CN110981068A - Preparation method of acidic water for cosmetics - Google Patents
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
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- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F1/461—Treatment of water, waste water, or sewage by electrochemical methods by electrolysis
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- C02F1/00—Treatment of water, waste water, or sewage
- C02F2001/007—Processes including a sedimentation step
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/08—Seawater, e.g. for desalination
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A20/00—Water conservation; Efficient water supply; Efficient water use
- Y02A20/124—Water desalination
- Y02A20/131—Reverse-osmosis
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Abstract
The invention discloses a preparation method of acidic water for cosmetics, which comprises the steps of using seawater as raw water, carrying out sedimentation, filtration, secondary sedimentation and fine filtration, then evaporating to obtain primary target water with the conductivity of 80-150 mu s/cm, and then carrying out the following steps on the primary target water: carrying out fine filtration on the primary target water again, wherein the filtration precision is more than or equal to 0.2 mu m; performing reverse osmosis on the primary target water after the secondary fine filtration, wherein the conductivity of reverse osmosis effluent is 0-10 mu s/cm, and the volume ratio of the target water obtained by the reverse osmosis to the wastewater is more than or equal to 7-10: 1; and then adding marine minerals into the target water, adjusting the conductivity to 20-50 mu s/cm, and carrying out electrolysis to obtain acidic water with the pH value of 3.2-3.8 and the conductivity of 20-80 mu s/cm. The invention uses the seawater acid water for paper cups, and no chemical substance is added, so that the electrolyzed acid water has obvious whitening effect and also has obvious sterilization and bacteriostasis effects.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to acidic water for cosmetics.
Background
Human skin is often affected by oxidative stress, both endogenous and exogenous, caused by free radicals and Ultraviolet (UV) radiation. Studies have reported that skin exposed to oxidative stress or ultraviolet light is associated with photoaging and tumorigenesis. Solar uv exposure is associated with more than two-thirds of cases and may be the primary cause of skin cancer. The incidence of malignant melanoma of the skin has increased over the past few decades. It is one of the most aggressive diseases in skin cancer, because of its strong metastatic propensity. Unlike other cancers, metastatic melanoma is not easily treated by standard methods of surgery, radiation therapy or chemotherapy. Thus, metastatic melanoma often results in poor patient prognosis. Naturally occurring drugs that induce cancer cell death without significant side effects would be good chemopreventive agents.
Recently, acidic water has been used in medicine. CN201210157127.5, an acidic electrolyzed water and a composition containing the same, wherein the acidic electrolyzed water with weak acidity, low electrical conductivity and high oxidation potential is utilized to have the effects of bacteriostasis, anti-inflammation, anti-oxidation, wound healing promotion and the like, but has no cytotoxicity and no allergy, and can be proved to inhibit the proliferation and migration of skin melanoma cells, so that the acidic electrolyzed water can be safely applied to cosmetic compositions, medical compositions or other compositions for disinfecting the skin surface. The production process of the acid water for cosmetics is not yet mature.
In summary, the existing acidic water production process has the following defects: the addition of acidic substances is needed, so that skin health problems such as allergy and the like are easily caused; the acidic water prepared by the prior art has strong irritation and mild property, is not suitable for cosmetics, does not have a beautifying effect, and cannot tighten and brighten the skin.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: aiming at the defects in the prior art, the preparation method of the acidic water for the cosmetics is provided, no acidic substance is added in the preparation method, and the prepared acidic water has the effects of tightening and brightening the skin and has obvious effects of beautifying and protecting the skin.
In order to solve the technical problems, the technical scheme of the invention is as follows:
a preparation method of acidic water for cosmetics uses seawater/brine as raw water, and the raw water is subjected to sedimentation, filtration, secondary sedimentation and fine filtration and then is evaporated to obtain primary target water with the conductivity of 80-150 mu s/cm, and then the primary target water is subjected to the following steps:
fine filtering again: introducing the primary target water into a fine filter, and performing fine filtration again, wherein the filtration precision is more than or equal to 0.2 mu m;
reverse osmosis: introducing the primary target water subjected to secondary fine filtration into a reverse osmosis device for reverse osmosis, wherein the conductivity of reverse osmosis effluent is 0-10 mu s/cm, and the volume ratio of target water to wastewater obtained by reverse osmosis is more than or equal to 7-10: 1;
electrolysis: adding a marine mineral to the target water, the mineral content in the marine mineral being: 1-10% of magnesium, 0.5-4% of calcium, 1-6.5% of sulfate radical, 1-6.5% of sodium and 1-6% of potassium; adjusting the conductivity to 20-50 mu s/cm, and electrolyzing to obtain acidic water with the pH of 3.2-3.8 and the conductivity of 20-80 mu s/cm.
As an improved technical scheme, the seawater used as raw water is deep sea water 20-80 meters below sea level; which comprises the following components: 100-600 mg/L of calcium, 300-1500 mg/L of magnesium, 5000-12000 mg/L of sodium, 100-500 mg/L of potassium, 6000-20000 mg/L of chloride ions, 1000-3000 mg/L of sulfate radicals, 5000-20000 mg/L of TDS, and the conductivity of the deep sea water is 2000-6000 mu s/cm.
As a preferable technical scheme, the sedimentation is natural sedimentation of seawater, and the sedimentation time is more than or equal to 24 hours.
Preferably, the filtering comprises sand filteringAnd filtering with activated carbon; the sand filtration is to guide the settled seawater into a sand filter tank, quartz sand with the granularity of 1-10 meshes is filled in the sand filter tank, and the sand filtration speed is 5-20 m3The elapsed time is 5-20 min; the activated carbon filtration is to filter the seawater subjected to sand filtration by coconut shell activated carbon, wherein the adsorption iodine value of the coconut shell activated carbon is 500-800, and the filtration speed is 10-30 m3The elapsed time is 5-20 min.
Preferably, the secondary sedimentation is to introduce the seawater filtered by the activated carbon into a sedimentation tank, and the sedimentation tank is settled for 1-2 days.
As a preferable technical scheme, the filtering precision of the fine filtering is more than or equal to 5 mu m.
As an improved technical proposal, the method also comprises the steps of seawater preheating and secondary fine filtration after the fine filtration and before the evaporation; preheating the seawater by utilizing the steam drainage temperature, wherein the seawater preheating temperature is 40-60 ℃; the drainage temperature is 80-100 ℃, hot water is pumped into a coil pipe in the preheating tank through a water pump during preheating, and the water after heat exchange returns to the drainage tank again; the filtration precision of the secondary fine filtration is more than or equal to 1 mu m.
As a preferable technical scheme, the evaporation temperature is 100-120 ℃.
As an improved technical scheme, the marine minerals are obtained by further concentrating the mother liquor remaining after evaporation.
Due to the adoption of the technical scheme, the invention has the beneficial effects that:
according to the preparation method of the acidic water, seawater is used as raw water, and is subjected to sedimentation, filtration, secondary sedimentation and fine filtration and then evaporation to obtain primary target water with the conductivity of 80-150 mu s/cm, and then the primary target water is subjected to fine filtration, reverse osmosis and electrolysis again to obtain the acidic water with the pH of 3.2-3.8 and the conductivity of 20-80 mu s/cm; the invention adds the marine mineral substances during electrolysis, is also obtained by evaporation and concentration from seawater, does not add any chemical substances, is pure natural and purified, and the electrolyzed acidic water has obvious beauty effect, and the face is tapped by the acidic water, so that the skin can be tightened, and the skin can be kept smooth and not dry. Meanwhile, the skin can become bright; the acidic water obtained by the invention can make hair black and bright, and simultaneously has hair moistening effect and hair softness and smoothness increase. In addition, the acidic water obtained by the invention also has obvious sterilization and bacteriostasis effects. When the gargle is used for gargling, the oral cavity can be effectively cleaned, the decayed teeth can be prevented, the growth of oral fungi can be inhibited, and the ulcer can be relieved. When the foot bath lotion is used for bathing, the beriberi can be effectively relieved; can relieve diaper rash, miliaria, eczema, scald, sunburn, and inflammation. The detergent has high stain removing capacity when used for cleaning utensils, wiping furniture and washing clothes, such as tableware, tea sets and the like, and the washed clothes have no scale.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a comparison of the bactericidal effect of the acidic water of the present invention on lower concentration of Staphylococcus aureus bacteria;
FIG. 2 is a comparison of the bactericidal effect of the acidic water of the present invention on higher concentration of Staphylococcus aureus bacteria.
Detailed Description
The invention is further illustrated by the following figures and specific examples. It should be understood that these examples are for illustrative purposes only and are not intended to limit the scope of the present invention. Further, it should be understood that various changes or modifications of the present invention may be made by those skilled in the art after reading the teaching of the present invention, and such equivalents may fall within the scope of the present invention as defined in the appended claims.
In the present application, unless otherwise specified, the percentages are by weight.
Example 1
Seawater sedimentation: extracting deep sea water 50-60 meters below the sea level; which comprises the following components: 300mg/L of calcium, 500mg/L of magnesium, 8000mg/L of sodium, 200mg/L of potassium, 10000mg/L of chloride ions, 1200mg/L of sulfate radicals and 3000mg/L of TDS, wherein the conductivity of the deep sea water is 3500 mu s/cm; and naturally settling the extracted seawater for 36 h.
Sand filtration: guiding the settled seawater into a sand filter tank, wherein quartz sand with the granularity of 1-5 meshes is filled in the sand filter tank, and performing sand filtrationSpeed of 10m3H, the elapsed time is 10 min;
filtering with activated carbon: filtering the sand-filtered seawater with coconut shell activated carbon, wherein the coconut shell activated carbon has an iodine adsorption value of 600 and a filtering speed of 15m3The elapsed time is 8 min.
Secondary sedimentation: the seawater filtered by the active carbon is led into a settling tank, and the settling tank settles for 2 days.
Fine filtering: and (3) allowing the settled seawater to enter a fine filter for fine filtration, wherein the filtration precision of the fine filtration is 5 mu m.
Preheating seawater: preheating by utilizing steam hydrophobic temperature, and preheating the seawater to 50 ℃; the drainage temperature is 90 ℃, hot water is pumped into the coil pipe in the preheating tank through the water pump during preheating, and the water after heat exchange returns to the drainage tank again.
Secondary fine filtration: and (3) introducing the preheated seawater into a precision filter, and further filtering, wherein the filtering precision of the secondary fine filtering is 1 mu m.
And (3) evaporation: after secondary fine filtration, the seawater is introduced to an evaporation platform, the temperature of the evaporation platform is 110 ℃, and primary target water with the conductivity of 120 mu s/cm is obtained. And further concentrating the evaporated mother liquor to obtain the marine mineral concentrated solution.
Fine filtering again: introducing the primary target water into a fine filter, and performing fine filtration again with the filtration precision of 0.2 mu m;
reverse osmosis: introducing the primary target water after the secondary fine filtration into a reverse osmosis device for reverse osmosis, wherein the conductivity of reverse osmosis effluent is 2 mu s/cm, and the volume ratio of target water to wastewater obtained by reverse osmosis is 9: 1;
electrolysis: adding an evaporated marine mineral concentrate to the target water, wherein the mineral content in the marine mineral concentrate is as follows: 5% of magnesium, 2% of calcium, 3.5% of sulfate radical, 3.5% of sodium and 3% of potassium; adjusting the conductivity to 30 mus/cm, electrolyzing to obtain acid water with pH of 3.5 and conductivity of 60 mus/cm.
Example 2
Seawater sedimentation: extracting deep sea water 60-80 meters below the sea level; which comprises the following components: 500mg/L, 1100mg/L magnesium, 11000mg/L sodium, 400mg/L potassium, 10000mg/L chloride ion, 2000mg/L sulfate radical and 3500mg/L TDS, wherein the conductivity of the deep sea water is 3500 mu s/cm; and naturally settling the extracted seawater for 48 h.
Sand filtration: guiding the settled seawater into a sand filter tank, wherein quartz sand with the granularity of 6-8 meshes is filled in the sand filter tank, and the sand filtering speed is 8m3H, the elapsed time is 10 min;
filtering with activated carbon: filtering the sand-filtered seawater with coconut shell activated carbon, wherein the coconut shell activated carbon has an iodine adsorption value of 650 and a filtering speed of 22m3The elapsed time is 12 min.
Secondary sedimentation: the seawater filtered by the active carbon is led into a settling tank, and the settling tank settles for 1.5 days.
Fine filtering: and (3) allowing the settled seawater to enter a fine filter for fine filtration, wherein the filtration precision of the fine filtration is more than or equal to 5 mu m.
Preheating seawater: preheating by utilizing steam hydrophobic temperature, and preheating the seawater to 55 ℃; the drainage temperature is 95 ℃, hot water is pumped into the coil pipe in the preheating tank through the water pump during preheating, and the water after heat exchange returns to the drainage tank again.
Secondary fine filtration: and (3) introducing the preheated seawater into a precision filter, and further filtering, wherein the filtering precision of the secondary fine filtering is 1 mu m.
And (3) evaporation: after secondary fine filtration, the seawater is led to an evaporation platform, the temperature of the evaporation platform is 115 ℃, and primary target water with the conductivity of 110 mu s/cm is obtained. And further concentrating the evaporated mother liquor to obtain the marine mineral concentrated solution.
Fine filtering again: introducing the primary target water into a fine filter, and performing fine filtration again with the filtration precision of 0.2 mu m;
reverse osmosis: introducing the primary target water after the secondary fine filtration into a reverse osmosis device for reverse osmosis, wherein the conductivity of reverse osmosis effluent is 3 mu s/cm, and the volume ratio of target water to wastewater obtained by reverse osmosis is more than or equal to 8: 1;
electrolysis: adding an evaporated marine mineral concentrate to the target water, wherein the mineral content in the marine mineral concentrate is as follows: 4% of magnesium, 3% of calcium, 4% of sulfate radical, 3% of sodium and 2% of potassium; adjusting the conductivity to 35 mus/cm, electrolyzing to obtain acid water with pH3.5 and conductivity 50 mus/cm.
Example 3
Seawater sedimentation: extracting deep sea water 20-80 meters below sea level; which comprises the following components: 200mg/L of calcium, 1300mg/L of magnesium, 10000mg/L of sodium, 400mg/L of potassium, 9000mg/L of chloride ions, 1200mg/L of sulfate radicals and 3000 TDS3000mg/L, wherein the conductivity of the deep sea water is 4500 mu s/cm; and naturally settling the extracted seawater for 24 h.
Sand filtration: guiding the settled seawater into a sand filter tank, wherein quartz sand with the granularity of 3-6 meshes is filled in the sand filter tank, and the sand filtering speed is 12m3H, the elapsed time is 12 min;
filtering with activated carbon: filtering the sand-filtered seawater with coconut shell activated carbon, wherein the coconut shell activated carbon has an iodine adsorption value of 700 and a filtering speed of 20m3The elapsed time is 6 min.
Secondary sedimentation: the seawater filtered by the active carbon is led into a settling tank, and the settling tank settles for 2 days.
Fine filtering: and (3) allowing the settled seawater to enter a fine filter for fine filtration, wherein the filtration precision of the fine filtration is 5 mu m.
Preheating seawater: preheating by utilizing steam hydrophobic temperature, and preheating the seawater to 50 ℃; the drainage temperature is 98 ℃, hot water is pumped into the coil pipe in the preheating tank through the water pump during preheating, and the water after heat exchange returns to the drainage tank again.
Secondary fine filtration: and (3) introducing the preheated seawater into a precision filter, and further filtering, wherein the filtering precision of the secondary fine filtering is 1 mu m.
And (3) evaporation: after secondary fine filtration, the seawater is led to an evaporation platform, the temperature of the evaporation platform is 105 ℃, and primary target water with the conductivity of 100 mu s/cm is obtained. And further concentrating the evaporated mother liquor to obtain the marine mineral concentrated solution.
Fine filtering again: introducing the primary target water into a fine filter, and performing fine filtration again with the filtration precision of 0.2 mu m;
reverse osmosis: introducing the primary target water after the secondary fine filtration into a reverse osmosis device for reverse osmosis, wherein the conductivity of reverse osmosis effluent is 8 mu s/cm, and the volume ratio of target water to wastewater obtained by reverse osmosis is more than or equal to 7: 1;
electrolysis: adding an evaporated marine mineral concentrate to the target water, wherein the mineral content in the marine mineral concentrate is as follows: 6.5% of magnesium, 2.5% of calcium, 2.5% of sulfate radical, 4.5% of sodium and 4% of potassium; adjusting the conductivity to 40 mus/cm, electrolyzing to obtain acid water with pH of 3.4 and conductivity of 45 mus/cm.
Test examples
Respectively taking water samples from the acidic water prepared in the above examples, coating one face with an acidic water film, and coating the other face with an RO water film for comparison; after the application, the acidic water is smeared on the skin of two sides by using a cleaning cotton stick for sampling, and the results under the condition of different bacterial numbers show that the acidic water prepared by the method has good inhibitory effect on staphylococcus aureus, and the experimental result shows that the bacterial growth rate of the staphylococcus aureus is reduced by 90% after 5 seconds; within 30 seconds, the bacterial growth rate of staphylococcus aureus decreased by 95%. FIGS. 1 and 2 show the bactericidal effect at different bacterial concentrations.
The results of staphylococcus aureus, enterobacter chloroformans, candida albicans, and H004 in the acidic water, the blank control (MLB dish), and the RO water prepared according to the present invention were observed under a microscope and after 5 seconds are shown in table 1 below.
TABLE 1
| Staphylococcus aureus | Enterobacter viridis | Candida albicans | H004 | |
| Acidic water | ++ | ++ | +++ | ++++ |
| MLB culture dish | +++++ | +++++ | +++++ | +++++ |
| RO water | +++ | +++ | +++ | +++ |
The water samples of the present invention were tested for their properties in inflammatory cytokine release using human Peripheral Blood Mononuclear Cells (PBMCs) cultured in vitro, without inducing inflammatory cytokine release from unstimulated normal PBMCs TNF- α, an inflammatory cytokine that was able to inhibit bacterial Lipopolysaccharide (LPS) -induced PBMCS release, showed anti-inflammatory potential.
The water sample of the invention has no stimulation effect on the degranulation reaction of rat basophilic leukemia cells (RBL-2H 3). In superoxide anion radical scavenging tests, ACW was shown to have strong antioxidant capacity.
In the mass spectrum information, the water sample of the invention shows anti-inflammatory of biological function detection on magnesium and zinc ions, and other metal ions, such as potassium and calcium. It also has less tyrosinase and melanin, and reduced activity in human epidermal melanocyte (HEMN-MP) without significant cytotoxicity. The cell proliferation test shows the growth resisting and migration resisting effect of the water sample of the present invention on human skin melanoma cell (A375.S2), and shows that the water sample has anticancer potential on skin cancer.
In conclusion, biological analysis results show that the water sample disclosed by the invention has multiple biological activities of antibiosis, anti-inflammation, no allergy, antioxidation, anti-melanin, anticancer and the like.
Claims (9)
1. A preparation method of acidic water for cosmetics is characterized in that seawater/brine is used as raw water, and is subjected to sedimentation, filtration, secondary sedimentation and fine filtration and then evaporation to obtain primary target water with the conductivity of 80-150 mu s/cm, and then the primary target water is subjected to the following steps:
fine filtering again: introducing the primary target water into a fine filter, and performing fine filtration again, wherein the filtration precision is more than or equal to 0.2 mu m;
reverse osmosis: introducing the primary target water subjected to secondary fine filtration into a reverse osmosis device for reverse osmosis, wherein the conductivity of reverse osmosis effluent is 0-10 mu s/cm, and the volume ratio of target water to wastewater obtained by reverse osmosis is more than or equal to 7-10: 1; electrolysis: adding a marine mineral to the target water, the mineral content in the marine mineral being: 1-10% of magnesium, 0.5-4% of calcium, 1-6.5% of sulfate radical, 1-6.5% of sodium and 1-6% of potassium; electrolyzing to obtain acidic water with pH of 3.2-3.8 and conductivity of 20-80 mus/cm.
2. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: the seawater used as raw water is deep sea water 20-80 meters below sea level; which comprises the following components: 100-600 mg/L of calcium, 300-1500 mg/L of magnesium, 5000-12000 mg/L of sodium, 100-500 mg/L of potassium, 6000-20000 mg/L of chloride ions, 1000-3000 mg/L of sulfate radicals, 5000-20000 mg/L of TDS, and the conductivity of the deep sea water is 2000-6000 mu s/cm.
3. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: the sedimentation is natural sedimentation of seawater, and the sedimentation time is more than or equal to 24 hours.
4. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: the process isThe filtering comprises sand filtering and active carbon filtering; the sand filtration is to guide the settled seawater into a sand filter tank, quartz sand with the granularity of 1-10 meshes is filled in the sand filter tank, and the sand filtration speed is 5-20 m3H; the activated carbon filtration is to filter the seawater subjected to sand filtration by coconut shell activated carbon, wherein the adsorption iodine value of the coconut shell activated carbon is 500-800, and the filtration speed is 10-30 m3/h。
5. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: and the secondary sedimentation is to guide the seawater filtered by the activated carbon into a sedimentation tank, and the sedimentation tank is sedimentated for 1-2 days.
6. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: the filtration precision of the fine filtration is more than or equal to 5 mu m.
7. The method for producing acidic water for cosmetics according to any one of claims 1 to 6, characterized in that: after the fine filtration and before the evaporation, the steps of seawater preheating and secondary fine filtration are also included; the seawater preheating is to preheat by using steam, and the seawater is preheated to 40-60 ℃; the filtration precision of the secondary fine filtration is more than or equal to 1 mu m.
8. The method for preparing acidic water for cosmetics according to claim 7, characterized in that: the evaporation temperature is 100-120 ℃.
9. The method for preparing acidic water for cosmetics according to claim 1, characterized in that: the marine mineral is obtained by further concentrating the mother liquor remained after evaporation.
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Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000014587A (en) * | 1998-06-29 | 2000-01-18 | Meisei Sansho Kk | Discoloration preventive wet tissue and cosmetic pack sheet compounded with chloride |
| JP2001278767A (en) * | 2000-03-28 | 2001-10-10 | Matsukawa Kagaku:Kk | Cosmetic |
| JP2002165868A (en) * | 2000-12-05 | 2002-06-11 | Kanebo Ltd | Aerosol product |
| KR20080092572A (en) * | 2007-04-12 | 2008-10-16 | 서희동 | A method to produce electrolysis oxidation water and electrolysis reduction water from deep sea water |
| CN101702880A (en) * | 2007-04-25 | 2010-05-05 | 阿夸特克股份有限公司 | Highly stable electrolytic water with reduced NMR half line width |
| CN102068019A (en) * | 2010-11-23 | 2011-05-25 | 上海心动科技有限公司 | Multi-ion health-preserving solution and preparation method and application thereof |
| CN102557319A (en) * | 2012-01-17 | 2012-07-11 | 青岛九远医疗科技有限公司 | Physiological seawater making method |
| CN103387277A (en) * | 2012-05-11 | 2013-11-13 | 台盐实业股份有限公司 | Acidic electrolyzed water and composition thereof |
| TW201545770A (en) * | 2014-06-13 | 2015-12-16 | Ming-Ren Chen | Electrolytic acidic water |
| FR3041253A1 (en) * | 2015-09-21 | 2017-03-24 | Fabienne Bresdin | USE OF AN OSMOTIC ISOTONIC ELECTROLYTE SOLUTION AS A CELLULAR LIFE MEDIUM IN A COSMETIC, DERMATOLOGICAL OR NUTRITIONAL COMPOSITION |
| CN206308193U (en) * | 2016-12-26 | 2017-07-07 | 杭州菲丝凯化妆品有限公司 | The preparation system of Cosmetic Manufacture water |
| US10292911B1 (en) * | 2017-12-22 | 2019-05-21 | Reoxcyn, Llc | Stable redox compositions and methods of use |
-
2019
- 2019-12-25 CN CN201911356064.4A patent/CN110981068B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000014587A (en) * | 1998-06-29 | 2000-01-18 | Meisei Sansho Kk | Discoloration preventive wet tissue and cosmetic pack sheet compounded with chloride |
| JP2001278767A (en) * | 2000-03-28 | 2001-10-10 | Matsukawa Kagaku:Kk | Cosmetic |
| JP2002165868A (en) * | 2000-12-05 | 2002-06-11 | Kanebo Ltd | Aerosol product |
| KR20080092572A (en) * | 2007-04-12 | 2008-10-16 | 서희동 | A method to produce electrolysis oxidation water and electrolysis reduction water from deep sea water |
| CN101702880A (en) * | 2007-04-25 | 2010-05-05 | 阿夸特克股份有限公司 | Highly stable electrolytic water with reduced NMR half line width |
| CN102068019A (en) * | 2010-11-23 | 2011-05-25 | 上海心动科技有限公司 | Multi-ion health-preserving solution and preparation method and application thereof |
| CN102557319A (en) * | 2012-01-17 | 2012-07-11 | 青岛九远医疗科技有限公司 | Physiological seawater making method |
| CN103387277A (en) * | 2012-05-11 | 2013-11-13 | 台盐实业股份有限公司 | Acidic electrolyzed water and composition thereof |
| TW201545770A (en) * | 2014-06-13 | 2015-12-16 | Ming-Ren Chen | Electrolytic acidic water |
| FR3041253A1 (en) * | 2015-09-21 | 2017-03-24 | Fabienne Bresdin | USE OF AN OSMOTIC ISOTONIC ELECTROLYTE SOLUTION AS A CELLULAR LIFE MEDIUM IN A COSMETIC, DERMATOLOGICAL OR NUTRITIONAL COMPOSITION |
| CN206308193U (en) * | 2016-12-26 | 2017-07-07 | 杭州菲丝凯化妆品有限公司 | The preparation system of Cosmetic Manufacture water |
| US10292911B1 (en) * | 2017-12-22 | 2019-05-21 | Reoxcyn, Llc | Stable redox compositions and methods of use |
Non-Patent Citations (2)
| Title |
|---|
| 冯清等: "《营养与美容 揭开健康与美丽的奥秘》", 31 March 2013, 华中理工大学出版社 * |
| 沈晓盛等: ""电解海水的抑菌活性及对食品加工表面材料的消毒效果"", 《微生物学通报》 * |
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