CN111214157B - Wormwood sterilizing wet tissue and preparation method thereof - Google Patents
Wormwood sterilizing wet tissue and preparation method thereof Download PDFInfo
- Publication number
- CN111214157B CN111214157B CN202010024813.XA CN202010024813A CN111214157B CN 111214157 B CN111214157 B CN 111214157B CN 202010024813 A CN202010024813 A CN 202010024813A CN 111214157 B CN111214157 B CN 111214157B
- Authority
- CN
- China
- Prior art keywords
- wormwood
- layer
- moxa
- wood pulp
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47K—SANITARY EQUIPMENT NOT OTHERWISE PROVIDED FOR; TOILET ACCESSORIES
- A47K10/00—Body-drying implements; Toilet paper; Holders therefor
- A47K10/16—Paper towels; Toilet paper; Holders therefor
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Biomedical Technology (AREA)
- Nonwoven Fabrics (AREA)
Abstract
The invention discloses a wormwood disinfection wet tissue and a preparation method thereof, wherein the wormwood disinfection wet tissue comprises a wormwood base material and a wet tissue solution, and the wormwood base material comprises the following raw materials in parts by weight: 30-50 parts of wood pulp, 60-80 parts of terylene, 10-20 parts of wormwood powder particles and 20-30 parts of moxa, wherein the wet tissue solution comprises the following components in parts by weight: 0.5-2 parts of surfactant and 50-150 parts of deionized water. The wormwood disinfection wet tissue prepared by the invention is not added with chemical preservatives, is soft and non-irritant to skin, and has the effects of cleaning, disinfection, mosquito prevention, itching relieving, lasting moisture retention and long shelf life.
Description
Technical Field
The invention relates to the technical field of wet tissues, and particularly relates to a wormwood disinfection wet tissue and a preparation method thereof.
Background
With the increasing living standard of people, the wet tissue gradually becomes a necessity in the life of people. Of course, the demand for the wet tissue is higher and higher, and a plurality of wet tissue products with different functions appear on the market. The disinfection wet tissue is a product sold in domestic markets at present, most of the products are added with chemical bacteriostatic agents, and although the disinfection wet tissue has good bactericidal activity, the disinfection wet tissue has certain irritation to skin, and skin allergy can be caused after long-term use. Some disinfection wet wipe products contain natural herbaceous plant disinfection components, are mild and non-irritant to skin, but have common sterilization effects, and natural component substances are not stable enough and are easy to deteriorate to influence the sterilization effects, so that the shelf life of the product is shortened, and the development of the product is limited. Therefore, the existing disinfection wet tissue has the problems of unsatisfactory sterilization effect, short product quality guarantee period and easy damage to skin.
Therefore, there is a need to develop a wormwood disinfection wet tissue to solve the problems in the prior art.
Disclosure of Invention
The technical problems to be solved by the invention are as follows: aiming at the problems of poor sterilization effect, skin damage and short shelf life of the existing disinfection wet tissue, the wormwood disinfection wet tissue and the preparation method thereof are provided.
In order to solve the technical problems, the invention adopts the technical scheme that:
the preparation method of the wormwood disinfection wet tissue is characterized by comprising the following steps:
(1) pulping and grinding wood pulp, adjusting the water content, and then making paper and forming to obtain wood pulp paper;
(2) carding polyester, moxa and moxa powder particles into a net to form a moxa polyester layer, compounding the moxa polyester layer with wood pulp paper, and sequentially performing spunlace, flat net suction and drying to obtain a moxa base material;
(3) and soaking the wormwood base material in the wet tissue liquid for 3-5h, and packaging to obtain the wormwood disinfection wet tissue.
The moxa base material comprises the following raw materials in parts by weight: 30-50 parts of wood pulp, 60-80 parts of terylene, 10-20 parts of wormwood powder particles and 20-30 parts of moxa.
The wet tissue liquid comprises the following raw materials in parts by weight: 0.5-2 parts of surfactant and 50-150 parts of deionized water.
The wood pulp raw material in the step (1) is coniferous wood, and pine wood is further preferred.
And (2) after the wood pulp in the step (1) is disc-milled, controlling the beating degree to be 17-20 DEG SR.
The mass concentration of the wood pulp after the water content is adjusted in the step (1) is 1-3 wt%, more preferably 1-1.5 wt%, and most preferably 1.3 wt%.
The weight of the wood pulp paper in the step (1) is 10-30 g/m2。
The terylene in the step (2) is polyethylene terephthalate (PET); the fineness of the terylene is 1.28 to 1.54dtex, and the length is 23 to 38 mm.
The length of the moxa in the step (2) is controlled to be 50-100 mm, and the fineness of the moxa is controlled to be 5-30D.
The mugwort powder particles in the step (2) are smaller than 100 meshes.
The weight of the wormwood polyester layer in the step (2) is 10-30 g/m2。
The step (2) is as follows: the compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The carded web in the step (2) is: and (3) feeding the mixture of the terylene, the wormwood powder particles and the moxa into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a wormwood terylene layer.
The water jet process in the step (2) comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then sending the fiber webs after the pre-wetting into a spunlace device, sending the fiber webs into a spunlace machine through a conveying net curtain, and carrying out four-step front and back spunlace reinforcement, wherein the spunlace pressure is 60-100 bar, 90-110 bar, 120-160 bar and 70-120bar respectively, so that the fiber webs of all layers are mutually entangled and are compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process in the step (2) is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process in the step (2) is that the spunlace nonwoven fabric is sent into a vacuum drying oven with the temperature of 100-120 ℃ for drying for 3-5 h.
The weight of the wormwood base material in the step (2) is 30-90 g/m2。
The surfactant in the step (3) is one or a mixture of disodium coconut monoethanolamide sulfosuccinate and dirhamnolipid lauryl ester.
Preferably, the surfactant is prepared by mixing disodium cocomonoethanolamide sulfosuccinate and dirhamnolipid lauryl ester according to the mass ratio of 1: 1.
The invention has the beneficial effects that:
(1) the prepared disinfection wet tissue contains natural herbaceous plant wormwood, and contains various chemical components, mainly including eucalyptol, thujone, borneol, caryophyllene oxide, alpha-terpineol, camphene, beta-terpinene, isoborneol, citral, beta-pinene, cis-carveol, (-) -4-terpineol, o-cymene, isoborneol, phellandrene, eucalyptol, 1-octen-3-ol and the like. A large number of researches show that the active ingredients can inhibit or kill various bacteria, fungi, viruses and mycoplasma, and especially can play a remarkable bactericidal role in staphylococcus aureus, candida albicans, escherichia coli, bacillus subtilis, candida albicans and aspergillus niger.
(2) The existing disinfection wet tissue containing natural herbaceous plant disinfection components is prepared by adding natural herbaceous plant extract into wet tissue liquid, and antibacterial components lose activity easily in the long-term wet tissue liquid and influence antibacterial effect. According to the invention, the natural herbaceous plant wormwood is added in the base material preparation method to prepare the wormwood base material, and the wormwood base material is soaked in the wet tissue liquid, so that the antibacterial substance can be continuously and effectively released.
(3) According to the invention, the surfactant in the wet tissue liquid is disodium coco monoethanolamide sulfosuccinate and/or dirhamnolipid lauryl ester, the wetting power and the penetrating power of the surfactant are fully acted with the wormwood component in the wet tissue base material, antibacterial chemical substances in the wormwood are extracted and slowly and effectively released in the wet tissue liquid, and the wet tissue can keep an excellent sterilization effect for a long time.
(4) According to the invention, the moxa is added in the preparation process of the moxa base material, so that the surface tension of the base material can be reduced, the base material is promoted to be softened, the flexibility of the wet tissue is enhanced, and the situation of breakage can not occur in the use process.
Detailed Description
Surfactant (b): the method for synthesizing dirhamnolipid lauryl ester and dirhamnolipid refers to the preparation method of example 3 and example 1 in the patent of CN108699097A invention respectively.
Example 1
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 1 part of disodium coconut monoethanolamide sulfosuccinate serving as a surfactant and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulpRegulating the water content after disc grinding, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Example 2
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 1 part of dirhamnolipid lauryl ester serving as a surfactant and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Example 3
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 0.5 part of disodium coconut monoethanolamide sulfosuccinate, 0.5 part of dirhamnolipid lauryl ester and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Comparative example 1
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Comparative example 2
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp and 110 parts of terylene, wherein the raw materials of the wet tissue disinfectant comprise the following components in parts by weight: 0.5 part of disodium coconut monoethanolamide sulfosuccinate, 0.5 part of dirhamnolipid lauryl ester and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Polyethylene terephthalate (PET) terylene with the fineness of 1.32dtex and the length of 34mm is carded into a terylene layer, then the terylene layer is compounded with the wood pulp paper layer, and the terylene layer is sequentially subjected to spunlace, flat net suction and drying to obtain a base material without wormwood; the weight of the terylene layer is 20g/m2(ii) a The weight of the non-mugwort-containing base material is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the terylene into a cotton dropping box by using a fan, primarily carding the terylene into a flocculent structure, and mutually winding, interweaving and filling the flocculent structure to form a terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer into a net, wherein the polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood-free base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood-free disinfection wet tissue.
Comparative example 3
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the wet tissue disinfectant comprises the following raw materials in parts by weight: 0.5 part of disodium coconut monoethanolamide sulfosuccinate, 0.5 part of dirhamnolipid lauryl ester and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) carding polyethylene terephthalate (PET) terylene with fineness of 1.32dtex and length of 34mm, moxa with length of 80mm and fineness of 10D and 70 meshes of moxa powder particles into a moxa terylene layer, compounding the two moxa terylene layers,sequentially carrying out spunlace, flat net suction and drying to obtain wood pulp-free wormwood base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The wood pulp-free mugwort substrate has a weight of 40g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer and the lower layer by webs, wherein the wormwood polyester layer is the upper layer and the lower layer to form a composite structure of which the upper layer and the lower layer are the wormwood polyester layer carding webs.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Comparative example 4
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 1 part of surfactant dirhamnolipid and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; controlling the beating degree to be 19 degrees SR after disc grindingThe mass concentration of the pulp after adjusting the water content is 1.3 wt%, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Comparative example 5
A folium Artemisiae Argyi disinfectant wet towel comprises folium Artemisiae Argyi base material and wet towel disinfectant; the moxa base material comprises the following raw materials in parts by weight: 40 parts of wood pulp, 70 parts of terylene, 15 parts of wormwood powder particles and 25 parts of moxa, wherein the disinfectant liquid for the wet tissue comprises the following raw materials in parts by weight: 0.5 part of disodium cocomonoethanolamide sulfosuccinate serving as a surfactant, 0.5 part of dirhamnolipid serving as a surfactant and 90 parts of deionized water.
The preparation method of the wormwood disinfection wet tissue comprises the following steps:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2。
(2) Carding 1.32dtex polyethylene terephthalate (PET) terylene with the length of 34mm, moxa with the length of 80mm and the fineness of 10D and 70 meshes of moxa powder particles into a net to form a moxa terylene layer, compounding the moxa terylene layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2。
The carding and web forming process comprises the following steps: and (3) feeding the mixture of the terylene, the moxa and the moxa powder particles into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a moxa terylene layer.
The compounding process comprises the following steps: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
The water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs are mutually entangled and compounded into a whole to form the spunlace nonwoven fabric.
The flat screen suction process is as follows: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
The drying process comprises the following steps: and (3) drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 h.
(3) Soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
Test example 1
Detection of bactericidal Activity
Test strains: escherichia coli (ACCC01630), Staphylococcus aureus (CICC10384), and Candida albicans (CMCC 98001).
The test steps are as follows:
1) the cultured test strains were washed with 1% peptone PBS on fresh slants and diluted to 10%5cfu/mL concentration;
2) the wet tissue of the example and the wet tissue of the comparative example are made into the size of 1 multiplied by 4cm and are placed in a sterile plate;
3) respectively dripping 50 mu L of bacterial liquid on the wet tissues of the examples and the comparative examples, uniformly smearing and starting timing; after the reaction lasts for 5 hours, putting the wet tissue into a test tube containing 5mL of neutralizer by using sterile tweezers, and fully shaking and uniformly mixing;
4) taking the final solution of 1.0 to stand for pouring into a flat plate, and carrying out inverted culture at the constant temperature of 37 ℃ for 48 h;
5) and calculating the quantity of the control recovered bacteria and the quantity of the sample recovered bacteria to obtain the bacteriostasis rate.
Test results
TABLE 1 bactericidal Activity test results
| Sample (I) | Escherichia coli | Staphylococcus aureus | Candida albicans |
| Example 1 | 95.12％ | 95.23％ | 95.43％ |
| Example 2 | 93.37％ | 94.12％ | 93.68％ |
| Example 3 | 99.54％ | 99.33％ | 99.26％ |
| Comparative example 1 | 75.16％ | 74.23％ | 76.12％ |
| Comparative example 2 | 51.23％ | 50.36％ | 53.17％ |
| Comparative example 3 | 80.18％ | 81.35％ | 80.36％ |
| Comparative example 4 | 92.46％ | 92.04％ | 91.21％ |
| Comparative example 5 | 93.26％ | 93.47％ | 93.34％ |
The sterilization test proves that the wormwood disinfection wet tissue is used for some main pathogenic bacteria; the bacteriostatic effect of escherichia coli, staphylococcus aureus and candida albicans is very ideal, and the bacteriostatic rate is over 99 percent.
Secondly, stability determination
Five wet tissue samples of examples 1-3 and comparative examples 1-2 were placed in a thermostat at 50 ℃ for 15 days. Taking out and returning to room temperature, and observing whether precipitation and discoloration occur; thereafter, the bactericidal activity was determined using the same methods and conditions as described above. The results are as follows:
table 2 stability measurement results 1
| Sample (I) | Traits |
| Example 1 | No precipitation and no discoloration |
| Example 2 | No precipitation and no discoloration |
| Example 3 | No precipitation and no discoloration |
| Comparative example 1 | No precipitation and no discoloration |
| Comparative example 2 | No precipitate and yellowing of wet towel liquid |
Table 3 stability test results 2
Stability tests prove that the wormwood disinfection wet tissue is used for some main pathogenic bacteria; the bacteriostasis and bacteriostasis rates of escherichia coli, staphylococcus aureus and candida albicans are still over 98 percent, and the stability is proved to be good.
Test example 2
Mechanical Property test
The breaking strength and elongation were determined according to ISO 9073-3-1989 textile nonwoven test method.
TABLE 4 mechanical Property results
Mechanical property tests prove that the wormwood disinfection wet tissue base material prepared by the invention has good mechanical property.
The foregoing detailed description of the preferred embodiments of the invention has been presented. It should be understood that numerous modifications and variations could be devised by those skilled in the art in light of the present teachings without departing from the inventive concepts. Therefore, the technical solutions available to those skilled in the art through logic analysis, reasoning and limited experiments based on the prior art according to the concept of the present invention should be within the scope of protection defined by the claims.
Claims (8)
1. The preparation method of the wormwood disinfection wet tissue is characterized by comprising the following steps:
(1) pulping and grinding wood pulp, adjusting the water content, and then making paper and forming to obtain wood pulp paper;
(2) carding polyester, moxa and moxa powder particles into a net to form a moxa polyester layer, compounding the moxa polyester layer with wood pulp paper, and sequentially performing spunlace, flat net suction and drying to obtain a moxa base material;
(3) soaking the wormwood base material in wet tissue liquid for 3-5h, and packaging to obtain the wormwood disinfection wet tissue;
the wet tissue liquid comprises the following raw materials in parts by weight: 0.5-2 parts of surfactant and 50-150 parts of deionized water;
the surfactant is formed by mixing disodium coconut monoethanolamide sulfosuccinate and dirhamnolipid lauryl ester according to the mass ratio of 1: 1;
the moxa base material comprises the following raw materials in parts by weight: 30-50 parts of wood pulp, 60-80 parts of terylene, 10-20 parts of wormwood powder particles and 20-30 parts of moxa.
2. The method for preparing a wet moxa roll for sterilization according to claim 1, wherein the web is carded by: and (3) feeding the mixture of the terylene, the wormwood powder particles and the moxa into a cotton dropping box by using a fan, preliminarily carding the mixture into a flocculent structure, and mutually winding, interweaving and filling to form a wormwood terylene layer.
3. The method for preparing the wormwood disinfection wet tissue as claimed in claim 1, wherein the compound process comprises: and compounding the upper layer, the middle layer and the lower layer to form a net, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer as the wormwood polyester layer carding net is formed.
4. The method for preparing the wormwood disinfectant wet wipe as set forth in claim 1, wherein the water-punching process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; and then the fiber web after the pre-wetting is sent into a spunlace device, and is sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement.
5. The method for preparing a wet moxa roll for sterilization as claimed in claim 1, wherein the flat web suction process comprises: and (4) pumping and dehydrating between the upper and lower flat nets by a vacuum pump.
6. The method for preparing a wet moxa roll for sterilization as claimed in claim 1, wherein the drying process comprises: the wormwood base material is sent into a vacuum drying oven with the temperature of 100-120 ℃ for drying for 3-5 h.
7. The method for preparing a wet moxa roll towel as claimed in claim 1, comprising the steps of:
(1) pulping pine wood pulp, carrying out disc grinding, adjusting the water content, and then making paper and forming to obtain wood pulp paper; the beating degree is controlled to be 19 degrees SR after disc grinding, the mass concentration of the wood pulp after the water content is adjusted to be 1.3 weight percent, and the weight of the wood pulp paper layer is 20g/m2；
(2) Carding moxa with the fineness of 1.32dtex and the length of 34mm of polyethylene terephthalate polyester, the length of 80mm and the fineness of 10D and 70-mesh moxa powder particles into a net to form a moxa polyester layer, compounding the moxa polyester layer with a wood pulp paper layer, and sequentially carrying out spunlace, flat net suction and drying to obtain a moxa base material; the weight of the wormwood polyester layer is 20g/m2(ii) a The weight of the mugwort substrate is 60g/m2；
The carding and web forming process comprises the following steps: sending the mixture of terylene, moxa and moxa powder particles into a cotton dropping box by a fan, preliminarily carding the mixture into a flocculent structure, mutually winding, interweaving and filling to form a moxa terylene layer;
the compounding process comprises the following steps: compounding an upper layer, a middle layer and a lower layer of nets, wherein the wormwood polyester layer is the upper layer and the lower layer, the wood pulp paper layer is the middle layer, and a composite structure with the wood pulp paper layer in the middle and the upper layer and the lower layer of nets formed by carding the wormwood polyester layer is formed;
the water jet process comprises the following steps: the fiber webs formed by carding webs are overlapped together, and are pre-wetted and compacted by a pre-wetting device after off-line compounding; then the fiber webs after the pre-wetting are sent into a spunlace device, and are sent into a spunlace machine through a conveying net curtain to be subjected to four times of front and back spunlace reinforcement, wherein the spunlace pressure is 90bar, 100bar, 150bar and 80bar respectively, so that the fiber webs of all layers are mutually entangled and are compounded into a whole to form the spunlace non-woven fabric;
the flat screen suction process is as follows: pumping and dehydrating between the upper and lower layers of flat nets by a vacuum pump; the drying process comprises the following steps: drying the spunlaced nonwoven fabric in a vacuum drying oven at the temperature of 110 ℃ for 4 hours;
(3) soaking the prepared 1kg of wormwood base material in 10kg of wet tissue liquid for 2h, and packaging to obtain the wormwood disinfection wet tissue.
8. A wormwood disinfection wet tissue, which is characterized by being prepared by the preparation method of the wormwood disinfection wet tissue as claimed in any one of claims 1 to 7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010024813.XA CN111214157B (en) | 2020-01-10 | 2020-01-10 | Wormwood sterilizing wet tissue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010024813.XA CN111214157B (en) | 2020-01-10 | 2020-01-10 | Wormwood sterilizing wet tissue and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111214157A CN111214157A (en) | 2020-06-02 |
| CN111214157B true CN111214157B (en) | 2022-04-22 |
Family
ID=70810341
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010024813.XA Active CN111214157B (en) | 2020-01-10 | 2020-01-10 | Wormwood sterilizing wet tissue and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111214157B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115522409B (en) * | 2021-06-27 | 2023-06-16 | 艾无量(河南)健康科技有限公司 | Moxa papermaking method |
Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525797A (en) * | 2009-04-17 | 2009-09-09 | 杨北成 | Blended textile and manufacture craft thereof |
| CN102535007A (en) * | 2012-01-12 | 2012-07-04 | 马骏 | Moxa non-woven fabric and production method thereof |
| CN102551580A (en) * | 2012-01-12 | 2012-07-11 | 杭州国光旅游用品有限公司 | Multifunctional moist towelette |
| CN102973927A (en) * | 2012-11-29 | 2013-03-20 | 李安平 | Manufacturing method of antipruritic toilet paper |
| CN106149449A (en) * | 2016-08-17 | 2016-11-23 | 安庆市新宜纸业有限公司 | A kind of preparation method of the napkin containing jasmine aroma |
| CN106192579A (en) * | 2016-08-17 | 2016-12-07 | 安庆市新宜纸业有限公司 | A kind of preparation method of the napkin containing orchid fragrance |
| CN106223108A (en) * | 2016-08-17 | 2016-12-14 | 安庆市新宜纸业有限公司 | A kind of preparation method of itch-stopping bactericidal napkin |
| CN106283840A (en) * | 2016-08-17 | 2017-01-04 | 安庆市新宜纸业有限公司 | A kind of preparation method of water solublity toilet paper |
| CN107981767A (en) * | 2017-11-29 | 2018-05-04 | 山东昌诺新材料科技有限公司 | A kind of terylene wood pulp wet tissue and preparation method thereof |
| CN109554825A (en) * | 2019-01-30 | 2019-04-02 | 宁波艾克本草纤维有限公司 | A kind of wormwood non-woven fabrics and its manufacturing method |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3485470B2 (en) * | 1998-08-11 | 2004-01-13 | ユニ・チャーム株式会社 | Wet tissue laminate and products containing it |
| JP2000273492A (en) * | 1999-03-29 | 2000-10-03 | Nicca Chemical Co Ltd | Cleaning agent composition and cleaning goods impregnated with the same |
| CN101745137A (en) * | 2009-12-31 | 2010-06-23 | 北京欧凯纳斯科技有限公司 | Degradable disinfectant wet tissue and production method and application thereof |
| CN102488473A (en) * | 2011-12-05 | 2012-06-13 | 铜陵洁雅生物科技股份有限公司 | Bamboo fiber makeup-removing wet tissue with whitening and moisturizing effects |
| CN102961286A (en) * | 2012-12-06 | 2013-03-13 | 杭州贝巧母婴用品有限公司 | Hygienic disinfectant wet tissue and preparation method thereof |
| US20140294925A1 (en) * | 2013-03-08 | 2014-10-02 | AGAE Technologies LLC | Formulations combining ramoplanin and rhamnolipids for combating bacterial infection |
| CN103215143A (en) * | 2013-03-15 | 2013-07-24 | 金红叶纸业集团有限公司 | Cleaning composition and facial tissue using the same |
| EP3419985A1 (en) * | 2016-02-22 | 2019-01-02 | Evonik Degussa GmbH | Rhamnolipid esters as nonionic surfactants for cosmetic use |
| PT3471541T (en) * | 2016-06-20 | 2021-07-20 | Capretto Ehf | Synergistic effects, augmenting antimicrobial effects of lipids |
| CN108095617B (en) * | 2017-11-30 | 2019-12-31 | 湖州科博信息科技有限公司 | Antibacterial and moisture-absorbing bath towel fabric |
| CN108192748A (en) * | 2017-12-28 | 2018-06-22 | 泉州市晋江恒安卫生科技有限公司 | A kind of impregnated wipe and preparation method thereof |
| KR102005266B1 (en) * | 2019-03-08 | 2019-07-31 | 주식회사 명진뉴텍 | Wet wipes composition comprising laurylpyridinium chloride and organic acid, polyhydric alcohol or mixtures thereof and wet wipes containing the same |
-
2020
- 2020-01-10 CN CN202010024813.XA patent/CN111214157B/en active Active
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525797A (en) * | 2009-04-17 | 2009-09-09 | 杨北成 | Blended textile and manufacture craft thereof |
| CN102535007A (en) * | 2012-01-12 | 2012-07-04 | 马骏 | Moxa non-woven fabric and production method thereof |
| CN102551580A (en) * | 2012-01-12 | 2012-07-11 | 杭州国光旅游用品有限公司 | Multifunctional moist towelette |
| CN102973927A (en) * | 2012-11-29 | 2013-03-20 | 李安平 | Manufacturing method of antipruritic toilet paper |
| CN106149449A (en) * | 2016-08-17 | 2016-11-23 | 安庆市新宜纸业有限公司 | A kind of preparation method of the napkin containing jasmine aroma |
| CN106192579A (en) * | 2016-08-17 | 2016-12-07 | 安庆市新宜纸业有限公司 | A kind of preparation method of the napkin containing orchid fragrance |
| CN106223108A (en) * | 2016-08-17 | 2016-12-14 | 安庆市新宜纸业有限公司 | A kind of preparation method of itch-stopping bactericidal napkin |
| CN106283840A (en) * | 2016-08-17 | 2017-01-04 | 安庆市新宜纸业有限公司 | A kind of preparation method of water solublity toilet paper |
| CN107981767A (en) * | 2017-11-29 | 2018-05-04 | 山东昌诺新材料科技有限公司 | A kind of terylene wood pulp wet tissue and preparation method thereof |
| CN109554825A (en) * | 2019-01-30 | 2019-04-02 | 宁波艾克本草纤维有限公司 | A kind of wormwood non-woven fabrics and its manufacturing method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN111214157A (en) | 2020-06-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR100902961B1 (en) | Antimicrobial formulations | |
| CN101669518B (en) | Germicidal antiviral composite containing chlorine dioxide | |
| CN1890359B (en) | Adhesion inhibition of micro organisms by non-ionic surfactants | |
| US5152996A (en) | Nonwoven wipes impregnated with an aqueous solution of a zinc acetate peroxide and a surfactant | |
| US10456437B1 (en) | Antibacterial wet wipe for skin care | |
| KR102067701B1 (en) | Fabric softener composition | |
| EP1285579B1 (en) | Bactericidal guanidine derivatives, dermally applicable composition, washing composition, and antibacterial fibre aggregate | |
| CN108166259A (en) | A kind of non-woven cloth composite antibacterial agent and preparation method thereof | |
| KR101983990B1 (en) | Cleansing composition comprising natural raw material extract and wet tissue comprising the same | |
| KR20060052521A (en) | Anti-microbial fiber products | |
| CN101658397A (en) | Functional wipes containing chlorine dioxide and application thereof | |
| CN111518635A (en) | Composite long-acting disinfection and bacteriostasis cleaning agent for medical textiles and preparation method thereof | |
| CN111214157B (en) | Wormwood sterilizing wet tissue and preparation method thereof | |
| CN111110574A (en) | Wet tissue with three-in-one functions of cleaning, sterilizing and moisturizing and preparation method thereof | |
| KR101566223B1 (en) | Water-tissue containing extract of artemisia | |
| JP2009268698A (en) | Antibacterial sheet-like article | |
| CN113637454A (en) | Natural herbal anti-mite anti-static bacteriostatic dust remover | |
| CN111691062A (en) | Antibacterial spunlace non-woven fabric for facial soft towel | |
| JP2002233471A (en) | Wet tissue | |
| KR20210024659A (en) | Composition comprising an antimicrobial enhancer comprising ampocarboxylate and a method of increasing the antimicrobial effect of the composition | |
| Nalankilli et al. | Antimicrobial cotton textiles by finishing with extracts of an Ethiopian plant (Solanum incanum) fruit | |
| CN114836271A (en) | Surface cleaning wet tissue for down garment | |
| CN102132704B (en) | Efficient sterilization crosslinking agent and method of for preparing hygienic sterilization product by using efficient sterilization crosslinking agent | |
| CN112006968A (en) | Disinfection wet tissue | |
| CN101513197B (en) | Sterilization and disinfection solution for cleaning tissues and method for preparing sterilization and disinfection cleaning tissues |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20220331 Address after: 410000 4th floor, scientific research office building, No. 169, environmental protection Middle Road, Yuhua District, Changsha City, Hunan Province Applicant after: Zhuhaitang (Hunan) Medical Chain Management Co.,Ltd. Address before: 453400 9 Chuangye Avenue, Chuangye Park, Fanxiang Town, Changyuan City, Xinxiang City, Henan Province Applicant before: Henan Runhe New Material Co.,Ltd. |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |