CN212236024U - Environment-friendly chemical distillation plant - Google Patents
Environment-friendly chemical distillation plant Download PDFInfo
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- CN212236024U CN212236024U CN202020419085.8U CN202020419085U CN212236024U CN 212236024 U CN212236024 U CN 212236024U CN 202020419085 U CN202020419085 U CN 202020419085U CN 212236024 U CN212236024 U CN 212236024U
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- 238000004821 distillation Methods 0.000 title claims abstract description 78
- 239000000126 substance Substances 0.000 title claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 32
- 239000007787 solid Substances 0.000 claims description 13
- 238000005485 electric heating Methods 0.000 claims description 10
- 238000009833 condensation Methods 0.000 claims description 5
- 230000005494 condensation Effects 0.000 claims description 5
- 230000029058 respiratory gaseous exchange Effects 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 abstract description 8
- 230000003670 easy-to-clean Effects 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 8
- 238000009835 boiling Methods 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000010977 unit operation Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model provides an environment-friendly chemical distillation device, which comprises a distillation still, a feed inlet, a suction pipe is fixedly connected with the upper end of the left side of the distillation still, a vacuum pump is fixedly connected with the other end of the suction pipe, a discharge conduit is fixedly connected with the upper end of the right side of the distillation still, a solenoid valve is arranged on the left side of the upper end of the discharge conduit, a condenser pipe is sleeved on the upper end of the discharge conduit, a feed inlet is arranged on the left side of the central position of the top of the distillation still, a motor is fixedly connected with the central position of the top of the distillation still, a motor output shaft extends into a connecting shaft fixedly connected with the distillation still, stirring impellers are fixedly connected with the left side and the right side of the connecting shaft in sequence at equal intervals from top to bottom, a fixed cylinder, the utility model provides an environment-friendly chemical distillation device, which solves the problem that the existing distillation kettle is not easy to clean.
Description
Technical Field
The utility model relates to a chemical industry equipment technical field especially relates to an environment-friendly chemical industry distillation plant.
Background
Distillation is a thermodynamic separation process that utilizes the difference in boiling points of components in a mixed liquid or liquid-solid system to vaporize lower boiling components and recondense to separate the entire component, a unit operation that combines the two unit operations of evaporation and condensation. Compared with other separation means, such as extraction, filtration crystallization and the like, the method has the advantages that other solvents except system components are not needed, so that new impurities cannot be introduced, in chemical production, impurities are often removed from raw materials, then chemical reaction can be carried out, meanwhile, a product is purified through distillation, and a distillation device is needed in the production processes.
Based on the above description, and retrieve an application number: CN201820606537.6, it relates to a chemical distillation device, including distillation column (1), its characterized in that: be equipped with distillation chamber (2) in distillation column (1), be equipped with (mixing) shaft (3) in distillation chamber (2), condenser (17) downside is equipped with inlet tube (20), and condenser (17) upside is equipped with outlet pipe (21). Mainly through setting up air exhaust device and pressure sensor, can make and be in stable negative pressure state in the distillation chamber, and then reduced the boiling point of solution, reduced the energy resource consumption among the distillation process, still be equipped with temperature sensor and heat preservation device in addition, can effectually reduce thermal loss, still be equipped with agitating unit simultaneously, can be so that the reaction is even more rapid to reach the purpose of sparingly consuming.
After retrieval and analysis, the existing chemical distillation device needs to be cleaned regularly, and the interior of the distillation kettle is not thoroughly cleaned only by stirring with the stirring shaft, so that the chemical distillation device needs to be further researched, and the environment-friendly chemical distillation device is provided.
SUMMERY OF THE UTILITY MODEL
In order to solve the technical problem, the utility model provides an environment-friendly chemical distillation device to solve the difficult abluent problem of current stills.
The utility model relates to an environment-friendly chemical industry distillation plant's purpose and efficiency is reached by following concrete technical means: an environment-friendly chemical distillation device comprises a distillation kettle, a feed inlet, a first slide block, a solenoid valve, a condenser pipe, a water inlet, a water outlet, a discharge conduit, a collection tank, a heat collection box, a fixed cylinder, a first slide groove, a water outlet pipe, a second slide block, a distillation box, an electric heating pipe, a cylinder, a second slide groove, a screw cover, a vacuum pump, an air suction pipe, a first motor, a connecting shaft, a stirring impeller and a second motor, wherein the upper end of the left side of the distillation kettle is fixedly connected with the air suction pipe, the other end of the air suction pipe is fixedly connected with the vacuum pump, the upper end of the right side of the distillation kettle is fixedly connected with the discharge conduit, the left side of the upper end of the discharge conduit is provided with the solenoid valve, the upper end of the discharge conduit is sleeved with the condenser pipe, the left side of, the left side of stills top central point puts and is equipped with the feed inlet, stills top central point puts a fixedly connected with motor, a motor output shaft extends to the interior fixedly connected with connecting axle of stills, the connecting axle left and right sides is from last to the equidistant fixedly connected with impeller down in proper order, stills bottom central point puts the solid fixed cylinder of fixedly connected with, the inside cavity position joint of solid fixed cylinder has the outlet pipe, outlet pipe top fixedly connected with distillation retort, stills top right side is equipped with pressure sensor, temperature sensor.
Preferably, the distillation box is round platform form, and the distillation box outside is from last to having cup jointed the dress electric heating pipe down, and distillation box top fixedly connected with drum, drum outside center are equipped with the spout No. two, and the inboard upper end fixedly connected with slider of stills corresponds the joint with the spout No. two.
Preferably, the right side of the bottom in the distillation kettle is fixedly connected with a second motor, the upper end of an output shaft of the second motor is sleeved with a flange plate, the upper end of a water outlet pipe is sleeved with a flange plate, and the flange plate is connected with a flange plate synchronous belt on the upper end of the output shaft of the second motor.
Preferably, the upper end of the air suction pipe is provided with a valve.
Preferably, the outlet pipe is located the fixed cylinder inside and outside fixedly connected with slider No. two, is equipped with the spout No. one in the fixed cylinder, and slider No. two corresponds the joint with the fixed cylinder.
Preferably, the outer side of the fixed cylinder is provided with a thread groove, and the outer side of the fixed cylinder is in threaded connection with a screw cap.
Preferably, the bottom of the heat collection box is provided with a connecting pipe, and the upper end of the connecting pipe is clamped with a water pump.
Has the advantages that:
(1) the utility model discloses the ring flange has been cup jointed on outlet pipe outside upper end, and the ring flange is connected with No. two motor upper end output shaft ring flange hold-in ranges, drives the outlet pipe and rotates after starting No. two motors to drive the distillation case and rotate, start a motor simultaneously, a motor drives the connecting axle and rotates with impeller, adds washing liquid and clear water through the feed inlet and then can thoroughly wash the distillation case, open at last screw cap put out after the washing water can, it is convenient to wash, do not influence next distillation operation.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention.
Fig. 2 is a schematic diagram of the structure of the distillation still of the present invention.
Fig. 3 is a schematic side view structure diagram of the distillation box of the present invention.
Fig. 4 is an enlarged schematic view of fig. 2A according to the present invention.
Fig. 5 is an enlarged schematic structural diagram of fig. 2B according to the present invention.
In fig. 1-5, the correspondence between the component names and the reference numbers is:
the device comprises a distillation kettle 1, a feed inlet 101, a first slide block 102, an electromagnetic valve 2, a condenser pipe 3, a water inlet 301, a water outlet 302, a discharge guide pipe 4, a collection tank 5, a heat collection box 6, a fixed cylinder 7, a first sliding groove 701, a water outlet pipe 8, a second slide block 801, a distillation box 9, an electric heating pipe 901, a cylinder 902, a second sliding groove 903, a screw cap 10, a vacuum pump 11, an air suction pipe 12, a first motor 13, a connecting shaft 14, a stirring impeller 1401 and a second motor 15.
Detailed Description
The technical solution in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person of ordinary skill in the art without creative work belong to the protection scope of the present invention based on the embodiments of the present invention.
Example (b):
as shown in figures 1 to 5: an environment-friendly chemical distillation device comprises a distillation kettle 1, a feed inlet 101, a first slide block 102, an electromagnetic valve 2, a condenser pipe 3, a water inlet 301, a water outlet 302, a discharge conduit 4, a collection tank 5, a heat collection box 6, a fixed cylinder 7, a first slide groove 701, a water outlet pipe 8, a second slide block 801, a distillation box 9, an electric heating pipe 901, a cylinder 902, a second slide groove 903, a screw cover 10, a vacuum pump 11, an air suction pipe 12, a first motor 1401, a connecting shaft 14, a stirring impeller and a second motor 15, wherein the upper end of the left side of the distillation kettle 1 is fixedly connected with the air suction pipe 12, the other end of the air suction pipe 12 is fixedly connected with the vacuum pump 11, the upper end of the right side of the distillation kettle 1 is fixedly connected with the discharge conduit 4, the electromagnetic valve 2 is arranged on the left side of the upper end of the discharge conduit 4, the condenser pipe 3, delivery port 302 bottom fixedly connected with heat collection box 6, 4 right side end fixedly connected with collection tank 5 of ejection of compact pipe, 5 right side lower extremes of collection tank are equipped with the discharge gate, 1 top central point of stills puts the left side and is equipped with feed inlet 101, stills 1 top central point puts a fixedly connected with motor 13, a motor 13 output shaft extends to stills 1 interior fixedly connected with connecting axle 14, connecting axle 14 left and right sides is from last to equidistant fixedly connected with impeller 1401 down in proper order, stills 1 bottom central point fixedly connected with solid fixed cylinder 7, the inside cavity position joint of solid fixed cylinder 7 has outlet pipe 8, outlet pipe 8 top fixedly connected with distillation case 9, stills 1 top right side is equipped with pressure sensor, temperature sensor.
Wherein: the distilling box 9 is in a circular truncated cone shape, the outer side of the distilling box 9 is sleeved with an electric heating pipe 901 from top to bottom, the top of the distilling box 9 is fixedly connected with a cylinder 902, the center of the outer side of the cylinder 902 is provided with a second sliding groove 903, the upper end of the inner side of the distilling kettle 1 is fixedly connected with a first sliding block 102, the first sliding block 102 is correspondingly clamped with the second sliding groove 903, the electric heating pipe 901 enables the distilling box 9 to be fully covered, the heating speed is high, and the distilling efficiency is improved, when the distilling kettle 1 needs to be cleaned, a second motor 15 can be started, the second motor 15 drives a water outlet pipe 8 to rotate so as to drive the distilling box 9 to rotate, the first sliding block 102 rotates in the second sliding groove 903 so as to improve the stability in the rotating process of the distilling box 9, the first motor 13 is started simultaneously, the first motor 13 drives a connecting shaft 14 and a stirring, finally, the screw cap 10 is opened to discharge the cleaned water, so that the cleaning is convenient, and the next distillation operation is not influenced.
Wherein: no. two motors 15 of bottom right side fixedly connected with in stills 1, the ring flange has been cup jointed to No. two 15 output shafts of motor, and the ring flange has been cup jointed to 8 upper ends of outlet pipe, and the ring flange is connected with No. two 15 output shaft upper end ring flange hold-in ranges, can drive distillation box 9 through No. two motors 15 and rotate to make the inside washing of distillation box 9 convenient.
Wherein: the upper end of the air suction pipe 12 is provided with a valve, the upper end valve of the air suction pipe 12 is opened, the vacuum pump 11 is started to suck the air in the distillation kettle 1 through the air suction pipe 12, so that the pressure in the distillation kettle 1 is lowered, the boiling point of liquid is reduced, the liquid distillation efficiency is higher, the consumption during distillation is saved, and the distillation kettle is more environment-friendly.
Wherein: the outlet pipe 8 is located No. two slider 801 of solid fixed cylinder 7 inside and outside fixedly connected with, is equipped with spout 701 in the solid fixed cylinder 7, and No. two slider 801 correspond the joint with solid fixed cylinder 7, and No. two motors 15 drive outlet pipe 8 and rotate for No. two slider 801 is at spout 701 internal rotation, thereby improves the stability when outlet pipe 8 rotates.
Wherein: the outside of the fixed cylinder 7 is provided with a thread groove, the outside of the fixed cylinder 7 is in threaded connection with a screw cap 10, and the screw cap 10 is convenient to mount and dismount during cleaning.
Wherein: the bottom of the heat collecting box 6 is provided with a connecting pipe, the upper end of the connecting pipe is clamped with a water pump, and water after heat absorption is extracted to a using place through the water pump 6 to be reused.
Wherein: the first motor 13, the second motor 15, the vacuum pump 11, the water pump, the electric heating pipe 901 and the electromagnetic valve 2 are all connected with an external power supply.
The working principle is as follows: putting liquid into a distillation kettle 1 through a feed inlet 101, enabling the liquid to fall into a distillation box 9, blocking the feed inlet 101, opening a valve at the upper end of an air suction pipe 12, opening a vacuum pump 11 to draw air in the distillation kettle 1, stopping after matching with the induction of a pressure sensor and a certain value of internal pressure, then opening an electric heating pipe 901 to enable the interior to carry out distillation operation, simultaneously opening a motor 13 to drive a connecting shaft 14 and a stirring impeller 1401 to rotate, accelerating the distillation efficiency, after inducing the temperature sensor to a boiling point, opening an electromagnetic valve 2, outputting steam through a discharge conduit 4, simultaneously, enabling cold water to enter a condensation pipe 3 through a water inlet 301, entering a heat collection tank 6 through a water outlet 302, pumping the heat-absorbed water to a using place through a water pump 6 in the heat collection tank 6 for recycling, enabling the condensed liquid to enter a collection tank 5, and driving a water outlet pipe 8 to rotate after starting, thereby drive the distillation case 9 and rotate, start a motor 13 simultaneously, a motor 13 drives connecting axle 14 and impeller 1401 and rotates, adds washing liquid and clear water through feed inlet 101 and then can thoroughly wash distillation case 9, opens screw cap 10 at last and discharges the water after the washing can, and it is convenient to wash, does not influence next distillation operation.
Claims (7)
1. The utility model provides an environment-friendly chemical industry distillation plant, including stills (1), feed inlet (101), slider (102), solenoid valve (2), condenser pipe (3), water inlet (301), delivery port (302), ejection of compact pipe (4), collection tank (5), heat collecting box (6), solid fixed cylinder (7), spout (701), outlet pipe (8), slider (801) No. two, distillation retort (9), electric heating pipe (901), drum (902), spout (903) No. two, twist cap (10), vacuum pump (11), breathing pipe (12), motor (13), connecting axle (14), impeller (1401), motor (15) No. two, its characterized in that: the vacuum distillation kettle is characterized in that an air suction pipe (12) is fixedly connected to the upper end of the left side of the distillation kettle (1), a vacuum pump (11) is fixedly connected to the other end of the air suction pipe (12), a discharge pipe (4) is fixedly connected to the upper end of the right side of the distillation kettle (1), an electromagnetic valve (2) is arranged on the left side of the upper end of the discharge pipe (4), a condensation pipe (3) is sleeved on the upper end of the discharge pipe (4), a water inlet (301) is arranged on the left side of the upper end of the condensation pipe (3), a water outlet (302) is arranged on the right side of the lower end of the condensation pipe (3), a heat collecting box (6) is fixedly connected to the bottom of the water outlet (302), a collecting tank (5) is fixedly connected to the right end of the discharge pipe (4), a discharge port is arranged on the lower end, a motor (13) output shaft extends to fixedly connected with connecting axle (14) in stills (1), the connecting axle (14) left and right sides is from last to equidistant fixedly connected with impeller (1401) down in proper order, stills (1) bottom central point puts fixedly connected with solid fixed cylinder (7), the inside cavity position joint of solid fixed cylinder (7) has outlet pipe (8), outlet pipe (8) top fixedly connected with distillation retort (9), stills (1) top right side is equipped with pressure sensor, temperature sensor.
2. The environment-friendly chemical distillation device according to claim 1, wherein: distilling box (9) are round platform form, distilling box (9) outside from last to having cup jointed ring dress electric heating pipe (901) down, distilling box (9) top fixedly connected with drum (902), drum (902) outside center is equipped with spout (903) No. two, No. one slider (102) of still (1) inboard upper end fixedly connected with, No. one slider (102) corresponds the joint with spout (903) No. two.
3. The environment-friendly chemical distillation device according to claim 1, wherein: bottom right side fixedly connected with No. two motor (15) in stills (1), the ring flange has been cup jointed on No. two motor (15) output shaft, the ring flange has been cup jointed on outlet pipe (8) upper end, and the ring flange is connected with No. two motor (15) output shaft upper end ring flange hold-in range.
4. The environment-friendly chemical distillation device according to claim 1, wherein: the upper end of the air suction pipe (12) is provided with a valve.
5. The environment-friendly chemical distillation device according to claim 1, wherein: outlet pipe (8) are located No. two slider (801) of solid fixed cylinder (7) inside and outside fixedly connected with, be equipped with spout (701) in gu fixed cylinder (7), No. two slider (801) correspond the joint with solid fixed cylinder (7).
6. The environment-friendly chemical distillation device according to claim 1, wherein: the outer side of the fixed cylinder (7) is provided with a thread groove, and the outer side of the fixed cylinder (7) is in threaded connection with a screw cap (10).
7. The environment-friendly chemical distillation device according to claim 1, wherein: the bottom of the heat collection box (6) is provided with a connecting pipe, and the upper end of the connecting pipe is clamped with a water pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020419085.8U CN212236024U (en) | 2020-03-27 | 2020-03-27 | Environment-friendly chemical distillation plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020419085.8U CN212236024U (en) | 2020-03-27 | 2020-03-27 | Environment-friendly chemical distillation plant |
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| Publication Number | Publication Date |
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| CN212236024U true CN212236024U (en) | 2020-12-29 |
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|---|---|---|---|
| CN202020419085.8U Active CN212236024U (en) | 2020-03-27 | 2020-03-27 | Environment-friendly chemical distillation plant |
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| CN (1) | CN212236024U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842855A (en) * | 2021-09-01 | 2021-12-28 | 齐齐哈尔大学 | Chemical raw material separation tower |
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2020
- 2020-03-27 CN CN202020419085.8U patent/CN212236024U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842855A (en) * | 2021-09-01 | 2021-12-28 | 齐齐哈尔大学 | Chemical raw material separation tower |
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Effective date of registration: 20210508 Address after: 344000 Dongshan plate, Donghui Industrial Park, Dongxiang Economic Development Zone, Fuzhou City, Jiangxi Province Patentee after: Jiangxi Yufan bioenergy Co.,Ltd. Address before: 232000 No.78, Xinhuai Road, tianjia'an District, Huainan City, Anhui Province Patentee before: Zhang Hui |