CN110812522A - Flock essence and application thereof - Google Patents

Flock essence and application thereof Download PDF

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Publication number
CN110812522A
CN110812522A CN201911182257.2A CN201911182257A CN110812522A CN 110812522 A CN110812522 A CN 110812522A CN 201911182257 A CN201911182257 A CN 201911182257A CN 110812522 A CN110812522 A CN 110812522A
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fragrance
velvet
flower
methyl
essence
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Inventor
雷冬明
林常腾
陈金明
陈恺嘉
石灿焕
林立涌
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GUANGZHOU LEVON FLAVOUR AND FRAGRANCE TECHNOLOGY Co
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GUANGZHOU LEVON FLAVOUR AND FRAGRANCE TECHNOLOGY Co
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Priority to CN201911182257.2A priority Critical patent/CN110812522A/en
Publication of CN110812522A publication Critical patent/CN110812522A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Zoology (AREA)
  • Organic Chemistry (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a velvet flower essence and application thereof, wherein raw materials of the velvet flower essence comprise a velvet flower extract, a main fragrance agent, 2-methyl-5-phenylpentanol, phenylacetaldehyde glycerol acetal, 2, 6-dimethyl-2-heptenol, 1-methyl-4- (4-methyl-3-pent-1-enyl) -3-cyclohexene formaldehyde, 1- (4-isopropyl cyclohexyl) ethanol, a flower fragrance freshener, a flower fragrance sweetener, a wax fragrance agent, a fruit fragrance agent, a wood fragrance agent, a fragrance fixative and a solvent. The lint essence has harmonious fragrance and the characteristic fragrance of natural lint, can be widely used for fragrances of air fresheners and the like, gives sweet fragrance to lint, and is expected to remove deficiency and temper and mind, so that people feel calm and happy; in addition, the velvet essence can also be used for perfuming products such as perfume, daily cosmetics and the like, and has important application value.

Description

Flock essence and application thereof
Technical Field
The invention belongs to the field of fine chemical engineering, and particularly relates to a fine hair essence and application thereof.
Background
The downy flower tree is a leguminous deciduous tree, flowers bloom in six and seven months every year, the flowers are like silks, the fragrance is strong, a plurality of small flowers grow into head-shaped inflorescences which are arranged into an umbrella-like shape, and the flower silks are pink, so that the downy inflorescences are far expected to be removed to be pink downy flower balls. The pompon is flourishing between leaves of dark green like feathers, and is additionally provided with a wide crown and a beautiful tree posture, and is particularly beautiful, and the pompon is full of pink plums, is colored and fragrant, and is an excellent garden tree species.
The velvet flower has sweet fragrance and fragrance. Meanwhile, the velvet flower also has the effects of regulating qi, resolving depression, stimulating appetite, activating collaterals, nourishing heart and soothing nerves. The medicinal value is recorded as early as the book Ben Cao Jing: "calm five internal organs, harmonize the mind, and make people happy and carefree". In addition, the velvet flower also has good treatment effect on sedation, pain relief and chest distress. The fragrance of the velvet flower can calm the human body, remove the dysphoria and make the human body relaxed and happy.
However, the simulation and blending of the fragrance of the lint is only reported, if the lint essence is developed, the fragrance of the lint essence can be widely used for the fragrance of an air freshener and the like, the fragrance of the sweet lint is endowed, and the deficiency and the mood are expected to be removed, so that the people feel calm and happy; in addition, the velvet essence can also be used for perfuming products such as perfume, daily cosmetics and the like, has important application value and can generate certain social benefit. Therefore, the development of the velvet essence has important significance.
Disclosure of Invention
The invention aims to provide a velvet flower essence which has characteristic fragrance of velvet flowers, sweet fragrance and harmonious whole fragrance.
The invention also aims to provide the application of the velvet flower essence.
The purpose of the invention is realized by the following technical scheme:
the velvet essence comprises the following raw materials in percentage by mass:
Figure BDA0002291584190000021
the main aromatic agent is more than one of 3, 7-dimethyl-trans-2, 6-octadiene-1-alcohol, 3, 7-dimethyl-cis-2, 6-octadiene-1-alcohol, 2-dimethyl-3-phenyl-1-propanol, 3-methyl-1-phenyl-3-pentanol, 2, 5-trimethyl-5-pentyl cyclopentanone or 2-methyl-4- (2,6, 6-trimethyl-1-cyclohex-1-enyl) -2-butyraldehyde;
in the formula, the 2-methyl-5-phenylpentanol can simulate the fragrance of flower buds, is slightly greasy and slightly sweet, and can ensure that the flower fragrance of velvet flowers is fuller; phenylacetaldehyde glycerol acetal can strongly reflect the fragrance of sweet petals; the 2, 6-dimethyl-2-heptenol has soft flower fragrance, and can make the flower fragrance of the velvet flower softer in the formula; the 1-methyl-4- (4-methyl-3-pent-1-enyl) -3-cyclohexene formaldehyde has warm volatile fragrance, and can enhance the warm feeling and diffusivity of the fragrance of the velvet flowers; the 1- (4-isopropyl cyclohexyl) ethanol has a transparent flower fragrance, can enable the flower fragrance of the fine hair flower to be more transparent, shows the head fragrance in the whole flower fragrance, and can be well coordinated with the sweet fragrance and the green fragrance; and other auxiliary agents are added to finally obtain the fine hair essence with sweet, soft, fine and vivid fragrance, coordinated overall fragrance, prominent characteristic fragrance of natural fine hair, fresh fragrance and strong natural sense.
The velvet flower extract is obtained by adopting a supercritical carbon dioxide extraction process; specifically, the velvet flower is placed in an extraction kettle, carbon dioxide is introduced, the extraction flow rate is 17g/min, the extraction pressure is 250bar, the extraction temperature is 50 ℃, and the extraction time is 2 hours.
The flower fragrance freshener is acetic p-cresol ester and/or 2, 2-dimethyl-3- (3-methylphenyl) propanol;
the floral sweetener is preferably beta-damascone;
the lipid wax fragrance agent is stearic acid and/or methyl palmitate;
the fruit flavor agent is dibutyl phthalate and/or diisobutyl phthalate;
the wood scent agent is more than one of 3,5, 7-trihydroxy-2- (4-hydroxyphenyl) -4H-benzopyran-4-ketone, quercetin or 5-hydroxymethyl furfural;
the perfume fixative is preferably 6,10, 14-trimethyl-2-pentadecanone.
Preferably, the velvet flower essence comprises the following raw materials in percentage by mass:
Figure BDA0002291584190000031
Figure BDA0002291584190000041
the solvent is any one of ethanol, benzyl alcohol or dipropylene glycol.
The preparation method of the velvet flower essence is to mix the raw materials and stir the mixture evenly.
The velvet flower essence can be applied to fine chemicals such as cosmetics, air fresheners and the like.
Compared with the prior art, the invention has the following advantages and effects:
at present, no report of preparation of the lint essence exists, the lint essence has harmonious fragrance and has the characteristic fragrance of natural lint, the fragrance can be widely used for fragrances of air fresheners and the like, sweet fragrance is given to lint, deficiency and noise can be removed, and people are happy and happy; in addition, the velvet essence can also be used for perfuming products such as perfume, daily cosmetics and the like, and has important application value.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.
Each of the raw materials used in the following examples is a commercially available product except for those specifically mentioned herein.
Example 1
The lint essence with natural lint characteristic fragrance comprises the following raw materials in percentage by mass:
0.05 percent of p-cresol acetate; b-damascone 5%; 1% of 3, 7-dimethyl-trans-2, 6-octadien-1-ol; 5% of 3, 7-dimethyl-cis-2, 6-octadien-1-ol; 0.1% of quercetin; 5% of 2, 6-dimethyl-2-heptenol; 1% of 1- (4-isopropylcyclohexyl) ethanol; 2%, 2-dimethyl-3-phenyl-1-propanol; 2%, 2-dimethyl-3- (3-methylphenyl) propanol; 1.5% of octadecanoic acid; 1% of 2-methyl-5-phenylpentanol; 3% of 3-methyl-1-phenyl-3-pentanol; phenylacetaldehyde glycerol acetal 0.5%; 0.5 percent of dibutyl phthalate; 0.5% of 3,5, 7-trihydroxy-2- (4-hydroxyphenyl) -4H-benzopyran-4-one; 1-methyl-4- (4-methyl-3-pent-1-enyl) -3-cyclohexenecarbaldehyde 2%; 1% of 2,2, 5-trimethyl-5-pentylcyclopentanone; 6%, 10, 14-trimethyl-2-pentadecanone; 1% of 2-methyl-4- (2,6, 6-trimethyl-1-cyclohex-1-enyl) -2-butyraldehyde; diisobutyl phthalate 0.5%; 1% of methyl palmitate; 0.2 percent of 5-hydroxymethyl furfural; 5% of velvet flower extract; the balance being benzyl alcohol.
The velvet flower essence obtained by blending has characteristic fragrance of velvet flowers, sweet fragrance and coordinated overall fragrance by smelling.
Example 2
The lint essence with natural lint characteristic fragrance comprises the following raw materials in percentage by mass:
0.5 percent of p-cresol acetate; 0.5% of beta-damascone; 3% of 3, 7-dimethyl-trans-2, 6-octadien-1-ol; 1% of 3, 7-dimethyl-cis-2, 6-octadien-1-ol; 1% of quercetin; 2% of 2, 6-dimethyl-2-heptenol; 3% of 1- (4-isopropylcyclohexyl) ethanol; 0.5% of 2, 2-dimethyl-3-phenyl-1-propanol; 2, 2-dimethyl-3- (3-methylphenyl) propanol 8%; octadecanoic acid 0.5%; 5% of 2-methyl-5-phenylpentanol; 0.5% of 3-methyl-1-phenyl-3-pentanol; phenylacetaldehyde glycerol acetal 3%; 0.05 percent of dibutyl phthalate; 3%, 5, 7-trihydroxy-2- (4-hydroxyphenyl) -4H-chromen-4-one; 0.2% of 1-methyl-4- (4-methyl-3-pent-1-enyl) -3-cyclohexenecarbaldehyde; 5% of 2,2, 5-trimethyl-5-pentylcyclopentanone; 2% of 6,10, 14-trimethyl-2-pentadecanone; 3% of 2-methyl-4- (2,6, 6-trimethyl-1-cyclohex-1-enyl) -2-butyraldehyde; diisobutyl phthalate 0.01%; 3% of methyl palmitate; 0.05% of 5-hydroxymethylfurfural; 20% of velvet flower extract; the balance of ethanol.
The velvet flower essence obtained by blending the components smells, has fresh fragrance and strong natural sense, has the characteristic fragrance of velvet flowers, and has harmonious integral fragrance.
Example 3
The lint essence with natural lint characteristic fragrance comprises the following raw materials in percentage by mass:
0.1 percent of p-cresol acetate; 3.5 percent of beta-damascone; 2% of 3, 7-dimethyl-trans-2, 6-octadien-1-ol; 3% of 3, 7-dimethyl-cis-2, 6-octadien-1-ol; 0.3% of quercetin; 3% of 2, 6-dimethyl-2-heptenol; 2% of 1- (4-isopropylcyclohexyl) ethanol; 1% of 2, 2-dimethyl-3-phenyl-1-propanol; 4% of 2, 2-dimethyl-3- (3-methylphenyl) propanol; 1% of octadecanoic acid; 3% of 2-methyl-5-phenylpentanol; 2% of 3-methyl-1-phenyl-3-pentanol; phenylacetaldehyde glycerol acetal 2%; 0.15 percent of dibutyl phthalate; 1.5% of 3,5, 7-trihydroxy-2- (4-hydroxyphenyl) -4H-benzopyran-4-one; 1% of 1-methyl-4- (4-methyl-3-pent-1-enyl) -3-cyclohexenecarbaldehyde; 3% of 2,2, 5-trimethyl-5-pentylcyclopentanone; 3% of 6,10, 14-trimethyl-2-pentadecanone; 2% 2-methyl-4- (2,6, 6-trimethyl-1-cyclohex-1-enyl) -2-butyraldehyde; diisobutyl phthalate 0.1%; 2% of methyl palmitate; 0.1% of 5-hydroxymethylfurfural; velvet flower extract 19%; the balance being dipropylene glycol.
The natural velvet flower essence obtained by blending the components is smelled, the characteristic fragrance of the natural velvet flower is prominent, the whole fragrance is coordinated, the fragrance is fresh and natural, and the fragrance is sweet, soft, fine and vivid.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims (10)

1. The velvet essence is characterized by comprising the following raw materials in percentage by mass:
Figure FDA0002291584180000011
the main aromatic agent is more than one of 3, 7-dimethyl-trans-2, 6-octadiene-1-alcohol, 3, 7-dimethyl-cis-2, 6-octadiene-1-alcohol, 2-dimethyl-3-phenyl-1-propanol, 3-methyl-1-phenyl-3-pentanol, 2, 5-trimethyl-5-pentyl cyclopentanone or 2-methyl-4- (2,6, 6-trimethyl-1-cyclohex-1-enyl) -2-butyraldehyde.
2. The velvet flower essence according to claim 1, characterized in that: the velvet flower extract is obtained by adopting a supercritical carbon dioxide extraction process.
3. The velvet flower essence according to claim 1, characterized in that: the velvet flower extract is prepared by the following steps: putting the velvet flowers into an extraction kettle, introducing carbon dioxide, and extracting at the flow rate of 17g/min, the extraction pressure of 250bar, the extraction temperature of 50 ℃ and the extraction time of 2 hours.
4. The velvet flower essence according to claim 1, characterized in that:
the flower fragrance freshener is acetic p-cresol ester and/or 2, 2-dimethyl-3- (3-methylphenyl) propanol;
the floral sweetener is beta damascone.
5. The velvet flower essence according to claim 1, characterized in that:
the lipid wax fragrance agent is stearic acid and/or methyl palmitate;
the fruit flavor agent is dibutyl phthalate and/or diisobutyl phthalate.
6. The velvet flower essence according to claim 1, characterized in that:
the wood scent agent is more than one of 3,5, 7-trihydroxy-2- (4-hydroxyphenyl) -4H-benzopyran-4-ketone, quercetin or 5-hydroxymethyl furfural;
the fixative is 6,10, 14-trimethyl-2-pentadecanone.
7. The velvet flower essence according to claim 1, wherein the raw materials comprise the following components in percentage by mass:
Figure FDA0002291584180000021
Figure FDA0002291584180000031
8. the velvet flower essence according to claim 1 or 7, characterized in that: the solvent is any one of ethanol, benzyl alcohol or dipropylene glycol.
9. Use of a velvet flower essence according to any one of claims 1 to 8 in fine chemicals.
10. Use according to claim 9, characterized in that: the fine chemicals include cosmetics and air fresheners.
CN201911182257.2A 2019-11-27 2019-11-27 Flock essence and application thereof Pending CN110812522A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991255A (en) * 2020-09-11 2020-11-27 厦门馨米兰香精香料有限公司 Herbal shampoo and shower gel essence

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020136783A1 (en) * 2001-01-22 2002-09-26 Singh Anil Kumar Composition of herbal biscuits for lactating mothers acting as dietary supplement and process for preparation thereof
KR100443588B1 (en) * 2002-01-25 2004-08-09 나드리화장품주식회사 Cosmetic composition containing paeonia suffruticosa andrews extract and albizzia julibrissin dura extract having anti-ageing effect
CN102170859A (en) * 2008-10-28 2011-08-31 株式会社爱茉莉太平洋 Perfume composition for expressing the fragrance of silk tree flower
CN102234573A (en) * 2010-04-23 2011-11-09 徐德智 Preparation method of essence containing lily and acacia
CN104042475A (en) * 2014-05-31 2014-09-17 青岛博泓海洋生物技术有限公司 Tranquillizing floral water
CN106061459A (en) * 2013-12-13 2016-10-26 宝洁公司 Fragrance compositions
CN107287034A (en) * 2017-07-29 2017-10-24 安徽艺云玻璃有限公司 A kind of glass aromatic spray and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020136783A1 (en) * 2001-01-22 2002-09-26 Singh Anil Kumar Composition of herbal biscuits for lactating mothers acting as dietary supplement and process for preparation thereof
KR100443588B1 (en) * 2002-01-25 2004-08-09 나드리화장품주식회사 Cosmetic composition containing paeonia suffruticosa andrews extract and albizzia julibrissin dura extract having anti-ageing effect
CN102170859A (en) * 2008-10-28 2011-08-31 株式会社爱茉莉太平洋 Perfume composition for expressing the fragrance of silk tree flower
CN102234573A (en) * 2010-04-23 2011-11-09 徐德智 Preparation method of essence containing lily and acacia
CN106061459A (en) * 2013-12-13 2016-10-26 宝洁公司 Fragrance compositions
CN104042475A (en) * 2014-05-31 2014-09-17 青岛博泓海洋生物技术有限公司 Tranquillizing floral water
CN107287034A (en) * 2017-07-29 2017-10-24 安徽艺云玻璃有限公司 A kind of glass aromatic spray and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111991255A (en) * 2020-09-11 2020-11-27 厦门馨米兰香精香料有限公司 Herbal shampoo and shower gel essence

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