CN111407695A - Sea-buckthorn water and preparation method and application thereof - Google Patents
Sea-buckthorn water and preparation method and application thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The invention discloses sea-buckthorn water which is extracted from sea-buckthorn plants. The invention also discloses a preparation method of the sea buckthorn water, which is implemented according to the following steps: step 1, cleaning and pretreating sea buckthorn plants; and 2, extracting the raw materials obtained in the step 1 to obtain the sea buckthorn water. The fructus Hippophae water has effects of keeping moisture, preventing ultraviolet burn, repairing skin, whitening skin, resisting oxidation, and inhibiting skin melanin deposition. The research on sea buckthorn mostly focuses on the preparation and application of sea buckthorn oil. Compared with the seabuckthorn oil, the extraction and preparation of the seabuckthorn water are rarely researched, the seabuckthorn water is prepared by a supercritical carbon dioxide method, and the gap of preparation and research of the seabuckthorn water is filled.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to sea buckthorn water, and a preparation method and application of the sea buckthorn water.
Background
Sea-buckthorn (Hippophae rhamnoides L.) is a plant of the genus Hippophae in the family elaeageae, is drought-resistant and sand-resistant, and is an economic plant with multiple purposes in northwest plateaus, sea-buckthorn fruits are also homologous plants of medicine and food, roots, stems, leaves, flowers and fruits, particularly sea-buckthorn fruits contain rich nutrient substances and bioactive substances, the sea-buckthorn fruits have the effects of relieving cough and reducing sputum, invigorating stomach and promoting digestion, and activating blood circulation to dissipate blood stasis when used as medicines, sea-buckthorn seeds also contain various substances beneficial to human bodies, and the sea-buckthorn seed oil extracted from the sea-buckthorn seeds has application in various fields.
To investigate other effects of the aqueous solution, the company studied it. Extracting the sea buckthorn water by adopting a proper method aiming at different parts of the sea buckthorn, and researching the biological activity of the sea buckthorn water.
Disclosure of Invention
The invention aims to provide the sea buckthorn water which has the effects of delaying senescence, brightening skin, moistening skin, inhibiting bacteria, diminishing inflammation and removing acnes and can effectively solve the problems of dry skin, darkness, ageing and acne marks.
The second purpose of the invention is to provide a preparation method of the sea buckthorn water.
The third purpose of the invention is to provide the application of the sea buckthorn water.
The first technical scheme adopted by the invention is as follows: a fructus Hippophae water is prepared from fructus Hippophae plant by extracting.
The second technical scheme adopted by the invention is as follows: a preparation method of sea buckthorn water is specifically implemented according to the following steps:
and 2, extracting the raw materials obtained in the step 1 to obtain the sea buckthorn water.
The invention adopting the second technical proposal is also characterized in that,
the seabuckthorn plants in the step 1 comprise seabuckthorn seeds, dried seabuckthorn fruits, fresh seabuckthorn fruits, seabuckthorn leaves and seabuckthorn stems.
The pretreatment process of the sea buckthorn seeds or the dried sea buckthorn fruits in the step 1 is crushing and embryo pressing, the thickness of each piece is 0.3-0.5 mm, and the fine powder smaller than 18 meshes and smaller than 18 meshes after crushing does not exceed 10% of the total mass.
And 2, extracting the sea-buckthorn seeds/dried sea-buckthorn fruits by adopting supercritical carbon dioxide, extracting the fresh sea-buckthorn fruits by adopting a squeezing method, and extracting the sea-buckthorn leaves and the sea-buckthorn stems by adopting an azeotropic distillation method.
The invention adopts a third technical scheme that the invention is an application of sea buckthorn water in the field of cosmetics.
The invention has the beneficial effects that: the fructus Hippophae water has effects of keeping moisture, preventing ultraviolet burn, repairing skin, whitening skin, resisting oxidation, and inhibiting skin melanin deposition. The research on sea buckthorn mostly focuses on the preparation and application of sea buckthorn oil. Compared with the seabuckthorn oil, the extraction and preparation of the seabuckthorn water are rarely researched, the seabuckthorn water is prepared by a supercritical carbon dioxide method, and the gap of preparation and research of the seabuckthorn water is filled.
Drawings
FIG. 1 is a flow chart of the preparation of sea buckthorn water according to the present invention;
FIG. 2 is a graph showing the effect of extraction temperature and extraction pressure on extraction rate according to the present invention;
FIG. 3 is a graph showing the effect of extraction pressure and extraction time on extraction yield according to the present invention;
FIG. 4 is a graph showing the effect of extraction time and carbon dioxide flow rate on extraction rate according to the present invention;
FIG. 5 is a comparison of the face of a patient before 1 week, after 3 weeks and after recovery from the application of sea buckthorn water of the present invention;
FIG. 6 is a graph of the effect of sea buckthorn water on the rate of apoptosis of HaCaT cells by UVC radiation;
fig. 7 is a comparison of facial moisture content of the mask prepared using the present invention for the control group and the test group.
Detailed Description
The invention is further described with reference to the following figures and detailed description.
The invention relates to sea buckthorn water which is obtained by extracting and separating sea buckthorn plants. The method for preparing the sea buckthorn water from different parts of the sea buckthorn plant comprises the following steps:
the preparation method for extracting the sea buckthorn water from the sea buckthorn seeds or the dried sea buckthorn fruits is implemented according to the following steps:
And 3, performing primary separation on the substance extracted in the step 2 under the conditions that the pressure is 100-110 bar and the temperature is 45-50 ℃, performing secondary separation under the conditions that the pressure is 50-55 bar and the temperature is 30-35 ℃, and standing and separating the oil-water substance obtained by separation under the conditions that the temperature is 40-45 ℃ and the time is 5 hours to obtain the sea buckthorn water.
(II) the preparation method of the sea-buckthorn water in the fresh sea-buckthorn fruits is implemented according to the following steps:
squeezing fresh fructus Hippophae to obtain juice, centrifuging the juice in a centrifuge at 3000r/min for more than 10min, standing to obtain upper layer, rotary evaporating the upper layer solution at 45 deg.C, 40r/min and 0.1Mpa, and collecting distilled water to obtain the final product.
(III) the preparation method of the sea buckthorn water in the sea buckthorn leaves/sea buckthorn stems is implemented according to the following steps:
adding folium Hippophae and xylene at a mass ratio of 1:10 into an industrial distillation device, adjusting temperature at a heating rate of 2 deg.C/min, collecting the effluent when the temperature reaches azeotropic point of 92 deg.C, heating at constant temperature, and stopping heating when the temperature of azeotrope steam changes. Weighing the collected azeotrope, respectively placing the azeotrope in a liquid separating device, standing for layering, collecting a water sample after layering, weighing and calculating the water content of the water sample to obtain the sea buckthorn water,
as shown in table 1 below, the comparison of the amounts of water extracted from different parts of the sea buckthorn plant is performed, and the analysis of the amounts of water extracted from the dry sea buckthorn fruits, the sea buckthorn seeds, the fresh sea buckthorn fruits, the sea buckthorn leaves and the sea buckthorn stems extracted from the different parts of the plant sea buckthorn results in different amounts of water extracted from the different parts of the plant sea buckthorn, and the amount of water contained in the fresh sea buckthorn fruits is as large as 76-79%, which is caused by the fact that more water exists in the fresh sea buckthorn fruits.
TABLE 1 comparison table of water extraction amount of different parts of sea buckthorn
| Dried sea buckthorn fruit (%) | Sea buckthorn seed (%) | Sea buckthorn fresh fruit (%) | Sea buckthorn leaf (%) | Sea buckthorn stem (%) |
| 12～14.5 | 12～13 | 76～79 | 53～55 | 48～50 |
The invention relates to a method for preparing seabuckthorn oil, which comprises the steps of preparing seabuckthorn oil, preparing a liquid, mixing the liquid with a carrier, and carrying out extraction, wherein the seabuckthorn oil and the seabuckthorn oil both contain vitamins, flavone, carotene, linoleic acid, α -linolenic acid and amino acids, but the seabuckthorn oil contains esters, fatty acids and alcohols.
Optimizing the extraction process of sea buckthorn water by taking the extraction of sea buckthorn seed oil as an example
The method determines 4 main factors by integrating the influence of each factor on the extraction rate of the seabuckthorn seed oil-water mixture, adopts Box-Bohnken (BBD) combination Design in Design-Expert 8.0.6, and adopts the extraction temperature A, the extraction pressure B and the CO C2The flow and the extraction time D are independent variables, the extraction rate of the seabuckthorn seed oil is used as a dependent variable for analysis, and the factors and the coding level are shown in a table 2:
TABLE 2 response surface factor analysis and leveling
TABLE 3 response surface test design and results
The structure of the response surface BBD test scheme is shown in Table 3, and after the test is performed according to the response surface BBD test scheme, the least square method is used for fitting a relational equation between the response value Y and the independent variable X as follows:
Y＝21.46+0.03X1+0.99X2+0.37X3+2.57X4+0.25X1X2+0.0025X1X3+1.32X1X4+0.0025X2X3+0.11X2X4+0.72X3X4+7.7X1 2+0.076X2 2+8.24X3 2+3.61X4 2
the results of analysis of variance and significance test on the model equation show that the effect of extraction temperature, carbon dioxide flow and extraction time on the extraction of the seabuckthorn oil is more significant, and factors are amongThe interaction is more obvious. The regression significance of the model (P is less than 0.0001), the complex correlation coefficient of the model is 0.9935, and the correction decision coefficient Adj-R of the model20.9695, the model predicts a change in the 96.95% response value Y. Therefore, it is feasible that this model is used to optimize the extraction yield of the oil-water mixture of seabuckthorn. The optimal process conditions for extracting the seabuckthorn oil by the response surface optimization method are as follows: the extraction temperature is 53.7 ℃, the extraction pressure is 281bar, and CO is added2The flow rate is 2807kg/h, the extraction time is 5h, and the collection rate of the sea buckthorn oil-water mixture is 9.6%. Experiments verify that the response surface method can perform regression analysis and parameter optimization on the extraction of the sea buckthorn oil-water mixture.
(1) Influence of extraction temperature and extraction pressure on extraction rate
As shown in fig. 2, through the optimization of the response curved surface, under the condition of a certain extraction temperature, the increase of the extraction rate of the seabuckthorn oil-water mixture is not changed greatly along with the increase of the extraction pressure, and under the condition of a certain extraction pressure, the extraction rate is increased firstly and then reduced along with the increase of the extraction temperature. Through optimization, the optimal extraction temperature of the method is 57.3 ℃, and the extraction pressure is 281 bar.
(2) Influence of extraction pressure and extraction time on extraction rate
As shown in fig. 3, through the optimization of the response surface, under the condition of a certain extraction pressure, the extraction rate of the seabuckthorn oil-water mixture is gradually increased along with the increase of the extraction time, but the change of the extraction rate gradually decreases when the extraction rate is increased to a certain trend. The optimal extraction pressure is 281bar and the extraction time is 5h after optimization.
(3) Influence of extraction time and carbon dioxide flow on extraction rate
As shown in fig. 4, through the optimization of the response curved surface, under the condition of a certain extraction pressure, the growth rate of the seabuckthorn oil-water mixture is increased and then decreased along with the increase of the carbon dioxide flow. Under the condition of a certain carbon dioxide flow, the change range of the extraction rate of the sea buckthorn oil-water mixture is small along with the increase of the extraction pressure. The optimal extraction time of the invention is 5h and the flow of carbon dioxide is 2807kg/h after optimization.
The effective components and efficacy analysis and verification of the sea buckthorn water prepared by the invention are as follows:
the effective components of the medicinal composition are analyzed and researched, and the specific results are shown in table 4:
TABLE 4 effective components of Hippophae rhamnoides in water
The ratio of each active ingredient is shown in table 5:
TABLE 5 ratio of effective components of fructus Hippophae water
The sea-buckthorn water has the functions of reducing blood sugar concentration, promoting repair of bones, skin and muscle tissues, supplementing postoperative rehabilitation, reducing blood sugar concentration, promoting repair of bones, skin and muscle tissues, generating ketoacid after deamination during metabolism of amino acids in vivo, generating sugar according to glucose metabolism, effectively reducing generation of wrinkles, maintaining appearance of wrinkles, protecting body cells from free radical toxicity, resisting aging and cancer, preventing inflammatory skin diseases, alopecia, protecting skin from being damaged by ultraviolet rays and pollution, reducing deposition of scars and pigments, accelerating wound healing, preventing blood coagulation, reducing generation of tissues, reducing blood fat, preventing myocardial aging, preventing myocardial ischemia, aging.
The effect verification of the sea buckthorn water prepared by the invention is as follows:
(1) irritation property
The experimental process comprises the steps of smearing 5m L sea buckthorn water on one wrist, continuously smearing for 15 days after the sea buckthorn water is smeared on one wrist every day, selecting the other wrist as a control, and observing, wherein the experimental result is shown in table 6.
TABLE 6 integral of skin irritation response to repeated contact with sea buckthorn
As can be seen from Table 6: through analysis and comparison, the skin smeared by the sample does not have the adverse phenomena of red spots, skin edema and the like compared with a control group. It follows that the sea buckthorn water sample is not irritating to the skin.
(2) Water replenishing effect
Experimental procedure 50 persons were randomly selected by the company, 5m L was wiped on the left wrist, and the application was maintained once a day for one week, and the other wrist was used as a control for observation, and the results are shown in Table 7.
TABLE 7 Water supplement results
And (4) conclusion: the skin of the test person becomes moist, tender and smooth after insisting on using the sea buckthorn water for one month, and the roughness of the skin of the test person is obviously relieved. The ratio of good, ordinary and poor skin moisturizing performance after the product is considered by the test person is respectively as follows: 96%, 3% and 1%.
(3) Has effects in removing acne marks on skin.
Experiments randomly select face skin with acne marks at the age of 24-30 years, and the selection of the subjects meets the test standards of the experiments. The skin area is selected as the face in the test, and the tested object is required to be evenly smeared in the test process. The examinee needs to smear the pox-printed part under the regulation requirement, and the pox-printed part is smeared once every morning and evening, and the service cycle is 2 months. And in the testing stage, other cosmetics are stopped. The data were collected 4 times in total during the test, which were at initial use, first week, second week, and fourth week, respectively. The data acquisition and observation stage is the same time period every day. The measurement results are shown in Table 8, and as shown in Table 8, the acne marks on the skin of the test group become obviously light and gradually heal, the acne marks are completely eliminated for 25 days, and the acne marks of the skin of the test group are eliminated for a longer time period than those of the skin of the test group without the sea buckthorn water. 80.0% of the subjects had significantly reduced acne marks, and as shown in FIG. 5, the skin of one of the patients had significantly reduced acne marks after one month of administration of the sea buckthorn water of the present invention.
TABLE 8 Effect on healing of skin acne marks
The results of comparing the curative effects of the test group and the control group are shown in the following table 9, the number of people who have lightened skin acne marks is obviously more than that of the control group by applying seabuckthorn lotion, the cure rate of the acne marks reaches 62.85 percent and is obviously higher than that of the control group, the seabuckthorn lotion is further proved to have the function of dispelling and lightening the skin acne marks, and the skin becomes more delicate after the seabuckthorn lotion is used.
TABLE 9 comparison of the therapeutic effects of the two groups of patients with acne marks on their skins
(4) Against the influence of UVC radiation
HaCaT cells are cultured, tests are divided into groups and subjected to UVC radiation, the cell survival rate is measured by a CCK-8 method, the results are shown in Table 10, a control group refers to a test group which is not subjected to ultraviolet radiation, a UVC group refers to a test group which is subjected to ultraviolet radiation, a sea buckthorn water 2m L group refers to a sea buckthorn water observation cell survival state which is subjected to ultraviolet radiation and coated with 2m L, and a sea buckthorn water 20m L group refers to a sea buckthorn water observation cell survival state which is subjected to ultraviolet radiation and coated with 20m L.
TABLE 10 Effect of Hippophae rhamnoides Water on apoptosis Rate of UVC radiation HaCaT cells
Remarking: superoxide dismutase (SOD); glutathione peroxidase (GSH-PX); catalase (CAT).
As shown in FIG. 6, the test groups with sea buckthorn water amounts of 2m L and 20m L have lower cell death rate and higher survival rate than the test groups with ultraviolet radiation.
(5) Sea buckthorn water whitening effect
The test selects 30 subjects (without allergic history) between the ages of 25-50, wherein 15 men and 15 women, the tested part selects the forearm of the human body close to the wrist, wherein the left arm is the tested object coated with sea buckthorn water, the right arm is the reference object, the test part of each tested subject is tested by adopting an L ab colorimetric tester for 1 month, 2 months and 3 months before the test, the skin color change of the tested part is observed, the average value of the test results is taken
(Δ E represents color difference Δ Eab) determined as shown in Table 11.
TABLE 11 color difference comparison of the test sites of the subjects at different time periods
From the above table, it can be seen that: after the use for 1 month, the left arm color difference is obvious from the right arm color difference, and the number of people accounts for 60 percent. After 2 months of use, the left arm color difference is obvious from the right arm color difference, and the number of people accounts for 67%. After 3 months of use, the left arm color difference is obvious more than the right arm color difference, and the percentage of people is 77%. Therefore, the sea buckthorn water prepared by the invention is beneficial to whitening skin and has whitening effect.
(6) Safety feature
The results of the detection of the microorganism content of the present invention are shown in Table 12.
TABLE 12 microorganisms and hygiene indicators for sea buckthorn water
From table 12, it can be seen that: the number of the sea-buckthorn water flora does not exceed the standard and heavy metal ions and other harmful ions are not detected, so that the sea-buckthorn aquatic product has high safety.
The application of the sea buckthorn water of the invention is as follows: the sea buckthorn water has the effects of maintaining beauty, keeping young, resisting inflammation and sterilizing, can be applied to the cosmetic fields of facial masks, facial cream, toning lotion, essence and the like, and the application of the sea buckthorn water in the cosmetic field is described by taking the facial masks, the toning lotion, the emulsion and the essence as examples.
The method for preparing the repairing and nourishing mask by utilizing the sea buckthorn water comprises the following steps:
And 2, adding the propylene glycol, the glycerol, the sodium hyaluronate, the carbomer, the corn gluten amino acids and the allantoin weighed in the step 1 into a sterilized emulsifying pot, stirring and heating to 80-85 ℃, and continuing stirring for 40-45 minutes after all solutes are dissolved.
And 3, uniformly mixing the sea buckthorn water obtained by the method with the sodium acrylate/sodium acryloyldimethyl taurate copolymer at normal temperature, then adding the mixture into the emulsifying pot obtained in the step 1, starting stirring for 3 minutes, cooling the emulsifying pot to 55 ℃, adding triethanolamine and stirring uniformly.
And 4, cooling the emulsifying pot in the step 3 to 45 ℃, adding β -dextran, oligopeptide-1 and bis (hydroxymethyl) imidazolidinyl urea, and uniformly stirring.
And 5, cooling the emulsifying pot to 38 ℃ in the step 4, taking a small sample for detection, preparing the sea-buckthorn water restoration and nourishing facial mask by using the human-skin-imitated facial mask after the detection is qualified, wherein the appearance detection of the facial mask is shown in a table 13.
TABLE 13 sensory indices of facial mask
The use method of the facial mask comprises the following steps: the face is cleaned, then the facial mask is applied to the face for 15-20 min, and then the face is cleaned with warm water. Selecting 30 test persons, continuously using the mask for 3 days, and testing the results as shown in a table 14.
TABLE 14 comparison of skin condition of Hippophae rhamnoides mask after application
| Group of | Change in skin condition |
| Common face pack | No obvious change of skin state |
| Sea-buckthorn water mask | The skin becomes tender and smooth, and the fine lines of the skin become obviously shallow |
In the invention, the preparation flows of the common facial mask and the sea buckthorn water facial mask are the same, but the water in the preparation process of the common facial mask is distilled water, the sea buckthorn water facial mask replaces the distilled water with the sea buckthorn water, the test results are shown in table 15, and the test results are shown in table 15: the sea-buckthorn water mask prepared by the invention can obviously make the skin of a subject become tender and the fine wrinkles become shallow, and has a good water replenishing effect.
The skin moisture content of the test subjects in the control group and the test group was measured with a moisture meter every 5 minutes, and the measurement results are shown in fig. 7, from which it is clear that: the relative facial skin moisture values of the control group and the test group are the same when the mask is just applied, the relative facial skin moisture values of the control group and the test group tend to increase along with the increase of the mask application time, and the relative facial skin moisture values of the control group and the test group tend to be stable in 20 minutes, but obviously, the moisturizing effect of the seabuckthorn water mask prepared by the invention is superior to that of a common mask, so that the moisturizing, wrinkle removing and whitening effects of the seabuckthorn water mask prepared by the invention are obviously superior to that of the common mask.
(II) the method for preparing the sea-buckthorn toner by utilizing the sea-buckthorn water comprises the following steps:
And 2, adding the propylene glycol, the glycerol, the sodium hyaluronate, the carbomer, the corn gluten amino acids and the allantoin weighed in the step 1 into a sterilized emulsifying pot, stirring and heating to 84 ℃, and continuing stirring for 40-45 minutes after all solutes are dissolved.
And step 3: adding sea buckthorn water and the sodium acrylate/sodium acryloyldimethyl taurate copolymer under the premise of the step 2, homogenizing for 5 minutes, keeping for 30 minutes, cooling the emulsifying pot to 45 ℃, adding triethanolamine, and stirring uniformly. Standing, discharging, inspecting, and packaging after qualified inspection.
The use method of the sea buckthorn toner comprises the following steps: cleaning face, and then applying the sea buckthorn water toner on cheek. Selecting 30 test users, continuously using for 1 week, wherein the test results are shown in a table 14, and the following results can be obtained from the table 14: the appearance and the fragrance of the sea buckthorn water toner prepared by the invention both meet the regulations of the national relevant standards.
TABLE 14 sensory indices of Hippophae rhamnoides toner
TABLE 15 comparison of skin condition of the applied sea buckthorn water toner
| Group of | Change in skin condition |
| Common toner | No obvious change of skin state |
| Sea-buckthorn toner | The skin becomes tender and the fine lines become shallow |
In the invention, the preparation flows of the common toner and the sea buckthorn water toner are the same, the water in the preparation process of the common toner is distilled water, the sea buckthorn water toner is distilled water instead of distilled water, the test results are shown in table 15, and the test results are shown in table 15: the sea-buckthorn water toner prepared by the invention can obviously make the skin of a subject become tender and the fine lines become shallow, and has a good water replenishing effect.
(III) the preparation method of the sea buckthorn water moisturizing emulsion comprises the following steps:
And 2, adding the propylene glycol, the glycerol, the sodium hyaluronate, the carbomer, the corn gluten amino acids and the allantoin weighed in the step 1 into a sterilized emulsifying pot, stirring and heating to 84 ℃, and continuing stirring for 40-45 minutes after all solutes are dissolved.
And 3, adding sea buckthorn water and the sodium acrylate/sodium acryloyldimethyl taurate copolymer on the premise of the step 2, homogenizing for 5 minutes, keeping for 30 minutes, cooling the emulsifying pot to 45 ℃, adding triethanolamine, β -glucan, oligopeptide-1 and bis (hydroxymethyl) imidazolidinyl urea, and uniformly stirring.
And 4, cooling the emulsifying pot to 35-40 ℃ in the step 3, taking a small sample for detection, and packaging after the detection is qualified.
The application method of the sea buckthorn aqueous emulsion comprises the following steps: cleaning face, and applying the aqueous emulsion of fructus Hippophae to cheek. 30 subjects were selected and used continuously for 1 week, and sensory results of aqueous emulsion of Hippophae rhamnoides are shown in Table 16.
TABLE 16 sensory indices of aqueous emulsion of Hippophae rhamnoides
| Serial number | Inspection item | Index (I) | Test results |
| 1 | Appearance of the product | Compliance with regulations | Qualified |
| 2 | Fragrance | Compliance with regulations | Qualified |
TABLE 17 comparison of skin conditions of the moisturizing lotion of Hippophae rhamnoides after application
| Group of | Change in skin condition |
| Ordinary moisturizing emulsion | No obvious change of skin state |
| Aqueous emulsion of seabuckthorn fruit | The skin becomes tender and moist, and the fine wrinkles become shallow |
In the invention, the preparation flows of the common moisturizing emulsion and the sea-buckthorn aqueous emulsion are the same, distilled water is adopted in the preparation process of the common moisturizing emulsion, and the sea-buckthorn aqueous emulsion replaces the distilled water with the sea-buckthorn water. The test results are shown in Table 17, and it can be seen from Table 17 that: the sea-buckthorn aqueous emulsion prepared by the invention can obviously make the skin of a subject become tender and moist and thin wrinkles become shallow.
(IV) the preparation method of the sea buckthorn water essence comprises the following steps:
And 2, adding the butanediol, the glycerol, the sodium hyaluronate, the carbomer and the hydrolyzed yeast protein weighed in the step 1 into a sterilized emulsifying pot, stirring and heating to 84 ℃, and continuing stirring for 30-45 minutes after all solutes are dissolved.
And 3, adding sea buckthorn water and the sodium acrylate/sodium acryloyldimethyl taurate copolymer under the premise of the step 2, homogenizing for 5 minutes, keeping for 25 minutes, cooling the emulsifying pot to 45 ℃, adding triethanolamine, collagen, oligopeptide-1 and propyl hydroxybenzoate, and uniformly stirring.
The use method of the sea buckthorn water essence comprises the following steps: cleaning face, applying conventional cosmetic water and lotion on skin, and applying the essence solution on cheek. Selecting 30 test persons, continuously using for 1 week, wherein the test results are shown in a table 18, and the following results can be obtained from the table 18: the appearance and the fragrance of the sea buckthorn water toner prepared by the invention both meet the regulations of the national relevant standards.
TABLE 18 sensory indices of aqueous extract and liquid of Hippophae rhamnoides
| Serial number | Inspection item | Index (I) | Test results |
| 1 | Appearance of the product | Compliance with regulations | Qualified |
| 2 | Fragrance | Compliance with regulations | Qualified |
TABLE 19 comparison of skin conditions of fructus Hippophae water essence after application
| Group of | Change in skin condition |
| Common essence | No obvious change of skin state |
| Sea-buckthorn water essence | The skin becomes more moist and tender |
In the invention, the preparation flows of the common essence and the sea-buckthorn water essence are the same, water is distilled water in the preparation process of the common essence, the sea-buckthorn water essence replaces distilled water with sea-buckthorn water, the test results are shown in table 19, and the test results are shown in table 19: the skin of a subject can be obviously moisturized and tender by the sea-buckthorn water toner prepared by the invention, which shows that the sea-buckthorn water essence prepared by the invention has better effects of moisturizing, brightening and moistening the skin.
Claims (7)
1. A sea buckthorn water is characterized in that the sea buckthorn water is extracted from sea buckthorn plants.
2. The preparation method of sea buckthorn water according to claim 1, which is implemented by the following steps:
step 1, cleaning and pretreating sea buckthorn plants;
and 2, extracting the raw materials obtained in the step 1 to obtain the sea buckthorn water.
3. The method according to claim 2, wherein the seabuckthorn plants in step 1 comprise seabuckthorn seeds, dried seabuckthorn fruits, fresh seabuckthorn fruits, seabuckthorn leaves and seabuckthorn stems.
4. The method for preparing sea buckthorn water, according to claim 3, wherein the pretreatment of the sea buckthorn seeds or the dried sea buckthorn fruits in the step 1 is crushing and tabletting, the thickness of the tablets is 0.3-0.5 mm, and the crushed tablets are smaller than 18 meshes.
5. The method according to claim 3, wherein the dried seabuckthorn seeds/seabuckthorn fruits in step 2 are extracted by supercritical carbon dioxide, the fresh seabuckthorn fruits are extracted by squeezing distillation, and the seabuckthorn leaves and the seabuckthorn stems are extracted by azeotropic distillation.
6. The method for preparing sea buckthorn water, according to claim 3, wherein the specific process of extracting the sea buckthorn seeds/dried sea buckthorn berries by using supercritical carbon dioxide comprises the following steps: the raw material after tabletting is carried out at the pressure of 270-290 bar, the temperature of 52-55 ℃ and CO2Extracting for 4.5-5.5 h under the condition that the flow is 2750-2850kg/h, performing primary separation under the conditions that the pressure is 100-110 bar and the temperature is 45-50 ℃ after extraction, performing secondary separation under the conditions that the pressure is 50-55 bar and the temperature is 30-35 ℃, and standing and separating oil-water substances obtained by separation under the conditions that the temperature is 40-45 ℃ and the time is 5hThe sea-buckthorn water of the invention can be obtained.
7. The use of sea buckthorn water according to claim 1 in the cosmetic field.
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| CN116135215A (en) * | 2023-04-06 | 2023-05-19 | 白玉 | Sea buckthorn water and preparation method and application thereof |
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