CN111184659A - Hair care essential oil block and preparation method and application thereof - Google Patents

Hair care essential oil block and preparation method and application thereof Download PDF

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Publication number
CN111184659A
CN111184659A CN202010206119.XA CN202010206119A CN111184659A CN 111184659 A CN111184659 A CN 111184659A CN 202010206119 A CN202010206119 A CN 202010206119A CN 111184659 A CN111184659 A CN 111184659A
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CN
China
Prior art keywords
essential oil
hair care
hair
block
silica gel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN202010206119.XA
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Chinese (zh)
Inventor
崔彦斌
陈帅超
于书权
宗振龙
朱彬
曹博
朱恒男
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Yantai Zhongkongjike Innovation Industrial Park Management Co Ltd
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Yantai Zhongkongjike Innovation Industrial Park Management Co Ltd
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Priority to CN202010206119.XA priority Critical patent/CN111184659A/en
Publication of CN111184659A publication Critical patent/CN111184659A/en
Priority to CN202010561397.7A priority patent/CN112057365A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216Solid or semisolid forms
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/87Application Devices; Containers; Packaging

Abstract

The invention relates to a hair care essential oil block, which comprises an essential oil part and a forming part; the essential oil part comprises plant essential oil and an essential oil adsorbent; the molding part comprises liquid silica gel and a curing catalyst; the mass ratio of the essential oil to the molding part is 1:1-1: 5; the essential oil part is wrapped in a solid block formed by solidifying the forming part. Also relates to a preparation method and application of the hair care essential oil block, comprising the following steps: firstly, preparing an essential oil mixture; secondly, preparing an essential oil adsorbent; thirdly, adding the essential oil mixture obtained in the first step into the container obtained in the second step, and stirring to obtain an essential oil part; fourthly, preparing a forming part precursor; fifthly, weighing the essential oil in the third step according to a proportion, adding the essential oil into the container in the fourth step, stirring, carrying out injection molding, and standing to obtain the hair care essential oil block. The hair care essential oil block is carried at an air outlet of the hair drier through the air nozzle, and the plant essential oil is blown to the hair to achieve the hair care effect. The hair care shampoo can effectively slow down the volatilization of plant essential oil, can be used with a hair drier for uniformly caring hair, reduces the waste in the using process and improves the hair care effect.

Description

Hair care essential oil block and preparation method and application thereof
Technical Field
The invention relates to a hair care essential oil block and a preparation method and application thereof, belonging to the technical field of hair care and beauty treatment.
Background
With the increasing living standard of substances, people are more deeply pursuing high-quality life and are more willing to enjoy the convenience brought by high-tech products to life. Among them, consumers are increasingly demanding personal care products, promoting the development of the washing, care and makeup industries, and hair care products are more and more. In the field of hair care, more and more hair care products are favored by people, such as hair conditioner, hair care film, hair care spray and the like, while plant essential oil is taken as the hair care product which is just started in China in recent years and gradually enters the eyes of people.
The plant essential oil is volatile aromatic substance extracted from flowers, roots, stems and fruits of plants, and has the characteristics of aromatic smell, high volatility, small molecules, easy absorption and beauty and skin care effects. Generally, plant essential oils contain more than one hundred components such as alcohols, aldehydes, acids, phenols, propiones, terpenes, and the like; the lipids and alcohols have important effects in hair care.
At present most people are after the hair washing, generally all can select the dry hair of mode through electric hair dryer, electric hair dryer is the mode through the air supply makes the equipment of wet hair rapid draing, for hair rapid draing, people generally adopt hot-blast hair drying, at this in-process, the electric heat arouses hair moisture loss easily, amino acid is heated the degeneration, thereby lead to hair scale damage, and then induce the hair frizzy, withered, the degree of depth damage leads to the split scheduling problem of hair, so people pay more and more attention to hair nursing and restoration after the hair dryer dries, and hair care essential oil is because of repairing hair damage effectual, be difficult for leading to the hair to go out advantages such as oil knot and smell fragrance, become people in the hair washing, the hair care product of liking the use after drying.
People generally apply essential oils to hair after drying the hair to repair damage to the hair. However, the essential oil is difficult to be evenly coated by manually coating the essential oil, so that the situations that the hair essential oil coated firstly is too much and the hair essential oil coated later is not enough are easily caused, the hair care effect is greatly reduced, and more essential oil is often used for coating the hair care essential oil on all the hairs; moreover, the hand painting can cause the waste of the essential oil on both hands, and the trouble of cleaning the essential oil on the hands causes inconvenience and trouble. The Chinese patent document with the publication number of CN203662188U discloses an essential oil electric hair dryer, wherein an air outlet net of the electric hair dryer is provided with an oil storage cotton, essential oil is dripped on the oil storage cotton, the essential oil can be blown to the hair while the hair is dried, the effect of protecting the hair by the essential oil is achieved, and inconvenience and trouble caused by the fact that the essential oil is smeared by hands are avoided. However, since plant essential oil is a substance with high volatility, the volatilization of the essential oil is stronger under the action of electric hot air, the essential oil on the oil storage cotton is limited, the essential oil is volatilized in a short time after hot air is started, too much essential oil is blown to the hair firstly, and the essential oil is not enough to the hair blown later, so that the hair care effect is influenced, and the essential oil waste is also caused.
Therefore, the technical problem to be solved by those skilled in the art is to find a hair care essential oil product which can avoid the inconvenience of coating by hands, and can not lead to the waste of essential oil and the uneven coating because the essential oil can not volatilize rapidly when in use.
Disclosure of Invention
The invention aims to overcome the defects that in the prior art, the hair care essential oil is smeared by bare hands and is not uniform and inconvenient to clean; the hair care essential oil block has the defects that the volatility of the hair care essential oil is strong, the essential oil is volatilized rapidly when an air blower blows the essential oil for hair care, the concentration of the essential oil blown to the hair is not uniform, the essential oil is wasted, the hair care effect is not good and the like, and the hair care essential oil block and the preparation method and the application thereof are provided.
The technical scheme for solving the technical problems is as follows: a hair care essential oil block comprises essential oil and molding part; the essential oil part comprises plant essential oil and an essential oil adsorbent; the molding part comprises liquid silica gel and a curing catalyst;
the mass ratio of the essential oil to the molding part is 1:1-1: 5;
the mass ratio of the plant essential oil to the essential oil adsorbent is 1:1-1: 10;
the mass ratio of the liquid silica gel to the curing catalyst is 1:0.01-1: 0.05;
the essential oil part is wrapped in the molding part.
According to the invention, volatile essential oil is wrapped in the macromolecular grid in a physical adsorption and curing wrapping mode, the volatile essential oil is extremely little volatilized at room temperature, can be slowly volatilized under the action of hot air, and cannot be rapidly volatilized to cause waste.
On the basis of the technical scheme, the invention can also make the following improvements:
further, the plant essential oil is one or more of peppermint essential oil, eucalyptus essential oil, lemongrass essential oil and lavender essential oil.
Further, the essential oil adsorbent comprises medium-pore silica gel and coarse-pore silica gel; the mass ratio of the medium-pore silica gel to the coarse-pore silica gel is 1:1-1: 3. Wherein the mesoporous silica gel has a pore volume of 0.6-0.75mL/g and a specific surface area of 400-500m2The pore volume of the coarse-pore silica gel is 0.75-1mL/g, the specific surface area is 300-2/g。
The pores of the mesoporous silica gel and the macroporous silica gel have good effect on the adsorption of the plant essential oil, are not easy to react with the essential oil, and have stable performance when being used at high temperature.
Further, the curing catalyst is a platinum vulcanizing agent.
The platinum vulcanizing agent is a non-toxic vulcanizing agent, has the characteristics of low vulcanizing temperature and high speed, can catalyze the curing reaction at normal temperature, is environment-friendly and tasteless, and does not influence the taste and the hair care effect of the hair care essential oil.
The invention also discloses a preparation method of the hair care essential oil block, which comprises the following steps:
step one, preparing plant essential oil: placing one or more plant essential oils and a solvent in a container, and stirring at room temperature to mix thoroughly;
step two, preparing an essential oil adsorbent: placing the essential oil adsorbent in a container, fully stirring, grinding, placing in a drying oven, drying at 105 deg.C for 12 hr, and naturally returning to room temperature;
step three, preparation of essential oil: adding the plant essential oil in the step one into the container in the step two, and fully stirring to obtain apparent dry powder;
step four, preparation of molding parts: placing liquid silica gel and curing catalyst in a container, and stirring for 10 min;
step five, curing and forming: and (3) adding the essential oil prepared in the third step into the container in the fourth step, stirring for 15min, injecting into a mold, and standing for 10 hours in shade to form a hair care essential oil block.
On the basis of the technical scheme, the invention can also make the following improvements:
further, the solvent is one or more of purified water, glycerol, absolute ethyl alcohol and silicone oil. The volume ratio of the plant essential oil to the solvent is 1:1-1: 10.
The plant essential oil is dissolved in the solvent, so that the plant essential oil can be better and more uniformly adsorbed on the essential oil adsorbent, and the loss of the plant essential oil in the preparation process is reduced. Meanwhile, solvents such as glycerol, silicone oil and the like have the functions of nourishing and caring hair.
Further, the maximum sample injection thickness of the mold is 5 mm.
Further, the third step further includes: weighing fiber non-woven fabric, cutting into particles, and ultrasonically dispersing for 1-3 hours; placing the mixture in a drying oven, and drying the mixture for 12 hours at 105 ℃; adding the mixture into the container obtained in the second step, and fully stirring; the above-mentionedThe mass ratio of the fiber non-woven fabric to the essential oil adsorbent is 1: 60; the gram weight of the fiber non-woven fabric is 20-200g/m2
The fiber non-woven fabric can increase the bridging among porous silica gel particles and increase the contact among the particles, thereby increasing the uniformity of essential oil in the system, preventing the occurrence of closed pores and avoiding unnecessary essential oil waste.
The invention also discloses an application of the hair care essential oil block, and the hair care essential oil block is carried at an air outlet of a hair drier through an air nozzle.
On the basis of the technical scheme, the invention can also make the following improvements:
furthermore, two clamping grooves are symmetrically arranged, and the width of each clamping groove is matched with the thickness of the hair care essential oil block; the hair care essential oil block is clamped in the clamping groove.
The invention has the advantages that:
(1) the volatile plant essential oil is dissolved in the solvent, physically adsorbed by the essential oil adsorbent and then wrapped in the curing block, so that the volatilization of the plant essential oil can be effectively slowed down;
(2) the hair care essential oil block is carried at the air outlet of the hair dryer by the air nozzle and is matched with the hair dryer for use, the plant essential oil cannot be volatilized completely at high temperature instantly, the waste in the using process is reduced, the plant essential oil is volatilized uniformly in the hair drying process, the plant essential oil is guaranteed to be blown to all parts of the hair, the hair care effect is improved, and the inconvenience of smearing the hair care essential oil by hands is avoided;
(3) the hair care essential oil block can be cut at will according to different air outlet carriers of the hair dryer so as to match the shape and the use requirements of the carriers, and the use is convenient and simple;
(4) the solid block essential oil is easier to store and transport, and does not need to be stored in a sealed way in the gap between two uses, so that the trouble in the use process is reduced;
(5) the manufacturing process is simple and can be realized at normal temperature; the material is non-toxic and high in stability, and has no influence on the physical and chemical properties of the essential oil; stable performance and lasting fragrance.
Drawings
FIG. 1 is a front view of a tuyere;
FIG. 2 is a top view of the tuyere;
FIG. 3 is a left side view of the tuyere;
FIG. 4 is a schematic view of a hair care essential oil block mounted on a tuyere;
the reference numbers are recorded as follows: 1-tuyere, 2-neck, 3-air inlet end and 4-hair care essential oil block.
Detailed Description
The principles and features of this invention are described below in conjunction with the following drawings, which are set forth by way of illustration only and are not intended to limit the scope of the invention.
Example 1
A preparation method of hair care essential oil blocks comprises the following steps:
1) weighing 6ml of glycerol and 1.5ml of plant essential oil, adding into a conical flask, and magnetically stirring at room temperature for 0.5h for later use; wherein the plant essential oil is any one of peppermint essential oil, eucalyptus essential oil, lemongrass essential oil and lavender essential oil;
2) weighing 6g of coarse silica gel and 6g of medium-pore silica gel, adding into a beaker, stirring for 0.5h at room temperature, fully grinding and mixing in a pot body, placing in an air-blast drying oven, setting the temperature to be 105 ℃, drying for 12h, and naturally returning to room temperature;
3) adding the mixture obtained in the step 1) into the beaker obtained in the step 2), and fully stirring the mixture until dry powder is obtained;
4) weighing 20g of liquid silica gel, placing in a beaker, adding 0.6g of platinum vulcanizing agent, and stirring for 10min for later use;
5) adding the powder in the step 3) into the beaker in the step 4), stirring for 15min, injecting into a prefabricated mold with the sample injection thickness of 5mm, and standing in the shade for 10 hours to prepare the hair care essential oil block.
Example 2
A preparation method of hair care essential oil blocks comprises the following steps:
1) weighing 1.25g of peppermint essential oil, Eucalyptus essential oil, lemongrass essential oil and lavender essential oil respectively, placing in a conical flask, and magnetically stirring at room temperature for 0.5 h;
2) weighing 2ml of glycerol and 3ml of purified water, adding into the conical flask obtained in the step 1), and continuously magnetically stirring for 0.5h at room temperature for later use;
3) weighing 4g of coarse silica gel and 6g of medium-pore silica gel, adding into a beaker, stirring for 0.5h at room temperature, and fully grinding in a pot body; placing in an air-blast drying oven, setting the temperature at 105 ℃, drying for 12h, and naturally returning to the room temperature;
4) adding the mixture obtained in the step 2) into the beaker obtained in the step 3), and fully stirring the mixture until dry powder is obtained;
5) weighing 20g of liquid silica gel, placing in a beaker, adding 0.5g of platinum vulcanizing agent, and stirring for 10min for later use;
6) adding the powder in the step 4) into the beaker in the step 5), stirring for 15min, injecting into a prefabricated mold with the sample injection thickness of 5mm, and standing in the shade for 10 hours to prepare the hair care essential oil block.
Example 3
A preparation method of hair care essential oil blocks comprises the following steps:
1) weighing 6ml of glycerol and 1.5ml of plant essential oil, adding into a conical flask, and magnetically stirring at room temperature for 0.5h for later use; wherein the plant essential oil is any one of peppermint essential oil, eucalyptus essential oil, lemongrass essential oil and lavender essential oil;
2) weighing 6g of coarse silica gel and 6g of medium-pore silica gel, adding into a beaker, stirring for 0.5h at room temperature, fully grinding and mixing in a pot body, placing in an air-blast drying oven, setting the temperature to be 105 ℃, drying for 12h, and naturally returning to room temperature;
3) weighing 200mg of fiber non-woven fabric, cutting into granules, adding into a beaker, ultrasonically dispersing for 2h, placing in an air-blast drying oven, setting the temperature to be 105 ℃, and drying for 12 h;
4) adding the mixture obtained in the step 1) into the beaker obtained in the step 2, stirring for 10min, adding the fiber non-woven fabric obtained in the step 3), and continuously stirring until powder with dry appearance is obtained;
5) weighing 20g of liquid silica gel in a beaker, adding 0.55g of platinum vulcanizing agent, and stirring for 10min to obtain a molded part precursor;
6) adding the powder in the step 4) into the beaker in the step 5), stirring for 15min, standing for 20min, injecting into a square prefabricated mold with the sample injection thickness of 5mm, and standing in the shade for 10 hours to obtain the hair care essential oil block.
Example 4
Referring to fig. 1-4, an application of a hair care essential oil block, the hair care essential oil block prepared by the above embodiment is carried at an air outlet of a hair dryer by an air nozzle 1; the inner diameter of the tuyere 1 is matched with the width of the hair care essential oil block 4; two clamping grooves 2 are symmetrically arranged in the air nozzle 1, and the width of each clamping groove 2 is matched with the thickness of the hair care essential oil block 4; the hair care essential oil block 4 is clamped in the clamping groove 2; the end part of the air nozzle 1 is provided with a flat air inlet end 3, and the width of the air inlet end 3 is matched with the inner diameter of an air outlet of the blower; the air nozzle 1 is clamped on an air outlet of the blower through an air inlet end 3.
The order of execution of the various steps set forth in the claims and description of the invention is not limited by the number of steps.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (10)

1. A hair care essential oil block is characterized by comprising essential oil parts and molding parts; the essential oil part comprises plant essential oil and an essential oil adsorbent; the molding part comprises liquid silica gel and a curing catalyst;
the mass ratio of the essential oil to the molding part is 1:1-1: 5;
the mass ratio of the plant essential oil to the essential oil adsorbent is 1:1-1: 10;
the mass ratio of the liquid silica gel to the curing catalyst is 1:0.01-1: 0.05;
the essential oil part is wrapped in the molding part.
2. The hair care essential oil block according to claim 1, wherein the plant essential oil is one or more of peppermint essential oil, eucalyptus essential oil, lemongrass essential oil, and lavender essential oil.
3. The hair care essential oil cake according to claim 2, wherein the essential oil adsorbent comprises medium pore silica gel and coarse pore silica gel; the mass ratio of the medium-pore silica gel to the coarse-pore silica gel is 1:1-1: 3.
4. The hair conditioning essential oil block according to claim 3, wherein the curing catalyst is a platinum vulcanizing agent.
5. A process for the preparation of hair care essential oil pieces according to any one of claims 1 to 4, comprising the steps of:
step one, preparing plant essential oil: placing one or more plant essential oils and a solvent in a container, and stirring at room temperature to mix thoroughly;
step two, preparing an essential oil adsorbent: placing the essential oil adsorbent in a container, fully stirring, grinding, placing in a drying oven, drying at 105 deg.C for 12 hr, and naturally returning to room temperature;
step three, preparation of essential oil: adding the plant essential oil in the step one into the container in the step two, and fully stirring to obtain apparent dry powder;
step four, preparation of molding parts: placing liquid silica gel and curing catalyst in a container, and stirring for 10 min;
step five, curing and forming: and (3) adding the essential oil prepared in the third step into the container in the fourth step, stirring for 15min, injecting into a mold, and standing for 10 hours in shade to form a hair care essential oil block.
6. The preparation method according to claim 5, wherein the solvent is one or more of purified water, glycerol, absolute ethyl alcohol, and silicone oil; the volume ratio of the plant essential oil to the solvent is 1:1-1: 10.
7. The method of claim 5, wherein the mold has a maximum injection depth of 5 mm.
8. The method of claim 5, wherein the third step further comprises: weighing fiber non-woven fabric, cutting into granules, ultrasonically dispersing for 1-3 hours, placing in a drying oven, and drying at 105 ℃ for 12 hours; adding the mixture into the container obtained in the second step, and fully stirring; the mass ratio of the fiber non-woven fabric to the essential oil adsorbent is 1: 60.
9. Use of a hair care essential oil patch according to any one of claims 1 to 4, wherein the hair care essential oil patch is carried at the outlet of a hair dryer by a tuyere.
10. The use of the hair care essential oil block according to claim 9, wherein two clamping grooves are symmetrically arranged in the air nozzle, and the width of each clamping groove is matched with the thickness of the hair care essential oil block; the hair care essential oil block is clamped in the clamping groove.
CN202010206119.XA 2020-03-23 2020-03-23 Hair care essential oil block and preparation method and application thereof Withdrawn CN111184659A (en)

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CN202010561397.7A CN112057365A (en) 2020-03-23 2020-06-18 Hair care essential oil block and preparation method and application thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111759785A (en) * 2020-08-19 2020-10-13 烟台中科恩吉科创新产业园管理有限公司 Preparation method of hair care and hair nourishing essential oil module

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203662188U (en) * 2013-12-25 2014-06-25 胡宇展 Electric hair dryer with essential oil blowing-out function
CN107047554A (en) * 2017-05-12 2017-08-18 中国科学院植物研究所 With natural plant essential oils attractant that function is trapped for Bemisia tabaci and preparation method thereof
CN107411306A (en) * 2017-09-14 2017-12-01 温州市日增电器有限公司 Hair-dryer essential oil tuyere
CN107595578B (en) * 2017-09-18 2020-07-07 广州精点高分子材料制品有限公司 Beauty roller
CN109549869A (en) * 2017-09-26 2019-04-02 谢玮 A kind of plant embellish hair essence oil
CN209376961U (en) * 2018-09-17 2019-09-13 朱弘 A kind of essential oil nursing tuyere for hair dryer
CN110292650A (en) * 2019-07-11 2019-10-01 广州佳伲斯防霉抗菌科技有限公司 A kind of preparation method of the deodorization pearl that absorbs water with core-shell structure
CN110339258A (en) * 2019-08-22 2019-10-18 新疆伊帕尔汗香料股份有限公司 A kind of sleeping essential oil and its cured granulate preparation method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111759785A (en) * 2020-08-19 2020-10-13 烟台中科恩吉科创新产业园管理有限公司 Preparation method of hair care and hair nourishing essential oil module

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Application publication date: 20200522