CN110845924A - Preparation method of inorganic modified water-based multicolor paint - Google Patents
Preparation method of inorganic modified water-based multicolor paint Download PDFInfo
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- CN110845924A CN110845924A CN201911266188.3A CN201911266188A CN110845924A CN 110845924 A CN110845924 A CN 110845924A CN 201911266188 A CN201911266188 A CN 201911266188A CN 110845924 A CN110845924 A CN 110845924A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
- C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
- C09D1/04—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates with organic additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
- C09D5/1668—Vinyl-type polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
Abstract
The invention discloses a preparation method of an inorganic modified water-based multicolor paint, which comprises the following steps: 1) preparing water-based colorful base paint; 2) preparing a colorful protective glue solution; 3) preparing an aqueous colorful continuous phase; 4) preparing the inorganic modified water-based multicolor paint. The invention adopts reasonable collocation of inorganic resin and organic acrylic emulsion, improves the stability of the system, especially the stability of viscosity and color point, and ensures that the system can not be changed during transportation to construction; the water resistance is enhanced, the soaking water is not whitened, and the strength is not obviously changed after soaking; the surface hardness, the stain resistance, the alkali resistance and the weather resistance of the paint film are improved.
Description
Technical Field
The invention relates to a preparation method of an inorganic modified water-based multicolor paint.
Background
The water-based colorful paint has been developed into a mainstream exterior wall decoration system so far, is a pure water environment-friendly paint, can achieve more than 95% of stone imitation effect, is simple to construct, has light dead weight, only has 1/40 stone weight, is higher in safety, has a price less than 1/4 of dry-hanging stone, is low in cost, is pollution-free during construction, has great significance for environmental protection and energy conservation, and is more and more widely used.
The existing water-based multicolor paint system mainly takes an acrylic acid system as a main part, and is matched with special protective glue for the water-based multicolor paint and proper pigments, fillers and auxiliaries, compared with the traditional system, the existing water-based multicolor paint system has great improvement, but still has a plurality of problems, and is more outstanding in storage property and water resistance. At present, part of systems on the market still have the normal temperature storage of no more than one month, the obvious post-thickening phenomenon appears, the low viscosity rises by twenty-thirty KU, the high viscosity even exceeds sixty-seventy KU, and the normal use is greatly influenced; more systems still cannot pass the national relevant detection standards, particularly the detection of the thermal storage stability and the low-temperature stability, and the phenomena of precipitation, layering, water diversion and the like can occur after one week of thermal storage; because the quality of the emulsion, protective glue and some related auxiliary products used in the existing colorful system are different, the water resistance of part of the system has a great problem, after a paint film is dried, the obvious whitening phenomenon appears after soaking in water for three days, and if the paint film is serious, the colorful point particles can fall off; the series of problems can lead to the condition that the product quality can not be ensured, and can generate extremely adverse effects on the normal development of a later-stage colorful system.
Disclosure of Invention
The invention mainly solves the technical problem of providing a method for improving the stability of a system, particularly the stability of viscosity and color points by reasonably matching inorganic resin and organic acrylic emulsion, and ensuring that the system cannot be changed in the transportation to construction process; the water resistance is enhanced, the soaking water is not whitened, and the strength is not obviously changed after soaking; the preparation method of the inorganic modified water-based multicolor paint improves the surface hardness, the stain resistance, the alkali resistance and the weather resistance of a paint film.
In order to solve the technical problems, the invention adopts a technical scheme that: the preparation method of the inorganic modified water-based multicolor paint comprises the following steps:
1) preparation of the aqueous colorful base paint: adding 550 parts of deionized water and 10 parts of cellulose into a container according to parts by weight for dispersing, then adding 10 parts of titanium dioxide, 100 parts of calcined kaolin, 2 parts of dispersing agent and 3 parts of multicolor protective adhesive powder according to parts by weight, after dispersing for 30 minutes at high speed, sequentially adding 2 parts of pH regulator, 2 parts of defoamer, 2 parts of wetting agent, 10 parts of propylene glycol, 10 parts of film-forming assistant, 150 parts of organic silicon modified acrylic emulsion, 150 parts of inorganic resin mixture and 2 parts of sterilizing preservative according to parts by weight, and stirring for more than 30 minutes to obtain the waterborne multicolor base paint for later use;
2) preparing a multicolor protection glue solution: adding 950 parts of deionized water and 50 parts of colorful protective adhesive powder into a container according to parts by weight, and dispersing at a high speed for more than 1 hour until the solution is uniform and transparent without obvious particles to obtain a colorful protective adhesive solution for later use;
3) preparation of aqueous multicolor continuous phase: adding 500 parts by weight of organic silicon modified acrylic emulsion and 150 parts by weight of deionized water into a container, sequentially adding 10 parts by weight of propylene glycol, 30 parts by weight of a film forming aid, 2 parts by weight of a pH regulator, 2 parts by weight of a defoaming agent, 300 parts by weight of an inorganic resin mixture, 2 parts by weight of a bactericidal preservative and 4 parts by weight of an alkali swelling thickener after stirring, and stirring for more than 30 minutes to obtain an aqueous colorful continuous phase;
4) preparing an inorganic modified water-based multicolor paint: dividing the aqueous multicolor base paint into a plurality of parts, respectively adding different amounts of aqueous color paste for toning to obtain toning base paints of various colors, weighing 400 parts by weight of the toning base paints of various colors according to the proportion, adding the toning base paints of various colors into 300 parts of the multicolor protective glue solution, then putting the solution into a granulator for granulation, controlling the rotation speed and the mesh number of a screen of the granulator to obtain color points of various sizes, then adding 300 parts by weight of aqueous multicolor continuous phase, and uniformly mixing to obtain the inorganic modified aqueous multicolor coating.
In a preferred embodiment of the invention, the cellulose is a mixture of hydroxyethyl cellulose and ethyl hydroxyethyl cellulose.
In a preferred embodiment of the present invention, the multicolor protective gum powder is a mixture of modified hectorite and polyvalent phosphate.
In a preferred embodiment of the present invention, the inorganic resin mixture is one or more of low modulus potassium silicate, high modulus potassium silicate, lithium silicate and silica sol.
In a preferred embodiment of the invention, the coalescent is a dodecyl alcohol ester.
The invention has the beneficial effects that: the invention adopts reasonable collocation of inorganic resin and organic acrylic emulsion, improves the stability of the system, especially the stability of viscosity and color point, and ensures that the system can not be changed during transportation to construction; the water resistance is enhanced, the soaking water is not whitened, and the strength is not obviously changed after soaking; the surface hardness, the stain resistance, the alkali resistance and the weather resistance of the paint film are improved.
Detailed Description
The following detailed description of the preferred embodiments of the present invention is provided to enable those skilled in the art to more readily understand the advantages and features of the present invention, and to clearly and unequivocally define the scope of the present invention.
The embodiment of the invention comprises the following steps: a preparation method of an inorganic modified water-based multicolor paint comprises the following steps:
1) preparation of the aqueous colorful base paint: adding 550 parts of deionized water and 10 parts of cellulose consisting of a mixture of hydroxyethyl cellulose and ethyl hydroxyethyl cellulose into a container according to parts by weight for dispersing, then adding 10 parts of titanium dioxide, 100 parts of calcined kaolin, 2 parts of a dispersing agent and 3 parts of multicolor protective glue powder consisting of a mixture of modified hectorite and polyvalent phosphate according to parts by weight, after dispersing for 30 minutes at a high speed, sequentially adding 2 parts of a pH regulator, 2 parts of a defoaming agent, 2 parts of a wetting agent, 10 parts of propylene glycol, 10 parts of a film-forming assistant consisting of dodecyl alcohol ester, 150 parts of an organic silicon modified acrylic emulsion, 150 parts of an inorganic resin mixture consisting of one or more of low-modulus potassium silicate, high-modulus potassium silicate, lithium silicate and silica sol and 2 parts of a sterilizing preservative according to parts by weight, and stirring for more than 30 minutes to obtain an aqueous base paint for later use;
2) preparing a multicolor protection glue solution: adding 950 parts of deionized water and 50 parts of colorful protective adhesive powder consisting of a mixture of modified hectorite and multivalent phosphate into a container according to parts by weight, and dispersing at a high speed for more than 1 hour until the solution is uniform and transparent and has no obvious particles, so as to obtain a colorful protective adhesive solution for later use;
3) preparation of aqueous multicolor continuous phase: adding 500 parts by weight of organic silicon modified acrylic emulsion and 150 parts by weight of deionized water into a container, sequentially adding 10 parts by weight of propylene glycol, 30 parts by weight of a film forming aid consisting of dodecyl alcohol ester, 2 parts by weight of a pH regulator, 2 parts by weight of a defoaming agent, 300 parts by weight of an inorganic resin mixture consisting of one or more of low-modulus potassium silicate, high-modulus potassium silicate, lithium silicate and silica sol, 2 parts by weight of a sterilizing preservative and 4 parts by weight of an alkali swelling thickener after stirring, and stirring for more than 30 minutes to obtain an aqueous colorful continuous phase;
4) preparing an inorganic modified water-based multicolor paint: dividing the aqueous multicolor base paint into a plurality of parts, respectively adding different amounts of aqueous color paste for toning to obtain toning base paints of various colors, weighing 400 parts by weight of the toning base paints of various colors according to the proportion, adding the toning base paints of various colors into 300 parts of the multicolor protective glue solution, then putting the solution into a granulator for granulation, controlling the rotation speed and the mesh number of a screen of the granulator to obtain color points of various sizes, then adding 300 parts by weight of aqueous multicolor continuous phase, and uniformly mixing to obtain the inorganic modified aqueous multicolor coating.
The invention relates to a preparation method of an inorganic modified water-based multicolor paint, which adopts reasonable collocation of inorganic resin and organic acrylic emulsion to improve the stability of a system, particularly the stability of viscosity and color points, and ensures that the inorganic modified water-based multicolor paint cannot change in the transportation to construction process; the water resistance is enhanced, the soaking water is not whitened, and the strength is not obviously changed after soaking; the surface hardness, the stain resistance, the alkali resistance and the weather resistance of the paint film are improved.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes performed by the present invention or directly or indirectly applied to other related technical fields are included in the scope of the present invention.
Claims (5)
1. A preparation method of an inorganic modified water-based multicolor paint is characterized by comprising the following steps: the method comprises the following steps:
1) preparation of the aqueous colorful base paint: adding 550 parts of deionized water and 10 parts of cellulose into a container according to parts by weight for dispersing, then adding 10 parts of titanium dioxide, 100 parts of calcined kaolin, 2 parts of dispersing agent and 3 parts of multicolor protective adhesive powder according to parts by weight, after dispersing for 30 minutes at high speed, sequentially adding 2 parts of pH regulator, 2 parts of defoamer, 2 parts of wetting agent, 10 parts of propylene glycol, 10 parts of film-forming assistant, 150 parts of organic silicon modified acrylic emulsion, 150 parts of inorganic resin mixture and 2 parts of sterilizing preservative according to parts by weight, and stirring for more than 30 minutes to obtain the waterborne multicolor base paint for later use;
2) preparing a multicolor protection glue solution: adding 950 parts of deionized water and 50 parts of colorful protective adhesive powder into a container according to parts by weight, and dispersing at a high speed for more than 1 hour until the solution is uniform and transparent without obvious particles to obtain a colorful protective adhesive solution for later use;
3) preparation of aqueous multicolor continuous phase: adding 500 parts by weight of organic silicon modified acrylic emulsion and 150 parts by weight of deionized water into a container, sequentially adding 10 parts by weight of propylene glycol, 30 parts by weight of a film forming aid, 2 parts by weight of a pH regulator, 2 parts by weight of a defoaming agent, 300 parts by weight of an inorganic resin mixture, 2 parts by weight of a bactericidal preservative and 4 parts by weight of an alkali swelling thickener after stirring, and stirring for more than 30 minutes to obtain an aqueous colorful continuous phase;
4) preparing an inorganic modified water-based multicolor paint: dividing the aqueous multicolor base paint into a plurality of parts, respectively adding different amounts of aqueous color paste for toning to obtain toning base paints of various colors, weighing 400 parts by weight of the toning base paints of various colors according to the proportion, adding the toning base paints of various colors into 300 parts of the multicolor protective glue solution, then putting the solution into a granulator for granulation, controlling the rotation speed and the mesh number of a screen of the granulator to obtain color points of various sizes, then adding 300 parts by weight of aqueous multicolor continuous phase, and uniformly mixing to obtain the inorganic modified aqueous multicolor coating.
2. The method for preparing an inorganic modified aqueous multicolor paint as claimed in claim 1, characterized in that: the cellulose is a mixture of hydroxyethyl cellulose and ethyl hydroxyethyl cellulose.
3. The method for preparing an inorganic modified aqueous multicolor paint as claimed in claim 1, characterized in that: the colorful protective glue powder is a mixture of modified hectorite and multivalent phosphate.
4. The method for preparing an inorganic modified aqueous multicolor paint as claimed in claim 1, characterized in that: the inorganic resin mixture is one or more of low-modulus potassium silicate, high-modulus potassium silicate, lithium silicate and silica sol.
5. The method for preparing an inorganic modified aqueous multicolor paint as claimed in claim 1, characterized in that: the film-forming assistant is dodecyl alcohol ester.
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| CN201911266188.3A CN110845924A (en) | 2019-12-11 | 2019-12-11 | Preparation method of inorganic modified water-based multicolor paint |
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| CN201911266188.3A CN110845924A (en) | 2019-12-11 | 2019-12-11 | Preparation method of inorganic modified water-based multicolor paint |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111849279A (en) * | 2020-07-21 | 2020-10-30 | 北京莱恩斯新材料科技有限公司 | Large-color-point water-coated sand base paint, preparation method and large-color-point water-coated sand coating |
| CN112694771A (en) * | 2020-12-22 | 2021-04-23 | 广东顺德派齐新材料有限公司 | Inorganic fireproof heat-preservation multicolor paint synthesized by inorganic resin and preparation method thereof |
| CN113150686A (en) * | 2021-05-26 | 2021-07-23 | 四川嘉宝莉涂料有限公司 | Marble-imitated reflective heat-insulation inorganic multi-color paint and preparation method thereof |
| CN113354999A (en) * | 2021-06-29 | 2021-09-07 | 广东施彩新材料科技有限公司 | Granite paint and preparation method thereof |
| CN113881302A (en) * | 2020-12-25 | 2022-01-04 | 上海磐彩环保科技股份有限公司 | Water-based 5G granite imitation coating and preparation method thereof |
| CN114133768A (en) * | 2021-11-10 | 2022-03-04 | 合肥科天水性科技有限责任公司 | Base paint, water-based inorganic sandstone-containing colored paint for exterior wall and preparation method thereof |
| CN114437601A (en) * | 2020-11-03 | 2022-05-06 | 湖南梨树园涂料有限公司 | Spraying type water-based inorganic multicolor paint |
| CN115477862A (en) * | 2021-05-31 | 2022-12-16 | 立邦涂料（中国）有限公司 | Inorganic water-in-water multicolor interior wall coating and preparation method thereof |
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| CN103923512A (en) * | 2014-04-22 | 2014-07-16 | 常熟林润氟硅材料有限公司 | Preparation method of organic modified hectorite for W/W multicolor coating protection glue |
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| CN108300047A (en) * | 2018-01-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of indoor anti-pollution water-water coating and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111849279A (en) * | 2020-07-21 | 2020-10-30 | 北京莱恩斯新材料科技有限公司 | Large-color-point water-coated sand base paint, preparation method and large-color-point water-coated sand coating |
| CN111849279B (en) * | 2020-07-21 | 2021-10-15 | 北京莱恩斯新材料科技有限公司 | Large-color-point water-coated sand base paint, preparation method and large-color-point water-coated sand coating |
| CN114437601A (en) * | 2020-11-03 | 2022-05-06 | 湖南梨树园涂料有限公司 | Spraying type water-based inorganic multicolor paint |
| CN112694771A (en) * | 2020-12-22 | 2021-04-23 | 广东顺德派齐新材料有限公司 | Inorganic fireproof heat-preservation multicolor paint synthesized by inorganic resin and preparation method thereof |
| CN113881302A (en) * | 2020-12-25 | 2022-01-04 | 上海磐彩环保科技股份有限公司 | Water-based 5G granite imitation coating and preparation method thereof |
| CN113150686A (en) * | 2021-05-26 | 2021-07-23 | 四川嘉宝莉涂料有限公司 | Marble-imitated reflective heat-insulation inorganic multi-color paint and preparation method thereof |
| CN115477862A (en) * | 2021-05-31 | 2022-12-16 | 立邦涂料（中国）有限公司 | Inorganic water-in-water multicolor interior wall coating and preparation method thereof |
| CN115477862B (en) * | 2021-05-31 | 2023-09-05 | 立邦涂料（中国）有限公司 | Inorganic water-in-water multicolor interior wall coating and preparation method thereof |
| CN113354999A (en) * | 2021-06-29 | 2021-09-07 | 广东施彩新材料科技有限公司 | Granite paint and preparation method thereof |
| CN114133768A (en) * | 2021-11-10 | 2022-03-04 | 合肥科天水性科技有限责任公司 | Base paint, water-based inorganic sandstone-containing colored paint for exterior wall and preparation method thereof |
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