CN111408332A - A multi-functional reation kettle for chemical industry purification - Google Patents
A multi-functional reation kettle for chemical industry purification Download PDFInfo
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- CN111408332A CN111408332A CN202010386595.4A CN202010386595A CN111408332A CN 111408332 A CN111408332 A CN 111408332A CN 202010386595 A CN202010386595 A CN 202010386595A CN 111408332 A CN111408332 A CN 111408332A
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- auger
- fixedly connected
- kettle
- box
- thick bamboo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a multifunctional reaction kettle for chemical purification, which comprises a kettle body and a kettle cover fixedly connected with the top of the kettle body through bolts, wherein the bottom of the kettle body is communicated with a discharge pipe, a valve is fixedly connected onto the discharge pipe, the top of the kettle cover is communicated with a feed pipe, the bottom of an inner cavity of the kettle body is respectively and fixedly connected with a base and an auger barrel, and the top of the base is movably connected with a filter cylinder. This a multifunctional reaction cauldron for chemical purification, through setting up the auger in auger section of thick bamboo cooperation it, can drive and get into the inside solution of auger section of thick bamboo and turn over upwards, reentrant is strained the interior back of section of thick bamboo and is opened outward, can reach the effect of stirring, and the comparatively thorough of stirring, and strain a section of thick bamboo and can reach filterable effect, can filter the purification to impurity in the solution or crystallization, the internal steam of cauldron then can be derived to the condensing box, both can be used to the concentration purification, also can be used to the distillation purification, make this reation kettle possess multiple functions, the commonality is stronger.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a multifunctional reaction kettle for chemical purification.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The reaction kettle is widely applied to pressure vessels for petroleum, chemical engineering, rubber, pesticides, dyes, medicines and foods, and is used for completing technological processes such as vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation and the like, such as a reactor, a reaction kettle, a decomposition kettle, a polymerization kettle and the like; the material is generally carbon manganese steel, stainless steel, zirconium, nickel-based (Hastelloy, Monel, Inconel) alloy and other composite materials.
Solution purification methods are various, including filtration, crystallization, concentration, distillation and the like, and are generally processed by adopting special processing equipment, while the existing reaction kettle is generally only a simple heatable container, has single function, cannot adapt to different types of purification methods, has poor universality, needs to be added with a plurality of sets of equipment, and increases the cost.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a multifunctional reaction kettle for chemical purification, which solves the problems that the existing reaction kettle is only a simple heatable container generally, has single function, cannot adapt to different types of purification modes and has poor universality.
In order to achieve the purpose, the invention is realized by the following technical scheme: the utility model provides a multi-functional reation kettle for chemical purification, passes through bolt fixed connection's kettle cover including the cauldron body and top, the bottom intercommunication of the cauldron body has the discharging pipe, and fixedly connected with valve on the discharging pipe, the top intercommunication of kettle cover has the inlet pipe, the bottom difference fixedly connected with base and an auger section of thick bamboo of cauldron internal chamber, and the top swing joint of base has a section of thick bamboo, the feed inlet has been seted up to the bottom of auger section of thick bamboo lateral wall, the inside of an auger section of thick bamboo is rotated and is connected with the auger, the top fixedly connected with guide housing of an auger section of thick bamboo, the guide housing is equipped with the opening towards one side of straining a section of thick bamboo, the top of auger center pin runs through the guide housing and extends to the top of guide housing.
Preferably, it all is provided with two to strain a section of thick bamboo and an auger section of thick bamboo, and crisscross setting each other, the top of kettle cover just is located an auger section of thick bamboo fixedly connected with transmission box, and the top fixedly connected with motor of right side transmission box.
Preferably, the bottom of motor output shaft runs through kettle cover and transmission box in proper order and with the top sliding connection of auger center pin, the surface of motor and the top of auger center pin all set up to assorted prism shape.
Preferably, the left side it has the prism axle to run through between the bottom of transmission box and the inside of kettle cover, and the bottom of prism axle and the top sliding connection of left side auger center pin, the equal fixedly connected with belt pulley in the inside that motor output shaft and prism axle just are located the transmission box, and is connected through belt transmission between two belt pulleys.
Preferably, the inside fixedly connected with spiral condenser pipe of condenser box, the right side intercommunication at condenser box top has the exhaust fan, the left end of spiral condenser pipe runs through condenser box and the cauldron body in proper order and extends to the upper right corner of cauldron internal chamber, the right-hand member of spiral condenser pipe runs through the lower right corner of condenser box and extends to the outside of condenser box.
Preferably, the surface of the cauldron body and the below fixedly connected with infrared electric heating jacket that is located the condensing box, the surface of the cauldron body and the top cover that is located infrared electric heating jacket are equipped with the insulation cover, and leave the space between insulation cover and the cauldron body, the intercommunication has the steam pipe between insulation cover and the condensing box.
Advantageous effects
The invention provides a multifunctional reaction kettle for chemical purification. Compared with the prior art, the method has the following beneficial effects:
(1) the multifunctional reaction kettle for chemical purification is characterized in that a base and an auger cylinder are respectively and fixedly connected to the bottom of an inner cavity of a kettle body, a filter cylinder is movably connected to the top of the base, a feed inlet is formed in the bottom of the side wall of the auger cylinder, an auger is rotatably connected to the inside of the auger cylinder, a guide cover is fixedly connected to the top of the auger cylinder, an opening is formed in one side, facing the filter cylinder, of the guide cover, the top end of a central shaft of the auger penetrates through the guide cover and extends to the upper part of the guide cover, a condensing box is fixedly connected to the top of the right side of the kettle body, the auger cylinder is matched with the auger in the auger cylinder to drive solution entering the auger cylinder to be overturned upwards and then to be scattered outwards after entering the filter cylinder, the stirring effect can be achieved, the stirring is thorough, the filter cylinder can achieve the filtering effect, impurities or crystals in the solution, the device can be used for concentration and purification and also can be used for distillation and purification, so that the reaction kettle has multiple functions and strong universality.
(2) The multifunctional reaction kettle for chemical purification is characterized in that a spiral condenser pipe is fixedly connected inside a condenser box, the right side of the top of the condenser box is communicated with an exhaust fan, the outer surface of a kettle body is fixedly connected with an infrared electric heating sleeve below the condenser box, the outer surface of the kettle body is sleeved with a heat insulation sleeve above the infrared electric heating sleeve, a gap is reserved between the heat insulation sleeve and the kettle body, a hot air pipe is communicated between the heat insulation sleeve and the condenser box, the infrared electric heating sleeve is arranged on the next shift part of the kettle body to heat only the next shift part, so that the waste of electric quantity caused by the fact that the solution in the kettle body is not full can be avoided, the exhaust fan at the top of the condenser box can absorb external cold air to enter the condenser box to condense the spiral condenser pipe, and the discharged hot air can be guided into the heat insulation sleeve at the upper half part of the kettle body through the hot air pipe to insulate the upper half part of the kettle body, the heat is reasonably utilized, the heat loss of the kettle body is reduced, and the energy is saved.
Drawings
FIG. 1 is a cross-sectional view of a structure of the present invention;
FIG. 2 is a front view of the structure of the present invention;
FIG. 3 is a top view of the pod and feed tube arrangement of the present invention;
FIG. 4 is a top view of the auger barrel and filter cartridge distribution structure of the present invention;
fig. 5 is a sectional view of the condensation tank of the present invention.
In the figure: 1-kettle body, 2-kettle cover, 3-discharge pipe, 4-feed pipe, 5-base, 6-auger cylinder, 7-filter cylinder, 8-auger, 9-guide cover, 10-condensation box, 11-transmission box, 12-motor, 13-prism shaft, 14-belt pulley, 15-belt, 16-spiral condensation pipe, 17-exhaust fan, 18-infrared electric heating jacket, 19-heat preservation jacket and 20-hot air pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-5, the present invention provides a technical solution: a multifunctional reaction kettle for chemical purification comprises a kettle body 1 and a kettle cover 2 fixedly connected with the top of the kettle body through bolts, an infrared electric heating sleeve 18 is fixedly connected with the outer surface of the kettle body 1 and is positioned below a condensing box 10, a heat insulation sleeve 19 is sleeved on the outer surface of the kettle body 1 and is positioned above the infrared electric heating sleeve 18, a gap is reserved between the heat insulation sleeve 19 and the kettle body 1, a hot air pipe 20 is communicated between the heat insulation sleeve 19 and the condensing box 10, the infrared electric heating sleeve 18 is arranged on the next shift part of the kettle body 1 to heat only the next shift part, so that the waste of electric quantity caused by the fact that the solution in the kettle body 1 is not full can be avoided, an exhaust fan 17 at the top of the condensing box 10 can suck external cold air to enter the condensing box 10 to condense a spiral condensing pipe 16, the exhausted hot air can be guided into the heat insulation sleeve 19 at the upper half part of the kettle body 1 through the hot air pipe 20 to insulate the upper half part of the kettle body 1, the heat is reasonably utilized, the heat loss of the kettle body 1 is reduced, energy is saved, the bottom of the kettle body 1 is communicated with a discharge pipe 3, a valve is fixedly connected to the discharge pipe 3, the top of a kettle cover 2 is communicated with a feed pipe 4, the bottom of an inner cavity of the kettle body 1 is respectively and fixedly connected with a base 5 and an auger cylinder 6, the top of the base 5 is movably connected with a filter cylinder 7, the filter cylinder 7 and the auger cylinder 6 are respectively provided with two parts which are arranged in a mutually staggered manner, the top of the kettle cover 2 is fixedly connected with a transmission box 11 right above the auger cylinder 6, the top of a right side transmission box 11 is fixedly connected with a motor 12, the bottom of an output shaft of the motor 12 sequentially penetrates through the kettle cover 2 and the transmission box 11 and is in sliding connection with the top of a central shaft of the auger 8, the surface of the motor 12 and the top of the central shaft of the auger 8 are both arranged in a matched prism shape, the bottom end of the prism shaft 13 is connected with the top end of the central shaft of the packing auger 8 at the left side in a sliding way, belt pulleys 14 are fixedly connected with the surfaces of the output shaft of the motor 12 and the prism shaft 13 and positioned in the transmission box 11, the two belt pulleys 14 are connected with each other in a transmission way through a belt 15, a feed inlet is arranged at the bottom of the side wall of the packing auger cylinder 6, the packing auger 8 is rotatably connected with the inside of the packing auger cylinder 6, a guide cover 9 is fixedly connected with the top of the packing auger cylinder 6, an opening is arranged at one side of the guide cover 9 facing the filter cartridge 7, the top end of the central shaft of the packing auger 8 penetrates through the guide cover 9 and extends to the upper part of the guide cover 9, a condensation box 10 is fixedly connected with the top at the right side of the kettle body 1, the solution entering the packing auger cylinder 6 can be driven to be overtur, and strain a section of thick bamboo 7 and can reach filterable effect, can filter the purification to impurity or crystallization in the solution, condensing box 10 then can derive the internal steam of cauldron 1, both can be used to the concentration purification, also can be used to the distillation purification, make this reation kettle possess multiple functions, the commonality is stronger, the inside fixedly connected with spiral condenser pipe 16 of condensing box 10, the right side intercommunication at condensing box 10 top has exhaust fan 17, the left end of spiral condenser pipe 16 runs through condensing box 10 and cauldron body 1 in proper order and extends to the upper right corner of cauldron body 1 inner chamber, the right-hand member of spiral condenser pipe 16 runs through the lower right corner of condensing box 10 and extends to the outside of condensing box 10.
And those not described in detail in this specification are well within the skill of those in the art.
When the device is used, a solution is poured into the kettle body 1 through the feeding pipe 4, then the feeding pipe 4 is sealed, the motor 12 and the infrared electric heating sleeve 18 are started, the infrared electric heating sleeve 18 heats the kettle body 1, the motor 12 drives the auger 8 and the belt pulley 14 on the right side to rotate, the belt 15 is utilized to drive the belt pulley 14 on the left side to rotate, the auger 8 on the left side is further synchronously rotated, the solution in the auger cylinder 6 is pushed upwards, meanwhile, the solution outside the auger cylinder 6 enters the auger cylinder 6 from the bottom, the solution pushed upwards is fed into the filter cylinder 7 through the guide cover 9, then flows out of the filter cylinder 7 after being filtered by the filter cylinder 7, and at the moment, the effect of filtering and purifying can be achieved; simultaneously, moisture in the solution can evaporate, and discharge through spiral condenser pipe 16, can reach the effect of concentrated purification, if the solution needs the distillation purification, exhaust fan 17 can be started, steam gets into back in the spiral condenser pipe 16, exhaust fan 17 cools off spiral condenser pipe 16 in discharging into the condensing box 10 with the outside air, the solution after the condensation flows from spiral condenser pipe 16 right-hand member, and hot-air passes through in hot-air pipe 20 gets into insulation cover 19, keep warm to cauldron body 1, open the valve on the discharging pipe after the purification, discharge solution, and open kettle cover 2, will strain a section of thick bamboo 7 and propose the waste residue of clearing up its inside straining.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. The utility model provides a multi-functional reation kettle for chemical purification, passes through bolt fixed connection's kettle cover (2) including the cauldron body (1) and top thereof, the bottom intercommunication of the cauldron body (1) has discharging pipe (3), and fixedly connected with valve on discharging pipe (3), the top intercommunication of kettle cover (2) has inlet pipe (4), its characterized in that: the bottom of the cauldron body (1) inner chamber is fixedly connected with base (5) and auger section of thick bamboo (6) respectively, and the top swing joint of base (5) has a section of thick bamboo (7) of straining, the feed inlet has been seted up to the bottom of auger section of thick bamboo (6) lateral wall, the inside of auger section of thick bamboo (6) is rotated and is connected with auger (8), the top fixedly connected with guide housing (9) of auger section of thick bamboo (6), one side that guide housing (9) were strained to the orientation is equipped with the opening, the top of auger (8) center pin runs through guide housing (9) and extends to the top of guide housing (9), top fixedly connected with condensing box (10) on cauldron body (1) right side.
2. The multifunctional reaction kettle for chemical purification according to claim 1, wherein: the filter cartridge (7) and the auger cylinder (6) are both provided with two parts and are arranged in a staggered mode, the top of the kettle cover (2) is located directly above the auger cylinder (6) and is fixedly connected with a transmission box (11), and the top of the right transmission box (11) is fixedly connected with a motor (12).
3. The multifunctional reaction kettle for chemical purification according to claim 2, wherein: the bottom of motor (12) output shaft runs through kettle cover (2) and transmission box (11) in proper order and with the top sliding connection of auger (8) center pin, the surface of motor (12) and the top of auger (8) center pin all set up to assorted prism shape.
4. The multifunctional reaction kettle for chemical purification according to claim 2, wherein: left side it has prism axle (13) to run through between the bottom of transmission box (11) and the inside of kettle cover (2), and the top sliding connection of the bottom of prism axle (13) and left side auger (8) center pin, the equal fixedly connected with belt pulley (14) in the inside that motor (12) output shaft and prism axle (13) just are located transmission box (11), and is connected through belt (15) transmission between two belt pulley (14).
5. The multifunctional reaction kettle for chemical purification according to claim 1, wherein: the inside fixedly connected with spiral condenser pipe (16) of condenser box (10), the right side intercommunication at condenser box (10) top has exhaust fan (17), the left end of spiral condenser pipe (16) runs through condenser box (10) and the cauldron body (1) in proper order and extends to the upper right corner of the cauldron body (1) inner chamber, the right-hand member of spiral condenser pipe (16) runs through the lower right corner of condenser box (10) and extends to the outside of condenser box (10).
6. The multifunctional reaction kettle for chemical purification according to claim 1, wherein: the surface of the cauldron body (1) just is located the infrared electric heating jacket (18) of below fixedly connected with of condensing box (10), the surface of the cauldron body (1) just is located the top cover of infrared electric heating jacket (18) and is equipped with insulation cover (19), and leaves the space between insulation cover (19) and the cauldron body (1), the intercommunication has steam pipe (20) between insulation cover (19) and condensing box (10).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010386595.4A CN111408332A (en) | 2020-05-09 | 2020-05-09 | A multi-functional reation kettle for chemical industry purification |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010386595.4A CN111408332A (en) | 2020-05-09 | 2020-05-09 | A multi-functional reation kettle for chemical industry purification |
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| Publication Number | Publication Date |
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| CN111408332A true CN111408332A (en) | 2020-07-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202010386595.4A Pending CN111408332A (en) | 2020-05-09 | 2020-05-09 | A multi-functional reation kettle for chemical industry purification |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114870764A (en) * | 2022-05-17 | 2022-08-09 | 陈卫 | Catalytic cracking catalyst preparation equipment |
| CN117138429A (en) * | 2023-10-26 | 2023-12-01 | 内蒙古东景生物环保科技有限公司 | Control device for concentrating filter to extract clear liquid and turbid liquid |
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| CN208901841U (en) * | 2018-07-25 | 2019-05-24 | 营口建科玄武岩纤维研究所 | A kind of basalt mine material deironing device |
| CN209065864U (en) * | 2018-10-11 | 2019-07-05 | 杭州人合农业科技有限公司 | A kind of essential oil distillation extraction element |
| CN210215202U (en) * | 2019-07-12 | 2020-03-31 | 济宁市圣奥精细化工有限公司 | 1-aminoanthraquinone rectifier unit |
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2020
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003213032A (en) * | 2001-11-14 | 2003-07-30 | Minoru Suzuki | Dissolving and recycling device of synthetic resin |
| CN206435179U (en) * | 2016-12-08 | 2017-08-25 | 福建省梦娇兰日用化学品有限公司 | The convenient deimpurity reactor of filter of one kind |
| CN208901841U (en) * | 2018-07-25 | 2019-05-24 | 营口建科玄武岩纤维研究所 | A kind of basalt mine material deironing device |
| CN209065864U (en) * | 2018-10-11 | 2019-07-05 | 杭州人合农业科技有限公司 | A kind of essential oil distillation extraction element |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114870764A (en) * | 2022-05-17 | 2022-08-09 | 陈卫 | Catalytic cracking catalyst preparation equipment |
| CN117138429A (en) * | 2023-10-26 | 2023-12-01 | 内蒙古东景生物环保科技有限公司 | Control device for concentrating filter to extract clear liquid and turbid liquid |
| CN117138429B (en) * | 2023-10-26 | 2024-01-26 | 内蒙古东景生物环保科技有限公司 | Control device for concentrating filter to extract clear liquid and turbid liquid |
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Application publication date: 20200714 |