CN110679604A - Plant growth regulator composition and preparation method thereof - Google Patents
Plant growth regulator composition and preparation method thereof Download PDFInfo
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- CN110679604A CN110679604A CN201910816116.5A CN201910816116A CN110679604A CN 110679604 A CN110679604 A CN 110679604A CN 201910816116 A CN201910816116 A CN 201910816116A CN 110679604 A CN110679604 A CN 110679604A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/36—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< directly attached to at least one heterocyclic ring; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group, wherein Cn means a carbon skeleton not containing a ring; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N45/00—Biocides, pest repellants or attractants, or plant growth regulators, containing compounds having three or more carbocyclic rings condensed among themselves, at least one ring not being a six-membered ring
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a plant growth regulator composition and a preparation method thereof, wherein the plant growth regulator composition is prepared from gibberellic acid GA3The composition comprises a suspending agent consisting of forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a thickening agent, a preservative, an antifreezing agent, a defoaming agent and water, wherein the suspending agent comprises the following components in percentage by weight: GA31 to 3 percent of forchlorfenuron, 1 to 2 percent of diethyl aminoethyl hexanoate, 1 to 3 percent of wetting agent, 2 to 5 percent of dispersing agent and 0.1 to 0 percent of thickening agent3%, preservative 0.1% -0.4%, anti-freezing agent 2% -6%, defoaming agent 0.1% -0.2%, and the balance of water. The proportion design of the weight percentage of each component of the regulator can obviously improve the fruit setting rate of the plant, and the fruit type and the fruit coloring of the plant are normal.
Description
Technical Field
The present invention belongs to a plant growth regulator composition and a preparation method thereof.
Background
Gibberellic acid is a broad-spectrum plant growth regulator composition, and GA containing gibberellic acid is widely applied to agricultural production3Gibberellic acid GA4And gibberellic acid GA7Is promoting GA in flowering and fruit setting3Greatest effect, secondly GA4However, GA is present in promoting apple fruit set and pentagonal ridges4And GA7Most preferably. Gibberellic acid can promote the growth and development of crops, so that the crops mature early, the yield is increased, and the quality is improved; can rapidly break the dormancy of organs such as seeds, tubers and bulbs and promote germination; reduce the falling of buds, flowers, bolls and fruits, improve the fruit bearing rate or form seedless fruits. Some 2-year-old plants can also flower in the same year.
Forchlorfenuron belongs to cytokinin growth regulators. Can promote cell division, differentiation and expansion, promote organ formation and protein synthesis, improve photosynthesis efficiency, enhance stress resistance, delay aging, improve fruit setting rate, and promote fruit enlargement. Is suitable for fruit trees and melon and fruit plants.
Whereas in the prior art, GA is due to gibberellic acid3The forchlorfenuron technical material is insoluble in water and soluble in organic solvents such as alcohols, so that the pesticide preparation for the traditional administration is generally processed into two dosage forms of emulsion or solution; volatile organic solvents are required to be uniformly added into both the missible oil and the soluble agent, and are toxic and harmful to human bodies and the environment, so that the pesticide has great harm to the human bodies and the environment.
Disclosure of Invention
The invention aims to provide a plant growth regulator composition to solve the problem that a volatile organic solvent is added into a plant growth medicament in the prior art to cause harm to human bodies and environment, and also aims to provide a preparation method of the plant growth regulator.
In order to achieve the above object, the plant growth regulator composition of the present invention adopts the following technical scheme:
a plant growth regulator composition is prepared from gibberellic acid GA3The composition comprises a suspending agent consisting of forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a thickening agent, a preservative, an antifreezing agent, a defoaming agent and water, wherein the suspending agent comprises the following components in percentage by weight: GA31 to 3 percent of forchlorfenuron, 1 to 3 percent of diethyl aminoethyl hexanoate, 1 to 2 percent of wetting agent, 2 to 5 percent of dispersing agent, 0.1 to 0.3 percent of thickening agent, 0.1 to 0.4 percent of preservative, 2 to 6 percent of antifreezing agent, 0.1 to 0.2 percent of defoaming agent and the balance of water;
wherein the wetting agent is at least one selected from alkyl benzene sulfonate, succinate sulfonic acid sodium salt, diisooctyl succinic acid sodium salt, fatty amide sulfonic acid sodium salt, fatty amide N-methyl taurinic acid sodium salt, fatty alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether and lauryl sodium sulfate;
the dispersing agent is at least one selected from lignosulfonate, alkyl naphthalene sulfonate formaldehyde condensate, phosphate of alkylphenol polyoxyethylene, sulfate of alkylaryl phenol polyoxyethylene, phosphate of alkylaryl phenol polyoxyethylene, formaldehyde condensate of alkylphenol polyoxyethylene sulfate, alkylphenol polyoxyethylene, fatty alcohol polyoxyethylene and polyalkyl aryl phenol polyoxyethylene;
the thickener is at least one of xanthan gum, carboxymethyl cellulose polyvinyl alcohol, polyvinyl pyrrolidone, magnesium aluminum silicate and bentonite;
the antiseptic is at least one selected from benzoic acid, acetaldehyde, propionic acid, polyformaldehyde, sodium citrate, sodium salicylate, and sorbitol;
the antifreeze is at least one selected from ethylene glycol, propylene glycol, glycerol, diethylene glycol, triethylene glycol and polyethylene glycol;
the defoaming agent is at least one of organosilicon, aliphatic carboxylic acid, mineral oil, EO-PO polyether and modified polyether polysiloxane.
Further, the weight percentage of each component is as follows: GA32 percent of forchlorfenuron, 2 percent of diethyl aminoethyl hexanoate, 1.5 percent of wetting agent, 3.5 percent of dispersing agent, 0.2 percent of thickening agent, 0.25 percent of preservative, 4 percent of antifreezing agent and 0.15 percent of defoaming agent.
The preparation method of the plant growth regulator composition adopts the following technical scheme:
a method of preparing a plant growth regulator composition comprising the steps of:
(1) firstly, preparing a thickening agent into mother liquor 1 day ahead;
(2) mixing gibberellic acid GA3Weighing raw materials such as forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a preservative, an antifreezing agent, a defoaming agent and the like, mixing the raw materials with a thickening agent, adding zirconium beads, and grinding by adopting a grinder;
(3) and filtering residues after grinding is finished, and packaging.
Further, in the step (2), the speed of the grinder is adjusted to 2000 revolutions, and the grinding is carried out for 2 hours.
The invention has the following beneficial effects: compared with the prior art, the plant growth regulator composition provided by the invention mainly adopts gibberellic acid GA3, forchlorfenuron and diethyl aminoethyl hexanoate as raw materials to be mixed and prepared into a suspending agent dosage form, and the regulator has the advantages that firstly, because water is adopted as a dispersion medium, the problems of flammability and phytotoxicity caused by an organic solvent are avoided; secondly, no dust hazard exists, and the method is safe for applicators and the environment; thirdly, the suspending agent has good dispersibility and spreadability, high suspension rate, strong ability of adhering to the surface of a crop object, rain wash resistance and lasting drug effect; the suspending agent has the advantages of small particles, large surface activity, strong permeability, no dust during dispensing, low cost, high drug effect, emulsifiable concentrate and soluble solvent, can be wetted by water, and has good suspension property after being diluted by water. Furthermore, the proportion of each component of the regulator is designed according to the weight percentage, so that the fruit setting rate of the plant can be obviously improved, and the fruit type and the fruit coloring of each plant are normal.
Detailed Description
In order to make the technical purpose, technical solutions and advantageous effects of the present invention more clear, the technical solutions of the present invention are further described below with reference to specific embodiments.
Specific examples of plant growth regulator compositions to which the present invention relates: example 1: in this example, the plant growth regulator composition was prepared as a suspension concentrate from the following raw materials in weight percent: gibberellic acid GA31 percent of forchlorfenuron, 1 percent of diethyl aminoethyl hexanoate, 1 percent of wetting agent, 2 percent of dispersing agent, 0.1 percent of thickening agent, 0.1 percent of preservative, 2 percent of antifreezing agent, 0.1 percent of defoaming agent and the balance of water.
Example 2: in this example, the plant growth regulator composition was prepared as a suspension concentrate from the following raw materials in weight percent: gibberellic acid GA 32%, forchlorfenuron 2%, diethyl aminoethyl hexanoate 1.5%, wetting agent 2%, dispersing agent 3.5%, thickening agent 0.2%, preservative 0.25%, antifreezing agent 4%, defoaming agent 0.15%, and the balance of water.
Example 3: in this example, the plant growth regulator composition was prepared as a suspension concentrate from the following raw materials in weight percent: gibberellic acid GA33 percent of forchlorfenuron, 3 percent of diethyl aminoethyl hexanoate, 3 percent of wetting agent, 5 percent of dispersing agent, 0.3 percent of thickening agent, 0.4 percent of preservative, 6 percent of antifreezing agent, 0.2 percent of defoaming agent and the balance of water.
The various embodiments described above use water as the dispersing medium to form the suspending agent.
The fruit setting rate of fruit plants is one of important characteristics, and the fruit setting test of kiwi fruits is carried out by taking kiwi fruit trees as test crops: the test protocol was as follows:
as described in the following table, treatment protocols 1, 2, and 3 were each prepared by diluting 1625-fold the pharmaceutical agents prepared in examples 1-3 above; treatment protocols 4, 5, and 6 were 1875-fold dilutions of the agents prepared in examples 1-3 above, respectively; the treatment scheme 7 is to dilute 4 percent gibberellic acid missible oil by 1600 times; treatment protocol 8 was 100-fold dilution of 0.1% forchlorfenuron soluble solvent; treatment protocol 9 was a direct comparison with treatment with clear water.
TABLE 1 design of test Agents
| Treatment of | Medicament | Dilution factor |
| 1 | The agent prepared in example 1 of the present invention | 1625 |
| 2 | The agent prepared in example 2 of the present invention | 1625 |
| 3 | The agent prepared in example 3 of the present invention | 1625 |
| 4 | The agent prepared in example 1 of the present invention | 1875 |
| 5 | The agent prepared in example 2 of the present invention | 1875 |
| 6 | The agent prepared in example 3 of the present invention | 1875 |
| 7 | 4% gibberellic acid emulsifiable concentrate | 1600 |
| 8 | 0.1% forchlorfenuron solubles | 100 |
| 9 | Clear water control |
The investigation method comprises the following steps:
according to a five-point sampling method, one kiwi fruit tree is taken from each point, the number of results is investigated, and the fruit setting rate is calculated; after ripening, the individual fruits were picked and weighed.
Increasing the fruit set rate (%) (treatment zone results-control zone results)/control zone results) by 100;
yield increase (%) - (fresh weight of fruit in treatment zone-fresh weight of fruit in control zone)/fresh weight of fruit in control zone) × 100.
The calculation of the above samples shows the effect of the plant growth regulator composition on fruit set and yield of kiwi fruits as shown in the following table:
TABLE 2 fruit set and yield impact of Kiwi
As shown in Table 2, the plant growth regulator composition of the invention can be sprayed on kiwi fruit trees to clearly improve the fruit setting rate of kiwi fruits, and the fruit type and fruit coloring are normal without abnormal physiological changes after each application treatment.
The fruit setting of the kiwi fruits is increased after the pesticide is applied, and the gibberellic acid GA is adopted in the invention3Forchlorfenuron and aminesThe plant growth regulator composition of the fresh ester is diluted 1625 times and sprayed: the fruit setting rate increases of 3.35%, 7.26% and 6.15% in example 1, example 2 and example 3, respectively, compared with the blank, and the fruit setting rate increases of 2.79% and 2.23% in 4% gibberellic acid emulsifiable solution and 0.1% forchlorfenuron soluble solution, respectively, compared with the blank; the medicament of the invention is diluted 1875 times and sprayed: the fruit set increases of 3.91%, 8.38% and 6.70% for example 1, example 2 and example 3, respectively, compared with the blank control.
The weight of single fruit of the kiwi fruit is increased after the medicine is applied, and the gibberellic acid GA is added in the invention3Diluting 1625 times of plant growth regulator composition of forchlorfenuron and diethyl aminoethyl hexanoate, and spraying: the fruit setting rate increases of example 1, example 2 and example 3 are 7.14%, 13.10% and 10.71% respectively compared with the blank control, and the fruit setting rate increases of 4.76% and 3.57% respectively compared with the 4% gibberellic acid emulsifiable solution and the 0.1% forchlorfenuron soluble solution; the medicament of the invention is diluted 1875 times and sprayed: the fruit set increases of 9.52%, 16.67% and 13.10% for example 1, example 2 and example 3, respectively, compared with the blank control.
After the application, the fruit setting yield of the kiwi fruits is increased, and the plant growth regulator composition of gibberellic acid GA3, forchlorfenuron and diethyl aminoethyl hexanoate is diluted 1625 times and sprayed: the yield increase of the example 1, the example 2 and the example 3 is respectively 6.15%, 13.08% and 11.31% compared with the blank, and the yield increase of the 4% gibberellic acid missible oil and the 0.1% forchlorfenuron soluble solution is 4.77% and 3.60% compared with the blank; the medicament of the invention is diluted 1875 times and sprayed: the fruit set increases of 9.48%, 16.68% and 11.84% for example 1, example 2 and example 3, respectively, compared with the blank control.
In conclusion, the fruit setting rate, yield increase rate and single fruit increasing rate of the plants are obviously increased by adopting the plant growth regulator composition, and the increasing effect of the plant growth regulator composition in the example 5 is more obvious.
In addition, the thickener in each of the above embodiments is preferably xanthan gum; the wetting agent is preferably sodium dodecyl sulfate; the dispersant is preferably sodium lignosulfonate; the antiseptic is preferably benzoic acid; the antifreezing agent is preferably glycol; the defoaming agent is preferably silicone.
Of course, in other embodiments, the thickening agent may also be at least one selected from the group consisting of carboxymethyl cellulose polyvinyl alcohol, polyvinyl pyrrolidone, magnesium aluminum silicate, and bentonite;
the dispersant can also be at least one selected from alkyl naphthalene sulfonate, alkyl naphthalene sulfonate formaldehyde condensate, phosphate of alkylphenol polyoxyethylene, sulfate of alkylaryl phenol polyoxyethylene, phosphate of alkylaryl phenol polyoxyethylene, formaldehyde condensate of alkylphenol polyoxyethylene sulfate, alkylphenol polyoxyethylene, fatty alcohol polyoxyethylene and polyalkyl aryl phenol polyoxyethylene;
the thickener can also be at least one selected from carboxymethyl cellulose polyvinyl alcohol, polyvinyl pyrrolidone, magnesium aluminum silicate, and bentonite;
the antiseptic can also be at least one selected from acetaldehyde, propionic acid, polyformaldehyde, sodium citrate, sodium salicylate, and sorbitol;
the antifreeze can also be at least one selected from propylene glycol, glycerol, diethylene glycol, triethylene glycol and polyethylene glycol; the defoaming agent may be at least one selected from the group consisting of aliphatic carboxylic acids, mineral oil, EO-PO polyether, and modified polyether polysiloxane.
Examples of the method for preparing the plant growth regulator composition according to the present invention:
mainly relates to the following steps: (1) the thickener was formulated as a mother liquor 1 day ahead.
(2) Weighing gibberellic acid GA3, forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a preservative, an antifreezing agent, a defoaming agent and the like, putting the raw materials into a tank, and adding a proper amount of zirconium beads.
(3) The mill was started and adjusted to 2000 revolutions for 2 hours.
(4) And after grinding is finished, filtering and packaging.
It should be noted that in other embodiments, the rotation speed and the grinding time of the grinding machine may be adaptively modified according to the actual powder grinding effect.
Finally, it should be noted that: the above embodiments are merely illustrative and not restrictive of the technical solutions of the present invention, and any equivalent substitutions and modifications or partial substitutions made without departing from the spirit and scope of the present invention should be included in the scope of the claims of the present invention.
Claims (4)
1. A plant growth regulator composition is characterized by comprising gibberellic acid GA3The composition comprises a suspending agent consisting of forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a thickening agent, a preservative, an antifreezing agent, a defoaming agent and water, wherein the suspending agent comprises the following components in percentage by weight: GA31 to 3 percent of forchlorfenuron, 1 to 3 percent of diethyl aminoethyl hexanoate, 1 to 2 percent of wetting agent, 2 to 5 percent of dispersing agent, 0.1 to 0.3 percent of thickening agent, 0.1 to 0.4 percent of preservative, 2 to 6 percent of antifreezing agent, 0.1 to 0.2 percent of defoaming agent and the balance of water;
wherein the wetting agent is at least one selected from alkyl benzene sulfonate, succinate sulfonic acid sodium salt, diisooctyl succinic acid sodium salt, fatty amide sulfonic acid sodium salt, fatty amide N-methyl taurinic acid sodium salt, fatty alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether and lauryl sodium sulfate;
the dispersing agent is at least one selected from lignosulfonate, alkyl naphthalene sulfonate formaldehyde condensate, phosphate of alkylphenol polyoxyethylene, sulfate of alkylaryl phenol polyoxyethylene, phosphate of alkylaryl phenol polyoxyethylene, formaldehyde condensate of alkylphenol polyoxyethylene sulfate, alkylphenol polyoxyethylene, fatty alcohol polyoxyethylene and polyalkyl aryl phenol polyoxyethylene;
the thickener is at least one of xanthan gum, carboxymethyl cellulose polyvinyl alcohol, polyvinyl pyrrolidone, magnesium aluminum silicate and bentonite;
the antiseptic is at least one selected from benzoic acid, acetaldehyde, propionic acid, polyformaldehyde, sodium citrate, sodium salicylate, and sorbitol;
the antifreeze is at least one selected from ethylene glycol, propylene glycol, glycerol, diethylene glycol, triethylene glycol and polyethylene glycol;
the defoaming agent is at least one of organosilicon, aliphatic carboxylic acid, mineral oil, EO-PO polyether and modified polyether polysiloxane.
2. The plant growth regulator composition according to claim 1, wherein the weight percentage of each component is: GA32 percent of forchlorfenuron, 2 percent of diethyl aminoethyl hexanoate, 1.5 percent of wetting agent, 3.5 percent of dispersing agent, 0.2 percent of thickening agent, 0.25 percent of preservative, 4 percent of antifreezing agent and 0.15 percent of defoaming agent.
3. A method of making a plant growth regulator composition according to claim 1, comprising the steps of: (1) firstly, preparing a thickening agent into mother liquor 1 day ahead; (2) mixing gibberellic acid GA3Weighing raw materials such as forchlorfenuron, diethyl aminoethyl hexanoate, a wetting agent, a dispersing agent, a preservative, an antifreezing agent, a defoaming agent and the like, mixing the raw materials with a thickening agent, adding zirconium beads, and grinding by adopting a grinder; (3) and filtering residues after grinding is finished, and packaging.
4. The method according to claim 3, wherein in the step (2), the speed of the mill is adjusted to 2000 revolutions for 2 hours.
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