tumors, can be synergistically acted with the saponin, enhances the surface activity of the shampoo and enhances the effect of the shampoo; the cortex moutan has strong antibacterial effect on staphylococcus albus, bacillus subtilis, escherichia coli, typhoid bacillus and the like, and has an antibacterial effect in shampoo; the main components of the cacumen biotae are volatile oil, flavonoid compounds and tannin, the cacumen biotae has the effects of growing and blackening hair, inhibiting bacteria, resisting tumor, inflammation, red blood cell oxidation and hemostasis, preventing alopecia, and can effectively inhibit the growth of scalp bacteria by cooperating with cortex moutan; the rhizoma Ligustici has antiinflammatory, antibacterial and antioxidant effects, and can promote the effects of other components; the angelica dahurica has different degrees of inhibition effects on escherichia coli, dysenteriae sonnei and freund dysentery bacillus, proteus bacillus, typhoid bacillus, paratyphoid bacillus, pseudomonas aeruginosa, vibrio cholerae, certain gram-positive bacteria, human tubercle bacillus and the like in vitro, and can also play a role in protecting hair and preventing alopecia.
3. The methyl glucoside polyoxyethylene (120) ether dioleate is used as a thickening agent, has a good rheological effect, can reduce the irritation of the shampoo, and can solve the problem of thickening of mild washing products of amino acid surfactants; n-lauroyl sodium sarcosinate is an amino acid type surfactant, has the functions of antibiosis, sterilization, mildew prevention and corrosion resistance, has a good washing and decontamination effect by the synergistic effect with a thickening agent, and solves the problem of product thickening; the ethylhexyl glycerin has the moisturizing effect, antibacterial property and strong stability, is often used as a moisturizing agent, can improve the moisturizing effect of the product, has a smooth skin feeling, can enhance and reduce the use of the traditional preservative, and increases the safety of the product.
4. The shampoo is prepared by a water extraction method, the preparation process is simple and easy to control, the Chinese honeylocust and the soapberry are soaked and then heated and extracted with water in an amount which is 8-10 times that of the Chinese honeylocust and the soapberry, active ingredients in the Chinese honeylocust and the soapberry can be effectively extracted, the effect of the shampoo is enhanced, then the tree peony bark, the Chinese arborvitae twig, the Chinese ligusticum rhizome and the dahurian angelica root are added, and the heating and water extraction is carried out again, antibacterial ingredients in raw materials are extracted, and the components can also reduce the stimulation; methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sarcosine sodium and ethylhexyl glycerol are respectively added into the medicinal juice, and vacuum stirring is respectively carried out after each addition, so that the thickening agent, the surfactant, the humectant and the medicinal juice are fully mixed, the corresponding functions are exerted, and the effects of the traditional Chinese medicine components are promoted to be exerted; and finally, standing and removing surface foam to obtain the traditional Chinese medicine shampoo, wherein no redundant foam is generated on the surface of the shampoo, and the appearance quality is good. The active ingredients and the bacteriostatic ingredients in the shampoo raw materials can be effectively extracted in the preparation process, a large amount of useless cold water can not be generated, the environmental pollution is avoided, and the shampoo is environment-friendly.
Detailed Description
Example 1
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 1 part of Chinese honeylocust fruit, 1 part of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae, 1 part of ligusticum and 1 part of angelica dahurica; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sodium sarcosinate and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sodium sarcosinate and the ethylhexyl glycerol respectively account for 4%, 10% and 0.1% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) respectively weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 20h, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 8 times of water to 100 deg.C, maintaining the temperature for 120min, adding cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae into water, heating at 100 deg.C for 30min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 70 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 1min in vacuum, then adding a surfactant, stirring for 1min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Example 2
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae, 1 part of ligusticum and 1 part of angelica dahurica; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sodium sarcosinate and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sodium sarcosinate and the ethylhexyl glycerol respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) respectively weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 24 hr, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 9 times of water at 100 deg.C, keeping the temperature for 140min, adding cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae into water, heating at 100 deg.C for 40min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 75 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 1min in vacuum, then adding a surfactant, stirring for 1min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Example 3
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 4 parts of Chinese honeylocust fruit, 4 parts of soapberry, 2 parts of tree peony bark, 2 parts of Chinese arborvitae twig, 2 parts of Chinese ligusticum rhizome and 2 parts of dahurian angelica root; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sarcosine sodium and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sarcosine sodium and the ethylhexyl glycerol respectively account for 6%, 20% and 0.5% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) respectively weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 30h, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 10 times of water to 100 deg.C, keeping the temperature for 150min, adding cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae into water, heating at 100 deg.C for 50min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 80 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 3min in vacuum, then adding a surfactant, stirring for 3min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Comparative example 1
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae, 1 part of ligusticum and 1 part of angelica dahurica; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sodium sarcosinate and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sodium sarcosinate and the ethylhexyl glycerol respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) respectively weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 24h, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 9 times of water at 100 deg.C, keeping the temperature for 140min, adding folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae into water, heating at 100 deg.C for 40min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 75 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 1min in vacuum, then adding a surfactant, stirring for 1min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Comparative example 2
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of Chinese ligusticum rhizome and 1 part of dahurian angelica root; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sodium sarcosinate and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sodium sarcosinate and the ethylhexyl glycerol respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, cortex moutan, rhizoma Ligustici and radix Angelicae Dahuricae respectively, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 24h, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 9 times of water at 100 deg.C, keeping the temperature for 140min, adding cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae in water, heating at 100 deg.C for 40min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 75 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 1min in vacuum, then adding a surfactant, stirring for 1min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
Comparative example 3
A traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae and 1 part of ligusticum; the traditional Chinese medicine shampoo also comprises methyl glucoside polyoxyethylene (120) ether dioleate, N-lauroyl sodium sarcosinate and ethylhexyl glycerol, wherein the methyl glucoside polyoxyethylene (120) ether dioleate, the N-lauroyl sodium sarcosinate and the ethylhexyl glycerol respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
The preparation method of the traditional Chinese medicine shampoo comprises the following steps:
(1) respectively weighing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, cortex moutan, folium Platycladi and rhizoma Ligustici, soaking fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in clear water for 24 hr, heating fructus Gleditsiae Abnormalis and fructus Sapindi Mukouossi in 9 times of water at 100 deg.C, keeping the temperature for 140min, adding cortex moutan, folium Platycladi, rhizoma Ligustici and radix Angelicae Dahuricae in water, heating at 100 deg.C for 40min, and filtering to obtain medicinal liquid;
(2) and (2) cooling the medicinal liquid obtained in the step (1) to 75 ℃ in air, adding a thickening agent into the medicinal liquid, then stirring for 1min in vacuum, then adding a surfactant, stirring for 1min in vacuum, cooling to below 40 ℃ in air, then adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
120 volunteers with greasy hair, alopecia and allergy in 20-45 years old are randomly selected, divided into 6 groups of 20 persons in each group, and then the traditional Chinese medicine shampoo obtained in examples 1-3 and comparative examples 1-3 is used once every 2 days for 3 months, and the conditions of all the volunteers are counted after 3 months, and the results are shown in table 1.
During the use period, the volunteers should not use other cosmetics, health products and drugs which affect the experimental results. (effect evaluation: significant effect: significant improvement of greasy hair, alopecia and allergy after use; effective effect: certain improvement of greasy hair, alopecia and allergy after use; ineffective effect: no improvement of greasy hair, alopecia and allergy after use; effective rate (significant number of people + effective number of people)/total number of people).
TABLE 1 statistical tables of the use conditions of examples 1 to 3 and comparative examples 1 to 3
As can be seen from Table 1, the traditional Chinese medicine shampoo provided by the invention has good effects of removing oil, preventing alopecia and resisting scalp allergy, and has a good using effect. As can be seen from examples 1-3 and comparative examples 1-3, the moutan bark, the cacumen biotae and the radix angelicae have an antibacterial effect, can inhibit the growth of scalp bacteria, prevent allergy and also have an anti-alopecia effect.
While the present invention has been described in detail with reference to the specific embodiments thereof, it should not be construed as limited by the scope of the present patent. Various modifications and changes may be made by those skilled in the art without inventive step within the scope of the appended claims.
Claims (8)
1. The traditional Chinese medicine shampoo is characterized by comprising the following raw materials in parts by weight: 1-4 parts of saponin, 1-4 parts of soapberry, 1-2 parts of tree peony bark, 1-2 parts of cacumen biotae, 1-2 parts of ligusticum and 1-2 parts of radix angelicae.
2. The traditional Chinese medicine shampoo as claimed in claim 1, wherein the traditional Chinese medicine shampoo comprises the following raw materials in parts by weight: 2 parts of Chinese honeylocust fruit, 2 parts of soapberry, 1 part of tree peony bark, 1 part of cacumen biotae, 1 part of ligusticum and 1 part of angelica dahurica.
3. The traditional Chinese medicine shampoo as claimed in claim 1 or 2, further comprising a thickener, a surfactant and a humectant, wherein the thickener, the surfactant and the humectant respectively account for 4-6%, 10-20% and 0.1-0.5% of the total weight of the shampoo.
4. The traditional Chinese medicine shampoo as claimed in claim 3, wherein the thickener, the surfactant and the humectant respectively account for 5%, 15% and 0.3% of the total weight of the shampoo.
5. The traditional Chinese medicine shampoo as claimed in claim 3, wherein the thickener is methyl glucoside polyoxyethylene (120) ether dioleate, the surfactant is N-lauroyl sarcosine sodium, and the humectant is ethylhexyl glycerol.
6. The preparation method of the traditional Chinese medicine shampoo as defined in any one of claims 1 to 5, which is characterized by comprising the following steps:
(1) weighing Chinese honeylocust fruit, soapberry, tree peony bark, cacumen biotae, ligusticum and radix angelicae, soaking the Chinese honeylocust fruit and the soapberry in clear water for 20-30 h, heating the Chinese honeylocust fruit and the soapberry in 8-10 times of water to 90-100 ℃, preserving heat for 120-150 min, finally adding the tree peony bark, the cacumen biotae, the ligusticum and the radix angelicae into the water, heating for 30-50 min at 90-100 ℃, and filtering to obtain medicine juice;
(2) and (2) cooling the medicinal juice obtained in the step (1) in air to 70-80 ℃, adding a thickening agent into the medicinal juice, then stirring in vacuum for 1-3 min, then adding a surfactant, stirring in vacuum for 1-3 min, cooling in air to below 40 ℃, adding a humectant, mixing uniformly, standing for more than 2h, and removing surface foams to obtain the traditional Chinese medicine shampoo.
7. The preparation method of the traditional Chinese medicine shampoo as claimed in claim 6, wherein in the step (1), the Chinese honeylocust fruit and the soapberry are soaked in clear water for 24h, then the Chinese honeylocust fruit and the soapberry are heated to 100 ℃ in 9 times of water and are kept warm for 140min, finally the moutan bark, the Chinese arborvitae twig, the ligusticum sinense oliver and the dahurian angelica root are added into the water and are heated again for 40min at the temperature of 100 ℃.
8. The method for preparing traditional Chinese medicine shampoo as claimed in claim 6, wherein in the step (2), the medicine juice is cooled to 75 ℃ in air, the thickening agent is added into the medicine juice and then stirred in vacuum for 1min, then the surfactant is added and then stirred in vacuum for 1min, and the medicine juice is cooled to below 40 ℃ in air.
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Application publication date: 20200814 |