CN110742840A - Camellia seed oil cleansing flour and preparation method thereof - Google Patents

Camellia seed oil cleansing flour and preparation method thereof Download PDF

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Publication number
CN110742840A
CN110742840A CN201910985326.7A CN201910985326A CN110742840A CN 110742840 A CN110742840 A CN 110742840A CN 201910985326 A CN201910985326 A CN 201910985326A CN 110742840 A CN110742840 A CN 110742840A
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oil
cleansing
powder
seed oil
flour
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林树真
龙婷
余洁芝
林树红
谢洁梅
林小琳
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Guangdong Golden Dragon Technology Development Co Ltd
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Guangdong Golden Dragon Technology Development Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/11Encapsulated compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/732Starch; Amylose; Amylopectin; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/412Microsized, i.e. having sizes between 0.1 and 100 microns
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/56Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms

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Abstract

The invention discloses oil tea seed oil cleansing flour which comprises vegetable oil microcapsules and cleansing powder components; the capsule core of the vegetable oil microcapsule comprises camellia seed oil and macadamia nut oil; the vegetable oil microcapsule accounts for 15-25% of the total weight of the oil tea seed oil cleansing powder; the cleansing powder comprises sodium lauroyl glutamate, tea saponin, starch sodium octenylsuccinate, trehalose, oat grain powder, wild soybean seed extract, witch hazel extract powder, tea polyphenol and sodium hydroxybenzoate. The oil tea seed oil cleansing powder is softer and is suitable for most of skin; the foam is fine and soft, and the grease and dirt purifying effect is good.

Description

Camellia seed oil cleansing flour and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to camellia seed oil cleansing powder and a preparation method thereof.
Background
With the social development and the improvement of living standard, people pay more attention to skin care. The exposed skin of people can adsorb dust, smoke, microorganisms and the like, and the face is always in a greasy state due to the possibility of sweating, so that the skin is not beneficial to maintenance; and the makeup for women is more and more popular when going out. If the skin is not thoroughly cleaned, the problems of pore blockage, skin oil-water imbalance, sensitive skin, skin aging and the like are easily caused; therefore, the skin cleaning is very important, and the face cleaning also becomes the most important link of daily skin care.
In the process of implementing the invention, the inventor finds that at least the following problems exist in the existing face cleansing product:
the cleaning products on the market are various and are generally in a paste or emulsion state, the existing interface products use a large amount of surfactants for decontamination, have abundant foams and strong cleaning capability, but have large stimulation; there are also anti-sensitivity cleansing products, which, although milder, have poor cleansing ability. Meanwhile, the existing face cleaning product has a single function and can cause certain damage to the skin.
Disclosure of Invention
The invention aims to solve the technical problems and provides camellia seed oil cleansing flour and a preparation method thereof.
In order to solve the problems, the invention is realized according to the following technical scheme:
the camellia seed oil cleansing flour comprises vegetable oil microcapsules and cleansing powder components;
the capsule core of the vegetable oil microcapsule comprises camellia seed oil and macadamia nut oil; the vegetable oil microcapsule accounts for 15-25% of the total weight of the oil tea seed oil cleansing powder;
the cleansing powder comprises sodium lauroyl glutamate, tea saponin, starch sodium octenylsuccinate, trehalose, oat grain powder, wild soybean seed extract, witch hazel extract powder, tea polyphenol and sodium hydroxybenzoate.
Preferably, the mass ratio of the capsule core to the capsule wall of the vegetable oil microcapsule is 1: 2-3.
Preferably, the mass ratio of the camellia seed oil to the macadamia nut oil is 1-2: 1.
Preferably, the capsule wall of the vegetable oil microcapsule comprises an a component and water, and the a component comprises soy protein isolate and maltodextrin.
Preferably, the mass ratio of the component A to the water is 1: 8-9.
Preferably, the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1-2.
Preferably, the face cleansing powder is prepared from the following powdery raw materials in percentage by weight:
25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of a wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium hydroxybenzoate.
Preferably, the vegetable oil microcapsule is prepared by the following method:
step 101: adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the capsule core, and emulsifying for 20 minutes to prepare emulsion;
step 102: homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa;
step 103: and (3) carrying out spray drying on the high-pressure homogenized emulsion, wherein the air inlet temperature of the spray drying is 190 ℃, and the feeding speed is 1L/min, so as to prepare the vegetable oil microcapsule.
The invention also provides a preparation method of the camellia seed oil cleansing flour, which comprises the following steps:
step 100, preparing vegetable oil microcapsules; adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the camellia oleosa seed oil and the hawaii nut oil, and emulsifying for 20 minutes to prepare emulsion; homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa; spray drying the high-pressure homogenized emulsion at the air inlet temperature of 190 ℃ and the feeding speed of 1L/min to obtain vegetable oil microcapsules;
step 200, weighing powdery raw materials of the flour cleaning component according to the following weight percentage: 25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of a wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium methylphenidate;
300, putting the vegetable oil microcapsules and the cleansing powder into a high-speed stirrer, wherein the vegetable oil microcapsules account for 15-25% of the total weight of the oil tea seed oil cleansing powder; setting the rotating speed of the high-speed stirrer to be 300r/min, stirring for 30 minutes to fully and uniformly mix, and filling after irradiation sterilization to obtain the camellia seed oil cleansing powder.
Preferably, the particle size of each powdery raw material of the flour component is 100-200 meshes.
Compared with the prior art, the invention has the beneficial effects that:
1. the oil tea seed oil cleansing powder is softer and is suitable for most of skin; the foam is fine and soft, and the grease and dirt purifying effect is good.
2. The capsule core of the vegetable oil microcapsule comprises camellia seed oil and macadamia nut oil. The oil tea seed oil contains abundant vitamin E and other antioxidants, and can protect skin, especially prevent skin injury and aging. The macadamia nut oil contains nutrients which are necessary for forming an oil protective layer on the skin, and most importantly, the macadamia nut oil is mild in oiliness and does not irritate the skin. The oil can be easily mixed with color cosmetics, oil stains and the like on the face through the emulsifier of the face cleaning component, and the dirt on the face is uniformly carried away in a water emulsification mode during washing. On the other hand, the coating of the capsule wall protects the nutrient components of the vegetable oil, solves the problem of difficult storage and has the characteristics of stability and high efficiency.
3. According to the invention, sodium lauroyl glutamate, tea saponin, sodium starch octenyl succinate, trehalose, a witch hazel extract, a wild soybean seed extract and tea polyphenol are added into the face cleaning powder according to a certain proportion, so that the product has good antioxidant effect, and also has good effects of nutrition, moisture retention, skin color brightening and the like.
The present invention will be further described with reference to the following examples.
Detailed Description
The following description is given in conjunction with the preferred embodiments of the present invention, and it should be understood that the preferred embodiments described herein are only for illustrating and explaining the present invention and are not to be construed as limiting the present invention.
The camellia seed oil cleansing flour comprises vegetable oil microcapsules and cleansing powder components. Wherein the vegetable oil microcapsule accounts for 15-25% of the total weight of the oil tea camellia seed oil cleansing flour.
Wherein the capsule core of the vegetable oil microcapsule is camellia seed oil and macadamia nut oil. The oil tea seed oil is unsaturated and fatty acid mainly containing oleic acid and linoleic acid, and is easy to be absorbed by human body. Unsaturated fatty acids are called "cosmetic acids", and the supply of unsaturated fatty acids is sufficient, so that human skin is tender and moist. Moreover, because the camellia oleosa seed oil contains abundant vitamin A, E, D, K and other antioxidants, the camellia oleosa seed oil can protect the skin, especially can prevent skin damage and aging, and can make the skin glossy. After the components of the face cleaning powder are emulsified with the grease, the face cleaning powder can be easily fused with the makeup oil stain on the face, and the dirt on the face is taken away in a general way in a water emulsification mode during washing. The macadamia nut oil contains nutrients which are necessary for forming an oil protective layer on the skin, and most importantly, the macadamia nut oil is mild in oiliness and does not irritate the skin.
The capsule wall of the vegetable oil microcapsule comprises a component A and water, wherein the mass ratio of the component A to the water is 1: 8-9. Specifically, the component A comprises soybean protein isolate and maltodextrin, wherein the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1-2.
Through the design, no emulsifier is adopted to prepare the vegetable oil microcapsule powder, and the soybean protein isolate and the maltodextrin are selected, wherein the soybean protein isolate has good emulsifying property but poor water solubility, and the maltodextrin has good water solubility, and the formed solution has low viscosity but poor emulsifying property. The oil tea seed oil and the macadamia nut oil can be mutually matched and can be well embedded; simple components and high wrapping rate. Compared with other microcapsule preparation methods, the method has the advantages of simple formula, energy-saving and environment-friendly process, good powder fluidity of the prepared microcapsule, and more importantly, the method can protect unsaturated fatty acid, vitamin and the like in the camellia seed oil and the macadamia nut from being damaged, thereby improving the oxidation stability of the microcapsule.
Specifically, the cleansing powder comprises sodium lauroyl glutamate, tea saponin, sodium starch octenyl succinate, trehalose, oat grain powder, wild soybean seed extract, witch hazel extract powder, tea polyphenol and sodium hydroxybenzoate. The raw materials of the components are all in powder form. The powder is very fine and smooth to touch and has no skin stabbing and pain feeling.
Wherein the functions of the components are as follows:
1. sodium lauroyl glutamate is an amino acid type surfactant having an amino acid skeleton in the molecule, is excellent in foaming performance, has the unique mildness of an acylamino acid surfactant, is safe to use, has low irritation to eyes and skin, is a very mild skin and hair cleansing agent, and gives a soft and moist feeling to the skin after washing. Can be combined with other anionic surfactant such as AES and fatty acid soap to reduce residual amount on skin, thereby reducing skin irritation.
2. The tea saponin is a natural nonionic surfactant with excellent performance, has good functions of emulsification, dispersion, foaming, moistening and the like, and also has pharmacological effects of diminishing inflammation, easing pain, resisting permeation and the like.
3. Sodium starch octenylsuccinate: the sodium starch octenyl succinate has excellent emulsifying performance and good oil stain adsorbing effect.
4. Trehalose is a natural saccharide, belongs to a micromolecular humectant, has good affinity with membrane protein, and can be used as a skin penetrating agent to increase the absorption of skin on nutrient components; trehalose can effectively inhibit the oxidative rancidity of fatty acid and ester products. Trehalose has a stabilizing effect against oxidative tea polyphenols, thereby reducing the possibility of product problems.
5. The oat grain powder can absorb excessive surface oil and is helpful for removing dead skin.
6. The extract of semen glycines contains abundant specific isoflavone (which is a powerful antioxidant and skin brightening agent) and fructus Gleditsiae Abnormalis (which helps to clean and purify skin). The phytosterol contained in the collagen protein emulsion helps to improve the concentration of collagen protein and also can resist the negative effect of a surfactant.
7. The witch hazel extract is helpful for relieving inflammation and removing free radicals, can be used for treatment, and has a certain relieving effect on skin. At the same time, the body is protected from inflammatory infections and free radical attacks. The witch hazel extract is mild and free of any irritation, and even sensitive skin can not be affected, but symptoms such as red spots, pain and itch caused by allergy can be inhibited, so that the skin is well protected, and the skin can be conditioned to be in a normal state.
8. Tea polyphenols is water soluble substance, and can be used for cleaning face to remove greasy dirt on face, astringe follicular orifice, and has disinfectant, antibacterial, and skin aging resisting effects.
Preferably, the face cleansing powder is prepared from the following powdery raw materials in percentage by weight: 25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium methylphenidate.
Furthermore, the mesh number of each raw material component is 100-200. The powder is finer and finer, can deeply permeate into the bottom of the skin, has finer foam, can reduce friction on the skin, has strong cleaning power, and purifies grease and dirt.
The invention also provides a preparation method of the camellia seed oil cleansing flour, which comprises the following steps:
step 100, preparing the vegetable oil microcapsule, comprising the following steps:
step 101: adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the capsule core, and emulsifying for 20 minutes to prepare emulsion;
step 102: homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa;
step 103: and (3) carrying out spray drying on the high-pressure homogenized emulsion, wherein the air inlet temperature of the spray drying is 190 ℃, and the feeding speed is 1L/min, so as to prepare the vegetable oil microcapsule.
Step 200, weighing powdery raw materials of the flour cleaning component according to the following weight percentage: 25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of a wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium methylphenidate.
Wherein the granularity of each powdery raw material of the flour component is 100-200 meshes.
300, putting the vegetable oil microcapsules and the cleansing powder into a high-speed stirrer, wherein the vegetable oil microcapsules account for 15-25% of the total weight of the oil tea seed oil cleansing powder; setting the rotating speed of the high-speed stirrer to be 300r/min, stirring for 30 minutes to fully and uniformly mix, and filling after irradiation sterilization to obtain the camellia seed oil cleansing powder.
Example 1
The camellia seed oil cleansing powder of the embodiment 1 comprises vegetable oil microcapsules and a cleansing powder component;
1. preparing raw materials of the vegetable oil microcapsule:
and (3) capsule wall: comprises a component A and water, wherein the mass ratio of the component A to the water is 1:8. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1:1.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil.
Wherein the mass ratio of the capsule core to the capsule wall is 1:2.
2. Preparing the vegetable oil microcapsule:
step 101: adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the capsule core, and emulsifying for 20 minutes to prepare emulsion;
step 102: homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa;
step 103: and (3) carrying out spray drying on the high-pressure homogenized emulsion, wherein the air inlet temperature of the spray drying is 190 ℃, and the feeding speed is 1L/min, so as to prepare the vegetable oil microcapsule.
3. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
25% of sodium lauroyl glutamate, 12% of tea saponin, 6% of starch sodium octenylsuccinate, 12% of trehalose, 3% of oat grain powder, 2% of a wild soybean seed extract, 2% of witch hazel extract powder, 2% of tea polyphenol and 0.05% of sodium methylphenidate; the granularity of each powdery raw material of the face cleaning powder component is 100 meshes.
4. Preparing the camellia seed oil cleansing flour:
putting the vegetable oil microcapsule and the face cleaning powder into a high-speed stirrer, wherein the vegetable oil microcapsule accounts for 15% of the total weight of the oil tea seed oil makeup removing face cleaning powder; setting the rotating speed of the high-speed stirrer to be 300r/min, stirring for 30 minutes to fully and uniformly mix, and filling after irradiation sterilization to obtain the camellia seed oil cleansing flour.
Example 2
The preparation process of this example 2 is the same as that of example 1 except that:
1. the vegetable oil microcapsule comprises the following raw materials:
and (3) capsule wall: comprises a component A and water, wherein the mass ratio of the component A to the water is 1: 8.2. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1.2.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil-maca.
Wherein the mass ratio of the capsule core to the capsule wall is 1: 2.2.
2. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
27% of sodium lauroyl glutamate, 14% of tea saponin, 8% of starch sodium octenylsuccinate, 14% of trehalose, 4% of oat grain powder, 3% of a wild soybean seed extract, 3% of witch hazel extract powder, 3% of tea polyphenol and 0.06% of sodium methylparaben; the granularity of each powdery raw material of the face cleaning powder component is 100 meshes.
Wherein the vegetable oil microcapsule accounts for 18 percent of the total weight of the oil tea seed oil cleansing flour.
Example 3
The preparation method of example 3 is the same as that of example 1 except that:
1. the vegetable oil microcapsule comprises the following raw materials:
and (3) capsule wall: comprises a component A and water, wherein the mass ratio of the component A to the water is 1: 8.4. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1.4.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil-maca.
Wherein the mass ratio of the capsule core to the capsule wall is 1: 2.4.
2. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
29% of sodium lauroyl glutamate, 16% of tea saponin, 10% of starch sodium octenylsuccinate, 16% of trehalose, 5% of oat grain powder, 4% of a wild soybean seed extract, 4% of witch hazel extract powder, 3% of tea polyphenol and 0.08% of sodium methylphenidate; the granularity of each powdery raw material of the face cleaning powder component is 120 meshes.
Wherein the vegetable oil microcapsule accounts for 20% of the total weight of the oil tea seed oil cleansing powder.
Example 4
The preparation method of example 3 is the same as that of example 1 except that:
1. the vegetable oil microcapsule comprises the following raw materials:
and (3) capsule wall: comprises a component A and water, wherein the mass ratio of the component A to the water is 1: 8.6. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1.6.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil-maca.
Wherein the mass ratio of the capsule core to the capsule wall is 1: 2.6.
2. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
30% of sodium lauroyl glutamate, 18% of tea saponin, 14% of starch sodium octenylsuccinate, 18% of trehalose, 6% of oat grain powder, 5% of a wild soybean seed extract, 5% of witch hazel extract powder, 4% of tea polyphenol and 0.1% of sodium hydroxybenzoate; the granularity of each powdery raw material of the flour component is 160 meshes.
Wherein the vegetable oil microcapsule accounts for 22 percent of the total weight of the oil tea seed oil cleansing flour.
Example 5
The preparation process of this example 5 is the same as that of example 1 except that:
1. the vegetable oil microcapsule comprises the following raw materials:
and (3) capsule wall: comprises a component A and water, wherein the mass ratio of the component A to the water is 1: 8.8. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1.8.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil-maca.
Wherein the mass ratio of the capsule core to the capsule wall is 1: 2.8.
2. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
32% of sodium lauroyl glutamate, 20% of tea saponin, 18% of sodium starch octenylsuccinate, 20% of trehalose, 6% of oat grain powder, 5% of a wild soybean seed extract, 5% of witch hazel extract powder, 4% of tea polyphenol and 0.1% of sodium hydroxybenzoate; the granularity of each powdery raw material of the flour component is 100 meshes.
Wherein the vegetable oil microcapsule accounts for 25 percent of the total weight of the oil tea seed oil cleansing flour.
Example 6
The preparation process of this example 6 is the same as that of example 1 except that:
1. the vegetable oil microcapsule comprises the following raw materials:
and (3) capsule wall: the water-soluble paint comprises a component A and water, wherein the mass ratio of the component A to the water is 1:2. The component A comprises soybean protein isolate and maltodextrin, and the mass ratio of the soybean protein isolate to the maltodextrin is 1:2.
Capsule core preparation: the camellia oleifera seed oil-macadamia nut oil.
Wherein the mass ratio of the capsule core to the capsule wall is 1: 3.
2. Weighing powdery raw materials of the flour cleaning component according to the following weight percentage:
35% of sodium lauroyl glutamate, 20% of tea saponin, 20% of starch sodium octenylsuccinate, 20% of trehalose, 6% of oat grain powder, 5% of a wild soybean seed extract, 5% of witch hazel extract powder, 4% of tea polyphenol and 0.1% of sodium hydroxybenzoate; the granularity of each powdery raw material of the flour component is 200 meshes.
Wherein the vegetable oil microcapsule accounts for 25 percent of the total weight of the oil tea seed oil cleansing flour.
Comparative test
And (3) testing: comparative examples 1 to 4 the proportion of the vegetable oil microcapsules in the total weight of the oil tea seed oil cleansing powder was adjusted.
With example 3 as reference group:
comparative example 1
Comparative example 1 differs from example 3 in that: no vegetable oil microcapsules were added to comparative example 1. Directly putting each powdery raw material of the face cleaning powder component into a high-speed stirrer, setting the rotating speed of the high-speed stirrer to be 300r/min, stirring for 30 minutes to fully and uniformly mix, and filling after radiation sterilization.
Comparative example 2
Comparative example 2 differs from example 3 in that: the vegetable oil microcapsule accounts for 10% of the total weight of the camellia oleosa seed oil cleansing flour, and the rest is consistent with that in the embodiment 3.
Comparative example 3
Comparative example 3 differs from example 3 in that: the vegetable oil microcapsule accounts for 30% of the total weight of the camellia oleosa seed oil cleansing flour, and the rest is consistent with that in the embodiment 3.
Comparative example 4
Comparative example 3 differs from example 3 in that: the vegetable oil microcapsule accounts for 40% of the total weight of the camellia oleosa seed oil cleansing flour, and the rest is consistent with that in the example 3.
And (4) testing results:
selecting 10 volunteers with common skin and 10 volunteers with sensitive skin, wherein the volunteers with common skin and sensitive skin are female, and the age range is 20-40 years. The oil tea seed oil cleansing flour prepared in examples 1 to 6 and comparative examples 1 to 4 were used to clean facial skin once a day before makeup and once a night for five consecutive days.
The operation method comprises the following steps: the camellia seed oil cleansing powder is placed in the palm, water is added to knead the foam, the foam is smeared on the face skin which is wetted by water, the face skin is repeatedly massaged and scrubbed for 60 +/-10 seconds by hands, then the face skin is washed clean by clear water, the face skin is wiped dry, and then experience evaluation is given, and the evaluation standard is shown in table 1.
The scoring data fed back by each volunteer is actually recorded, the average scores given by 10 volunteers with general skin and 10 volunteers with sensitive skin are respectively calculated, and the results are counted in table 2.
Table 1 shows evaluation criteria of the oil tea seed oil cleansing powder
Figure BDA0002236515250000091
Table 2-1 is a statistical table of evaluation results of the camellia seed oil cleansing powder (neutral mixed skin type)
Figure BDA0002236515250000092
Figure BDA0002236515250000101
Table 2-2 is a statistical table of evaluation results (dry sensitive skin type) of the camellia seed oil cleansing powder
Figure BDA0002236515250000102
As can be seen from tables 2-1 and 2-2:
the evaluation of the cleaning powders of examples 1-6 was higher for neutral mixed skin volunteers or neutral sensitive skin volunteers, while the evaluation of the cleaning powders prepared in comparative examples 1-4 was lower. Therefore, in the components of the camellia seed oil cleansing powder, the specific gravity of the plant microcapsules is too high or too low, so that the cleansing effect and the cleansing effect of the camellia seed oil cleansing powder are affected, and the experience of the cleansing powder is also affected greatly; for example, the vegetable oil microcapsules have too low specific gravity, so the cleansing powder has large irritation to the skin and is not suitable for people with dry sensitive skin; and the vegetable oil microcapsule has too high specific gravity, so that a good cleaning effect cannot be achieved.
Therefore, through research and experiments of the applicant, the vegetable oil microcapsules account for 15% -25% of the total weight of the oil tea seed oil cleansing powder to be the most excellent, the prepared cleansing powder can be suitable for cleansing most of skin, the cleansing and makeup removing effects are good, and the cleansing powder is mild and does not irritate the skin.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.

Claims (10)

1. The camellia seed oil cleansing flour is characterized by comprising vegetable oil microcapsules and cleansing powder components;
the capsule core of the vegetable oil microcapsule comprises camellia seed oil and macadamia nut oil; the vegetable oil microcapsule accounts for 15-25% of the total weight of the oil tea seed oil cleansing powder;
the cleansing powder comprises sodium lauroyl glutamate, tea saponin, starch sodium octenylsuccinate, trehalose, oat grain powder, wild soybean seed extract, witch hazel extract powder, tea polyphenol and sodium hydroxybenzoate.
2. The camellia seed oil makeup removing cleansing flour according to claim 1, characterized in that:
the mass ratio of the capsule core to the capsule wall of the vegetable oil microcapsule is 1: 2-3.
3. The camellia seed oil makeup removing cleansing flour according to claim 1, characterized in that:
the mass ratio of the oil-tea camellia seed oil to the macadamia nut oil is 1-2: 1.
4. The camellia seed oil makeup removing cleansing flour according to claim 1, characterized in that:
the capsule wall of the vegetable oil microcapsule comprises a component A and water, wherein the component A comprises isolated soy protein and maltodextrin.
5. The camellia seed oil makeup removing cleansing flour according to claim 4, characterized in that:
the mass ratio of the component A to the water is 1: 8-9.
6. The camellia seed oil makeup removing cleansing flour according to claim 4 or 5, characterized in that:
the mass ratio of the soybean protein isolate to the maltodextrin is 1: 1-2.
7. The camellia seed oil cleansing flour according to claim 1, wherein the cleansing flour component is prepared from the following powdery raw materials in percentage by weight:
25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of a wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium methylphenidate.
8. The camellia seed oil cleansing flour according to claim 4, wherein the vegetable oil microcapsules are prepared by the following method:
step 101: adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the capsule core, and emulsifying for 20 minutes to prepare emulsion;
step 102: homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa;
step 103: and (3) carrying out spray drying on the high-pressure homogenized emulsion, wherein the air inlet temperature of the spray drying is 190 ℃, and the feeding speed is 1L/min, so as to prepare the vegetable oil microcapsule.
9. The preparation method of the camellia seed oil cleansing flour is characterized by comprising the following steps:
step 100, preparing vegetable oil microcapsules; adding water into a high-speed stirrer, starting stirring, slowly adding the soybean protein isolate and the maltodextrin, and uniformly stirring; setting the rotating speed of a high-speed stirrer to 4000r/min, slowly adding the camellia oleosa seed oil and the macadamia nut oil, and emulsifying for 20 minutes to prepare emulsion; homogenizing the emulsion for 2 times in a high-pressure homogenizer at a homogenizing pressure of 30 MPa; spray drying the high-pressure homogenized emulsion at the air inlet temperature of 190 ℃ and the feeding speed of 1L/min to obtain vegetable oil microcapsules;
step 200, weighing powdery raw materials of the flour cleaning component according to the following weight percentage: 25-35% of sodium lauroyl glutamate, 12-20% of tea saponin, 6-20% of sodium starch octenylsuccinate, 12-20% of trehalose, 3-6% of oat grain powder, 2-5% of a wild soybean seed extract, 2-5% of witch hazel extract powder, 2-4% of tea polyphenol and 0.05-0.1% of sodium methylphenidate;
300, putting the vegetable oil microcapsules and the face cleaning powder into a high-speed stirrer, wherein the vegetable oil microcapsules account for 15-25% of the total weight of the oil tea seed oil makeup removing face cleaning powder; setting the rotating speed of the high-speed stirrer to be 300r/min, stirring for 30 minutes to fully and uniformly mix, and filling after irradiation sterilization to obtain the camellia seed oil cleansing flour.
10. The preparation method of the camellia seed oil cleansing flour according to claim 9, wherein the particle size of each powdery raw material of the cleansing flour component is 100-200 meshes.
CN201910985326.7A 2019-10-16 2019-10-16 Camellia seed oil cleansing flour and preparation method thereof Pending CN110742840A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105419991A (en) * 2015-11-09 2016-03-23 重庆琥珀茶油有限公司 Face-cleansing skin-moisturizing tea oil soap
CN106038346A (en) * 2016-06-21 2016-10-26 北京兰厚化妆品有限责任公司 Washing powder and preparation method thereof
CN106572957A (en) * 2014-08-29 2017-04-19 昭和电工株式会社 Skin color-improving agent and composition for improving skin color
CN107518094A (en) * 2017-10-13 2017-12-29 广东金妮宝科技发展有限公司 The preparation method and camellia seed oil capsule powders of a kind of camellia seed oil microscapsule powder
CN108498405A (en) * 2018-06-01 2018-09-07 浙江她创美容科技有限公司 A kind of mild moisturizing face cleaning powder and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106572957A (en) * 2014-08-29 2017-04-19 昭和电工株式会社 Skin color-improving agent and composition for improving skin color
CN105419991A (en) * 2015-11-09 2016-03-23 重庆琥珀茶油有限公司 Face-cleansing skin-moisturizing tea oil soap
CN106038346A (en) * 2016-06-21 2016-10-26 北京兰厚化妆品有限责任公司 Washing powder and preparation method thereof
CN107518094A (en) * 2017-10-13 2017-12-29 广东金妮宝科技发展有限公司 The preparation method and camellia seed oil capsule powders of a kind of camellia seed oil microscapsule powder
CN108498405A (en) * 2018-06-01 2018-09-07 浙江她创美容科技有限公司 A kind of mild moisturizing face cleaning powder and preparation method thereof

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