CN110754482A - Bactericidal disinfectant for preventing avian influenza and preparation method thereof - Google Patents

Bactericidal disinfectant for preventing avian influenza and preparation method thereof Download PDF

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Publication number
CN110754482A
CN110754482A CN201911040254.5A CN201911040254A CN110754482A CN 110754482 A CN110754482 A CN 110754482A CN 201911040254 A CN201911040254 A CN 201911040254A CN 110754482 A CN110754482 A CN 110754482A
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disinfectant
photocatalyst
sterilizing
quaternary ammonium
ammonium salt
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韦良
李胜
杜国健
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Guangxi Wuhang Material Technology Co Ltd
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Guangxi Wuhang Material Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/12—Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
    • A61K31/05—Phenols
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/13—Amines
    • A61K31/14—Quaternary ammonium compounds, e.g. edrophonium, choline
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/24—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/24—Heavy metals; Compounds thereof
    • A61K33/32—Manganese; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04—Antibacterial agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/12—Antivirals
    • A61P31/14—Antivirals for RNA viruses
    • A61P31/16—Antivirals for RNA viruses for influenza or rhinoviruses

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Pest Control & Pesticides (AREA)
  • Virology (AREA)
  • Inorganic Chemistry (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oncology (AREA)
  • Communicable Diseases (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Organic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Pulmonology (AREA)
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Abstract

The invention discloses aThe disinfectant for preventing avian influenza comprises composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO2The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: 10-20% of composite phenol bacterium poisonous enemy disinfectant, 20-30% of quaternary ammonium salt disinfectant and nano TiO250% -70% of photocatalyst sterilization disinfectant; the compound phenol bacterium and poison enemy sterilizing disinfectant disclosed by the invention is simple in preparation equipment, low in process requirement, convenient to use in daily proportioning for inhibiting bacteria, sterilizing, killing viruses and other various bacteria, and has a good killing effect; the quaternary ammonium salt sterilizing disinfectant has low preparation cost and small environmental pollution in the production process; the nano TiO2 photocatalyst sterilization disinfectant can degrade organic pollutants, has stable chemical properties, no secondary pollution, no toxicity to human bodies and low cost, is widely applied to sewage treatment and air purification, has stable chemical properties of TiO2 in the sterilization disinfectant photocatalyst, has strong redox and photocathode corrosion resistance and low cost, and is convenient for large-scale production.

Description

Bactericidal disinfectant for preventing avian influenza and preparation method thereof
Technical Field
The invention belongs to the technical field of sterilizing disinfectants, and particularly relates to a sterilizing disinfectant for preventing avian influenza and a preparation method thereof.
Background
Avian Influenza Virus (AIV) belongs to the influenza a virus. Influenza virus belongs to the orthomyxoviridae of RNA virus, and is divided into 3 types, namely A, B and C. The influenza A virus is mostly sent to poultry, and some influenza A viruses can also infect various mammals such as pigs, horses, seals, whales and the like and human beings; influenza b and c viruses are found in seals and swine infections, respectively.
The avian influenza is an infectious disease with various symptoms of respiratory system to severe systemic septicemia of the poultry caused by influenza A virus. Avian influenza is easily epidemic among birds, and in the past, it was called "fowl plague" by folk, and is identified as a class a infectious disease by the international veterinary community. The existing disinfectant for avian influenza has poor preparation effect.
Disclosure of Invention
The invention aims to provide a bactericidal disinfectant for preventing avian influenza, which aims to solve the problems in the background technology. The bactericidal disinfectant for preventing avian influenza has the characteristics of low cost and good effect.
The invention also aims to provide a realization method of the bactericidal disinfectant for preventing avian influenza.
In order to achieve the purpose, the invention provides the following technical scheme: a kind ofThe disinfectant for preventing avian influenza comprises composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO2The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: 10-20% of composite phenol bacterium poisonous enemy disinfectant, 20-30% of quaternary ammonium salt disinfectant and nano TiO250% -70% of photocatalyst sterilization disinfectant;
the compound phenol bacterium and toxin dichlord disinfectant comprises the following components in percentage by mass: 0.1 to 5 percent of phenol; 0.5 to 1.5 percent of acetic acid; 1% -3% of dodecyl benzene sulfonic acid; adding water to 100%;
the quaternary ammonium salt sterilizing disinfectant comprises the following components in parts by mass: 1% -5% of C12-C18 alkyl dimethyl tertiary amine; 5% -8% of an alkylating agent; 1% -5% of benzyltriethylammonium chloride; 5% -8% of ethanol; adding water to 100%;
the nano TiO2The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: nano TiO221% -3% of photocatalyst; 0.1 to 0.3 percent of alkyl benzyl dimethyl ammonium chloride; 1% -3% of a sterilizing ultraviolet lamp; 0.1 to 0.3 percent of hexadecyl dimethyl ethyl ammonium bromide; 0.1% -0.3% of isopropanol; 0.1 to 0.3 percent of ethylene glycol ethyl ether; 0.1 to 0.3 percent of ethylenediamine tetraacetic acid; 1% -3% of glutaraldehyde; 1% -3% of potassium permanganate; water is added to 100%.
In addition, the invention also discloses a preparation method of the disinfectant for preventing avian influenza, which mainly comprises the following steps:
the preparation method of the compound phenol bacterium toxin-enemy sterilization disinfectant comprises the following steps: putting phenol into a reaction tank, adding glacial acetic acid, performing simple primary stirring, then putting into another reaction tank, adding dodecylbenzene sulfonic acid, performing secondary stirring, and performing sampling quality inspection to meet the standard;
the preparation method of the quaternary ammonium salt sterilizing disinfectant comprises the following steps: adding C12-C18 alkyl dimethyl tertiary amine into a reaction tank, adding an alkylating reagent and ethanol for reaction, adding a reaction product into another reaction kettle, adding benzyl triethyl ammonium chloride and water, and stirring for reaction to obtain the corresponding quaternary ammonium salt sterilizing disinfectant.
The nano TiO2The preparation method of the photocatalyst sterilizing disinfectant comprises the following steps: putting alkyl benzyl dimethyl ammonium chloride, hexadecyl dimethyl ethyl ammonium bromide, isopropanol, ethylene glycol ethyl ether, ethylene diamine tetraacetic acid, glutaraldehyde, potassium permanganate and water into a reaction container, and fixing nano TiO at the upper end of the reaction container2Photocatalyst in nano TiO2A sterilizing ultraviolet lamp is arranged above the photocatalyst, and the nano TiO is irradiated by the sterilizing ultraviolet lamp2The photocatalyst generates strong hydroxyl radicals, and cells of pollutants such as bacteria, viruses and the like are destroyed and decomposed by the hydroxyl radicals and are finally decomposed into water and carbon dioxide;
the prepared composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO are added2The photocatalyst disinfectant is prepared into the disinfectant for preventing avian influenza by mixing in proportion.
Compared with the prior art, the invention has the beneficial effects that:
the compound phenol bacterium and poison enemy sterilizing disinfectant disclosed by the invention is simple in preparation equipment, low in process requirement, convenient to use in daily proportioning for inhibiting bacteria, sterilizing, killing viruses and other various bacteria, and has a good killing effect; the quaternary ammonium salt sterilizing disinfectant has low preparation cost and small environmental pollution in the production process; the nano TiO2 photocatalyst sterilizing disinfectant can degrade organic pollutants, has stable chemical property, no secondary pollution, no toxicity to human bodies and low cost, so the nano TiO2 photocatalyst sterilizing disinfectant is widely applied to sewage treatment and air purification, and the TiO2 in the sterilizing photocatalyst has stable chemical property, stronger oxidation reduction and photocathode corrosion resistance, is insoluble and nontoxic, has low cost and is convenient for large-scale production.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Hair brushThe technical scheme is as follows: a disinfectant for preventing avian influenza comprises compound phenol bacteria molinate disinfectant, quaternary ammonium salt disinfectant, and nanometer TiO2The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: 10-20% of composite phenol bacterium poisonous enemy disinfectant, 20-30% of quaternary ammonium salt disinfectant and nano TiO250% -70% of photocatalyst sterilization disinfectant;
the compound phenol bacterium and toxin dichlord disinfectant consists of the following components in percentage by mass: 0.1 to 5 percent of phenol; 0.5 to 1.5 percent of acetic acid; 1% -3% of dodecyl benzene sulfonic acid; adding water to 100%;
the quaternary ammonium salt sterilizing disinfectant comprises the following components in percentage by mass: 1% -5% of C12-C18 alkyl dimethyl tertiary amine; 5% -8% of an alkylating agent; 1% -5% of benzyltriethylammonium chloride; 5% -8% of ethanol; adding water to 100%;
nano TiO22The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: nano TiO221% -3% of photocatalyst; 0.1 to 0.3 percent of alkyl benzyl dimethyl ammonium chloride; 1% -3% of a sterilizing ultraviolet lamp; 0.1 to 0.3 percent of hexadecyl dimethyl ethyl ammonium bromide; 0.1% -0.3% of isopropanol; 0.1 to 0.3 percent of ethylene glycol ethyl ether; 0.1 to 0.3 percent of ethylenediamine tetraacetic acid; 1% -3% of glutaraldehyde; 1% -3% of potassium permanganate; water is added to 100%.
Further, the preparation method of the disinfectant for preventing avian influenza mainly comprises the following steps:
the preparation method of the compound phenol bacterium toxin-enemy sterilizing disinfectant comprises the following steps: putting phenol into a reaction tank, adding glacial acetic acid, performing simple primary stirring, then putting into another reaction tank, adding dodecylbenzene sulfonic acid, performing secondary stirring, and performing sampling quality inspection to meet the standard;
the preparation method of the quaternary ammonium salt sterilizing disinfectant comprises the following steps: adding C12-C18 alkyl dimethyl tertiary amine into a reaction tank, adding an alkylating reagent and ethanol for reaction, adding a reaction product into another reaction kettle, adding benzyl triethyl ammonium chloride and water, and stirring for reaction to obtain the corresponding quaternary ammonium salt sterilizing disinfectant.
Nano TiO22The preparation method of the photocatalyst sterilizing disinfectant comprises the following steps: putting alkyl benzyl dimethyl ammonium chloride, hexadecyl dimethyl ethyl ammonium bromide, isopropanol, ethylene glycol ethyl ether, ethylene diamine tetraacetic acid, glutaraldehyde, potassium permanganate and water into a reaction container, and fixing nano TiO at the upper end of the reaction container2Photocatalyst in nano TiO2A sterilizing ultraviolet lamp is arranged above the photocatalyst, and the nano TiO is irradiated by the sterilizing ultraviolet lamp2The photocatalyst generates strong hydroxyl radicals, and cells of pollutants such as bacteria, viruses and the like are destroyed and decomposed by the hydroxyl radicals and are finally decomposed into water and carbon dioxide;
the prepared composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO are added2The photocatalyst disinfectant is prepared into the disinfectant for preventing avian influenza by mixing in proportion.
Example 1
The invention sequentially pairs the composite phenol bacterium toxophila disinfectant, the quaternary ammonium salt disinfectant and the nano TiO2Preparing a photocatalyst sterilizing disinfectant:
putting phenol into a reaction tank, adding glacial acetic acid, performing simple primary stirring, then putting into another reaction tank, adding dodecylbenzene sulfonic acid, performing secondary stirring, and performing sampling quality inspection to meet the standard;
adding C12-C18 alkyl dimethyl tertiary amine into a reaction tank, adding an alkylating reagent and ethanol for reaction, adding a reaction product into another reaction kettle, adding benzyl triethyl ammonium chloride and water, and stirring for reaction to obtain a corresponding quaternary ammonium salt sterilizing disinfectant;
putting alkyl benzyl dimethyl ammonium chloride, hexadecyl dimethyl ethyl ammonium bromide, isopropanol, ethylene glycol ethyl ether, ethylene diamine tetraacetic acid, glutaraldehyde, potassium permanganate and water into a reaction container, and fixing nano TiO at the upper end of the reaction container2Photocatalyst in nano TiO2A sterilizing ultraviolet lamp is arranged above the photocatalyst, and the nano TiO is irradiated by the sterilizing ultraviolet lamp2Photocatalyst generates strong hydroxyl radicals, and cells of contaminants such as bacteria and viruses are destroyed and decomposed by the hydroxyl radicalsFinally decomposed into water and carbon dioxide;
the prepared composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO are added2The photocatalyst disinfectant is prepared into the disinfectant for preventing avian influenza by mixing in proportion.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (2)

1. A disinfectant for preventing avian influenza comprises compound phenol bacteria molinate disinfectant, quaternary ammonium salt disinfectant, and nanometer TiO2The photocatalyst sterilizing disinfectant is characterized by comprising the following components in parts by mass: 10-20% of composite phenol bacterium poisonous enemy disinfectant, 20-30% of quaternary ammonium salt disinfectant and nano TiO250% -70% of photocatalyst sterilization disinfectant;
the compound phenol bacterium and toxin dichlord disinfectant comprises the following components in percentage by mass: 0.1 to 5 percent of phenol; 0.5 to 1.5 percent of acetic acid; 1% -3% of dodecyl benzene sulfonic acid; adding water to 100%;
the quaternary ammonium salt sterilizing disinfectant comprises the following components in parts by mass: 1% -5% of C12-C18 alkyl dimethyl tertiary amine; 5% -8% of an alkylating agent; 1% -5% of benzyltriethylammonium chloride; 5% -8% of ethanol; adding water to 100%;
the nano TiO2The photocatalyst sterilizing disinfectant comprises the following components in parts by mass: nano TiO221% -3% of photocatalyst; 0.1 to 0.3 percent of alkyl benzyl dimethyl ammonium chloride; 1% -3% of a sterilizing ultraviolet lamp; 0.1 to 0.3 percent of hexadecyl dimethyl ethyl ammonium bromide; 0.1% -0.3% of isopropanol; 0.1 to 0.3 percent of ethylene glycol ethyl ether; 0.1 to 0.3 percent of ethylenediamine tetraacetic acid; 1% -3% of glutaraldehyde; 1% -3% of potassium permanganate; water is added to 100%.
2. The bactericidal disinfectant for preventing avian influenza according to claim 1, the preparation method mainly comprises the following steps:
the preparation method of the compound phenol bacterium toxin-enemy sterilization disinfectant comprises the following steps: putting phenol into a reaction tank, adding glacial acetic acid, performing simple primary stirring, then putting into another reaction tank, adding dodecylbenzene sulfonic acid, performing secondary stirring, and performing sampling quality inspection to meet the standard;
the preparation method of the quaternary ammonium salt sterilizing disinfectant comprises the following steps: adding C12-C18 alkyl dimethyl tertiary amine into a reaction tank, adding an alkylating reagent and ethanol for reaction, adding a reaction product into another reaction kettle, adding benzyl triethyl ammonium chloride and water, and stirring for reaction to obtain the corresponding quaternary ammonium salt sterilizing disinfectant.
The nano TiO2The preparation method of the photocatalyst sterilizing disinfectant comprises the following steps: putting alkyl benzyl dimethyl ammonium chloride, hexadecyl dimethyl ethyl ammonium bromide, isopropanol, ethylene glycol ethyl ether, ethylene diamine tetraacetic acid, glutaraldehyde, potassium permanganate and water into a reaction container, and fixing nano TiO at the upper end of the reaction container2Photocatalyst in nano TiO2A sterilizing ultraviolet lamp is arranged above the photocatalyst, and the nano TiO is irradiated by the sterilizing ultraviolet lamp2The photocatalyst generates strong hydroxyl radicals, and cells of pollutants such as bacteria, viruses and the like are destroyed and decomposed by the hydroxyl radicals and are finally decomposed into water and carbon dioxide;
the prepared composite phenol bacterium toxophila disinfectant, quaternary ammonium salt disinfectant and nano TiO are added2The photocatalyst disinfectant is prepared into the disinfectant for preventing avian influenza by mixing in proportion.
CN201911040254.5A 2019-10-29 2019-10-29 Bactericidal disinfectant for preventing avian influenza and preparation method thereof Pending CN110754482A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114403141A (en) * 2022-02-10 2022-04-29 新乡市康大消毒剂有限公司 Compound phenol disinfectant and preparation method thereof

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CN103351301A (en) * 2013-07-01 2013-10-16 安徽奔马先端科技有限公司 Synthetic method for high-purity quaternary ammonium salt
CN104054753A (en) * 2014-06-30 2014-09-24 南通蛇类治疗研究所 Antibacterial and sterilization disinfectant for killing avian influenza viruses
CN108402079A (en) * 2018-01-15 2018-08-17 南通蛇类治疗研究所 Bird flu disinfection sanitizer

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114403141A (en) * 2022-02-10 2022-04-29 新乡市康大消毒剂有限公司 Compound phenol disinfectant and preparation method thereof
CN114403141B (en) * 2022-02-10 2022-12-27 新乡市康大消毒剂有限公司 Compound phenol disinfectant and preparation method thereof

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