CN110716060A - Novel material element detection and analysis system - Google Patents
Novel material element detection and analysis system Download PDFInfo
- Publication number
- CN110716060A CN110716060A CN201810757155.8A CN201810757155A CN110716060A CN 110716060 A CN110716060 A CN 110716060A CN 201810757155 A CN201810757155 A CN 201810757155A CN 110716060 A CN110716060 A CN 110716060A
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- 238000001514 detection method Methods 0.000 title claims abstract description 43
- 238000004458 analytical method Methods 0.000 title claims abstract description 27
- 239000000463 material Substances 0.000 title claims abstract description 16
- 238000012360 testing method Methods 0.000 claims abstract description 27
- 238000005070 sampling Methods 0.000 claims abstract description 25
- 238000002485 combustion reaction Methods 0.000 claims abstract description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 7
- 239000011593 sulfur Substances 0.000 claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 15
- 230000007246 mechanism Effects 0.000 claims description 15
- 238000003860 storage Methods 0.000 claims description 15
- 230000005540 biological transmission Effects 0.000 claims description 13
- 238000000034 method Methods 0.000 abstract description 14
- 230000008569 process Effects 0.000 abstract description 14
- 230000004907 flux Effects 0.000 description 11
- 239000002994 raw material Substances 0.000 description 6
- YQCIWBXEVYWRCW-UHFFFAOYSA-N methane;sulfane Chemical compound C.S YQCIWBXEVYWRCW-UHFFFAOYSA-N 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 2
- 230000033001 locomotion Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000078 claw Anatomy 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/00584—Control arrangements for automatic analysers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/00584—Control arrangements for automatic analysers
- G01N35/00722—Communications; Identification
- G01N35/00732—Identification of carriers, materials or components in automatic analysers
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/00584—Control arrangements for automatic analysers
- G01N35/00722—Communications; Identification
- G01N35/00732—Identification of carriers, materials or components in automatic analysers
- G01N2035/00821—Identification of carriers, materials or components in automatic analysers nature of coded information
- G01N2035/00831—Identification of carriers, materials or components in automatic analysers nature of coded information identification of the sample, e.g. patient identity, place of sampling
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a novel material element detection and analysis system, which comprises a carbon and sulfur analyzer, a sampling device, a sample test board and a computer, wherein the carbon and sulfur analyzer comprises a combustion furnace and an analysis host, the analysis host is connected with the computer, a crucible support is arranged below the combustion furnace, the sample test board is used for placing a crucible containing a sample to be detected, and the sampling device is arranged between the crucible support and the sample test board and is used for conveying the crucible on the sample test board to the crucible support; the analysis host is provided with a first two-dimensional code scanner, and the first two-dimensional code scanner is connected with the computer. The two-dimensional code scanner is arranged on the analysis host, the two-dimensional code label on the detection sample is read through the two-dimensional code scanner during detection, the information of the detection sample is obtained, the information is automatically stored in the computer, and the problem caused by manual entry in the detection process is reduced.
Description
Technical Field
The invention relates to the technical field of material detection equipment, in particular to a detection and analysis system for detecting the content of material elements.
Background
With the continuous development and progress of science and technology, various advanced technical means are widely applied to various fields. The processing quality of the product is the development foundation of enterprises, and the quality traceability system is more important in the production and operation of the enterprises. In the product processing process, the whole-flow information acquisition and monitoring are realized from each link of raw material purchasing, processing, inspection and packaging. In the purchasing process, the raw materials are often required to be detected to be qualified and then can be stored in a warehouse, and in order to effectively monitor the purchasing quality of the raw materials, raw material purchasing personnel can input relevant purchasing information and raw material information into a material database.
In the existing detection process of raw materials, a paper submission form is often adopted to send a detection sample and a submission form to a detection department for detection, so that the content of the submission form is often required to be repeatedly input into a computer in the detection of the detection department, each project is required to be repeatedly input, and the operation efficiency is low; the detected data needs to be manually input into a corresponding database, so that the detection workload is greatly increased; meanwhile, the problem of mixing of detection samples caused by manual operation errors is easy to occur, and effective tracing of detection quality is difficult to form.
Disclosure of Invention
The invention aims to solve the technical problems in the existing material detection process, and provides a novel material element detection analysis system which can realize automatic reading of detection sample information, enables the sample information and detection result data to correspond one to one, and avoids quality hidden troubles caused by manual operation.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
a novel material element detection and analysis system comprises a carbon and sulfur analyzer, a sampling device, a sample test board and a computer, wherein the carbon and sulfur analyzer comprises a combustion furnace and an analysis host, the analysis host is connected with the computer, a crucible support is arranged below the combustion furnace, the sample test board is used for placing a crucible containing a sample to be detected, and the sampling device is arranged between the crucible support and the sample test board and is used for conveying the crucible on the sample test board to the crucible support; the analysis host is provided with a first two-dimensional code scanner which is connected with a computer; be provided with sample platform, drying cabinet and automatic pushing mechanism on the sample test platform, automatic pushing mechanism and sample platform set up respectively in the drying cabinet both sides, automatic pushing mechanism includes second two-dimensional code scanner, first controller and electric putter, electric putter drives through step motor, first controller is connected respectively to second two-dimensional code scanner and step motor, electric putter one end is stretched into in the drying cabinet, lies in sample platform one side on the drying cabinet and is provided with the automatically-controlled door, and the automatically-controlled door is connected to the automatically-controlled door, opening and closing of first controller control automatically-controlled door.
In the above technical solution, further, the sampling device includes a second controller, a rotating motor, a rotating seat disposed on a rotating shaft of the rotating motor, and a sampling mechanism disposed on the rotating seat; the sampling mechanism comprises a main arm, two support arms symmetrically arranged on the main arm and clamping jaws respectively arranged on the two support arms, wherein a driving cylinder is arranged on the main arm, one ends of the two support arms are respectively hinged with the main arm, the middle parts of the support arms are respectively hinged with a push rod, the other end of the push rod is provided with a pin shaft, two parallel sliding grooves are arranged on the main arm along the axis direction of the main arm, one end of the pin shaft extends into the sliding grooves, the other end of the pin shaft is connected with a push plate, and the push plate is connected with a piston rod of the driving cylinder; the second controller is respectively connected with the rotating motor and the driving cylinder.
In the above technical scheme, a flux adding device is further arranged above the sample test platform and used for adding flux into the crucible, the flux adding device comprises a transmission belt arranged above the sample test platform and a storage pipe arranged on the transmission belt, a feeding pipe with a downward opening is arranged on the storage pipe, and a switch control valve is arranged on the feeding pipe.
Among the above-mentioned technical scheme, furtherly, driving motor is connected to the drive belt, and driving motor drive belt motion, be provided with the fixed bolster on the drive belt, the storage pipe is fixed to be set up on the fixed bolster, is provided with weighing transducer between storage pipe and the fixed bolster, the fluxing agent adds the device and still includes the third controller, weighing transducer, on-off control valve and driving motor are connected to the third controller respectively.
The invention has the following beneficial effects:
1) the two-dimensional code scanner is arranged on the analysis host, the two-dimensional code label on the detection sample is read by the two-dimensional code scanner during detection, the information of the detection sample is obtained, and the information is automatically stored in the computer, so that the problem caused by manual entry in the detection process is reduced;
2) a two-dimensional code scanner is arranged on the sample detection table, and when the two-dimensional code scanner reads two-dimensional code label information on a detected sample, the first controller starts the stepping motor to push the crucible in the drying box out of the sample table on the sample detection table; after the sample to be detected and the fluxing agent are respectively added into the crucible, the sample to be detected and the fluxing agent are sent into a carbon-sulfur analyzer through a sampling device for detection, the continuity of the whole process is guaranteed, and the problem that the detected sample is mixed due to human errors in the detection process is solved.
Drawings
FIG. 1 is a schematic view of the structure of the present invention.
FIG. 2 is a block diagram of a system control architecture according to the present invention.
FIG. 3 is a schematic diagram of a sample testing table according to the present invention.
FIG. 4 is a schematic view of a sampling device according to the present invention; wherein a) is a front view of the sampling device and b) is a top view of the sampling device.
FIG. 5 is a schematic view of a flux adding apparatus according to the present invention; wherein a) is a front view of the flux adding apparatus, and b) is a left view of the flux adding apparatus.
In the figure: 1. a carbon-sulfur analyzer 2, a computer 3, a sampling device 4, a sample test board 5 and a fluxing agent adding device;
101. a combustion furnace 102, an analysis host machine 103, a crucible support 104, a first two-dimensional code scanner 105 and a crucible;
301. the device comprises a rotating motor 302, a rotating base 303, a main arm 304, a support arm 305, a claw 306, a driving cylinder 307, a driving cylinder piston rod 308, a push rod 309, a pin shaft 310, a sliding groove 311 and a push plate;
401. the device comprises a sample table 402, a drying box 403, an electric push rod 404, a second two-dimensional code scanner 405 and an automatic door;
501. the device comprises a transmission belt 502, a transmission motor 503, a storage pipe 504, a feeding pipe 505, a bracket 506 and an on-off control valve.
Detailed Description
The invention is further described with reference to the following figures and specific embodiments.
As shown in fig. 1 and 3, the material element detecting and analyzing system in the present embodiment includes a carbon sulfur analyzer 1, a sampling device 3, a sample testing station 4, a flux adding device 5, and a computer 2.
The carbon-sulfur analyzer 1 comprises a combustion furnace 101 and an analysis host 102, wherein the analysis host 102 is connected with a computer 2, and a crucible support 103 is arranged below the combustion furnace 101. The sample test bench 4 is used for placing a crucible 105 filled with a sample to be detected, and the sampling device 3 is arranged between the crucible support 103 and the sample test bench 4 and is used for conveying the crucible on the sample test bench to the crucible support. In this embodiment, the analysis host is provided with a first two-dimensional code scanner 104, and the first two-dimensional code scanner 104 is connected to the computer 2, and is configured to read two-dimensional code information of the detection sample and transmit the two-dimensional code information to the computer.
As shown in fig. 3, in the present embodiment, the sample testing platform 4 is provided with a sample platform 401, a drying oven 402 and an automatic pushing mechanism, and the automatic pushing mechanism and the sample platform 401 are respectively disposed on two sides of the drying oven 402. The automatic pushing mechanism comprises a second two-dimensional code scanner 404, a first controller and an electric push rod 403, the electric push rod 403 is driven by a stepping motor, and the displacement of the electric push rod is controlled by the stepping motor; the second two-dimensional code scanner 404 and the stepping motor are respectively connected with a first controller; one end of the electric push rod 403 extends into the drying oven 402, an automatic door 405 is arranged on one side, located on the sample table 401, of the drying oven 402, the automatic door 405 is connected with a first controller, and the first controller controls the automatic door to be opened and closed. A second two-dimensional code scanner is arranged on the sample detection table, when the second two-dimensional code scanner reads two-dimensional code label information on a detected sample, the first controller starts the stepping motor and the automatic door, the automatic door is opened at the moment, and the electric push rod pushes the crucible in the drying oven out to the sample table on the sample detection table; respectively adding a sample to be detected and a fluxing agent into the crucible, and then sending the sample and the fluxing agent into a carbon-sulfur analyzer through a sampling device for detection; by adopting the control mode, the continuity of the whole process is ensured, and the problem that the detection sample is mixed due to human errors in the detection process is prevented. The control of the opening and closing of the automatic door by the controller is prior art and the specific structure and implementation thereof will not be described here.
As shown in fig. 4, the sampling device of the present invention includes a second controller, a rotating motor 301, a rotating base 302 disposed on a rotating shaft of the rotating motor, and a sampling mechanism disposed on the rotating base; the sampling mechanism comprises a main arm 303, two support arms 304 symmetrically arranged on the main arm and clamping jaws 305 respectively arranged on the two support arms, a driving cylinder 306 is arranged on the main arm 303, one ends of the two support arms 304 are respectively hinged with the main arm 303, the middle parts of the support arms 304 are respectively hinged with a push rod 308, a pin shaft 309 is arranged at the other end of the push rod 308, two parallel sliding grooves 310 are arranged on the main arm 303 along the axis direction of the main arm, one end of the pin shaft 309 extends into the sliding groove 310, the other end of the pin shaft is connected with a push plate 311, and the push plate 311 is connected with a piston rod 307 of the driving cylinder. The second controller is respectively connected with the rotating motor and the driving cylinder. The second controller control drives actuating cylinder action, when driving actuating cylinder piston rod and stretching out right, it promotes the push pedal to move right to drive actuating cylinder piston rod, the push pedal drives two round pin axles and moves right along the spout, the push rod opens and makes two support arms open this moment, the crucible that will wait to detect on the crucible sample presentation platform pushes away to the assigned position, it moves left to drive actuating cylinder piston rod, two round pin axles of push pedal drive move left along the spout, the push rod inwards draws in this moment, two support arms draw in under the effect of push rod and press from both sides the crucible on the crucible sample presentation platform through the jack catch and press from both sides tightly. The second controller starts the rotating motor, the rotating motor controls the rotating seat to rotate 180 degrees leftwards, the crucible is conveyed to the position of the crucible support, the starting cylinder repeats the operation, and the crucible can be placed on the crucible support, so that automatic sampling operation is realized.
As shown in fig. 5, a flux adding device 5 is disposed above the sample test platform, and the flux adding device is used for adding flux into the crucible, and in the embodiment, specifically, the flux adding device includes a conveyor belt 501 disposed above the sample test platform and a storage tube 503 disposed on the conveyor belt 501, a feeding tube 504 with a downward opening is disposed on the storage tube 503, and an on-off control valve 506 is disposed on the feeding tube 504. Preferably, the transmission belt 501 is connected with a transmission motor 502, the transmission motor 502 drives the transmission belt 501 to move, the transmission belt 501 is provided with a fixed bracket 505, the storage pipe 503 is fixedly arranged on the fixed bracket 505, a weight sensor is arranged between the storage pipe 503 and the fixed bracket 505, the fluxing agent adding device 5 further comprises a third controller, and the weight sensor, the on-off control valve and the transmission motor are respectively connected to the third controller. When the fluxing agent is added into the crucible, the third controller controls the movement of the transmission belt according to the type of the added fluxing agent so that the storage pipe filled with the corresponding fluxing agent moves to the upper part of the crucible, meanwhile, the opening and closing of the switch control valve are controlled according to the fluxing agent adding amount set in the third controller, the weight of the storage pipe is detected through the weight sensor, and the adding amount of the fluxing agent is controlled.
Fig. 2 is a block diagram of a system control structure of the present invention, in which a first controller, a second controller and a third controller are respectively connected to a computer, and program control of the first controller, the second controller and the third controller is realized through a control program of the computer, so as to sequentially realize an automatic control process of pushing, loading a sample and a fluxing agent, sampling and detecting a crucible, the process can be set and controlled through test software of the computer, and the process can be realized under the control of the test software, the present invention does not relate to the content of the test software, and even if the test software is not adopted, the detection process of the present invention can be realized by separately controlling the first controller, the second controller and the third controller; the block diagram of the system control architecture shown in fig. 2 is only one preferred way for the system to implement the detection analysis control.
The present specification and figures are to be regarded as illustrative rather than restrictive, and it is intended that all such alterations and modifications that fall within the true spirit and scope of the invention, and that all such modifications and variations are included within the scope of the invention as determined by the appended claims without the use of inventive faculty.
Claims (4)
1. A novel material element detection and analysis system is characterized in that: the carbon and sulfur analysis device comprises a carbon and sulfur analyzer, a sampling device, a sample test board and a computer, wherein the carbon and sulfur analyzer comprises a combustion furnace and an analysis host, the analysis host is connected with the computer, a crucible support is arranged below the combustion furnace, the sample test board is used for placing a crucible containing a sample to be detected, and the sampling device is arranged between the crucible support and the sample test board and is used for conveying the crucible on the sample test board to the crucible support; the analysis host is provided with a first two-dimensional code scanner which is connected with a computer; be provided with sample platform, drying cabinet and automatic pushing mechanism on the sample test platform, automatic pushing mechanism and sample platform set up respectively in the drying cabinet both sides, automatic pushing mechanism includes second two-dimensional code scanner, first controller and electric putter, electric putter drives through step motor, first controller is connected respectively to second two-dimensional code scanner and step motor, electric putter one end is stretched into in the drying cabinet, lies in sample platform one side on the drying cabinet and is provided with the automatically-controlled door, and the automatically-controlled door is connected to the automatically-controlled door, opening and closing of first controller control automatically-controlled door.
2. The novel material element detection and analysis system according to claim 1, wherein: the sampling device comprises a second controller, a rotating motor, a rotating seat arranged on a rotating shaft of the rotating motor and a sampling mechanism arranged on the rotating seat; the sampling mechanism comprises a main arm, two support arms symmetrically arranged on the main arm and clamping jaws respectively arranged on the two support arms, wherein a driving cylinder is arranged on the main arm, one ends of the two support arms are respectively hinged with the main arm, the middle parts of the support arms are respectively hinged with a push rod, the other end of the push rod is provided with a pin shaft, two parallel sliding grooves are arranged on the main arm along the axis direction of the main arm, one end of the pin shaft extends into the sliding grooves, the other end of the pin shaft is connected with a push plate, and the push plate is connected with a piston rod of the driving cylinder; the second controller is respectively connected with the rotating motor and the driving cylinder.
3. The novel material element detection and analysis system according to claim 1, wherein: a fluxing agent adding device is arranged above the sample test platform and used for adding a fluxing agent into the crucible, the fluxing agent adding device comprises a transmission belt arranged above the sample test platform and a storage pipe arranged on the transmission belt, a feeding pipe with a downward opening is arranged on the storage pipe, and a switch control valve is arranged on the feeding pipe.
4. The novel material element detection and analysis system according to claim 3, wherein: the driving belt is connected with the driving motor, the driving motor drives the driving belt to move, the driving belt is provided with a fixed support, the material storage pipe is fixedly arranged on the fixed support, a weight sensor is arranged between the material storage pipe and the fixed support, the fluxing agent adding device further comprises a third controller, and the weight sensor, the switch control valve and the driving motor are respectively connected to the third controller.
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CN201810757155.8A CN110716060A (en) | 2018-07-11 | 2018-07-11 | Novel material element detection and analysis system |
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CN201810757155.8A CN110716060A (en) | 2018-07-11 | 2018-07-11 | Novel material element detection and analysis system |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110716062A (en) * | 2018-07-11 | 2020-01-21 | 四川赛恩思仪器有限公司 | Automatic sampling device for metal material detection |
CN112611879A (en) * | 2020-11-20 | 2021-04-06 | 广西玉柴机器股份有限公司 | Analysis method of control system applied to material element analysis of internal combustion engine parts |
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CN206248676U (en) * | 2016-12-16 | 2017-06-13 | 宁波美康盛德生物科技有限公司 | Multiple sample introduction propulsive mechanism |
CN206399824U (en) * | 2016-12-30 | 2017-08-11 | 南京麒麟科学仪器集团有限公司 | Coreless induction furnace and infrared carbon sulfur analyzer |
CN207066983U (en) * | 2017-08-14 | 2018-03-02 | 四川赛恩思仪器有限公司 | A kind of combustion furnace of fast assembling-disassembling burner |
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2018
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Patent Citations (8)
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CN101960312A (en) * | 2008-03-07 | 2011-01-26 | 希森美康株式会社 | Analysis apparatus and measurement unit |
CN104493832A (en) * | 2014-12-12 | 2015-04-08 | 重庆强达力科技发展有限公司 | Workpiece grabbing mechanism provided with elastic body |
CN105486879A (en) * | 2015-11-30 | 2016-04-13 | 钢研纳克检测技术有限公司 | Vertical-type tubular furnace infrared carbon sulfur analyzer |
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CN206248676U (en) * | 2016-12-16 | 2017-06-13 | 宁波美康盛德生物科技有限公司 | Multiple sample introduction propulsive mechanism |
CN106766913A (en) * | 2016-12-30 | 2017-05-31 | 南京麒麟科学仪器集团有限公司 | Novel high-frequency stove and infrared carbon sulfur analyzer |
CN206399824U (en) * | 2016-12-30 | 2017-08-11 | 南京麒麟科学仪器集团有限公司 | Coreless induction furnace and infrared carbon sulfur analyzer |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110716062A (en) * | 2018-07-11 | 2020-01-21 | 四川赛恩思仪器有限公司 | Automatic sampling device for metal material detection |
CN112611879A (en) * | 2020-11-20 | 2021-04-06 | 广西玉柴机器股份有限公司 | Analysis method of control system applied to material element analysis of internal combustion engine parts |
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