CN111011594A - Microcapsule for embedding fish oil and preparation method thereof - Google Patents

Microcapsule for embedding fish oil and preparation method thereof Download PDF

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Publication number
CN111011594A
CN111011594A CN201911393192.6A CN201911393192A CN111011594A CN 111011594 A CN111011594 A CN 111011594A CN 201911393192 A CN201911393192 A CN 201911393192A CN 111011594 A CN111011594 A CN 111011594A
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CN
China
Prior art keywords
parts
fish oil
solution
microcapsule
purified water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911393192.6A
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Chinese (zh)
Inventor
夏亮
卢鹏飞
倪静
濮楷人
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Jiangsu Yabo Animal Health Technology Co ltd
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Jiangsu Yabo Animal Health Technology Co ltd
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Publication date
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Priority to CN201911393192.6A priority Critical patent/CN111011594A/en
Publication of CN111011594A publication Critical patent/CN111011594A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/10Animal feeding-stuffs obtained by microbiological or biochemical processes
    • A23K10/16Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • A23K10/22Animal feeding-stuffs from material of animal origin from fish
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K40/00Shaping or working-up of animal feeding-stuffs
    • A23K40/30Shaping or working-up of animal feeding-stuffs by encapsulating; by coating

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Biomedical Technology (AREA)
  • Physiology (AREA)
  • Animal Husbandry (AREA)
  • Molecular Biology (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Microbiology (AREA)
  • Marine Sciences & Fisheries (AREA)
  • Biochemistry (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Fodder In General (AREA)

Abstract

The invention discloses an embedded fish oil microcapsule and a preparation method thereof, aiming at providing a microcapsule which is designed for pets, has good palatability (including but not limited to cats and dogs), has low fishy smell of fish oil and is more willing to be eaten by pets; the technical key points are as follows: the fish oil microcapsule for pets comprises the following components in parts by weight: 10-40 parts of fish oil, 0-1 part of natural vitamin E, 0-1 part of rosemary extract, 1-5 parts of Arabic gum, 1-50 parts of sodium starch octenyl succinate, 1-50 parts of soybean protein isolate, 1-10 parts of sodium caseinate, 0-3 parts of monoglyceride, 0-3 parts of sucrose fatty acid ester, 10-30 parts of chicken liver powder, 1-10 parts of yeast extract and 300-500 parts of purified water, and spray drying is carried out to obtain final powder; relates to the field of livestock breeding.

Description

Microcapsule for embedding fish oil and preparation method thereof
Technical Field
The invention belongs to the field of livestock breeding, and particularly relates to an embedded fish oil microcapsule and a preparation method thereof.
Background
In recent years, with the continuous improvement of the living standard of people in China, the living conditions of the raised pets are better and better, but the health problem and the obesity problem of the pets also come along. The fish oil serving as a novel nutrient is well established in the market for improving the immunity of pets, reducing cholesterol, maintaining the health of heart and blood vessels, brightening hair and the like, but most of the fishy smell of the fish oil is rather unpleasant, so that most of pets are unwilling to eat the fish oil.
Therefore, it is necessary to provide fish oil microcapsules for pets, which can effectively mask the fishy smell of fish oil and are designed for pets.
Disclosure of Invention
The invention aims to provide a fish oil microcapsule and an embedding preparation method thereof, which solve the technical problems.
In order to achieve the technical purpose and achieve the technical requirements, the invention adopts the technical scheme that: an embedded fish oil microcapsule is characterized in that: the composition comprises the following components in parts by weight: 10-40 parts of fish oil, 0-2 parts of antioxidant, 1-110 parts of wall material, 0-6 parts of emulsifier, 10-30 parts of chicken liver powder, 1-10 parts of yeast extract and 300-500 parts of purified water, and the final powder is obtained by a centrifugal spray drying technology.
Further: the antioxidant is one or more of sodium erythorbate, tocopherol, BHT, TBHQ, BHA, and herba Rosmarini officinalis extract.
Further: the wall material is one or more of soybean protein isolate, concentrated whey protein, sodium caseinate, Arabic gum, sodium alginate and gelatin.
Further: the emulsifier is one or more of sucrose fatty acid ester, sodium stearyl lactate, monoglyceride, polyglycerol ester and diacetyl tartaric acid monoglyceride.
A preparation method of an embedded fish oil microcapsule comprises the following steps: the method comprises the following steps:
1) weighing the components in parts by weight according to the claim 1;
2) and (2) adding 300-500 parts of purified water weighed in the step 1), heating the purified water to 30-60 ℃, sequentially adding 1-110 parts of wall materials, 10-30 parts of chicken liver powder and 1-10 parts of yeast extract, stirring, dissolving completely to obtain a solution A, and standing for later use.
3) Heating 10-40 parts of the fish oil weighed in the step 1) to 80 ℃, adding 0-2 parts of antioxidant into the fish oil, adding 0-6 parts of emulsifier into purified water after the antioxidant is completely dissolved, stirring, and standing the obtained solution B for later use after the emulsifier is completely dissolved;
4) pouring the solution A obtained in the step 1) into an emulsifying pot, starting stirring and emulsifying, slowly adding the solution B obtained in the step 3) into the emulsifying pot through a liquid feeding hole, starting timing and emulsifying for 20 minutes after adding, and obtaining a solution C after emulsifying;
5) adding the solution C obtained in the step 4) into a high-pressure homogenizer, homogenizing at the homogenizing pressure of 30Mpa twice, and standing the homogenized solution for later use;
6) drying the solution obtained in the step 5) into powder by using a centrifugal spray drying technology, wherein the spray drying parameters are as follows: air inlet temperature: the temperature of 180 ℃, the air outlet temperature of 90 ℃, the air inlet frequency of 20Hz, the air outlet frequency of 50Hz and the feeding speed of 100 r/min.
The invention has the following beneficial effects:
compared with the prior pet fish oil, the fish oil microcapsule provided by the invention has the following advantages: 1. the fish oil has lighter fishy smell, and chicken liver powder and yeast extract are added as food calling ingredients, so that the fish oil has better palatability; 2. the product of the invention is powdery, is easier to feed compared with the existing liquid fish oil on the market, and is convenient to be sprayed on pet food or directly fed.
The specific implementation mode is as follows:
example 1
The invention relates to an embedded fish oil microcapsule, which consists of the following components in parts by weight: 30 parts of fish oil, 0.1 part of natural vitamin E, 0.1 part of rosemary extract, 2 parts of Arabic gum, 5 parts of sodium starch octenyl succinate, 20 parts of soybean protein isolate, 3 parts of sodium caseinate, 2 parts of monoglyceride, 0.5 part of sucrose fatty acid ester, 10 parts of chicken liver powder, 3 parts of yeast extract and 300 parts of purified water.
Example 2
The invention relates to an embedded fish oil microcapsule, which consists of the following components in parts by weight: 20 parts of fish oil, 0.2 part of natural vitamin E, 0.1 part of rosemary extract, 2 parts of Arabic gum, 10 parts of sodium starch octenyl succinate, 50 parts of isolated soy protein, 2 parts of sodium caseinate, 1 part of monoglyceride, 0.5 part of sucrose fatty acid ester, 15 parts of chicken liver powder, 5 parts of yeast extract and 350 parts of purified water.
Example 3
The invention relates to an embedded fish oil microcapsule, which consists of the following components in parts by weight: 35 parts of fish oil, 0.3 part of natural vitamin E, 0.3 part of rosemary extract, 3 parts of Arabic gum, 20 parts of starch sodium octenyl succinate, 40 parts of isolated soy protein, 3 parts of sodium caseinate, 1.5 parts of monoglyceride, 1 part of sucrose fatty acid ester, 20 parts of chicken liver powder, 8 parts of yeast extract and 400 parts of purified water.
Example 4
The invention relates to an embedded fish oil microcapsule, which consists of the following components in parts by weight: 25 parts of fish oil, 0.4 part of natural vitamin E, 0.4 part of rosemary extract, 4 parts of Arabic gum, 30 parts of sodium starch octenyl succinate, 30 parts of isolated soy protein, 6 parts of sodium caseinate, 2 parts of monoglyceride, 2 parts of sucrose fatty acid ester, 25 parts of chicken liver powder, 9 parts of yeast extract and 450 parts of purified water.
Example 5
The invention relates to an embedded fish oil microcapsule, which consists of the following components in parts by weight: 15 parts of fish oil, 0.3 part of natural vitamin E, 0.2 part of rosemary extract, 3 parts of Arabic gum, 40 parts of sodium starch octenyl succinate, 20 parts of soybean protein isolate, 8 parts of sodium caseinate, 2.5 parts of monoglyceride, 3 parts of sucrose fatty acid ester, 20 parts of chicken liver powder, 2 parts of yeast extract and 350 parts of purified water.
Examples 1 to 5 preparation of microcapsules containing embedded fish oil: comprises the following steps in sequence
1) Weighing the following components in parts by weight: 10-40 parts of fish oil, 0-1 part of natural vitamin E, 0-1 part of rosemary extract, 1-5 parts of Arabic gum, 1-50 parts of sodium starch octenyl succinate, 1-50 parts of soybean protein isolate, 1-10 parts of sodium caseinate, 0-3 parts of monoglyceride, 0-3 parts of sucrose fatty acid ester, 10-30 parts of chicken liver powder, 1-10 parts of yeast extract and 300-500 parts of purified water;
2) weighing 300-500 parts of purified water, heating the purified water to 30-60 ℃, then sequentially adding 1-5 parts of Arabic gum, 1-50 parts of sodium starch octenyl succinate, 1-50 parts of soybean protein isolate, 1-10 parts of sodium caseinate, 10-30 parts of chicken liver powder and 1-10 parts of yeast extract, stirring, and completely dissolving to obtain a solution A for later use.
3) Heating 10-40 parts of the fish oil weighed in the step to 80 ℃, then adding 0-1 part of natural vitamin E and 0-1 part of rosemary extract into the fish oil, adding 0-3 parts of monoglyceride and 0-3 parts of sucrose fatty acid ester into the fish oil after all antioxidants are dissolved, stirring, and standing the obtained solution B for later use after all emulsifiers are dissolved;
4) pouring the solution A into an emulsifying pot, starting stirring and emulsifying, slowly adding the solution B into the emulsifying pot through a liquid feeding hole, starting timing and emulsifying for 20 minutes after adding, and emulsifying to obtain a solution C;
5) adding the solution C into a high-pressure homogenizer with the homogenizing pressure of 30Mpa, homogenizing twice, and standing the homogenized solution for later use;
6) drying the solution obtained in the step 5) into powder by using a centrifugal spray drying technology, wherein the spray drying parameters are as follows: air inlet temperature: the temperature of 180 ℃, the air outlet temperature of 90 ℃, the air inlet frequency of 20Hz, the air outlet frequency of 50Hz and the feeding speed of 100 r/min. Spray drying to obtain the fish oil microcapsule product.
In particular use: directly feeding the pet or adding the pet into food.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that it is obvious to those skilled in the art that various modifications and improvements can be made without departing from the principle of the present invention, and these modifications and improvements should also be considered as the protection scope of the present invention.

Claims (5)

1. An embedded fish oil microcapsule is characterized in that: the composition comprises the following components in parts by weight: 10-40 parts of fish oil, 0-2 parts of antioxidant, 1-110 parts of wall material, 0-6 parts of emulsifier, 10-30 parts of chicken liver powder, 1-10 parts of yeast extract and 300-500 parts of purified water, and the final powder is obtained by a centrifugal spray drying technology.
2. The encapsulated fish oil microcapsule of claim 1, wherein: the antioxidant is one or more of sodium erythorbate, tocopherol, BHT, TBHQ, BHA, and herba Rosmarini officinalis extract.
3. The encapsulated fish oil microcapsule of claim 1, wherein: the wall material is one or more of soybean protein isolate, concentrated whey protein, sodium caseinate, Arabic gum, sodium alginate and gelatin.
4. The encapsulated fish oil microcapsule of claim 1, wherein: the emulsifier is one or more of sucrose fatty acid ester, sodium stearyl lactate, monoglyceride, polyglycerol ester and diacetyl tartaric acid monoglyceride.
5. A preparation method of an embedded fish oil microcapsule comprises the following steps: the method comprises the following steps:
1) weighing the components in parts by weight according to the claim 1;
2) adding 300-500 parts of purified water weighed in the step 1), heating the purified water to 30-60 ℃, sequentially adding 1-110 parts of wall materials, 10-30 parts of chicken liver powder and 1-10 parts of yeast extract, stirring, dissolving completely to obtain a solution A, and placing for later use;
3) heating 10-40 parts of the fish oil weighed in the step 1) to 80 ℃, adding 0-2 parts of antioxidant into the fish oil, adding 0-6 parts of emulsifier into purified water after the antioxidant is completely dissolved, stirring, and standing the obtained solution B for later use after the emulsifier is completely dissolved;
4) pouring the solution A obtained in the step 1) into an emulsifying pot, starting stirring and emulsifying, slowly adding the solution B obtained in the step 3) into the emulsifying pot through a liquid feeding hole, starting timing and emulsifying for 20 minutes after adding, and obtaining a solution C after emulsifying;
5) adding the solution C obtained in the step 4) into a high-pressure homogenizer, homogenizing at the homogenizing pressure of 30Mpa twice, and standing the homogenized solution for later use;
6) drying the solution obtained in the step 5) into powder by using a centrifugal spray drying technology, wherein the spray drying parameters are as follows: air inlet temperature: the temperature of 180 ℃, the air outlet temperature of 90 ℃, the air inlet frequency of 20Hz, the air outlet frequency of 50Hz and the feeding speed of 100 r/min.
CN201911393192.6A 2019-12-30 2019-12-30 Microcapsule for embedding fish oil and preparation method thereof Pending CN111011594A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113261620A (en) * 2021-06-07 2021-08-17 山东省汇富农牧发展有限公司 Preparation method of female rabbit feed additive containing oregano oil

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101669920A (en) * 2008-09-10 2010-03-17 阜宁怀仁生物有限公司 Strong anti-oxidation DHA microcapsule and preparation method thereof
CN102511664A (en) * 2012-01-16 2012-06-27 天津农学院 Fish oil feed additive and production method thereof
CN107439801A (en) * 2017-09-01 2017-12-08 南通香佳纺织科技有限公司 A kind of treble cut fish oil micro-capsule cat food additive and preparation method thereof
CN108142643A (en) * 2018-02-07 2018-06-12 上海宠幸宠物用品有限公司 It is a kind of for health food of pet dog allotriophagy and preparation method thereof
CN108902503A (en) * 2018-07-26 2018-11-30 湖南普菲克生物科技有限公司 A kind of functional powder grease and its preparation and application

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101669920A (en) * 2008-09-10 2010-03-17 阜宁怀仁生物有限公司 Strong anti-oxidation DHA microcapsule and preparation method thereof
CN102511664A (en) * 2012-01-16 2012-06-27 天津农学院 Fish oil feed additive and production method thereof
CN107439801A (en) * 2017-09-01 2017-12-08 南通香佳纺织科技有限公司 A kind of treble cut fish oil micro-capsule cat food additive and preparation method thereof
CN108142643A (en) * 2018-02-07 2018-06-12 上海宠幸宠物用品有限公司 It is a kind of for health food of pet dog allotriophagy and preparation method thereof
CN108902503A (en) * 2018-07-26 2018-11-30 湖南普菲克生物科技有限公司 A kind of functional powder grease and its preparation and application

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
熊华等: "饲用微胶囊鱼油粉末添加剂中试研究", 《饲料研究》 *
苏阳等: "鱼油微胶囊化研究进展", 《食品研究与开发》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113261620A (en) * 2021-06-07 2021-08-17 山东省汇富农牧发展有限公司 Preparation method of female rabbit feed additive containing oregano oil

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Application publication date: 20200417

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