CN111411349A - Ti/TiO2Method for manufacturing composite coating electrode - Google Patents

Ti/TiO2Method for manufacturing composite coating electrode Download PDF

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CN111411349A
CN111411349A CN202010257439.8A CN202010257439A CN111411349A CN 111411349 A CN111411349 A CN 111411349A CN 202010257439 A CN202010257439 A CN 202010257439A CN 111411349 A CN111411349 A CN 111411349A
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frame
electrode
annular
titanium metal
composite coating
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CN111411349B (en
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徐根水
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Anhui Sunsing Chemicals Co ltd
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Anhui Sunsing Chemicals Co ltd
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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1291—Process of deposition of the inorganic material by heating of the substrate

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The invention relates to Ti/Ti02The method for manufacturing the composite coating electrode needs to perform a plurality of procedures such as titanium metal substrate treatment, coating composite slurry preparation, substrate treatment, coating processing, drying treatment and the like. The invention can solve the following problems that the conventional Ti/TiO2 composite coating electrode needs to be dried in the processing and manufacturing process, the conventional drying mode takes long time, the electrode coated with composite coating slurry needs to be laid flatly in the drying operation, the occupied space is large, batch operation needs to be carried out on the electrode coated with the composite coating slurry on two sides, one side of the electrode is coated and dried firstly, the time consumption is long, the production cost is increased, if the slurry is coated on two sides simultaneously, the simultaneity of drying of the two sides cannot be ensured by using the conventional drying mode, the coatings on the two sides of the electrode are dried unevenly, the drying time of the coatings on the electrode is prolonged, and the quality of the composite coating electrode is influenced.

Description

Ti/TiO2Method for manufacturing composite coating electrode
Technical Field
The invention relates to the technical field of electrode coating preparation methods, in particular to Ti/TiO2A method for manufacturing a composite coating electrode.
Background
The electrode coating can prolong the service life of the electrode, the stability of the electrode surface coating directly determines whether the electrode can be used for a long time, and for different adaptive environments, the selection of corresponding electrode materials and the electrode coating are particularly important, wherein Ti/TiO2The composite coating electrode has wide application in the fields of chemical industry, electric metallurgy, metal foil production and the like, and Ti/TiO2The composite coating electrode is subjected to titanium metal substrate treatment, coating composite slurry preparation, substrate treatment and coating in the production and preparation processThe method comprises a plurality of procedures such as layer processing and drying treatment, wherein the drying treatment of the coated electrode directly influences the use quality of the formed electrode.
However, the existing Ti/TiO2The following difficult problems a that exist in the processing and manufacturing process of the composite coating electrode, the composite coating on the electrode needs to be dried, the traditional drying mode is long in consumed time, the electrode coated with the composite coating slurry needs to be tiled and placed in the drying operation, the occupied space is large, batch operation needs to be carried out on the electrode coated with the composite coating slurry on two sides, one side of the electrode is coated and dried firstly, the consumed time is long, the production cost is increased, if the slurry is coated on two sides simultaneously, the simultaneity of double-side drying cannot be ensured by using the traditional drying mode, the coatings on two sides of the electrode are not uniformly dried, the drying time of the coatings on the electrode is prolonged, and the quality of the composite coating electrode is influenced.
For the technical problems existing in the production process of the current coating electrode, persons in the related technical field make adaptive improvements after research and study, for example, the invention patent of China with patent number 2015107632952, namely Ti0 prepared by composite sol electrophoresis2The coating method can improve the adhesion of the film and has good photocatalytic performance, but the problems mentioned above are not mentioned.
Disclosure of Invention
In order to solve the above problems, the present invention provides a Ti/TiO compound2The manufacturing method of the composite coating electrode can solve the problems mentioned above.
In order to achieve the purpose, the invention adopts the following technical scheme to realize the purpose: Ti/TiO2The manufacturing method of the composite coating electrode mainly comprises the following manufacturing methods;
step one, processing a titanium metal substrate: detecting the titanium metal substrate for manufacturing the electrode, selecting the titanium metal substrate meeting the requirements, cleaning the surface of the titanium metal substrate, and removing burrs, flashes, stains or dust on the surface of the titanium metal substrate;
step two, preparing coating composite slurry: mixing and stirring raw materials for manufacturing the electrode coating according to requirements to obtain composite coating slurry, uniformly stirring the raw materials from top to bottom in the mixing and stirring process, and stopping stirring operation when the raw materials are stirred to be in a sticky pasty state;
step three, substrate treatment: cutting the titanium metal substrate processed in the step one according to the requirement, removing burrs generated in cutting, grinding and polishing the cutting position of the titanium metal substrate to obtain a titanium metal substrate carrier;
step four, coating processing: uniformly coating the prepared composite coating rubber material on the titanium metal plate carrier in the third step, wherein the coating operation is carried out in a reciprocating staggered coating mode, and redundant coating slurry at corners is removed to obtain a titanium metal plate electrode blank;
step five, drying treatment: placing the titanium metal plate electrode blank in the fourth step into a drying device for drying treatment to obtain a titanium metal plate electrode;
the above Ti/TiO2The method comprises the following steps that firstly, a special drying device is matched for operation, the drying device comprises a bottom plate, an annular drying box is mounted on the bottom plate, electric heating pipes are uniformly arranged in the annular drying box, a taking and placing opening is formed in the front end of the annular drying box, a rotating piece is mounted between the inner walls of the annular drying box, a rotating and conveying device is arranged on the inner wall of the annular drying box, rotating columns are uniformly arranged on the left side and the right side of the inner wall of the annular drying box along the circumferential direction of the inner wall of the annular drying box, and an outer ring fan and an outer ring gear are sequentially mounted on the rotating columns from outside to inside;
the titanium metal plate electrode blank is placed on the rotary conveying device through the taking and placing opening, the rotary part is used for controlling the titanium metal plate electrode blank to slowly rotate circularly in the annular drying box after the titanium metal plate electrode blank is clamped by the rotary conveying device, the temperature in the annular drying box is quickly increased after the electric heating pipe is electrified, the titanium metal plate electrode blank is processed in two modes of high-temperature drying and wind-force drying through the wind sources of the inner part and the outer part of the annular drying box, the drying time of the titanium metal plate electrode blank is shortened through the three-dimensional circular conveying drying mode, and the space is saved.
The rotary conveying device comprises connecting rods symmetrically arranged on the left side and the right side of the rotating part, rotary circular rings are sleeved on the connecting rods, annular limiting grooves are formed in the rotary circular rings, annular limiting frames are arranged in the annular limiting grooves in a sliding mode, the annular limiting frames are fixed on the inner wall of the annular drying box, conveying mechanisms are uniformly arranged between the rotary circular rings on the left side and the right side of the rotating part, and control rods are connected between every two conveying mechanisms through pin shafts;
conveying mechanism is including fixing the erection column between two rotation rings, install conveying frame through the bearing on the erection column, conveying frame's front end is open structure, conveying frame's front end is provided with the branch chain that opens and shuts, conveying frame's inside is provided with the locking frame that is U type structure, rear end locking groove has been seted up to the rear end of locking frame, the left and right sides of locking frame evenly is provided with lateral wall locking groove, install the rear side spring beam on the inner wall of conveying frame rear end, the rear side locking plate is installed to the front end of rear side spring beam, the link gear that is L type structure is installed to the left and right sides symmetry of rear side locking plate, evenly be provided with the ladder piece on the link gear, it is provided with lateral wall locking plate to slide in the lateral wall locking groove, be connected with the lateral wall spring beam between lateral wall locking plate and the lateral wall locking groove, be provided with on the lateral wall locking plate and support the pole, support and.
Further, the rotation piece includes and installs the driving motor on annular stoving case left side outer wall through the motor cabinet, driving motor's output shaft extends to the inboard of annular stoving case and links to each other with the left end of solid pole, the right-hand member of solid pole is connected with annular rotating turret, the right-hand member of annular rotating turret is connected on hollow rod, hollow rod passes through the bearing and installs on annular stoving case, install the bracing piece on the outer wall of annular stoving case, the bracing piece runs through hollow rod, install the support ring on the bracing piece, be provided with the rotation post along its circumference direction on the support ring, the upper end of rotation post is provided with the inner circle fan, the lower extreme of rotation post is provided with inner circle bevel gear, the meshing has driving bevel gear on the inner circle bevel gear, driving bevel gear sets.
Further, the branch chain that opens and shuts includes the open-close plate of setting at conveying frame front end downside through the hinge, the fixed slot has been seted up on the last lateral wall of conveying frame front end open-ended, the mounting groove has been seted up to the upside of open-close plate, install the spring beam that opens and shuts in the mounting groove, the frame that opens and shuts is installed to the spring beam that opens and shuts, be provided with the control post through the bearing on the open-close plate, the control post extends to in the mounting groove and is located inside the frame that opens and shuts, be provided with the eccentric disc on the control post, the eccentric disc supports and leans on the lower extreme inner wall of.
Furthermore, the conveying frame and the locking frame are uniformly provided with vent holes.
Furthermore, an operation gear is sleeved on the outer wall of the rotating circular ring and meshed with the outer ring gear.
Furthermore, the cross sections of the annular limiting frame and the annular limiting groove are both T-shaped structures.
1. The invention can solve the problems of the existing Ti/TiO2The following difficult problems a that exist in the processing and manufacturing process of the composite coating electrode, the composite coating on the electrode needs to be dried, the traditional drying mode is long in consumed time, the electrode coated with the composite coating slurry needs to be tiled and placed in the drying operation, the occupied space is large, batch operation needs to be carried out on the electrode coated with the composite coating slurry on two sides, one side of the electrode is coated and dried firstly, the consumed time is long, the production cost is increased, if the slurry is coated on two sides simultaneously, the simultaneity of double-side drying cannot be ensured by using the traditional drying mode, the coatings on two sides of the electrode are not uniformly dried, the drying time of the coatings on the electrode is prolonged, and the quality of the composite coating electrode is influenced. The present invention can solve the problems mentioned above, and has unexpected effects.
2. According to the invention, the titanium metal plate electrode blank is placed on the rotary conveying device through the taking and placing opening, the rotary part controls the titanium metal plate electrode blank to slowly rotate circularly in the annular drying box after the rotary conveying device clamps the titanium metal plate electrode blank, the temperature in the annular drying box is quickly raised after the electric heating pipe is electrified, the titanium metal plate electrode blank is processed in two modes of high-temperature drying and wind-force drying through the wind sources of the inner part and the outer part of the annular drying box, the drying time of the titanium metal plate electrode blank is shortened through the three-dimensional circular conveying drying mode, and the space is saved.
3. The conveying mechanism designed by the invention is used for abutting and fixing the four side walls of the titanium metal plate electrode blank through the mutual matching of the rear side locking plate, the side wall locking plate and the closing plate, so that the titanium metal plate electrode blank can be fixed under the condition that the double-sided composite coating of the titanium metal plate electrode blank is not influenced in operation, and the manufacturing time of the composite coating electrode plate is shortened.
4. The inner ring fan and the outer ring fan designed by the invention are matched with each other, and the titanium metal plate electrode blank in the conveying frame is blown from the inner side and the outer side, so that the uniformity of drying of the double-sided coating can be ensured under the condition that the double-sided coating is coated with the composite coating, and the drying time of the titanium metal plate electrode blank is shortened.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a schematic representation of Ti/TiO of the present invention202A flow chart of a manufacturing method of the composite coating electrode;
FIG. 2 is a schematic perspective view of a drying apparatus according to the present invention;
FIG. 3 is a cross-sectional view of FIG. 2 of the present invention;
FIG. 4 is a schematic view of the structure between the rotating member and the rotary conveyor according to the present invention;
FIG. 5 is a partial schematic view of a rotor according to the present invention;
FIG. 6 is a cross-sectional view of the delivery mechanism of the present invention;
FIG. 7 is a cross-sectional view taken along line A-A of FIG. 6 in accordance with the present invention;
fig. 8 is a sectional view taken along line B-B of fig. 6 in accordance with the present invention.
Detailed Description
The embodiments of the invention will be described in detail below with reference to the drawings, but the invention can be implemented in many different ways as defined and covered by the claims.
As shown in FIGS. 1 to 8, a Ti/Ti02Composite coating electrodeThe manufacturing method mainly comprises the following manufacturing methods;
step one, processing a titanium metal substrate: detecting the titanium metal substrate for manufacturing the electrode, selecting the titanium metal substrate meeting the requirements, cleaning the surface of the titanium metal substrate, and removing burrs, flashes, stains or dust on the surface of the titanium metal substrate;
step two, preparing coating composite slurry: mixing and stirring raw materials for manufacturing the electrode coating according to requirements to obtain composite coating slurry, uniformly stirring the raw materials from top to bottom in the mixing and stirring process, and stopping stirring operation when the raw materials are stirred to be in a sticky pasty state;
step three, substrate treatment: cutting the titanium metal substrate processed in the step one according to the requirement, removing burrs generated in cutting, grinding and polishing the cutting position of the titanium metal substrate to obtain a titanium metal substrate carrier;
step four, coating processing: uniformly coating the prepared composite coating rubber material on the titanium metal plate carrier in the third step, wherein the coating operation is carried out in a reciprocating staggered coating mode, and redundant coating slurry at corners is removed to obtain a titanium metal plate electrode blank;
step five, drying treatment: placing the titanium metal plate electrode blank in the fourth step into a drying device for drying treatment to obtain a titanium metal plate electrode;
the above Ti/Ti02The method comprises the following steps that firstly, a special drying device is matched for operation, the drying device comprises a bottom plate 1, an annular drying box 2 is mounted on the bottom plate 1, electric heating pipes are uniformly arranged in the annular drying box 2, a taking and placing opening is formed in the front end of the annular drying box 2, a rotating piece 3 is mounted between the inner walls of the annular drying box 2, a rotating and conveying device 4 is arranged on the inner wall of the annular drying box 2, rotating columns 5 are uniformly arranged on the left side and the right side of the inner wall of the annular drying box 2 along the circumferential direction of the inner wall, and an outer ring fan 6 and an outer ring gear 7 are sequentially mounted on the rotating columns 5 from outside to inside; the outer wall of the rotating ring 42 is sleeved with an operation gear, and the operation gear is meshed with the outer ring gear 7.
The rotating ring 42 controls the operation gear to rotate synchronously in the rotating operation, the operation gear is matched with the outer ring gear 7 in the rotating operation to drive the rotating column 5 to rotate, the rotating column 5 controls the outer ring fan 6 to operate synchronously, the drying speed of the titanium metal plate electrode blank can be increased through the wind power generated by the outer ring fan 6 in the operation, and the drying time of the titanium metal plate electrode blank is shortened.
The titanium metal plate electrode blank is placed on the rotary conveying device 4 through the taking and placing opening, the rotary part 3 controls the titanium metal plate electrode blank to slowly rotate circularly in the annular drying box 2 after the titanium metal plate electrode blank is clamped by the rotary conveying device 4, the temperature inside the annular drying box 2 is quickly raised after the electric heating pipe is electrified, the titanium metal plate electrode blank is processed in two modes of high-temperature drying and wind-force drying through the wind sources of the inner part and the outer part of the annular drying box 2, the drying time of the titanium metal plate electrode blank is shortened through the three-dimensional circular conveying drying mode, and meanwhile, the space is saved.
The rotary conveying device 4 comprises connecting rods 41 symmetrically arranged on the left side and the right side of the rotating part 3, a rotary ring 42 is sleeved on the connecting rods 41, an annular limiting groove is formed in the rotary ring 42, an annular limiting frame 43 is arranged in the annular limiting groove in a sliding mode, the annular limiting frame 43 is fixed on the inner wall of the annular drying box 2, conveying mechanisms 44 are uniformly arranged between the rotary rings 42 on the left side and the right side of the rotating part 3, and a position control rod 45 is connected between every two conveying mechanisms 44 through a pin shaft;
the rotating piece 3 drives the rotating ring 42 to synchronously rotate through the connecting rod 41 in the rotating process, the rotating ring 42 drives the conveying mechanism 44 to synchronously rotate in the rotating process, and the facing positions of the conveying mechanisms 44 connected with each other through the position control rod 45 can be kept unchanged in the rotating process.
The cross sections of the annular limiting frame 43 and the annular limiting groove are both T-shaped structures.
The sliding fit between the annular limiting frame 43 and the annular limiting groove can improve the stability of the rotating ring 42 in the rotating operation.
The conveying mechanism 44 comprises a mounting column 441 fixed between two rotating rings 42, a conveying frame 442 is mounted on the mounting column 441 through a bearing, the front end of the conveying frame 442 is of an open structure, an opening and closing branched chain 46 is arranged at the front end of the conveying frame 442, a locking frame 443 of a U-shaped structure is arranged inside the conveying frame 442, rear end locking grooves are formed in the rear end of the locking frame 443, side wall locking grooves are uniformly formed in the left side and the right side of each locking frame 443, rear side spring rods 444 are mounted on the inner wall of the rear end of the conveying frame 442, rear side locking plates 445 are mounted at the front ends of the rear side spring rods 444, linkage frames 446 of L-shaped structures are symmetrically mounted on the left side and the right side of each rear side locking plate 445, stepped blocks 447 are uniformly arranged on the linkage frames 446, side wall locking plates 448 are slidably arranged in the side wall locking grooves, side wall spring rods 449 are connected between the side wall locking plates 448 and the side wall locking grooves, abutting rods 440 are arranged on the side wall locking plates 448, and.
The opening and closing branched chain 46 comprises an opening and closing plate 461 arranged on the lower side of the front end of the conveying frame 442 through a hinge, the opening and closing plate 461 is of a grid structure, an operation space for temporarily fixing a titanium metal plate electrode blank from the outside can be reserved in the process of closing the opening and closing plate 461, a fixing groove is formed in the upper side wall of the front end opening of the conveying frame 442, a mounting groove is formed in the upper side of the opening and closing plate 461, an opening and closing spring rod 462 is mounted in the mounting groove, an opening and closing frame 463 is mounted on the opening and closing spring rod 462, a control column 464 is arranged on the opening and closing plate 461 through a bearing, the control column 464 extends into the mounting groove and is located inside the opening and closing frame 463, an eccentric disc 465 is arranged on the control column 464, the eccentric disc 465 abuts against the inner wall of the lower end.
In the operation, the titanium metal plate electrode blank is inserted into the conveying frame 442, the rear end of the titanium metal plate electrode blank is abutted against the rear locking plate 445, the titanium metal plate electrode blank is controlled to extrude the rear locking plate 445, the extruded rear locking plate 445 synchronously drives the linkage frame 446 to move from front to back, the linkage frame 446 controls the stepped block 447 to extrude the abutting rod 440 during the movement, the extruded abutting rod 440 controls the side wall locking plate 448 to extrude the titanium metal plate electrode blank, thereby extruding and abutting the rear side and the left and right sides of the titanium metal plate electrode blank body, controlling the opening plate 461 on the opening and closing branched chain 46 to be closed, abutting and extruding the front end of the titanium metal plate electrode blank body by the opening plate 461, therefore, the four side walls of the titanium metal plate electrode blank are abutted and fixed, and the titanium metal plate electrode blank can be fixed under the condition that the double-sided composite coating of the titanium metal plate electrode blank is not influenced in operation.
The conveying frame 442 and the locking frame 443 are uniformly provided with vent holes. The vent holes enable high-temperature air inside the annular drying box 2 to smoothly circulate, so that high-temperature transmission and wind power drying are performed on the titanium metal plate electrode blank placed inside the conveying frame 442.
The rotating part 3 comprises a driving motor 31 installed on the outer wall of the left side of the annular drying box 2 through a motor base, an output shaft of the driving motor 31 extends to the inner side of the annular drying box 2 and is connected with the left end of the solid rod 32, the right end of the solid rod 32 is connected with an annular rotating frame 33, the right end of the annular rotating frame 33 is connected onto the hollow rod 34, the hollow rod 34 is installed on the annular drying box 2 through a bearing, a supporting rod 35 is installed on the outer wall of the annular drying box 2, the supporting rod 35 penetrates through the hollow rod 34, a supporting ring 36 is installed on the supporting rod 35, a rotating column 37 is arranged on the supporting ring 36 along the circumferential direction of the supporting rod, an inner ring fan 38 is arranged at the upper end of the rotating column 37, a bevel gear 39 is arranged at the lower end of the rotating column 37, a driving bevel gear 310.
When the driving motor 31 controls the solid rod 32 to rotate, the solid rod 32 drives the hollow rod 34 to rotate synchronously through the annular rotating frame 33, so as to ensure that the two rotating circular rings 42 symmetrically connected with the left side and the right side of the rotating part 3 can rotate synchronously, the support ring 36 is kept in a static state during the rotation operation of the annular rotating frame 33, the drive bevel gear 310 on the annular rotating frame 33 is matched with the inner bevel gear 39 to drive the inner fan 38 on the rotating column 37 to rotate during the rotation operation, wind power is conveyed from the inside, the inner fan 38 is matched with the outer fan 6, and the titanium sheet electrode blank in the conveying frame 442 is blown from the inner side and the outer side, so that the uniformity of drying of double-sided coatings can be ensured under the condition that the double-sided coatings are coated on the titanium sheet electrode blank, and the drying time of the titanium sheet electrode blank is shortened.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are given by way of illustration of the principles of the present invention, and that various changes and modifications may be made without departing from the spirit and scope of the invention as defined by the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (6)

1. Ti/Ti02The manufacturing method of the composite coating electrode is characterized by comprising the following steps: mainly comprises the following manufacturing method;
step one, processing a titanium metal substrate: detecting the titanium metal substrate for manufacturing the electrode, selecting the titanium metal substrate meeting the requirements, cleaning the surface of the titanium metal substrate, and removing burrs, flashes, stains or dust on the surface of the titanium metal substrate;
step two, preparing coating composite slurry: mixing and stirring raw materials for manufacturing the electrode coating according to requirements to obtain composite coating slurry, uniformly stirring the raw materials from top to bottom in the mixing and stirring process, and stopping stirring operation when the raw materials are stirred to be in a sticky pasty state;
step three, substrate treatment: cutting the titanium metal substrate processed in the step one according to the requirement, removing burrs generated in cutting, grinding and polishing the cutting position of the titanium metal substrate to obtain a titanium metal substrate carrier;
step four, coating processing: uniformly coating the prepared composite coating rubber material on the titanium metal plate carrier in the third step, wherein the coating operation is carried out in a reciprocating staggered coating mode, and redundant coating slurry at corners is removed to obtain a titanium metal plate electrode blank;
step five, drying treatment: placing the titanium metal plate electrode blank in the fourth step into a drying device for drying treatment to obtain a titanium metal plate electrode;
the first to fifth steps of the Ti/Ti02 composite coating electrode manufacturing method need to be matched with a special drying device for operation, the drying device comprises a bottom plate (1), an annular drying box (2) is installed on the bottom plate (1), a taking and placing opening is formed in the front end of the annular drying box (2), a rotating piece (3) is installed between the inner walls of the annular drying box (2), a rotating and conveying device (4) is arranged on the inner wall of the annular drying box (2), rotating columns (5) are uniformly arranged on the left side and the right side of the inner wall of the annular drying box (2) along the circumferential direction of the inner wall, and an outer ring fan (6) and an outer ring gear (7) are sequentially installed on the rotating columns (5) from outside to inside;
the rotary conveying device (4) comprises connecting rods (41) symmetrically arranged on the left side and the right side of the rotating part (3), a rotary circular ring (42) is sleeved on each connecting rod (41), an annular limiting groove is formed in each rotary circular ring (42), an annular limiting frame (43) is arranged in each annular limiting groove in a sliding mode, each annular limiting frame (43) is fixed on the inner wall of each annular drying box (2), conveying mechanisms (44) are uniformly arranged between the rotary circular rings (42) on the left side and the right side of the rotating part (3), and each two conveying mechanisms (44) are connected with a position control rod (45) through pin shafts;
conveying mechanism (44) is including fixing erection column (441) between two rotation rings (42), install conveying frame (442) through the bearing on erection column (441), the front end of conveying frame (442) is open structure, the front end of conveying frame (442) is provided with branch chain (46) that opens and shuts, the inside of conveying frame (442) is provided with locking frame (443) that is U type structure, rear end locking groove has been seted up to the rear end of locking frame (443), the left and right sides of locking frame (443) evenly is provided with lateral wall locking groove, install rear side spring beam (444) on the inner wall of conveying frame (442) rear end, rear side locking plate (445) is installed to the front end of rear side spring beam (444), linkage frame (446) that is L type structure is evenly installed to the left and right sides symmetry of rear side locking plate (445), evenly be provided with ladder piece (447) on linkage frame (446), it is provided with lateral wall locking plate (448) to slide in the lateral wall locking groove, be connected with between lateral wall locking plate (448) and lateral wall locking groove and be connected with lateral wall (449), it leans on the pole (448) to lean on the linkage frame (446), it leans on to lean on pole (440) to support to lean.
2. A Ti/Ti0 according to claim 12The manufacturing method of the composite coating electrode is characterized by comprising the following steps: the rotary piece (3) comprises a driving motor (31) arranged on the outer wall of the left side of the annular drying box (2) through a motor base, an output shaft of the driving motor (31) extends to the inner side of the annular drying box (2) and is connected with the left end of the solid rod (32), the right end of the solid rod (32) is connected with an annular rotating frame (33), the right end of the annular rotating frame (33) is connected with the hollow rod (34), the hollow rod (34) is arranged on the annular drying box (2) through a bearing, a support rod (35) is arranged on the outer wall of the annular drying box (2), the support rod (35) penetrates through the hollow rod (34), a support ring (36) is arranged on the support rod (35), a rotary column (37) is arranged on the support ring (36) along the circumferential direction of the support ring, an inner ring fan (38) is arranged at the upper end of the rotary column (37, the inner ring bevel gear (39) is engaged with a driving bevel gear (310), and the driving bevel gear (310) is arranged on the inner wall of the annular rotating frame (33).
3. A Ti/Ti0 according to claim 12The manufacturing method of the composite coating electrode is characterized by comprising the following steps: open and shut branch chain (46) include open and shut board (461) through the hinge setting at conveying frame (442) front end downside, the fixed slot has been seted up on the open-ended last lateral wall of conveying frame (442) front end, the mounting groove has been seted up to the upside of open and shut board (461), install opening and shutting spring lever (462) in the mounting groove, opening and shutting frame (463) are installed to opening and shutting spring lever (462), be provided with control post (464) through the bearing on open and shut board (461), control post (464) extend to the mounting groove in and be located inside opening and shutting frame (463), be provided with eccentric disc (465) on control post (464), eccentric disc (465) support and lean on the lower extreme inner wall of open and shut board (461), install fixed column (466) on opening and shutting frame (463), fixed column (466).
4. A Ti/Ti0 according to claim 12The manufacturing method of the composite coating electrode is characterized by comprising the following steps: the conveying frame (442) and the locking frame (443) are uniformly provided with vent holes.
5. A Ti/Ti0 according to claim 12The manufacturing method of the composite coating electrode is characterized by comprising the following steps: the outer wall of the rotating circular ring (42) is sleeved with an operation gear, and the operation gear is meshed with the outer ring gear (7).
6. A Ti/Ti0 according to claim 12The manufacturing method of the composite coating electrode is characterized by comprising the following steps: the sections of the annular limiting frame (43) and the annular limiting groove are both T-shaped structures.
CN202010257439.8A 2020-04-03 2020-04-03 Ti/TiO2Method for manufacturing composite coating electrode Active CN111411349B (en)

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CN208116103U (en) * 2018-02-08 2018-11-20 福建惠安县惠兴工贸有限公司 A kind of coating drying equipment
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201757576U (en) * 2010-08-10 2011-03-09 海南大学 Rotating disk type electrothermal blast drying cabinet
CN203120929U (en) * 2013-03-07 2013-08-14 上海镧泰微波设备制造有限公司 Vacuum microwave drying device for grosvener siraitia
CN103602967A (en) * 2013-12-03 2014-02-26 淮南师范学院 Preparation method for novel high catalytic activity Ti/TiO2/Ce-PbO2 electrode
CN104708696A (en) * 2015-02-04 2015-06-17 天津百圣利亨钢木家具有限公司 Anticorrosive treatment apparatus of furniture sheets
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