CN111498789A - Antibacterial and antiseptic down and preparation method thereof - Google Patents
Antibacterial and antiseptic down and preparation method thereof Download PDFInfo
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- CN111498789A CN111498789A CN202010340093.8A CN202010340093A CN111498789A CN 111498789 A CN111498789 A CN 111498789A CN 202010340093 A CN202010340093 A CN 202010340093A CN 111498789 A CN111498789 A CN 111498789A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B68—SADDLERY; UPHOLSTERY
- B68G—METHODS, EQUIPMENT, OR MACHINES FOR USE IN UPHOLSTERING; UPHOLSTERY NOT OTHERWISE PROVIDED FOR
- B68G1/00—Loose filling materials for upholstery
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic System
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M19/00—Treatment of feathers
Abstract
The invention relates to an antibacterial and antiseptic down, which comprises the following filler raw materials in percentage by mass: 70-75 parts of down fiber, 10-15 parts of modified artificial fiber, 5-10 parts of bamboo fiber and 5-10 parts of antibacterial powder. The invention relates to a preparation method of antibacterial and antiseptic down, which comprises the following steps: step 1: preparing down feather; step 2: primary water washing; step 3: performing antibacterial treatment; step 4: performing antiseptic treatment; step 5: processing antibacterial powder; step 6: mixing the bamboo fibers. Compared with the prior art, the invention has the following advantages: firstly, the antibacterial rate of the down feather is better improved by adopting the bamboo fiber and the antibacterial powder; secondly, on the aspect of antibiosis, the soaking effect of the antibacterial agent can be improved by adopting the mode of antibacterial soaking, drying in the shade and drying, the antibacterial effect is further improved by adopting the adhesion of antibacterial powder, and the soaking treatment for deodorization is carried out in the same way; and thirdly, the antibacterial powder can be gradually attached to the surface of the down feather by adopting a stirring and drying mode, and the influence on the lightness and thinness of the down feather is small.
Description
Technical Field
The invention relates to the technical field of down feather processing, in particular to an antibacterial and anticorrosive down feather and a preparation method thereof.
Background
Feather raw materials for producing the down feather are poultry feathers, and particularly, duck feathers are used mostly. The down feather has less washing times in the using process and is easy to breed bacteria and mites, so that the down feather has requirements on the antibacterial property. The following provides a down which is antibacterial and has reduced putrefactive flavor.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides the antibacterial and antiseptic down and the preparation method thereof.
In order to solve the problems, the technical scheme adopted by the invention is as follows:
the antibacterial and antiseptic velvet comprises the following filler raw materials in percentage by mass: 70-75 parts of down fiber, 10-15 parts of modified artificial fiber, 5-10 parts of bamboo fiber and 5-10 parts of antibacterial powder.
As an improvement of the technical scheme, the down fibers are natural down subjected to degreasing treatment.
As an improvement of the technical scheme, the antibacterial powder is ceramic powder.
As an improvement of the technical scheme, the antibacterial and antiseptic cashmere filler comprises the following raw materials in percentage by mass: 70 parts of down fiber, 10 parts of modified artificial fiber, 10 parts of bamboo fiber and 10 parts of antibacterial powder.
The preparation method of the antibacterial and antiseptic velvet comprises the following steps: step 1: preparing down feather; taking natural down feather and carrying out degreasing treatment; taking 10-15 parts of artificial fiber, and performing protein modification treatment; soaking 5-10 parts of bamboo fiber in clear water; step 2: primary water washing; adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather; then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried; guiding the dried down feather into a five-box machine for feather separation; taking 70-75 parts of common down feather obtained after feather separation; step 3: performing antibacterial treatment; mixing the modified artificial fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding an antibacterial agent, soaking for 2h, and draining; then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 55-70 ℃; step 4: performing antiseptic treatment; introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining; then placing the mixed fiber for more than 3 hours at room temperature; then the mixed fiber is led into a dryer to be dried for 1h at the temperature of 50-55 ℃; step 5: processing antibacterial powder; mixing 5-10 parts of ceramic powder with glue and water according to the ratio of 1:1:16 to obtain a mixed solution; placing the mixed fiber in step4 in the mixed solution, and soaking for 30 min; stirring the formed mixture under the condition of keeping no water drainage, drying the mixture at the temperature of between 35 and 60 ℃, transferring the mixture to the room temperature, and airing the mixture for more than 3 hours; step 6: mixing bamboo fibers; removing bamboo fiber in step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature; and mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
As an improvement of the technical scheme, the antibacterial agent in step3 comprises the following components: and (4) nano silver.
As an improvement of the technical proposal, the water washing process in step1 comprises three steps; and adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
As an improvement of the above technical means, the protein modification in step1 was carried out using sodium hydroxide solution.
Compared with the prior art, the invention has the following advantages: firstly, the antibacterial rate of the down feather is better improved by adopting the bamboo fiber and the antibacterial powder; secondly, on the aspect of antibiosis, the soaking effect of the antibacterial agent can be improved by adopting the mode of antibacterial soaking, drying in the shade and drying, the antibacterial effect is further improved by adopting the adhesion of antibacterial powder, and the soaking treatment for deodorization is carried out in the same way; and thirdly, the antibacterial powder can be gradually attached to the surface of the down feather by adopting a stirring and drying mode, and the influence on the lightness and thinness of the down feather is small.
Drawings
FIG. 1 is a table of the test of the degree of antisepsis and preservation of the sample of the present invention.
Detailed Description
The present invention will be described with reference to specific examples.
The filler of the antibacterial and antiseptic velvet comprises the following raw materials in percentage by mass: 70-75 parts of down fiber, 10-15 parts of modified artificial fiber, 5-10 parts of bamboo fiber and 5-10 parts of antibacterial powder. The down fiber is natural down subjected to degreasing treatment. The antibacterial powder is ceramic powder.
The preparation method of the antibacterial and antiseptic velvet comprises the following steps:
step 1: preparing down feather;
degreasing natural down feather. 10-15 parts of artificial fiber is taken for protein modification treatment. Soaking 5-10 parts of bamboo fiber in clear water.
Step 2: preliminary washing of wool
And (3) adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather. And then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried. And guiding the dried down feather into a five-box machine for feather separation. 70-75 parts of common down feather obtained after feather separation.
Step 3: performing antibacterial treatment;
mixing the modified rayon fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding the antibacterial agent, soaking for 2h, and draining. And then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 55-70 ℃.
Step 4: performing antiseptic treatment;
and (3) introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining. And then the mixed fiber is placed for more than 3 hours at room temperature. Then the mixed fiber is led into a dryer to be dried for 1 hour at the temperature of 50-55 ℃.
Step 5: processing antibacterial powder;
mixing 5-10 parts of ceramic powder with glue and water according to the proportion of 1:1:16 to obtain a mixed solution. The mixed fibers in step4 were placed in the mixture and soaked for 30 min. Stirring the mixture under the condition of not draining water, drying at 35-60 ℃, transferring the mixture to room temperature, and airing for more than 3 h.
Step 6: mixing bamboo fibers;
removing bamboo fiber from step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature. And mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
The antimicrobial agent composition in step3 comprises: and (4) nano silver.
The water washing process in step1 comprises three steps. And adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
Protein modification in step1 was performed using sodium hydroxide solution.
Example one
The filler of the antibacterial and antiseptic velvet comprises the following raw materials in percentage by mass: 75 parts of down fiber, 15 parts of modified artificial fiber, 5 parts of bamboo fiber and 5 parts of antibacterial powder. The down fiber is natural down subjected to degreasing treatment. The antibacterial powder is ceramic powder.
The preparation method of the antibacterial and antiseptic velvet comprises the following steps:
step 1: preparing down feather;
degreasing natural down feather. 15 parts of artificial fiber is taken for protein modification treatment. Soaking 5 parts of bamboo fiber in clear water.
Step 2: preliminary washing of wool
And (3) adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather. And then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried. And guiding the dried down feather into a five-box machine for feather separation. 75 parts of common down feather obtained after feather separation.
Step 3: performing antibacterial treatment;
mixing the modified rayon fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding the antibacterial agent, soaking for 2h, and draining. And then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 60 ℃.
Step 4: performing antiseptic treatment;
and (3) introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining. And then the mixed fiber is placed for more than 3 hours at room temperature. Then the mixed fiber is led into a dryer to be dried for 1h at the temperature of 60 ℃.
Step 5: processing antibacterial powder;
taking 2-3 parts of ceramic powder, mixing the ceramic powder with glue and water according to the proportion of 1:1:16 to obtain a mixed solution. The mixed fibers in step4 were placed in the mixture and soaked for 30 min. Stirring the mixture without draining, drying at 52 deg.C, transferring the mixture to room temperature, and air drying for more than 3 hr.
Step 6: mixing bamboo fibers;
removing bamboo fiber from step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature. And mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
The antimicrobial agent composition in step3 comprises: and (4) nano silver.
The water washing process in step1 comprises three steps. And adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
Protein modification in step1 was performed using sodium hydroxide solution.
The first sample was obtained by the above procedure.
Example two
The filler of the antibacterial and antiseptic velvet comprises the following raw materials in percentage by mass: 70 parts of down fiber, 10 parts of modified artificial fiber, 10 parts of bamboo fiber and 10 parts of antibacterial powder. The down fiber is natural down subjected to degreasing treatment. The antibacterial powder is ceramic powder.
The preparation method of the antibacterial and antiseptic velvet comprises the following steps:
step 1: preparing down feather;
degreasing natural down feather. 10 parts of artificial fiber is taken for protein modification treatment. Soaking 5 parts of bamboo fiber in clear water.
Step 2: preliminary washing of wool
And (3) adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather. And then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried. And guiding the dried down feather into a five-box machine for feather separation. 70 parts of common down feather obtained after feather separation.
Step 3: performing antibacterial treatment;
mixing the modified rayon fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding the antibacterial agent, soaking for 2h, and draining. And then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 60 ℃.
Step 4: performing antiseptic treatment;
and (3) introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining. And then the mixed fiber is placed for more than 3 hours at room temperature. Then the mixed fiber is led into a dryer to be dried for 1h at the temperature of 52 ℃.
Step 5: processing antibacterial powder;
mixing 5-10 parts of ceramic powder with glue and water according to the proportion of 1:1:16 to obtain a mixed solution. The mixed fibers in step4 were placed in the mixture and soaked for 30 min. Stirring the mixture without draining, drying at 52 deg.C, transferring the mixture to room temperature, and air drying for more than 3 hr.
Step 6: mixing bamboo fibers;
removing bamboo fiber from step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature. And mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
The antimicrobial agent composition in step3 comprises: and (4) nano silver.
The water washing process in step1 comprises three steps. And adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
Protein modification in step1 was performed using sodium hydroxide solution.
And obtaining a second sample through the steps.
EXAMPLE III
The filler of the antibacterial and antiseptic velvet comprises the following raw materials in percentage by mass: 73 parts of down fiber, 12 parts of modified artificial fiber, 8 parts of bamboo fiber and 7 parts of antibacterial powder. The down fiber is natural down subjected to degreasing treatment. The antibacterial powder is ceramic powder.
The preparation method of the antibacterial and antiseptic velvet comprises the following steps:
step 1: preparing down feather;
degreasing natural down feather. And taking 12 parts of artificial fiber for protein modification treatment. Soaking 8 parts of bamboo fiber in clear water.
Step 2: preliminary washing of wool
And (3) adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather. And then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried. And guiding the dried down feather into a five-box machine for feather separation. 72 parts of common down feather obtained after feather separation.
Step 3: performing antibacterial treatment;
mixing the modified rayon fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding the antibacterial agent, soaking for 2h, and draining. And then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 60 ℃.
Step 4: performing antiseptic treatment;
and (3) introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining. And then the mixed fiber is placed for more than 3 hours at room temperature. Then the mixed fiber is led into a dryer to be dried for 1h at the temperature of 52 ℃.
Step 5: processing antibacterial powder;
mixing 5-10 parts of ceramic powder with glue and water according to the proportion of 1:1:16 to obtain a mixed solution. The mixed fibers in step4 were placed in the mixture and soaked for 30 min. Stirring the mixture without draining, oven drying at 50 deg.C, transferring the mixture to room temperature, and air drying for more than 3 hr.
Step 6: mixing bamboo fibers;
removing bamboo fiber from step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature. And mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
The antimicrobial agent composition in step3 comprises: and (4) nano silver.
The water washing process in step1 comprises three steps. And adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
Protein modification in step1 was performed using sodium hydroxide solution.
Sample three was obtained by the above procedure.
The original down feather was taken as sample four. And (5) performing an antibacterial rate test and an anticorrosion test. Fig. 1 is a test table of the antibacterial and antiseptic degree of the sample, and it can be seen from fig. 1 that the ratio of the bamboo fiber and the antibacterial powder positively affects the antibacterial rate, and the down fiber and the modified fiber positively affects the antiseptic degree. And (4) integrating the numerical values, and optimizing the sample II.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.
Claims (8)
1. The antibacterial and antiseptic down is characterized in that the filler raw materials of the antibacterial and antiseptic down comprise the following components in percentage by mass: 70-75 parts of down fiber, 10-15 parts of modified artificial fiber, 5-10 parts of bamboo fiber and 5-10 parts of antibacterial powder.
2. The antibacterial and antiseptic down feather as claimed in claim 1, wherein the down feather fibers are natural down feather that has been degreased.
3. The antibacterial and antiseptic flannelette of claim 1, wherein the antibacterial powder is ceramic powder.
4. The antibacterial and antiseptic velvet as claimed in claim 1, wherein the filler raw materials comprise, by mass: 70 parts of down fiber, 10 parts of modified artificial fiber, 10 parts of bamboo fiber and 10 parts of antibacterial powder.
5. The preparation method of the antibacterial and antiseptic velvet is characterized by comprising the following steps:
step 1: preparing down feather;
taking natural down feather and carrying out degreasing treatment; taking 10-15 parts of artificial fiber, and performing protein modification treatment; soaking 5-10 parts of bamboo fiber in clear water;
step 2: preliminary washing of wool
Adding the degreased natural down feather in step1 into a water washing pool, and washing for multiple times to remove the odor of the natural down feather; then the down feather is guided into a dryer to be blown for 2 hours, and the down feather is dried; guiding the dried down feather into a five-box machine for feather separation; taking 70-75 parts of common down feather obtained after feather separation;
step 3: performing antibacterial treatment;
mixing the modified artificial fiber obtained in step1 and the down fiber obtained in step2, adding into a water washing pool, adding an antibacterial agent, soaking for 2h, and draining; then placing the mixed fiber at room temperature for more than 3h, and then introducing the mixed fiber into a dryer to dry for 1h at the temperature of 55-70 ℃;
step 4: performing antiseptic treatment;
introducing the mixed fiber obtained in step3 into a water washing pool, adding clear water and a preservative, soaking for 1h, and draining; then placing the mixed fiber for more than 3 hours at room temperature; then the mixed fiber is led into a dryer to be dried for 1h at the temperature of 50-55 ℃;
step 5: processing antibacterial powder;
mixing 5-10 parts of ceramic powder with glue and water according to the ratio of 1:1:16 to obtain a mixed solution; placing the mixed fiber in step4 in the mixed solution, and soaking for 30 min; stirring the formed mixture under the condition of keeping no water drainage, drying the mixture at the temperature of between 35 and 60 ℃, transferring the mixture to the room temperature, and airing the mixture for more than 3 hours;
step 6: mixing bamboo fibers;
removing bamboo fiber in step1, air drying under natural condition, steaming in steam environment for 30min, taking out, and air drying at room temperature; and mixing the mixed fiber in step5 with bamboo fiber to obtain the final product.
6. The method for preparing antibacterial and antiseptic down according to claim 5, wherein the antibacterial agent component in step3 comprises: and (4) nano silver.
7. The method for preparing antibacterial and antiseptic down according to claim 5, wherein the water washing process in step1 includes three steps; and adding clear water, a deodorant, clear water and a softening agent into the water for the third time.
8. The method for preparing antibacterial and antiseptic cashmere according to claim 5, wherein step1 is modified with sodium hydroxide solution.
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