CN111074084A - Ground soaks uranium mining full-flow circulation experimental apparatus - Google Patents
Ground soaks uranium mining full-flow circulation experimental apparatus Download PDFInfo
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- CN111074084A CN111074084A CN201911327521.7A CN201911327521A CN111074084A CN 111074084 A CN111074084 A CN 111074084A CN 201911327521 A CN201911327521 A CN 201911327521A CN 111074084 A CN111074084 A CN 111074084A
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0221—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching
- C22B60/0226—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes by leaching using acidic solutions or liquors
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/02—Apparatus therefor
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
- C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/0265—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries extraction by solid resins
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Abstract
The invention belongs to the technical field of in-situ leaching uranium mining experimental equipment, and particularly relates to an in-situ leaching uranium mining full-flow circulation experimental device. The constant-speed constant-pressure double-cylinder pump is connected with a high-pressure test column through a leaching agent liquid inlet valve, a column leaching port pressure regulating valve is arranged at the outlet of the high-pressure test column, the column leaching port pressure regulating valve is connected with the upper part of an ion exchange column after passing through a leaching agent liquid outlet valve, the lower part of the ion exchange column is connected into a liquid collecting tank through an adsorption tail liquid valve, and the liquid collecting tank is connected to a stirring tank through a reciprocating plunger pump and a liquid collecting valve; the oxygen steel cylinder is connected to the stirring tank through an oxygen pressure regulating valve, an oxygen flow controller and an oxygen one-way valve, and the carbon dioxide steel cylinder is connected to the stirring tank through a carbon dioxide pressure regulating valve, a carbon dioxide flow controller and a carbon dioxide one-way valve; the stirring tank is connected to a constant-speed constant-pressure double-cylinder pump through a liquid distribution valve; the pressure regulating valve of the column leaching port is connected to the liquid collecting tank through the non-adsorption valve of the leaching liquid. The whole equipment process adopts a process circulation flow, only the transparent pipeline needs to be checked and replaced regularly, and the operation is convenient.
Description
Technical Field
The invention belongs to the technical field of in-situ leaching uranium mining experimental equipment, and particularly relates to an in-situ leaching uranium mining full-flow circulation experimental device.
Background
The existing in-situ leaching uranium mining column leaching experimental device can only complete a leaching experiment, does not contain a resin adsorption experiment, and a leaching solution cannot be recycled, so that the result is that the process of in-situ leaching uranium mining cannot be truly simulated. Usually, the result of an indoor experiment is better than that of a field experiment because impurity ions are not accumulated during acid column leaching; CO 22+O2HCO of uranium complex in leaching solution during column leaching3 -Ions can not be accumulated, the indoor experiment result is worse than the field experiment, and CO is caused2+O2The solid ratio of the leaching liquid in the column leaching experiment is large, and the time is long.
Because the flow rate of a column leaching experiment in a laboratory is small, the accumulated flow rate of the column leaching experiment in a daily period is only dozens of milliliters to hundreds of milliliters, and the control and the measurement of the flow rate of the leaching solution by the conventional equipment can not meet the requirements in order to realize the full-flow cycle use and the accurate control of the leaching solution.
Disclosure of Invention
The invention aims to provide a full-flow circulation experimental device for in-situ leaching uranium mining, which overcomes the defects in the prior art.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a constant-speed constant-pressure double-cylinder pump is connected with a high-pressure test column through a leaching agent liquid inlet valve, a column leaching port pressure regulating valve is arranged at the outlet of the high-pressure test column, the column leaching port pressure regulating valve is connected with the upper part of an ion exchange column after passing through a leaching agent liquid outlet valve, the lower part of the ion exchange column is connected into a liquid collecting tank through an adsorption tail liquid valve, and the liquid collecting tank is connected to a stirring tank through a reciprocating plunger pump and a liquid collecting valve; the oxygen steel cylinder is connected to the stirring tank through an oxygen pressure regulating valve, an oxygen flow controller and an oxygen one-way valve, and the carbon dioxide steel cylinder is connected to the stirring tank through a carbon dioxide pressure regulating valve, a carbon dioxide flow controller and a carbon dioxide one-way valve; the stirring tank is connected to a constant-speed constant-pressure double-cylinder pump through a liquid distribution valve; the pressure regulating valve of the column leaching port is connected to the liquid collecting tank through the non-adsorption valve of the leaching liquid.
The leaching agent enters a high-pressure test column through a leaching agent liquid inlet valve under constant current or constant pressure by a constant-speed constant-pressure double-cylinder pump, the solution obtained after reaction in the high-pressure test column is called leaching solution, the leaching solution is subjected to pressure regulation by a column leaching port pressure regulating valve, enters an ion exchange column through a leaching solution liquid outlet valve and is adsorbed, and is called adsorption tail solution, the adsorption tail solution is collected in a liquid collection tank through an adsorption tail solution valve, collected to a certain volume in the liquid collection tank and pumped into a stirring tank through a liquid collection valve by a reciprocating plunger pump; after the gas in the oxygen steel cylinder and the gas in the carbon dioxide steel cylinder are gasified, the gas is respectively regulated by the oxygen pressure regulating valve and the carbon dioxide pressure regulating valve, the gas is metered by the oxygen flow controller and the carbon dioxide flow controller, enters the stirring tank after passing through the oxygen one-way valve and the carbon dioxide one-way valve, and is stirred at high pressure together with the solution pumped by the reciprocating plunger pump in the stirring tank, the gas-liquid mixture after being fully and uniformly dissolved is called a leaching agent, and the leaching agent enters the constant-speed constant-pressure double-cylinder pump through the liquid distribution.
And the common end of the constant-speed constant-pressure double-cylinder pump and the leaching agent liquid inlet valve is connected with a leaching agent sampling valve.
And the lower part of the stirring tank A1 is provided with a stirring tank emptying valve.
And a pressure release valve of the stirring tank is arranged at the upper part of the stirring tank.
And a liquid collecting emptying valve is arranged at the lower part of the liquid collecting tank.
And the common end of the ion exchange column and the adsorption tail liquid valve is connected with an adsorption tail liquid sampling valve.
And the common end of the leachate outlet valve and the ion exchange column is connected with a leachate sampling valve.
The beneficial effects obtained by the invention are as follows:
(1) the in-situ conditions of the uranium ore stratum can be simulated, the geological composition of upper and lower covering layers and middle uranium ores is simulated, the pressure of an overlying rock layer of the uranium ore can be simulated, the pressure can be adjusted, the uranium ore can correspond to different burial depths, and meanwhile, the stress of bedrock in the uranium ore mining process can be adjusted.
(2) The method can simulate the proportion of the leaching agent in the actual process, including the injection amount of carbon dioxide and oxygen and the amount of water, simulate the proportion of gas and water through a laboratory, and influence on the experimental result, including optimization and adjustment of the output rate of uranium and the economic purpose, and guide a series of parameters of actual field construction aiming at a specific stratum.
(3) The whole equipment process adopts a process circulation flow, the process circulation can realize automatic control, and the transparent pipeline is only required to be checked and replaced periodically, so that the operation is convenient. The liquid level meter measures the position of the liquid level in real time, and the liquid is automatically replenished when the liquid level is lower than a set value through software operation, so that no load is prevented.
(4) The potential difference between the two ends of the adsorption device is measured by using a potentiometer so as to judge the working condition of the ion exchange resin, and when the adsorption capacity reaches a limit value, the adsorption device is automatically switched by using a pneumatic valve, so that the purpose of long-term use is achieved. And the potential difference value can be set independently. When the single-tube adsorption capacity is large, the mode can be switched manually.
(5) The double-cylinder pump is used for continuous liquid injection. The two cylinders are automatically switched, and the cylinder A is emptied, and the cylinder B is automatically switched, so that continuous liquid injection is realized.
Drawings
FIG. 1 is a structural diagram of a full-flow circulation experimental device for in-situ leaching uranium mining;
in the figure: a1: a stirring tank (the volume is 200ml, and the pressure resistance is 5 MPa); a2: an ion exchange column; a3: a liquid collection tank (the volume is 500 ml); b: a high pressure test column; d1: a constant-speed constant-pressure double-cylinder pump (single cylinder volume 100 ml); d2: a reciprocating plunger pump; p1: an oxygen cylinder; p2: a carbon dioxide steel cylinder; e1: an oxygen check valve; e2: a carbon dioxide check valve; f1: an oxygen pressure regulating valve; f2: a carbon dioxide pressure regulating valve; f3: a pressure regulating valve for a column leaching outlet; l1: an oxygen flow controller; l2: a carbon dioxide flow controller; g1: a leaching agent liquid inlet valve; g2: a leachant sampling valve; g3: a leachate outlet valve; g4: a leachate sampling valve; g5: a leachate non-adsorption valve; g6: an adsorption tail liquid valve; g7: an adsorption tail liquid sampling valve; g8: a liquid collecting and emptying valve; g9: a liquid collection valve; g10: a pressure release valve of the stirring tank; g11: a liquid distribution valve; g12: and an emptying valve of the stirring tank.
Detailed Description
The invention is described in detail below with reference to the figures and specific embodiments.
As shown in fig. 1, the components and connection relationship of the in-situ leaching uranium mining full-flow cycle experimental device of the invention are as follows: the constant-speed constant-pressure double-cylinder pump D1 is connected with a high-pressure test column B through a leaching agent liquid inlet valve G1, a column leaching port pressure regulating valve F3 is arranged at the outlet of the high-pressure test column B, the column leaching port pressure regulating valve F3 is connected with the upper part of an ion exchange column A2 after passing through a leaching agent liquid outlet valve G3, the lower part of the ion exchange column A2 is connected with a liquid collecting tank A3 through an adsorption tail liquid valve G6, and the liquid collecting tank A3 is connected with a stirring tank A1 through a reciprocating plunger pump D2 and a liquid collecting valve G9; an oxygen cylinder P1 is connected to a stirring tank A1 through an oxygen pressure regulating valve F1, an oxygen flow controller L1 and an oxygen check valve E1, and a carbon dioxide cylinder P2 is connected to a stirring tank A1 through a carbon dioxide pressure regulating valve F2, a carbon dioxide flow controller L2 and a carbon dioxide check valve E2; the stirring tank A1 is connected to a constant-speed constant-pressure double-cylinder pump D1 through a liquid distribution valve G11; the column leach port pressure regulating valve F3 is connected to the liquor collection tank A3 through a leach liquor non-adsorption valve G5.
A leaching agent sampling valve G2 is connected with the common end of the constant-speed constant-pressure double-cylinder pump D1 and the leaching agent liquid inlet valve G1; a leachate sampling valve G4 is connected with the common end of the leachate outlet valve G3 and the ion exchange column A2; an adsorption tail liquid sampling valve G7 is connected with the common end of the ion exchange column A2 and the adsorption tail liquid valve G6; the lower part of the liquid collecting tank A3 is provided with a liquid collecting emptying valve G8; a stirring tank pressure relief valve G10 is arranged at the upper part of the stirring tank A1; the lower part of the stirring tank A1 is provided with a stirring tank emptying valve G12.
Gas-liquid path description: the leaching agent is parallelly connected by two cylinders of a constant-speed constant-pressure double-cylinder pump D1, then is constant-current or constant-pressure, enters a high-pressure test column B through a leaching agent liquid inlet valve G1, the solution obtained after the reaction in the high-pressure test column B is called leaching solution, the leaching solution is subjected to pressure regulation by a column leaching port pressure regulating valve F3, enters an ion exchange column A2 through a leaching solution liquid outlet valve G3 and is called adsorption tail solution after being adsorbed, the adsorption tail solution is collected in a liquid collection tank A3 through an adsorption tail solution valve G6, is collected to a certain volume in a liquid collection tank A3, and is pumped into a stirring tank A1 through a liquid collection valve G9 through a reciprocating plunger pump D2; after the gas in the oxygen cylinder P1 and the gas in the carbon dioxide cylinder P2 are gasified, the gas is respectively regulated by an oxygen pressure regulating valve F1 and a carbon dioxide pressure regulating valve F2, the gas is metered by an oxygen flow controller L1 and a carbon dioxide flow controller L2, the gas passes through an oxygen one-way valve E1 and a carbon dioxide one-way valve E2 and then enters an agitator tank A1, the solution pumped by a reciprocating plunger pump D2 is stirred at high pressure in the agitator tank A1, the gas-liquid mixture after being fully and uniformly dissolved is called a leaching agent, and the leaching agent enters a constant-speed constant-pressure double-cylinder pump D1 through a liquid distribution valve G11.
The leaching agent components are sampled and analyzed through a leaching agent sampling valve G2;
sampling and analyzing the components of the leaching solution through a leaching solution sampling valve G4;
sampling and analyzing the components of the adsorption tail liquid through an adsorption tail liquid sampling valve G7;
to replace the solution, the sump A3 may be vented via a sump vent valve G8; agitator tank A1 may be vented via agitator tank vent valve G12; agitator tank A1 was depressurized via agitator tank relief valve G10.
Sometimes, for experiment needs, the pressure of the outlet of the high-pressure test column B is regulated by a pressure regulating valve F3 of a column leaching port, and then the outlet directly enters a liquid collecting tank A3 without ion exchange of an ion exchange column A2.
After the leachate in the high-pressure test column B is discharged, the adsorption tail liquid passing through the ion exchange column A2 enters a liquid collecting tank A3, the solution in the liquid collecting tank A3 is periodically pumped into a stirring tank A1 through a reciprocating plunger pump D2, and O is discharged2And CO2The solution is metered by an oxygen flow controller L1 and a carbon dioxide flow controller L2 and then added into a stirring tank A1, and the stirred solution is injected into a high-pressure test column B by a constant-speed constant-pressure double-cylinder pump D1.
Wherein anion exchange resin capable of adsorbing uranium is filled in the ion exchange column A2, the general ion exchange column A2 is used for standby, and the ion exchange column A2 can be replaced in time after the resin is saturated in the experiment;
wherein the capacity of the liquid collection tank A3 is 500ml, the capacity of the stirring tank A1 is 200ml, and the volume of each cylinder body in the constant-speed constant-pressure double-cylinder pump D1 is 100 ml; when the solution in the liquid tank A3 to be collected is 200ml each time, the solution is pumped into the stirring tank A1 by a reciprocating plunger pump D2 at regular intervals, the solution pumped into the stirring tank A1 is about 150ml, and the liquid level height can be sensed by a liquid level meter in the stirring tank;
wherein the pressure of the stirring tank A1 is 5MPa, and the stirring function is to ensure O2And CO2Fully dissolving;
wherein the solution is absorbed into two cylinders of a constant-speed constant-pressure double-cylinder pump D1 after being fully dissolved in a stirring tank A1;
the solution can be injected into the high-pressure test column B at a constant flow (the flow rate is 0.02-0.1 ml/min) or at a constant pressure (less than 10MPa) through a constant-speed constant-pressure double-cylinder pump D1, and double cylinders of the constant-speed constant-pressure double-cylinder pump D1 can be automatically switched; as long as any one of the double cylinders of the constant-speed constant-pressure double-cylinder pump D1 has no solution, the solution in the stirring tank A1 can be automatically supplemented into the empty cylinder.
Claims (8)
1. The utility model provides a full flow circulation experimental apparatus of uranium mining is leached in ground which characterized in that: the constant-speed constant-pressure double-cylinder pump is connected with a high-pressure test column through a leaching agent liquid inlet valve, a column leaching port pressure regulating valve is arranged at the outlet of the high-pressure test column, the column leaching port pressure regulating valve is connected with the upper part of an ion exchange column after passing through a leaching agent liquid outlet valve, the lower part of the ion exchange column is connected into a liquid collecting tank through an adsorption tail liquid valve, and the liquid collecting tank is connected to a stirring tank through a reciprocating plunger pump and a liquid collecting valve; the oxygen steel cylinder is connected to the stirring tank through an oxygen pressure regulating valve, an oxygen flow controller and an oxygen one-way valve, and the carbon dioxide steel cylinder is connected to the stirring tank through a carbon dioxide pressure regulating valve, a carbon dioxide flow controller and a carbon dioxide one-way valve; the stirring tank is connected to a constant-speed constant-pressure double-cylinder pump through a liquid distribution valve; the pressure regulating valve of the column leaching port is connected to the liquid collecting tank through the non-adsorption valve of the leaching liquid.
2. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: the leaching agent enters a high-pressure test column through a leaching agent liquid inlet valve under constant current or constant pressure by a constant-speed constant-pressure double-cylinder pump, the solution obtained after reaction in the high-pressure test column is called leaching solution, the leaching solution is subjected to pressure regulation by a column leaching port pressure regulating valve, enters an ion exchange column through a leaching solution liquid outlet valve and is adsorbed, and is called adsorption tail solution, the adsorption tail solution is collected in a liquid collection tank through an adsorption tail solution valve, collected to a certain volume in the liquid collection tank and pumped into a stirring tank through a liquid collection valve by a reciprocating plunger pump; after the gas in the oxygen steel cylinder and the gas in the carbon dioxide steel cylinder are gasified, the gas is respectively regulated by the oxygen pressure regulating valve and the carbon dioxide pressure regulating valve, the gas is metered by the oxygen flow controller and the carbon dioxide flow controller, enters the stirring tank after passing through the oxygen one-way valve and the carbon dioxide one-way valve, and is stirred at high pressure together with the solution pumped by the reciprocating plunger pump in the stirring tank, the gas-liquid mixture after being fully and uniformly dissolved is called a leaching agent, and the leaching agent enters the constant-speed constant-pressure double-cylinder pump through the liquid distribution.
3. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and the common end of the constant-speed constant-pressure double-cylinder pump and the leaching agent liquid inlet valve is connected with a leaching agent sampling valve.
4. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and the lower part of the stirring tank A1 is provided with a stirring tank emptying valve.
5. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and a pressure release valve of the stirring tank is arranged at the upper part of the stirring tank.
6. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and a liquid collecting emptying valve is arranged at the lower part of the liquid collecting tank.
7. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and the common end of the ion exchange column and the adsorption tail liquid valve is connected with an adsorption tail liquid sampling valve.
8. The in-situ leaching uranium mining full-flow cycle experimental device according to claim 1, characterized in that: and the common end of the leachate outlet valve and the ion exchange column is connected with a leachate sampling valve.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911327521.7A CN111074084A (en) | 2019-12-20 | 2019-12-20 | Ground soaks uranium mining full-flow circulation experimental apparatus |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911327521.7A CN111074084A (en) | 2019-12-20 | 2019-12-20 | Ground soaks uranium mining full-flow circulation experimental apparatus |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667844A (en) * | 2021-08-23 | 2021-11-19 | 南华大学 | Device and method for leaching sandstone uranium ore through micro-nano bubble oxidation |
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| CN206418175U (en) * | 2016-12-30 | 2017-08-18 | 新疆中核天山铀业有限公司 | A kind of CO2+O2 ground-dipping uranium extractions oxygenation liquid check device |
| CN107460349A (en) * | 2017-07-06 | 2017-12-12 | 核工业北京化工冶金研究院 | A kind of in-situ acid uranium leaching laboratory simulation device and test method |
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2019
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| WO2011082453A1 (en) * | 2010-01-08 | 2011-07-14 | Adelaide Control Engineers Pty Ltd | Apparatus for the production of yellowcake from a uranium peroxide precipitate |
| WO2014029017A1 (en) * | 2012-08-23 | 2014-02-27 | Chemetics Inc. | Hydrometallurgical process using multi-stage nanofiltration |
| CN103711462A (en) * | 2012-10-09 | 2014-04-09 | 核工业北京化工冶金研究院 | Leaching experimental facility for in-situ leaching uranium mining |
| CN105506275A (en) * | 2015-12-15 | 2016-04-20 | 东华理工大学 | Flow uranium leaching system and flow uranium leaching process |
| CN206418175U (en) * | 2016-12-30 | 2017-08-18 | 新疆中核天山铀业有限公司 | A kind of CO2+O2 ground-dipping uranium extractions oxygenation liquid check device |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113667844A (en) * | 2021-08-23 | 2021-11-19 | 南华大学 | Device and method for leaching sandstone uranium ore through micro-nano bubble oxidation |
| CN113667844B (en) * | 2021-08-23 | 2022-09-27 | 南华大学 | Device and method for leaching sandstone uranium ore through micro-nano bubble oxidation |
| JP2023031231A (en) * | 2021-08-23 | 2023-03-08 | 南華大学 | Device and method for leaching sandstone uranium ore through micro-nano bubble oxidation |
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Application publication date: 20200428 |