CN110668698A - Titanium white overglaze for acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel and production method thereof - Google Patents
Titanium white overglaze for acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel and production method thereof Download PDFInfo
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- CN110668698A CN110668698A CN201910884648.2A CN201910884648A CN110668698A CN 110668698 A CN110668698 A CN 110668698A CN 201910884648 A CN201910884648 A CN 201910884648A CN 110668698 A CN110668698 A CN 110668698A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
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Abstract
The invention relates to the technical field of chemical industry, and discloses an acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium white overglaze for a gold burning barrel, which is prepared from the following raw materials in parts by weight: 60-70 parts of albite powder, 30-45 parts of zinc oxide, 7-12 parts of barite, 8-15 parts of zircon sand, 15-20 parts of quartz, 3-7 parts of calcite and 8-12 parts of low-temperature frit; the albite powder comprises the following specific components: the method is characterized in that the method adopts the albite powder with the granularity of 200 meshes as a raw material, a small amount of chloride powder is added into the albite powder, the mixture is subjected to ball milling for 2 to 5 hours, and the powder subjected to ball milling is calcined for 0.5 to 2 hours at the temperature of 800-900 ℃. The titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold firing barrel and the production method solve the problems that the gold firing barrel prepared by the porcelain glaze formula for forming overglaze on the ground glaze layer at present has poor performances of glossiness, acid resistance, alkali resistance, wear resistance and the like, and the quality and the service life of the product are seriously influenced.
Description
Technical Field
The invention relates to the technical field of chemical industry, in particular to an acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for a gold burning barrel and a production method thereof.
Background
The enamel for the gold burning barrel is a glassy silicate or borosilicate coating coated on a metal blank. The porcelain glaze comprises a matrix agent, a cosolvent, an opacifier, an adhesive, an oxidant, an adjuvant, a coloring agent and the like, and has different functions. The matrix agents are predominant, most of them being silicates, boron oxides, aluminum oxides and alkali metal oxides. The preparation method of the porcelain glaze comprises the steps of fully and uniformly mixing all the components (dry mixing, or adding 5-15% of water and preparing into small balls), melting in a tank furnace, a crucible furnace or a rotary furnace to a certain uniform degree, carrying out water quenching, air cooling or hot pressing to form sheets, and then grinding (using a ball mill or an airflow pulverizer) to form dry glaze powder or adding water to prepare glaze slurry.
The existing gold burning barrel made of the porcelain glaze formula for forming the overglaze on the ground glaze layer has poor performances of glossiness, acid resistance, alkali resistance, wear resistance and the like, and the quality and the service life of products are seriously influenced.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold firing barrel and the production method thereof, which have the advantages of improving the product quality and prolonging the service life, and solve the problems that the gold firing barrel prepared by the enamel formula for forming the overglaze on the ground glaze layer at present has poor performances of glossiness, acid resistance, alkali resistance, wear resistance and the like, and the product quality and the service life are seriously influenced.
(II) technical scheme
In order to achieve the purposes of improving the product quality and prolonging the service life, the invention provides the following technical scheme: the titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel is prepared from the following raw materials in parts by weight: 60-70 parts of albite powder, 30-45 parts of zinc oxide, 7-12 parts of barite, 8-15 parts of zircon sand, 15-20 parts of quartz, 3-7 parts of calcite and 8-12 parts of low-temperature frit;
the albite powder comprises the following specific components: taking the albite powder with the granularity of 200 meshes as a raw material, adding a small amount of chloride powder into the albite powder, mixing and ball-milling the mixture for 2 to 5 hours, calcining the ball-milled powder for 0.5 to 2 hours at the temperature of 800-900 ℃, pouring the calcined product into a pulping tank, adding water into the pulping tank to prepare ore pulp with the concentration of 25 to 40 percent, adding a dispersing agent with the mass of 0.05 to 0.1 percent of the ore pulp into the ore pulp, uniformly stirring the mixture by using a stirrer, heating the mixture to 60 ℃, adding oxalic acid into the mixture, pickling the mixture for 1.5 to 2.5 hours, filtering the ore pulp, feeding the filtered ore pulp into a calcining furnace to calcine for 2 hours, and naturally cooling the mixture to obtain a product;
preferably, the low-temperature frit comprises talc, silica, titanium dioxide and Longyan rock.
Preferably, the ratio of the oxalic acid to the ore pulp is 1:20 in parts by weight, and the mass fraction of the oxalic acid aqueous solution is 2-5%.
Preferably, the talcum powder consists of calcium carbonate and bentonite, raw materials of calcium carbonate ore and bentonite ore are simultaneously fed into a crusher to be crushed, and the crushed raw materials are fed into a ball mill to be ground into 200 meshes.
The production method of the acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for the gold burning barrel is characterized by comprising the following steps:
s1: mixing the albite powder, zinc oxide, barite, zircon sand, quartz, calcite and low-temperature frit sufficiently, and pouring into a smelting furnace;
s2: after the smelting furnace heats and melts the internal mixed material, the smelting furnace rapidly cools the mixed material to rapidly cool the mixed material into sheet borosilicate glass, so as to obtain a titanium surface glaze block;
s3: the titanium overglaze block is evenly mixed with the halloysite permanent porcelain, cadmium red, cadmium yellow, water and high alumina balls, and ball milling is carried out for 0.5h by a ball mill to obtain overglaze.
Preferably, in the step S2, the melting furnace mixes the internal mixed materials while stirring the internal mixed materials when the internal mixed materials are heated and melted, the temperature of the melting furnace is raised to 1000 ℃, and the internal mixed materials are rapidly cooled by a water cooling method when the temperature of the melting furnace is reduced.
Preferably, in the step S3, the ratio of the titanium-surface glaze blocks to the halloysite, cadmium red, cadmium yellow, water and high alumina balls is 100:5:2:0.2:55: 135.
(III) advantageous effects
Compared with the prior art, the invention provides the titanium dioxide overglaze for the gold burning barrel with acid resistance, alkali resistance, heat resistance and wear resistance and the production method, and the titanium dioxide overglaze has the following beneficial effects:
the acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for the gold burning barrel and the production method utilize sodium feldspar powder, zinc oxide, barite, zircon sand, quartz and calcite, and the fired overglaze has high glossiness and brightness and good acid-resistant, alkali-resistant, heat-resistant and wear-resistant properties.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel is prepared from the following raw materials in parts by weight: 60 parts of albite powder, 30 parts of zinc oxide, 7 parts of barite, 8 parts of zircon sand, 15 parts of quartz, 3 parts of calcite and 8 parts of low-temperature frit;
the albite powder comprises the following specific components: taking the albite powder with the granularity of 200 meshes as a raw material, adding a small amount of chloride powder into the albite powder, mixing and ball-milling the mixture for 2 hours, calcining the powder subjected to ball-milling for 0.5 hour at 800 ℃, pouring the calcined product into a pulping tank, adding water into the pulping tank to prepare pulp with the concentration of 25%, adding a dispersing agent with the mass of 0.05% of the pulp into the pulp, uniformly stirring the pulp by using a stirrer, heating the pulp to 60 ℃, adding oxalic acid into the pulp, pickling the pulp for 1.5 hours, filtering the pulp, feeding the filtered pulp into a calcining furnace to calcine for 2 hours, and naturally cooling the pulp to obtain a product;
the low-temperature frit comprises talcum powder, silicon dioxide, titanium dioxide and Longyan soil.
The ratio of the oxalic acid to the ore pulp is 1:20 by weight, and the mass fraction of the oxalic acid aqueous solution is 2%.
The talcum powder is composed of calcium carbonate and bentonite, and is prepared by feeding calcium carbonate ore and bentonite ore into a crusher for crushing, and then feeding into a ball mill for grinding to 200 meshes.
The production method of the acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for the gold burning barrel is characterized by comprising the following steps:
s1: mixing the albite powder, zinc oxide, barite, zircon sand, quartz, calcite and low-temperature frit sufficiently, and pouring into a smelting furnace;
s2: after the smelting furnace heats and melts the internal mixed material, the smelting furnace rapidly cools the mixed material to rapidly cool the mixed material into sheet borosilicate glass, so as to obtain a titanium surface glaze block;
s3: the titanium overglaze block is evenly mixed with the halloysite permanent porcelain, cadmium red, cadmium yellow, water and high alumina balls, and ball milling is carried out for 0.5h by a ball mill to obtain overglaze.
And step S2, when the smelting furnace heats and melts the internal mixed materials, the mixed materials are stirred and mixed at the same time, the temperature of the smelting furnace is raised to 1000 ℃, and when the temperature in the smelting furnace is reduced, the water cooling mode is adopted to rapidly reduce the temperature.
In the step of S3, the ratio of the titanium surface glaze blocks to the halloysite permanent porcelain clay, the cadmium red, the cadmium yellow, the water and the high alumina stone ball is 100:5:2:0.2:55: 13.
Example 2
The titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel is prepared from the following raw materials in parts by weight: 65 parts of albite powder, 38 parts of zinc oxide, 10 parts of barite, 12 parts of zircon sand, 117 parts of quartz, 5 parts of calcite and 10 parts of low-temperature frit;
the albite powder comprises the following specific components: taking the albite powder with the granularity of 200 meshes as a raw material, adding a small amount of chloride powder into the albite powder, mixing and ball-milling the mixture for 3.5 hours, calcining the powder subjected to ball-milling at 850 ℃ for 1.25 hours, pouring a calcined product into a pulping tank, adding water into the pulping tank to prepare pulp with the concentration of 35%, adding a dispersing agent with the mass of 0.08% of that of the pulp into the pulp, uniformly stirring the pulp by using a stirrer, heating the pulp to 60 ℃, adding oxalic acid into the pulp, pickling the pulp for 2 hours, filtering the pulp, calcining the filtered pulp in a calcining furnace for 2 hours, and naturally cooling the pulp to obtain a product;
the low-temperature frit comprises talcum powder, silicon dioxide, titanium dioxide and Longyan soil.
The ratio of the oxalic acid to the ore pulp is 1:20 by weight, and the mass fraction of the oxalic acid aqueous solution is 4%.
The talcum powder is composed of calcium carbonate and bentonite, and is prepared by feeding calcium carbonate ore and bentonite ore into a crusher for crushing, and then feeding into a ball mill for grinding to 200 meshes.
The processing technology of the titanium dioxide overglaze for the gold burning barrel with acid resistance, alkali resistance, heat resistance and wear resistance is characterized by comprising the following steps:
s1: mixing the albite powder, zinc oxide, barite, zircon sand, quartz, calcite and low-temperature frit sufficiently, and pouring into a smelting furnace;
s2: after the smelting furnace heats and melts the internal mixed material, the smelting furnace rapidly cools the mixed material to rapidly cool the mixed material into sheet borosilicate glass, so as to obtain a titanium surface glaze block;
s3: the titanium overglaze block is evenly mixed with the halloysite permanent porcelain, cadmium red, cadmium yellow, water and high alumina balls, and ball milling is carried out for 0.5h by a ball mill to obtain overglaze.
And step S2, when the smelting furnace heats and melts the internal mixed materials, the mixed materials are stirred and mixed at the same time, the temperature of the smelting furnace is raised to 1000 ℃, and when the temperature in the smelting furnace is reduced, the water cooling mode is adopted to rapidly reduce the temperature.
In the step of S3, the ratio of the titanium surface glaze blocks to the halloysite permanent porcelain clay, the cadmium red, the cadmium yellow, the water and the high alumina stone ball is 100:5:2:0.2:55: 13.
Example 3
The titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel is prepared from the following raw materials in parts by weight: 70 parts of albite powder, 45 parts of zinc oxide, 12 parts of barite, 15 parts of zircon sand, 20 parts of quartz, 7 parts of calcite and 12 parts of low-temperature frit;
the albite powder comprises the following specific components: taking the albite powder with the granularity of 200 meshes as a raw material, adding a small amount of chloride powder into the albite powder, mixing and ball-milling the mixture for 5 hours, calcining the ball-milled powder for 2 hours at 900 ℃, pouring a calcined product into a pulping tank, adding water into the pulping tank to prepare ore pulp with the concentration of 40%, adding a dispersing agent with the mass of 0.1% of that of the ore pulp into the ore pulp, uniformly stirring the mixture by using a stirrer, heating the mixture to 60 ℃, adding oxalic acid into the mixture, pickling the mixture for 2.5 hours, filtering the ore pulp, feeding the filtered ore pulp into a calcining furnace to calcine for 2 hours, and naturally cooling the ore pulp to obtain a product;
the low-temperature frit comprises talcum powder, silicon dioxide, titanium dioxide and Longyan soil.
The ratio of the oxalic acid to the ore pulp is 1:20 by weight, and the mass fraction of the oxalic acid aqueous solution is 5%.
The talcum powder is composed of calcium carbonate and bentonite, and is prepared by feeding calcium carbonate ore and bentonite ore into a crusher for crushing, and then feeding into a ball mill for grinding to 200 meshes.
The processing technology of the titanium dioxide overglaze for the gold burning barrel with acid resistance, alkali resistance, heat resistance and wear resistance is characterized by comprising the following steps:
s1: mixing the albite powder, zinc oxide, barite, zircon sand, quartz, calcite and low-temperature frit sufficiently, and pouring into a smelting furnace;
s2: after the smelting furnace heats and melts the internal mixed material, the smelting furnace rapidly cools the mixed material to rapidly cool the mixed material into sheet borosilicate glass, so as to obtain a titanium surface glaze block;
s3: the titanium overglaze block is evenly mixed with the halloysite permanent porcelain, cadmium red, cadmium yellow, water and high alumina balls, and ball milling is carried out for 0.5h by a ball mill to obtain overglaze.
And step S2, when the smelting furnace heats and melts the internal mixed materials, the mixed materials are stirred and mixed at the same time, the temperature of the smelting furnace is raised to 1000 ℃, and when the temperature in the smelting furnace is reduced, the water cooling mode is adopted to rapidly reduce the temperature.
In the step of S3, the ratio of the titanium surface glaze blocks to the halloysite permanent porcelain clay, the cadmium red, the cadmium yellow, the water and the high alumina stone ball is 100:5:2:0.2:55: 13.
The soybean dietary fiber potato chips obtained in examples 1 to 3 were examined, and the results were as follows:
| example number | Degree of gloss | Acid resistance | Alkali resistance | Heat resistance | Wear-resistant |
| 1 | +++ | ++ | + | ++ | +++ |
| 2 | +++ | +++ | ++ | + | ++ |
| 3 | ++++ | +++ | +++ | ++ | ++++ |
Note: the more "+" indicates the potato chip effect, the better the effect
Thus, example 3 showed the best gloss and had good acid, alkali, heat and abrasion resistance.
In conclusion, the acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for the gold burning barrel and the production method utilize the sodium feldspar powder, the zinc oxide, the barite, the zircon sand, the quartz and the calcite, and the fired overglaze has high glossiness and brightness and good acid-resistant, alkali-resistant, heat-resistant and wear-resistant properties.
It is to be noted that the term "comprises," "comprising," or any other variation thereof is intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The titanium dioxide overglaze for the acid-resistant, alkali-resistant, heat-resistant and wear-resistant gold burning barrel is characterized by being prepared from the following raw materials in parts by weight: 60-70 parts of albite powder, 30-45 parts of zinc oxide, 7-12 parts of barite, 8-15 parts of zircon sand, 15-20 parts of quartz, 3-7 parts of calcite and 8-12 parts of low-temperature frit;
the albite powder comprises the following specific components: the method comprises the steps of taking the albite powder with the granularity of 200 meshes as a raw material, adding a small amount of chloride powder into the albite powder, mixing and ball-milling the mixture for 2-5 hours, calcining the powder after ball-milling for 0.5-2 hours at the temperature of 800-900 ℃, pouring the calcined product into a pulping tank, adding water to prepare ore pulp with the concentration of 25-40%, adding a dispersing agent with the mass of 0.05-0.1% of the ore pulp into the ore pulp, uniformly stirring the mixture by using a stirrer, heating the mixture to 60 ℃, adding oxalic acid, pickling for 1.5-2.5 hours, filtering the ore pulp, feeding the filtered ore pulp into a calcining furnace, calcining for 2 hours, and naturally cooling to obtain the product.
2. The titanium dioxide overglaze for the gold burning barrel, which is acid-resistant, alkali-resistant, heat-resistant and wear-resistant according to claim 1, is characterized in that: the low-temperature frit comprises talcum powder, silicon dioxide, titanium dioxide and Longyan soil.
3. The titanium dioxide overglaze for the gold burning barrel, which is acid-resistant, alkali-resistant, heat-resistant and wear-resistant according to claim 1, is characterized in that: the ratio of the oxalic acid to the ore pulp is 1:20 in parts by weight, and the mass fraction of the oxalic acid aqueous solution is 2-5%.
4. The titanium dioxide overglaze for the gold burning barrel, which is acid-resistant, alkali-resistant, heat-resistant and wear-resistant according to claim 2, is characterized in that: the talcum powder is composed of calcium carbonate and bentonite, raw materials of calcium carbonate ore and bentonite ore are simultaneously sent into a crusher to be crushed, and the crushed raw materials are sent into a ball mill to be ground into 200 meshes.
5. The production method of the acid-resistant, alkali-resistant, heat-resistant and wear-resistant titanium dioxide overglaze for the gold burning barrel is characterized by comprising the following steps:
s1: mixing the albite powder, zinc oxide, barite, zircon sand, quartz, calcite and low-temperature frit sufficiently, and pouring into a smelting furnace;
s2: after the smelting furnace heats and melts the internal mixed material, the smelting furnace rapidly cools the mixed material to rapidly cool the mixed material into sheet borosilicate glass, so as to obtain a titanium surface glaze block;
s3: the titanium overglaze block is evenly mixed with the halloysite permanent porcelain, cadmium red, cadmium yellow, water and high alumina balls, and ball milling is carried out for 0.5h by a ball mill to obtain overglaze.
6. The method for producing the titanium dioxide overglaze for the gold firing barrel, which is resistant to acid, alkali, heat and abrasion, according to claim 5, is characterized in that: and in the step S2, when the smelting furnace heats and melts the internal mixed materials, the mixed materials are stirred and mixed at the same time, the temperature of the smelting furnace is raised to 1000 ℃, and when the temperature in the smelting furnace is reduced, the water cooling mode is adopted to rapidly reduce the temperature.
7. The method for producing the titanium dioxide overglaze for the gold firing barrel, which is resistant to acid, alkali, heat and abrasion, according to claim 5, is characterized in that: in the step of S3, the ratio of the titanium surface glaze blocks to the halloysite permanent porcelain clay, the cadmium red, the cadmium yellow, the water and the high alumina stone balls is 100:5:2:0.2:55: 135.
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