CN111499195A - Preparation method of rice paper imitation ceramic plate - Google Patents

Preparation method of rice paper imitation ceramic plate Download PDF

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Publication number
CN111499195A
CN111499195A CN202010347097.9A CN202010347097A CN111499195A CN 111499195 A CN111499195 A CN 111499195A CN 202010347097 A CN202010347097 A CN 202010347097A CN 111499195 A CN111499195 A CN 111499195A
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parts
rice paper
firing
biscuit
ceramic plate
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CN202010347097.9A
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Chinese (zh)
Inventor
黄明凯
黄翔
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time

Abstract

The invention discloses a preparation method of a rice paper imitation ceramic plate, which comprises the working procedures of glaze preparation and modulation, biscuit firing, secondary glaze firing, primary firing and the like. According to the invention, the biscuit firing treatment is carried out at a higher and proper temperature, and other procedures are combined, so that the finally obtained ceramic can be comparable to rice paper in writing: 1) the ink is not feathered; 2) the writing hand feeling is consistent with that of rice paper; 3) the effects of withered writing and whitening on the rice paper can be generated, and the color of the ancient rice paper can be highly imitated; 4) the tile can be preset on the bottom plate, and the line grid pattern can be displayed after being fired.

Description

Preparation method of rice paper imitation ceramic plate
Technical Field
The invention relates to the field of ceramics, in particular to a preparation method of a rice paper imitation ceramic plate.
Background
The prior high-temperature porcelain plate blank is difficult to adapt to writing and drawing for people who initially write or practice creation on rice paper for a long time, mainly shows that the writing and drawing are not moved by unsmooth pen dragging, mainly shows that the pen is sucked when the water absorption is large, the pigment is easy to flow when the water absorption is small, and the pigment cannot dry for a long time, so that the problem of the ceramic industry is solved, and the creation bottleneck of the ceramic industry is also realized.
Disclosure of Invention
In order to solve the technical problems, the invention provides a preparation method of rice paper imitation ceramic, which successfully solves the problem of difficult creation from rice paper to porcelain blank writing and painting, and enables more people engaged in paper creation to smoothly enter into ceramic creation.
The technical scheme of the invention is as follows:
a preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 40-60 parts of potassium feldspar, 20-40 parts of quartz, 1-5 parts of dolomite, 5-15 parts of talc, 1-5 parts of calcined alumina, 1-5 parts of bone meal, 5-15 parts of kaolin and 0.1-6 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to be 855-1000 ℃, and the biscuit firing time is 8-20 hours, so that a biscuit porcelain plate is obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate for secondary glaze firing at the temperature of 750-850 ℃ for 6-12 hours;
(4) and (3) carrying out primary firing at the temperature of 1360-1430 ℃ for 16-30 hours to obtain the rice paper imitation ceramic plate.
Further, 45-55 parts of potassium feldspar, 25-35 parts of quartz, 2-4 parts of dolomite, 8-12 parts of talc, 2-5 parts of calcined alumina, 3-5 parts of bone meal, 8-12 parts of ridge soil and 0.5-4 parts of vanadium-zirconium yellow.
Furthermore, the biscuit firing temperature is preferably 860-960 ℃.
Further, the temperature of the secondary glaze firing is preferably 760-820 ℃.
Further, the sintering temperature is preferably 1380-1420 ℃.
The invention has the beneficial effects that:
according to the invention, the biscuit firing treatment is carried out at a higher and proper temperature, and other procedures are combined, so that the finally obtained ceramic can be comparable to rice paper in writing: 1) the ink is not feathered; 2) the writing hand feeling is consistent with that of rice paper; 3) the effects of withered writing and whitening on the rice paper can be generated, and the color of the ancient rice paper can be highly imitated; 4) the tile can be preset on the bottom plate, and the line grid pattern can be displayed after being fired.
Drawings
FIG. 1 shows a shading pattern of a ceramic obtained in example 1 of the present invention.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the present invention is not limited thereto.
Example 1
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 50 parts of potassium feldspar, 30 parts of quartz, 3 parts of dolomite, 10 parts of talc, 4 parts of calcined alumina, 3 parts of bone meal, 9 parts of ridge soil and 2 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled at 900 ℃, and the biscuit firing time is 12 hours, so that a biscuit porcelain plate is obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate to perform secondary glaze firing at 820 ℃ for 8 hours;
(4) the ceramic plate is sintered at 1400 ℃ for 24 hours to obtain the rice paper imitation ceramic plate.
In order to meet the requirements of various patterns of the ceramic, a painting process is added in the step (3) and the step (4). In addition to this embodiment, a drawing process is added. On the basis of the process, after the secondary glaze firing, the painting becomes very simple and can be very close to the painting effect on the rice paper.
Before the firing process in the step (4), the drawing can be very easily completed, only the color of the ground pattern is not obvious enough, and the pattern becomes very clear after the firing process in the step (4), as shown in fig. 1, the ground pattern with obvious color can be presented after the firing process, including tiling pattern, lines, lattices and white-line patterns, and it is worth explaining that the similar grain patterns under the words are clear red, and the clear ground pattern can be generated by the process of the invention.
Example 2
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 45 parts of potassium feldspar, 35 parts of quartz, 4 parts of dolomite, 12 parts of talc, 3 parts of calcined alumina, 4 parts of bone meal, 12 parts of ridge soil and 4 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to be 860 ℃, and the biscuit firing time is 15 hours, so that biscuit porcelain plates are obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate to perform secondary glaze firing at the temperature of 840 ℃ for 6 hours;
(4) the ceramic plate is baked at 1380 ℃ for 16 hours to obtain the rice paper imitation ceramic plate.
Example 3
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 40 parts of potassium feldspar, 20 parts of quartz, 2 parts of dolomite, 5 parts of talc, 1 part of calcined alumina, 1 part of bone meal, 5 parts of ridge soil and 0.1 part of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to 855 ℃, and the time is 10 hours, so that a biscuit porcelain plate is obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate to perform secondary glaze firing at 800 ℃ for 12 hours;
(4) the ceramic plate is baked at 1420 ℃ for 30 hours to obtain the rice paper imitation ceramic plate.
Example 4
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 60 parts of potassium feldspar, 40 parts of quartz, 1 part of dolomite, 15 parts of talc, 5 parts of calcined alumina, 5 parts of bone meal, 15 parts of ridge soil and 6 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to be 1000 ℃, and the biscuit firing time is 16 hours, so that a biscuit porcelain plate is obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate for secondary glaze firing at 780 ℃ for 10 hours;
(4) the ceramic plate is baked at 1390 ℃ for 18 hours to obtain the rice paper imitation ceramic plate.
Example 5
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 48 parts of potassium feldspar, 25 parts of quartz, 5 parts of dolomite, 8 parts of talc, 2 parts of calcined alumina, 2 parts of bone meal, 10 parts of ridge soil and 5 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to be 930 ℃, and the time is 20 hours, so that biscuit porcelain plates are obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate to perform secondary glaze firing at 770 ℃ for 9 hours;
(4) the ceramic plate is sintered at 1360 ℃ for 22 hours to obtain the rice paper imitation ceramic plate.
Example 6
A preparation method of a rice paper-like ceramic plate comprises the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 55 parts of potassium feldspar, 32 parts of quartz, 3 parts of dolomite, 14 parts of talc, 3 parts of calcined alumina, 3 parts of bone meal, 14 parts of ridge soil and 3 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled at 960 ℃, and the biscuit firing time is 8 hours, so that biscuit porcelain plates are obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate for secondary glaze firing at 790 ℃ for 7 hours;
(4) the ceramic plate is sintered at 1430 ℃ for 27 hours to obtain the rice paper imitation ceramic plate.
In any of embodiments 2 to 6, the number of painting steps can be increased as required, and a good painting effect can be obtained.

Claims (5)

1. A preparation method of a rice paper imitation ceramic plate is characterized by comprising the following steps:
(1) preparing glaze and preparing the following raw materials in parts by mass: 40-60 parts of potassium feldspar, 20-40 parts of quartz, 1-5 parts of dolomite, 5-15 parts of talc, 1-5 parts of calcined alumina, 1-5 parts of bone meal, 5-15 parts of kaolin and 0.1-6 parts of vanadium-zirconium yellow;
(2) biscuit firing is carried out on the porcelain plate, the biscuit firing temperature is controlled to be 855-1000 ℃, and the biscuit firing time is 8-20 hours, so that a biscuit porcelain plate is obtained;
(3) spraying the prepared glaze on the sintered biscuit porcelain plate for secondary glaze firing at the temperature of 750-850 ℃ for 6-12 hours;
(4) and (3) carrying out primary firing at the temperature of 1360-1430 ℃ for 16-30 hours to obtain the rice paper imitation ceramic plate.
2. The preparation method of the rice paper-like ceramic plate as claimed in claim 1, wherein the potassium feldspar comprises 45-55 parts, quartz 25-35 parts, dolomite 2-4 parts, talc 8-12 parts, calcined alumina 2-5 parts, bone meal 3-5 parts, ridge clay 8-12 parts, and vanadium zirconium yellow 0.5-4 parts.
3. The preparation method of the rice paper-like ceramic plate according to claim 1, wherein the bisque firing temperature is 860 to 960 ℃.
4. The preparation method of the rice paper-like ceramic plate as claimed in claim 1, wherein the temperature of the secondary glaze firing is 760 to 820 ℃.
5. The method for manufacturing a rice paper-like ceramic plate according to claim 1, wherein the firing temperature is 1380 to 1420 ℃.
CN202010347097.9A 2020-04-27 2020-04-27 Preparation method of rice paper imitation ceramic plate Pending CN111499195A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112250430A (en) * 2020-08-31 2021-01-22 杨纲雄 Porcelain clay, porcelain and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN101613204A (en) * 2008-06-26 2009-12-30 庄助民 In-glaze decoration sclerotin porcelain production technique
CN101717276A (en) * 2009-11-20 2010-06-02 景德镇陶瓷学院 Transparent lead-free fritted glaze with low expansion coefficient and preparation method thereof
CN104476976A (en) * 2014-12-22 2015-04-01 山东硅元新型材料有限责任公司 Production process of art porcelain with Chinese art paper drawing effect
CN105060858A (en) * 2015-08-04 2015-11-18 刘伟华 Novel decoration method of Chinese art paper painting imitated ceramic plate
US20170190210A1 (en) * 2015-01-21 2017-07-06 Desong Ma Method for processing ink, stone and oil painting
CN110540406A (en) * 2019-10-17 2019-12-06 黑龙江省黑土地特种陶瓷有限公司 Rice paper porcelain and preparation method and application thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101613204A (en) * 2008-06-26 2009-12-30 庄助民 In-glaze decoration sclerotin porcelain production technique
CN101717276A (en) * 2009-11-20 2010-06-02 景德镇陶瓷学院 Transparent lead-free fritted glaze with low expansion coefficient and preparation method thereof
CN104476976A (en) * 2014-12-22 2015-04-01 山东硅元新型材料有限责任公司 Production process of art porcelain with Chinese art paper drawing effect
US20170190210A1 (en) * 2015-01-21 2017-07-06 Desong Ma Method for processing ink, stone and oil painting
CN105060858A (en) * 2015-08-04 2015-11-18 刘伟华 Novel decoration method of Chinese art paper painting imitated ceramic plate
CN110540406A (en) * 2019-10-17 2019-12-06 黑龙江省黑土地特种陶瓷有限公司 Rice paper porcelain and preparation method and application thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112250430A (en) * 2020-08-31 2021-01-22 杨纲雄 Porcelain clay, porcelain and preparation method thereof

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