CN111349411A - Preparation method for preparing moisture-proof cigarette middle line glue - Google Patents
Preparation method for preparing moisture-proof cigarette middle line glue Download PDFInfo
- Publication number
- CN111349411A CN111349411A CN202010361471.0A CN202010361471A CN111349411A CN 111349411 A CN111349411 A CN 111349411A CN 202010361471 A CN202010361471 A CN 202010361471A CN 111349411 A CN111349411 A CN 111349411A
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- Prior art keywords
- stirring
- moisture
- temperature
- vinyl acetate
- cigarette
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J131/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Adhesives based on derivatives of such polymers
- C09J131/02—Homopolymers or copolymers of esters of monocarboxylic acids
- C09J131/04—Homopolymers or copolymers of vinyl acetate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
Abstract
The invention discloses a preparation method for preparing moisture-proof cigarette middle line glue, which comprises the following steps of S1: selecting ingredients: 20g of vinyl acetate, 4g of potassium sulfate, 4g of polyvinyl alcohol solution, 3g of emulsifier, 2g of mint essential oil and 2g of mildew preventive; s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process; s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring; s4: and (3) corrosion prevention: the preservative in S1 was added to the mixed solution in S3, and mixed and stirred. The cigarette is simple to manufacture, can effectively prevent moisture and prolong the storage time of the cigarette by adding the mildew preventive, can provide pleasant fragrance by adding the mint, is more specific and better meets the differentiated requirements of people.
Description
Technical Field
The invention relates to the technical field of buildings, in particular to a preparation method of moisture-proof cigarette middle line glue.
Background
Cigarettes (cigarette paper is used for rolling tobacco shreds into strip-shaped cigarette products, also called cigarettes, cigarettes and cigarette rolls, cigarettes with filter tips and cigarettes without filter tips, light flavor and strong flavor, flue-cured tobacco types are divided into 4 grades, mixed types, cigar types and outer flavor types are divided into 3 grades, brands of the grades have flavor characteristics, the product tax rates of the grades have high and low differences, a novel cigarette appears in 80 years, namely Chinese herbal medicine components are added into the tobacco shreds to be beneficial to the improvement of the tobacco flavor, and the cigarette is generally stuck by glue in the production process.
Traditional line is glued and is being glued general no special smell of in-process that glues, and dampproofing effect is general, can not be fine satisfy people's user demand.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method for preparing moisture-proof cigarette middle line glue.
The invention provides a preparation method for preparing moisture-proof cigarette middle line glue;
the preparation method for preparing the moisture-proof cigarette middle line adhesive comprises the following steps:
s1: selecting ingredients: 20g of vinyl acetate, 4g of potassium sulfate, 4g of polyvinyl alcohol solution, 3g of emulsifier, 2g of mint essential oil and 2g of mildew preventive;
s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process;
s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring;
s4: and (3) corrosion prevention: adding the preservative in the S1 into the mixed solution in the S3, and mixing and stirring;
s5: mixing the mint: adding the mint essential oil in the S1 into the mixed solution in the S4;
s6: impurity removal and cooling: connecting a water pump with the upper opening of the condensation pipe, sucking and removing residual monomers which are not polymerized, and discharging after cooling.
Preferably, the temperature of the water bath heating in the S2 is 71 ℃.
Preferably, the temperature in S3 is maintained at 71 ℃, the vinyl acetate is added at a rate of 10 drops/min for a period of 2 hours.
Preferably, in the step S3, the temperature is increased by 10 ℃ for half an hour after the vinyl acetate is added, the temperature is increased by 5 ℃ for one time for half an hour, the temperature is increased by 5 ℃ for two times for half an hour, and stirring is continued during the half an hour, wherein the stirring speed is 100 revolutions per minute.
Preferably, the stirring in the S4 is carried out for 5min, and the stirring speed is 100 r/min.
Preferably, stirring is required to be performed in the adding process of S5, the stirring time is 10min, and the stirring speed is 100 rpm.
Preferably, the temperature is measured after cooling in S6, and the material is discharged after cooling to room temperature.
The invention has the beneficial effects that: the cigarette is simple to manufacture, can effectively prevent moisture and prolong the storage time of the cigarette by adding the mildew preventive, can provide pleasant fragrance by adding the mint, is more specific and better meets the differentiated requirements of people.
Drawings
FIG. 1 is a flow chart of a preparation method of the moisture-proof cigarette centerline gel provided by the invention.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The embodiment provides a preparation method for preparing moisture-proof cigarette middle line glue, which comprises the following steps:
s1: selecting ingredients: 20g of vinyl acetate, 4g of potassium sulfate, 4g of polyvinyl alcohol solution, 3g of emulsifier, 2g of mint essential oil and 2g of mildew preventive;
s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process;
s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring;
s4: and (3) corrosion prevention: adding the preservative in the S1 into the mixed solution in the S3, and mixing and stirring;
s5: mixing the mint: adding the mint essential oil in the S1 into the mixed solution in the S4;
s6: impurity removal and cooling: connecting a water pump with the upper opening of the condensation pipe, sucking and removing residual monomers which are not polymerized, and discharging after cooling.
The heating temperature of the water bath in the S2 is 71 ℃, the temperature in the S3 is kept at 71 ℃, the speed of adding vinyl acetate is 10 drops/min, the adding time is 2 hours, the temperature is increased by 10 ℃ for half an hour after the vinyl acetate is added in the S3, the temperature is increased by 5 ℃ for one time for half an hour, the temperature is increased by 5 ℃ for two times for half an hour, the stirring is continued for half an hour, the stirring speed is 100 revolutions/min, the stirring is performed for 5 minutes in the S4, the stirring speed is 100 revolutions/min, the stirring is required in the adding process in the S5, the stirring time is 10min, the stirring speed is 100 revolutions/min, the temperature is required to be measured after cooling in the S6, and the material can be discharged after being cooled to the room temperature.
Example two
The embodiment provides a preparation method for preparing moisture-proof cigarette midline gum, which comprises the following steps:
s1: selecting ingredients: 10g of vinyl acetate, 2g of potassium sulfate, 2g of polyvinyl alcohol solution, 1.5g of emulsifier, 1g of mint essential oil and 1g of mildew preventive;
s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process;
s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring;
s4: and (3) corrosion prevention: adding the preservative in the S1 into the mixed solution in the S3, and mixing and stirring;
s5: mixing the mint: adding the mint essential oil in the S1 into the mixed solution in the S4;
s6: impurity removal and cooling: connecting a water pump with the upper opening of the condensation pipe, sucking and removing residual monomers which are not polymerized, and discharging after cooling.
The heating temperature of the water bath in the S2 is 71 ℃, the temperature in the S3 is kept at 71 ℃, the speed of adding vinyl acetate is 10 drops/min, the adding time is 2 hours, the temperature is increased by 10 ℃ for half an hour after the vinyl acetate is added in the S3, the temperature is increased by 5 ℃ for one time for half an hour, the temperature is increased by 5 ℃ for two times for half an hour, the stirring is continued for half an hour, the stirring speed is 100 revolutions/min, the stirring is performed for 5 minutes in the S4, the stirring speed is 100 revolutions/min, the stirring is required in the adding process in the S5, the stirring time is 10min, the stirring speed is 100 revolutions/min, the temperature is required to be measured after cooling in the S6, and the material can be discharged after being cooled to the room temperature.
EXAMPLE III
The embodiment provides a preparation method for preparing moisture-proof cigarette middle line glue, which comprises the following steps:
s1: selecting ingredients: 15g of vinyl acetate, 3g of potassium sulfate, 3g of polyvinyl alcohol solution, 2g of emulsifier, 1.5g of mint essential oil and 1.5g of mildew preventive;
s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process;
s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring;
s4: and (3) corrosion prevention: adding the preservative in the S1 into the mixed solution in the S3, and mixing and stirring;
s5: mixing the mint: adding the mint essential oil in the S1 into the mixed solution in the S4;
s6: impurity removal and cooling: connecting a water pump with the upper opening of the condensation pipe, sucking and removing residual monomers which are not polymerized, and discharging after cooling.
The heating temperature of the water bath in the S2 is 71 ℃, the temperature in the S3 is kept at 71 ℃, the speed of adding vinyl acetate is 10 drops/min, the adding time is 2 hours, the temperature is increased by 10 ℃ for half an hour after the vinyl acetate is added in the S3, the temperature is increased by 5 ℃ for one time for half an hour, the temperature is increased by 5 ℃ for two times for half an hour, the stirring is continued for half an hour, the stirring speed is 100 revolutions/min, the stirring is performed for 5 minutes in the S4, the stirring speed is 100 revolutions/min, the stirring is required in the adding process in the S5, the stirring time is 10min, the stirring speed is 100 revolutions/min, the temperature is required to be measured after cooling in the S6, and the material can be discharged after being cooled to the room temperature.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. A preparation method for preparing moisture-proof cigarette middle line glue is characterized by comprising the following steps:
s1: selecting ingredients: 10-20g of vinyl acetate, 2-4g of potassium sulfate, 2-4g of polyvinyl alcohol solution, 1.5-3g of emulsifier, 1-2g of mint essential oil and 1-2g of mildew preventive;
s2: adding materials: selecting a three-neck flask, adding a polyvinyl alcohol solution and an emulsifier into the three-neck flask, and heating in a water bath, wherein a stirrer is required to be used for stirring in the heating process;
s3: adding materials and stirring: inserting a reflux condenser pipe on the three-neck flask, adding potassium persulfate from the upper opening of the reflux condenser pipe, slowly dropping vinyl acetate, and continuously stirring;
s4: and (3) corrosion prevention: adding the preservative in the S1 into the mixed solution in the S3, and mixing and stirring;
s5: mixing the mint: adding the mint essential oil in the S1 into the mixed solution in the S4;
s6: impurity removal and cooling: connecting a water pump with the upper opening of the condensation pipe, sucking and removing residual monomers which are not polymerized, and discharging after cooling.
2. The method for preparing the moisture-proof cigarette midline gum according to claim 1, wherein the water bath heating temperature in the S2 is 71 ℃.
3. The method for preparing the moisture-proof cigarette midline gum according to claim 1, wherein the temperature in the step S3 is kept at 71 ℃, the speed of adding the vinyl acetate is 10 drops/min, and the adding time is 2 hours.
4. The method for preparing the moisture-proof cigarette centerline adhesive according to claim 1, wherein the temperature is increased by 10 ℃ for half an hour after the vinyl acetate is added in the step S3, the temperature is increased by 5 ℃ for one time for half an hour, the temperature is increased by 5 ℃ for two times for half an hour, stirring is continued for half an hour, and the stirring speed is 100 revolutions per minute.
5. The preparation method of the moisture-proof cigarette centerline adhesive according to claim 1, wherein the stirring in the step S4 is carried out for 5min, and the stirring speed is 100 revolutions per minute.
6. The preparation method of the moisture-proof cigarette centerline adhesive according to claim 1, wherein stirring is required in the adding process of S5, the stirring time is 10min, and the stirring speed is 100 r/min.
7. The preparation method of the moisture-proof cigarette centerline adhesive according to claim 1, wherein the temperature is measured after cooling in S6, and the moisture-proof cigarette centerline adhesive is discharged after cooling to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010361471.0A CN111349411A (en) | 2020-04-30 | 2020-04-30 | Preparation method for preparing moisture-proof cigarette middle line glue |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010361471.0A CN111349411A (en) | 2020-04-30 | 2020-04-30 | Preparation method for preparing moisture-proof cigarette middle line glue |
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| Publication Number | Publication Date |
|---|---|
| CN111349411A true CN111349411A (en) | 2020-06-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010361471.0A Pending CN111349411A (en) | 2020-04-30 | 2020-04-30 | Preparation method for preparing moisture-proof cigarette middle line glue |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114525089A (en) * | 2022-02-21 | 2022-05-24 | 连云港昌瑞科技有限公司 | Environment-friendly flame-retardant cigarette adhesive and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229788A (en) * | 2011-05-13 | 2011-11-02 | 山西三维集团股份有限公司 | Preparation method for green and environment-friendly cigarette adhesive |
| CN104910863A (en) * | 2015-04-27 | 2015-09-16 | 湖北中烟工业有限责任公司 | Filter rod center line rubber and preparation process thereof |
| CN106108109A (en) * | 2016-08-22 | 2016-11-16 | 红云红河烟草(集团)有限责任公司 | A kind of filter stick containing color and fragrance centre-line glue and preparation method thereof |
| CN110699016A (en) * | 2019-11-11 | 2020-01-17 | 新乡市华洋粘合剂有限公司 | Middle line glue for cigarettes and preparation method thereof |
-
2020
- 2020-04-30 CN CN202010361471.0A patent/CN111349411A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102229788A (en) * | 2011-05-13 | 2011-11-02 | 山西三维集团股份有限公司 | Preparation method for green and environment-friendly cigarette adhesive |
| CN104910863A (en) * | 2015-04-27 | 2015-09-16 | 湖北中烟工业有限责任公司 | Filter rod center line rubber and preparation process thereof |
| CN106108109A (en) * | 2016-08-22 | 2016-11-16 | 红云红河烟草(集团)有限责任公司 | A kind of filter stick containing color and fragrance centre-line glue and preparation method thereof |
| CN110699016A (en) * | 2019-11-11 | 2020-01-17 | 新乡市华洋粘合剂有限公司 | Middle line glue for cigarettes and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 尹才龙等: "低固含量普通型卷烟胶的研制与应用 ", 《中国胶粘剂》 * |
| 黄亚侬等: "生产工艺参数对聚醋酸乙烯酯乳液黏度的影响研究 ", 《粘接》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114525089A (en) * | 2022-02-21 | 2022-05-24 | 连云港昌瑞科技有限公司 | Environment-friendly flame-retardant cigarette adhesive and preparation method thereof |
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