CN110680763A - Dry mask capable of releasing active oxygen, whitening skin and replenishing water - Google Patents

Dry mask capable of releasing active oxygen, whitening skin and replenishing water Download PDF

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Publication number
CN110680763A
CN110680763A CN201910959941.0A CN201910959941A CN110680763A CN 110680763 A CN110680763 A CN 110680763A CN 201910959941 A CN201910959941 A CN 201910959941A CN 110680763 A CN110680763 A CN 110680763A
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Prior art keywords
drying
stage
parts
active oxygen
collagen
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Inventor
刘学军
万炜
苏天健
侯哲
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Anhui Oxygen Biotechnology Co Ltd
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Anhui Oxygen Biotechnology Co Ltd
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Priority to CN201910959941.0A priority Critical patent/CN110680763A/en
Publication of CN110680763A publication Critical patent/CN110680763A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/447Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
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  • Microbiology (AREA)
  • Mycology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a dry mask capable of releasing active oxygen, whitening and moisturizing, which comprises the following raw materials in parts by weight: 72-85 parts of water, 5-10 parts of percarbamide, 0.05-0.15 part of ceramide, 0.05-0.15 part of squalane, 0.05-0.15 part of oligopeptide, 0.01-0.06 part of vitamin E, 0.01-0.06 part of polyglutamic acid, 0.1-0.15 part of seaweed extract, 0.02-0.0.06 parts of SOD, 0.07-0.13 part of glycerol, 0.08-0.12 part of sodium hyaluronate, 0.03-0.05 part of collagen, 0.02-0.06 part of nicotinamide and 0.01-0.05 part of L-cysteine.

Description

Dry mask capable of releasing active oxygen, whitening skin and replenishing water
Technical Field
The invention relates to a dry mask, in particular to a dry mask capable of releasing active oxygen, whitening skin and replenishing water, and belongs to the technical field of cosmetics.
Background
The popular facial mask is used as a beautifying and maintaining method, and products in the market are various in five flowers and different in functions. Most of the materials are difficult to be manufactured and stored in a wet way, and the defects are as follows: 1. the facial mask contains preservatives, 2, chemical components affecting skin health, a few effective components are attenuated, the beautifying and maintaining effects cannot be effectively maintained, 4, the formula is unscientific, the addition of ineffective components is excessive, antimicrobial agents such as hydroxybenzoic acid esters are often required to be added for storage, but the facial mask is easy to cause allergy, further has the worry of contact dermatitis, causes damage to users, even has the risk of causing cancer, and the effect of the commercially available facial mask is not ideal and is easy to cause allergy.
Disclosure of Invention
The invention aims to provide a dry mask capable of releasing active oxygen, whitening and moisturizing so as to solve the problem that skin health is affected and allergy is prone to occurring in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the active oxygen releasing, whitening and moisturizing dry mask comprises the following raw materials in parts by weight: 72-85 parts of water, 5-10 parts of percarbamide, 0.05-0.15 part of ceramide, 0.05-0.15 part of squalane, 0.05-0.15 part of oligopeptide, 0.01-0.06 part of vitamin E, 0.01-0.06 part of polyglutamic acid, 0.1-0.15 part of seaweed extract, 0.02-0.0.06 part of SOD, 0.07-0.13 part of glycerol, 0.08-0.12 part of sodium hyaluronate, 0.03-0.05 part of collagen, 0.02-0.06 part of nicotinamide and 0.01-0.05 part of L-cysteine.
In a preferred embodiment of the present invention, the water comprises 72 parts, 5 parts of percarbamide, 0.05 part of ceramide, 0.05 part of squalane, 0.05 part of oligopeptide, 0.01 part of vitamin E, 0.01 part of polyglutamic acid, 0.1 part of seaweed extract, 0.02 part of SOD, 0.05 part of glycerol, 0.05 part of sodium hyaluronate, 0.01 part of collagen, 0.05 part of nicotinamide and 0.01 part of L-cysteine.
In a preferred embodiment of the present invention, the water comprises 79 parts, percarbamide 7 parts, ceramide 0.1 part, squalane 0.1 part, oligopeptide 0.1 part, vitamin E0.03 part, polyglutamic acid 0.03 part, seaweed extract 0.12 part, SOD00.4 part, glycerin 0.1 part, sodium hyaluronate 0.1 part, collagen 0.03 part, nicotinamide 0.1 part, and L-cysteine 0.03 part.
In a preferred embodiment of the present invention, the water is 85 parts, the percarbamide is 10 parts, the ceramide is 0.15 part, the squalane is 0.15 part, the oligopeptide is 0.15 part, the vitamin E is 0.06 part, the polyglutamic acid is 0.06 part, the seaweed extract is 0.15 part, the SOD is 0.06 part, the glycerol is 0.15 part, the sodium hyaluronate is 0.15 part, the collagen is 0.06 part, the nicotinamide is 0.15 part, and the L-cysteine is 0.05 part.
In a preferred embodiment of the present invention, the collagen is soluble collagen.
As a preferable technical scheme of the invention, the method comprises the following steps:
s1: accurately weighing the water, the percarbamide, the ceramide, the squalane, the oligopeptide, the vitamin E, the polyglutamic acid, the seaweed extract, the SOD, the glycerol, the sodium hyaluronate, the collagen, the nicotinamide and the L-cysteine according to the proportion of claim 1 for later use.
S2: the raw materials of water, percarbamide, glycerin, sodium hyaluronate and collagen are put into a vacuum homogenizing emulsifying machine to be stirred, and the temperature is increased to 80-90 ℃ at the same time, so that the raw materials are melted.
S3: and after S2 is cooled, putting the nicotinamide and the L-cysteine into the oil phase pot for stirring, and fully and uniformly mixing the materials.
S4: sampling and detecting, and charging after the product is qualified.
S5: soaking the facial mask paper in the stock solution for 30min, taking out, freeze drying, and compressing to obtain dry facial mask.
S6: sealing and packaging with packaging bag.
As a preferred technical solution of the present invention, the specific conditions of the freeze drying are as follows:
stage 1: drying at 10 deg.C to-25 deg.C for 120 min;
stage 2: drying at-25 deg.C to-35 deg.C for 120 min;
stage 3: drying at-35 deg.C to-45 deg.C for 180 min;
and 4, stage: drying at-45 deg.C to-55 deg.C for 120 min;
stage 5: drying at-55 deg.C to-65 deg.C for 200 min;
stage 6: drying at-65 deg.C to-55 deg.C for 180 min;
stage 7: drying at-55 deg.C-45 deg.C for 150 min;
stage 8: drying at-45 deg.C to-35 deg.C for 270 min;
stage 9: drying at-35 to-25 deg.C for 140 min;
stage 10: drying at-25 deg.C to-15 deg.C for 240 min;
stage 11: drying at-15 deg.C to-5 deg.C for 200 min;
stage 12: drying at-5 deg.C to 0 deg.C for 300 min;
stage 13: drying at 0-20 deg.C for 120 min;
stage 14: drying at 20-25 deg.C for 60min,
stage 15: drying at 25-35 deg.C for 60 min;
stage 16: drying at 35 deg.C for 90 min.
As a preferred technical scheme of the invention, the percarbamide is a mixture formed by urea and hydrogen peroxide, has white crystal powder appearance, is non-toxic and odorless, is easily dissolved in an aqueous solution, and has the properties of both urea and hydrogen peroxide.
Compared with the prior art, the invention has the beneficial effects that: the invention provides an active oxygen whitening and moisturizing dry mask without additives and preservatives, which is easy to store, difficult to deteriorate, capable of having remarkable whitening, moisturizing and wrinkle removing effects after use, good in use safety, tender and elastic in skin and capable of enabling the skin to be glowing and shining, and when in use, the effective components for beautifying are uniformly coated on a mask paper layer and kept dry, so that the mask paper layer is easy to store, the probability of bacterial breeding is reduced, the use of preservatives is avoided, the sanitation and safety of users are guaranteed, and the harm to the skin is reduced; when in use, a bottle of high-temperature sterilized deionized water is poured into the facial mask containing groove, and the dry powder is dissolved and then applied to the face, so that a user can simply and conveniently soak the facial mask to keep the facial mask clean.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the invention provides a dry mask capable of releasing active oxygen, whitening and moisturizing, which comprises the following raw materials in parts by weight:
72 parts of water, 5 parts of percarbamide, 0.05 part of ceramide, 0.05 part of squalane, 0.05 part of oligopeptide, 0.01 part of vitamin E, 0.01 part of polyglutamic acid, 0.1 part of seaweed extract, 0.02 part of SOD, 0.05 part of glycerol, 0.05 part of sodium hyaluronate, 0.01 part of collagen, 0.05 part of nicotinamide and 0.01 part of L-cysteine.
Preferably, the collagen is soluble collagen.
Preferably, the method comprises the following steps:
s1: accurately weighing water, percarbamide, ceramide, squalane, oligopeptide, vitamin E, polyglutamic acid, seaweed extract, SOD, glycerol, sodium hyaluronate, collagen, nicotinamide and L-cysteine according to the proportion of claim 1 for later use.
S2: the raw materials of water, percarbamide, glycerin, sodium hyaluronate and collagen are put into a vacuum homogenizing emulsifying machine to be stirred, and the temperature is increased to 80-90 ℃ at the same time, so that the raw materials are melted.
S3: and after S2 is cooled, putting the nicotinamide and the L-cysteine into the oil phase pot for stirring, and fully and uniformly mixing the materials.
S4: sampling and detecting, and charging after the product is qualified.
S5: soaking the facial mask paper in the stock solution for 30min, taking out, freeze drying, and compressing to obtain dry facial mask.
S6: sealing and packaging with packaging bag.
Preferably, the specific conditions of freeze-drying are:
stage 1: drying at 10 deg.C to-25 deg.C for 120 min;
stage 2: drying at-25 deg.C to-35 deg.C for 120 min;
stage 3: drying at-35 deg.C to-45 deg.C for 180 min;
and 4, stage: drying at-45 deg.C to-55 deg.C for 120 min;
stage 5: drying at-55 deg.C to-65 deg.C for 200 min;
stage 6: drying at-65 deg.C to-55 deg.C for 180 min;
stage 7: drying at-55 deg.C-45 deg.C for 150 min;
stage 8: drying at-45 deg.C to-35 deg.C for 270 min;
stage 9: drying at-35 to-25 deg.C for 140 min;
stage 10: drying at-25 deg.C to-15 deg.C for 240 min;
stage 11: drying at-15 deg.C to-5 deg.C for 200 min;
stage 12: drying at-5 deg.C to 0 deg.C for 300 min;
stage 13: drying at 0-20 deg.C for 120 min;
stage 14: drying at 20-25 deg.C for 60min,
stage 15: drying at 25-35 deg.C for 60 min;
stage 16: drying at 35 deg.C for 90 min.
Preferably, the percarbamide is a mixture formed by urea and hydrogen peroxide, has white crystalline powder appearance, is non-toxic and odorless, is easily dissolved in an aqueous solution, has the properties of urea and hydrogen peroxide, is decomposed into hydrogen peroxide, urea, carbon dioxide, ammonia and the like in the aqueous solution, and has the bleaching active ingredients that the hydrogen peroxide is reported that 10-15 percent of the percarbamide is decomposed into 7-10 percent of urea and 3-5 percent of the hydrogen peroxide, and the peroxide content of products of different brands of the hydrogen peroxide is slightly different from that of other inorganic peroxides; the urea has a certain defense effect on water loss in skin, can reduce water loss of epidermis or outer skin, and can remove aged cutin and increase water retention of cutin. Has super-strong water-locking capability and can moisten dry skin areas. Can be used to help treat eczema or psoriasis; enhancing the skin barrier. Because urea can help skin cells to regenerate, the skin protection function and health can be enhanced, and the permeability of other components can be improved. Urea can help other components, especially some components with anti-inflammatory effect, permeate and absorb, and dry skin becomes softer, smoother and more elastic due to the excellent moisturizing capability of urea.
Example two:
the invention provides a dry mask capable of releasing active oxygen, whitening and moisturizing, which comprises the following raw materials in parts by weight:
79 parts of water, 7 parts of percarbamide, 0.1 part of ceramide, 0.1 part of squalane, 0.1 part of oligopeptide, 0.03 part of vitamin E, 0.03 part of polyglutamic acid, 0.12 part of seaweed extract, 00.4 parts of SOD, 0.1 part of glycerol, 0.1 part of sodium hyaluronate, 0.03 part of collagen, 0.1 part of nicotinamide and 0.03 part of L-cysteine.
Preferably, the collagen is soluble collagen.
Preferably, the method comprises the following steps:
s1: accurately weighing water, percarbamide, ceramide, squalane, oligopeptide, vitamin E, polyglutamic acid, seaweed extract, SOD, glycerol, sodium hyaluronate, collagen, nicotinamide and L-cysteine according to the proportion of claim 1 for later use.
S2: the raw materials of water, percarbamide, glycerin, sodium hyaluronate and collagen are put into a vacuum homogenizing emulsifying machine to be stirred, and the temperature is increased to 80-90 ℃ at the same time, so that the raw materials are melted.
S3: and after S2 is cooled, putting the nicotinamide and the L-cysteine into the oil phase pot for stirring, and fully and uniformly mixing the materials.
S4: sampling and detecting, and charging after the product is qualified.
S5: soaking the facial mask paper in the stock solution for 30min, taking out, freeze drying, and compressing to obtain dry facial mask.
S6: sealing and packaging with packaging bag.
Preferably, the specific conditions of freeze-drying are:
stage 1: drying at 10 deg.C to-25 deg.C for 120 min;
stage 2: drying at-25 deg.C to-35 deg.C for 120 min;
stage 3: drying at-35 deg.C to-45 deg.C for 180 min;
and 4, stage: drying at-45 deg.C to-55 deg.C for 120 min;
stage 5: drying at-55 deg.C to-65 deg.C for 200 min;
stage 6: drying at-65 deg.C to-55 deg.C for 180 min;
stage 7: drying at-55 deg.C-45 deg.C for 150 min;
stage 8: drying at-45 deg.C to-35 deg.C for 270 min;
stage 9: drying at-35 to-25 deg.C for 140 min;
stage 10: drying at-25 deg.C to-15 deg.C for 240 min;
stage 11: drying at-15 deg.C to-5 deg.C for 200 min;
stage 12: drying at-5 deg.C to 0 deg.C for 300 min;
stage 13: drying at 0-20 deg.C for 120 min;
stage 14: drying at 20-25 deg.C for 60min,
stage 15: drying at 25-35 deg.C for 60 min;
stage 16: drying at 35 deg.C for 90 min.
Preferably, the percarbamide is a mixture formed by urea and hydrogen peroxide, has white crystalline powder appearance, is non-toxic and odorless, is easily dissolved in an aqueous solution, has the properties of urea and hydrogen peroxide, is decomposed into hydrogen peroxide, urea, carbon dioxide, ammonia and the like in the aqueous solution, and has the bleaching active ingredients that the hydrogen peroxide is reported that 10-15 percent of the percarbamide is decomposed into 7-10 percent of urea and 3-5 percent of the hydrogen peroxide, and the peroxide content of products of different brands of the hydrogen peroxide is slightly different from that of other inorganic peroxides; the urea has a certain defense effect on water loss in skin, can reduce water loss of epidermis or outer skin, and can remove aged cutin and increase water retention of cutin. Has super-strong water-locking capability and can moisten dry skin areas. Can be used to help treat eczema or psoriasis; enhancing the skin barrier. Because urea can help skin cells to regenerate, the skin protection function and health can be enhanced, and the permeability of other components can be improved. Urea can help other components, especially some components with anti-inflammatory effect, permeate and absorb, and dry skin becomes softer, smoother and more elastic due to the excellent moisturizing capability of urea.
Example three:
the invention provides a dry mask capable of releasing active oxygen, whitening and moisturizing, which comprises the following raw materials in parts by weight:
85 parts of water, 10 parts of percarbamide, 0.15 part of ceramide, 0.15 part of squalane, 0.15 part of oligopeptide, 0.06 part of vitamin E, 0.06 part of polyglutamic acid, 0.15 part of seaweed extract, 0.06 part of SOD, 0.15 part of glycerol, 0.15 part of sodium hyaluronate, 0.06 part of collagen, 0.15 part of nicotinamide and 0.05 part of L-cysteine.
Preferably, the collagen is soluble collagen.
Preferably, the method comprises the following steps:
s1: accurately weighing the water, the percarbamide, the ceramide, the squalane, the oligopeptide, the vitamin E, the polyglutamic acid, the seaweed extract, the SOD, the glycerol, the sodium hyaluronate, the collagen, the nicotinamide and the L-cysteine according to the proportion of claim 1 for later use.
S2: the raw materials of water, percarbamide, glycerin, sodium hyaluronate and collagen are put into a vacuum homogenizing emulsifying machine to be stirred, and the temperature is increased to 80-90 ℃ at the same time, so that the raw materials are melted.
S3: and after S2 is cooled, putting the nicotinamide and the L-cysteine into the oil phase pot for stirring, and fully and uniformly mixing the materials.
S4: sampling and detecting, and charging after the product is qualified.
S5: soaking the facial mask paper in the stock solution for 30min, taking out, freeze drying, and compressing to obtain dry facial mask.
S6: sealing and packaging with packaging bag.
Preferably, the specific conditions of the freeze-drying are:
stage 1: drying at 10 deg.C to-25 deg.C for 120 min;
stage 2: drying at-25 deg.C to-35 deg.C for 120 min;
stage 3: drying at-35 deg.C to-45 deg.C for 180 min;
and 4, stage: drying at-45 deg.C to-55 deg.C for 120 min;
stage 5: drying at-55 deg.C to-65 deg.C for 200 min;
stage 6: drying at-65 deg.C to-55 deg.C for 180 min;
stage 7: drying at-55 deg.C-45 deg.C for 150 min;
stage 8: drying at-45 deg.C to-35 deg.C for 270 min;
stage 9: drying at-35 to-25 deg.C for 140 min;
stage 10: drying at-25 deg.C to-15 deg.C for 240 min;
stage 11: drying at-15 deg.C to-5 deg.C for 200 min;
stage 12: drying at-5 deg.C to 0 deg.C for 300 min;
stage 13: drying at 0-20 deg.C for 120 min;
stage 14: drying at 20-25 deg.C for 60min,
stage 15: drying at 25-35 deg.C for 60 min;
stage 16: drying at 35 deg.C for 90 min.
Preferably, the percarbamide is a mixture formed by urea and hydrogen peroxide, has white crystalline powder appearance, is non-toxic and odorless, is easily dissolved in an aqueous solution, has the properties of urea and hydrogen peroxide, is decomposed into hydrogen peroxide, urea, carbon dioxide, ammonia and the like in the aqueous solution, and has the bleaching active ingredients that the hydrogen peroxide is reported that 10-15 percent of the percarbamide is decomposed into 7-10 percent of urea and 3-5 percent of the hydrogen peroxide, and the peroxide content of products of different brands of the hydrogen peroxide is slightly different from that of other inorganic peroxides; the urea has a certain defense effect on water loss in skin, can reduce water loss of epidermis or outer skin, and can remove aged cutin and increase water retention of cutin. Has super-strong water-locking capability and can moisten dry skin areas. Can be used to help treat eczema or psoriasis; enhancing the skin barrier. Because urea can help skin cells to regenerate, the skin protection function and health can be enhanced, and the permeability of other components can be improved. Urea can help other components, especially some components with anti-inflammatory effect, permeate and absorb, and dry skin becomes softer, smoother and more elastic due to the excellent moisturizing capability of urea.
Comparative example 1 differs from example 3 in that it does not contain percarbamide and the other ingredients and preparation method are the same as example 3.
Comparative example 2
Comparative example 2 is different from example 3 in that hyaluronic acid is not contained, and other ingredients and preparation methods are compared with example 2.
Comparative example 3
A commercially available mask.
Effect test
The actual effects of the cosmetics prepared in the above examples were evaluated by comparative analysis.
The experimental method comprises the following steps:
grouping experiments: the experiment was divided into an experimental group and a control group, wherein the experimental group 1 to 3 were cosmetics prepared in the above examples 1 to 3, and the control group was cosmetics prepared in the above comparative examples 1 to 3 and a commercially available facial mask in comparative example 4.
Test objects: the groups are 50 middle-aged women, are 25-45 years old, are healthy, have no skin disease or allergic disease history, have non-sensitive skin, can use cosmetics according to the standard, are matched with workers to finish evaluation work according to requirements, have certain expression capability and can truly reflect the feeling after use;
testing an instrument: VISA digital skin analyzer (USA), Mexameter MX18(CK Electronic GmbH, Germany); test area: cheek area (avoid smiling lines, light reflecting areas, moles and hair as much as possible); the using method comprises the following steps: the preparation is administered 1 time each day in the morning and evening for 8 weeks;
and (3) testing and analyzing: the effects of the facial masks of the experimental group and the control group are evaluated by comparing color spots before use and after 8 weeks use and a comparison table after 8 weeks of disuse, and the average value of the color spot reduction rate of each group of people and the effective rate are calculated.
Table 1:
Figure BDA0002228584390000111
the data prove that the color spot reduction rate of the dry mask containing the percarbamide reaches more than 90 percent after the dry mask is used, the effective rate reaches more than 99 percent, the dry mask is obviously superior to the commercial spot-fading mask, and the dry mask does not rebound after being stopped.
The foregoing is a preferred embodiment of the present invention, and it should be noted that modifications and embellishments could be made by those skilled in the art without departing from the principle of the present invention, and these modifications and embellishments are also considered to be within the scope of the present invention.

Claims (8)

1. The dry mask capable of releasing active oxygen, whitening and moisturizing is characterized in that: the active oxygen releasing, whitening and moisturizing dry mask comprises the following raw materials in parts by weight: 72-85 parts of water, 5-10 parts of percarbamide, 0.05-0.15 part of ceramide, 0.05-0.15 part of squalane, 0.05-0.15 part of oligopeptide, 0.01-0.06 part of vitamin E, 0.01-0.06 part of polyglutamic acid, 0.1-0.15 part of seaweed extract, 0.02-0.0.06 part of SOD, 0.07-0.13 part of glycerol, 0.08-0.12 part of sodium hyaluronate, 0.03-0.05 part of collagen, 0.02-0.06 part of nicotinamide and 0.01-0.05 part of L-cysteine.
2. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized in that: 72 parts of water, 5 parts of percarbamide, 0.05 part of ceramide, 0.05 part of squalane, 0.05 part of oligopeptide, 0.01 part of vitamin E, 0.01 part of polyglutamic acid, 0.1 part of seaweed extract, 0.02 part of SOD, 0.05 part of glycerol, 0.05 part of sodium hyaluronate, 0.01 part of collagen, 0.05 part of nicotinamide and 0.01 part of L-cysteine.
3. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized in that: 79 parts of water, 7 parts of percarbamide, 0.1 part of ceramide, 0.1 part of squalane, 0.1 part of oligopeptide, 0.03 part of vitamin E, 0.03 part of polyglutamic acid, 0.12 part of seaweed extract, 00.4 parts of SOD, 0.1 part of glycerol, 0.1 part of sodium hyaluronate, 0.03 part of collagen, 0.1 part of nicotinamide and 0.03 part of L-cysteine.
4. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized in that: 85 parts of water, 10 parts of percarbamide, 0.15 part of ceramide, 0.15 part of squalane, 0.15 part of oligopeptide, 0.06 part of vitamin E, 0.06 part of polyglutamic acid, 0.15 part of seaweed extract, 0.06 part of SOD, 0.15 part of glycerol, 0.15 part of sodium hyaluronate, 0.06 part of collagen, 0.15 part of nicotinamide and 0.05 part of L-cysteine.
5. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized in that: the collagen is soluble collagen.
6. The method for preparing the formula of the dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized by comprising the following steps:
s1: accurately weighing the water, the percarbamide, the ceramide, the squalane, the oligopeptide, the vitamin E, the polyglutamic acid, the seaweed extract, the SOD, the glycerol, the sodium hyaluronate, the collagen, the nicotinamide and the L-cysteine according to the proportion of claim 1 for later use.
S2: the raw materials of water, percarbamide, glycerin, sodium hyaluronate and collagen are put into a vacuum homogenizing emulsifying machine to be stirred, and the temperature is increased to 80-90 ℃ at the same time, so that the raw materials are melted.
S3: and after S2 is cooled, putting the nicotinamide and the L-cysteine into the oil phase pot for stirring, and fully and uniformly mixing the materials.
S4: sampling and detecting, and charging after the product is qualified.
S5: soaking the facial mask paper in the stock solution for 30min, taking out, freeze drying, and compressing to obtain dry facial mask.
S6: sealing and packaging with packaging bag.
7. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 5, is characterized in that: the specific conditions of the freeze drying are as follows:
stage 1: drying at 10 deg.C to-25 deg.C for 120 min;
stage 2: drying at-25 deg.C to-35 deg.C for 120 min;
stage 3: drying at-35 deg.C to-45 deg.C for 180 min;
and 4, stage: drying at-45 deg.C to-55 deg.C for 120 min;
stage 5: drying at-55 deg.C to-65 deg.C for 200 min;
stage 6: drying at-65 deg.C to-55 deg.C for 180 min;
stage 7: drying at-55 deg.C-45 deg.C for 150 min;
stage 8: drying at-45 deg.C to-35 deg.C for 270 min;
stage 9: drying at-35 to-25 deg.C for 140 min;
stage 10: drying at-25 deg.C to-15 deg.C for 240 min;
stage 11: drying at-15 deg.C to-5 deg.C for 200 min;
stage 12: drying at-5 deg.C to 0 deg.C for 300 min;
stage 13: drying at 0-20 deg.C for 120 min;
stage 14: drying at 20-25 deg.C for 60min,
stage 15: drying at 25-35 deg.C for 60 min;
stage 16: drying at 35 deg.C for 90 min.
8. The dry mask capable of releasing active oxygen, whitening and moisturizing as claimed in claim 1, is characterized in that: the percarbamide is a mixture formed by urea and hydrogen peroxide, is white crystal powder in appearance, is non-toxic and odorless, is easily dissolved in an aqueous solution, and has the properties of urea and hydrogen peroxide.
CN201910959941.0A 2019-10-10 2019-10-10 Dry mask capable of releasing active oxygen, whitening skin and replenishing water Pending CN110680763A (en)

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