CN110637956A - Material treatment method and application thereof - Google Patents

Material treatment method and application thereof Download PDF

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Publication number
CN110637956A
CN110637956A CN201910892541.2A CN201910892541A CN110637956A CN 110637956 A CN110637956 A CN 110637956A CN 201910892541 A CN201910892541 A CN 201910892541A CN 110637956 A CN110637956 A CN 110637956A
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fruit
seed
root
rhizome
processing method
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刘立祥
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Shenzhen Huayuan Quantum Biology Co Ltd
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Shenzhen Huayuan Quantum Biology Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/38Other non-alcoholic beverages
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/04Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Botany (AREA)
  • Mycology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention provides a material processing method, which comprises the following steps: crushing and pretreating the material to the particle size of 150-200 μm; dispersing the pretreated material powder in a solvent to form a dispersion system; and processing the dispersion system by ultrahigh pressure nano equipment until the particle size is 1nm-100 nm. Compared with the prior art, the material processing method has wide applicability to materials, high efficiency, safety and low processing cost; in addition, the prepared nano material has uniform particle size, uniform dispersion system and good performance stability; finally, the equipment can be controlled by adjusting the temperature and the pressure, the original components and properties of the material are kept to the maximum extent when the material is processed, and the processed product can generate a plurality of unexpected properties due to the large change of the particle size.

Description

Material treatment method and application thereof
Technical Field
The invention belongs to the field of material processing, and particularly relates to a material processing method and application thereof.
Background
The particle size processing of the material is a very common processing means, and the application range is very wide. There are many materials that are very large in size for cost savings at the beginning of their production, or some materials themselves are very large in size. After being processed into a material with a small particle size, the material can adapt to a plurality of application scenes on one hand, and on the other hand, the material can have a plurality of properties which are not available in a macro scale when being processed to a nano scale. The current processing method generally adopts a mechanical processing method, and the mechanical processing method cannot reach the desired target grain diameter and cannot meet the requirement on uniformity.
Therefore, it is necessary to find a new processing method to meet the current material processing requirements.
Disclosure of Invention
The invention aims to solve the technical problems of high price and low efficiency of the existing material treatment method.
In order to solve the above problems, an aspect of the present invention provides a material processing method, including the steps of:
crushing and pretreating the material to the particle size of 150-200 μm;
dispersing the pretreated material powder in a solvent to form a dispersion system;
treating the dispersion system by ultrahigh pressure nano equipment until the particle size is 1nm-100 nm;
preferably, the material processing method further comprises filtering the powder after passing through the ultrahigh pressure nanocrystallization device.
Preferably, the processing mode of the ultrahigh pressure nanocrystallization device comprises at least one of high pressure processing and mixing processing.
Preferably, the working pressure range of the ultrahigh pressure nanometer equipment is 100MPa-250 MPa.
Preferably, the processing temperature of the ultrahigh pressure nanocrystallization device is greater than or equal to-6 ℃.
Preferably, the processing speed of the ultrahigh pressure nano-processing equipment is 30L/h.
Preferably, the material comprises any one or more of a plant material, a metal material, a heat conduction material, a stone material, a chemical material, a semiconductor material and a two-dimensional material.
In another aspect, the invention provides a plant beverage with dendrobium as a main raw material, wherein plant materials are treated by the material treatment method.
Preferably, the plant beverage further comprises sword bean, common fennel fruit, Chinese yam, hawthorn fruit, purslane, garter snake, dark plum fruit, papaya, fructus cannabis, seville orange flower, fragrant solomonseal rhizome, liquorice root, angelica root, ginkgo seed, white hyacinth bean, dried longan pulp, cassia seed, lily bulb, nutmeg, cinnamon, emblic leafflower fruit, finger citron, almond, sea buckthorn, oyster, gordon euryale seed, red bean, donkey-hide gelatin, chicken's gizzard-membrane, malt, kelp, jujube, momordica grosvenori, bunge cherry seed, honeysuckle, Chinese olive, houttuynia, ginger, hovenia dulcis thunb, medlar, gardenia, amomum fruit, scaphium scaphigerum, tuckahoe, citron, elsholtzia, peach kernel, mulberry leaf, mulberry fruit, tangerine, platycodon root, sharpleaf galangal fruit, lotus leaf, radish seed, lotus seed, galangal, lophatherum gracile, fermented soybean, chrysanthemum, chicory, mustard seed, sealwort, perilla fruit, perilla seed, kudzu vine root, black sesame, black pepper, spina date seed, fresh lalang grass rhizome, fresh reed rhizome, pallas pit viper, orange peel, mint, coix seed, allium macrostemon, raspberry, wrinkled gianthyssop, ginseng leaf, ginseng fruit, pseudo-ginseng, glabrous greenbrier rhizome, Japanese thistle herb, glossy privet fruit, dogwood fruit, medicinal cyathula root, unibract fritillary bulb, szechuan lovage rhizome, red deer fetus, hairy antler, red deer bone, red sage root, slenderstyle acanthopanax bark, Chinese magnoliavine fruit, largetrifolious bugbane rhizome, cochinchnese asparagus root, tall gastrodia tuber, heterophylly falsestarwort root, medicinal indian mulberry root, great burdock achene seed, plantain herb, coastal glehnia root, fritillaria bulb, figwort root, raw rehmannia root, tuber fleeceflower root, largehead atractylodes rhizome, white paeony fruit, white hyacinth bletilla, Chinese wolfberry root-bark, Chinese angelica, bamboo shavings, safflower, rhodiola root, medicinal herb, evodia fruit, achyranthes root, eucommia, One or more of prepared fleece-flower root, acanthopanax, rose hip, herba lycopi, rhizoma alismatis, rose, roselle, rhizoma anemarrhenae, apocynum venetum, broadleaf holly leaf, wild buckwheat rhizome, cherokee rose fruit, green tangerine peel, mangnolia officinalis, magnolia officinalis, turmeric, bitter orange, immature bitter orange, platycladi seed, pearl, gynostemma pentaphylla, fenugreek, madder, long pepper, Chinese chive seed, tuber fleeceflower stem, rhizoma cyperi, rhizoma drynariae, codonopsis pilosula, white mulberry root-bark, mulberry twig, thunberg fritillary bulb, motherwort, centella asiatica, epimedium herb, dodder, wild chrysanthemum, ginkgo leaf, astragalus, Hubei fritillary bulb, senna leaf, gecko, cowberry fruit, sophora fruit, cattail pollen, caltrop, propolis, tamarind fruit, eclipta, cooked rhubarb, prepared rehmannia. The plant beverage comprises at least one of flavonoids, saponins, polysaccharides, alkaloids, amino acids, microelements, phenols, phenanthrene compounds, wine, water and vinegar.
Compared with the prior art, the material processing method has wide applicability to materials, high efficiency, safety and low processing cost; in addition, the prepared nano material has uniform particle size, uniform dispersion system and good performance stability; finally, the equipment can be controlled by adjusting the temperature and the pressure, the original components and properties of the material are kept to the maximum extent when the material is processed, and the processed product can generate a plurality of unexpected properties due to the large change of the particle size.
The plant beverage is obtained by the material treatment method. On one hand, the treatment temperature of the equipment is low, so that the biological activity of the effective components in the plants is maintained; on the other hand, the high-pressure nanocrystallization equipment releases the dispersion liquid from ultrahigh pressure to atmospheric pressure, so that gas in the dispersion liquid generates a cavity effect, and an internal blasting effect is caused due to huge internal and external pressure difference, so that the components of the plant material are completely extracted; finally, the treated plant material has small grain size and is beneficial to the absorption of human body.
Drawings
FIG. 1 is a scanning electron microscope image of multilayer graphite according to an embodiment of the present invention;
FIG. 2 is a scanning electron microscope image of the multilayer graphite according to the embodiment of the present invention;
FIG. 3 is a scanning electron microscope image of multilayer graphite of the present invention;
fig. 4 is a particle size test analysis report for a multi-layered graphite according to an embodiment of the present invention.
Detailed Description
In order to make the technical problems, technical solutions and advantageous effects to be solved by the present invention more clearly apparent, the present invention is further described in detail below with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
In one aspect, an embodiment of the present invention provides a material processing method, including the following steps:
s01: crushing and pretreating the material to the particle size of 150-200 μm;
s02: dispersing the pretreated material powder in a solvent to form a dispersion system;
s03: treating the dispersion system by ultrahigh pressure nano equipment until the particle size is 1nm-100 nm;
in the specific step S01, the particle size can be processed to be larger for some materials with lower strength, such as plant materials, so as to save the pretreatment cost, and the material with higher hardness needs to be processed to be smaller in particle size so as not to damage the machine. Common processing means such as cutting, grinding, crushing and the like can be adopted, and parts with larger grain sizes which are difficult to process can be filtered out if necessary.
The solvent in step S02 may be water, an organic solvent, or a mixture of solvents.
Specifically, after the step S03, the powder after passing through the ultrahigh pressure nano-crystallization device may be subjected to a filtration process. On one hand, the filtering can optimize the particle size, and on the other hand, can remove some impurities with better toughness which cannot be crushed to play a role in purification.
More specifically, the material includes any one or more of a plant material, a metal material, a heat conduction material, a stone material, a chemical material, a semiconductor material and a two-dimensional material. The examples here are materials that have been used in the prior art, and the application range is not limited.
Specifically, in step S03, the processing method of the ultra-high pressure nanocrystallization apparatus includes at least one of high pressure processing and mixing processing. More specifically, the pretreated material is sent into an ultrahigh pressure nanometer device to be subjected to mixing treatment of 100Mpa, and the treatment mode comprises at least one of ultrasonic treatment and oscillation treatment. Then spraying the mixture into an atmospheric environment at 200-250 MPa.
Specifically, in the step S03, the working pressure range of the ultra-high pressure nano-device is 100MPa to 250 MPa. The advantage of the device is that at very high pressures, very high mechanical treatment of the material or heat treatment which impairs the activity is not necessary.
Specifically, in step S03, the processing temperature of the ultrahigh-pressure nanocrystallization apparatus is equal to or higher than-6 ℃. Because the dispersion generates heat at ultra-high pressures, some materials that generate relatively high amounts of heat require a temperature reduction process.
Specifically, in the step S03, the processing speed of the ultrahigh pressure nano-crystallization device is 20 to 40L/h. It can be seen that the processing speed of the apparatus employed in the present invention is very fast.
In conclusion, the material processing method is rapid and economical, the applicability is wide, the pressure difference between the inside and the outside of air in the dispersion liquid reaches two hundred times due to the fact that the processed material is processed under the condition of ultrahigh pressure, huge destructive power from the inside to the outside is achieved, the pressure of bubbles is all-directional and uniform, the crushing effect on the material is uniform, and the bubbles are uniformly distributed in the dispersion liquid after being processed in advance in a mixing mode. The technical effect when the dispersion is sprayed out through the nozzle is equivalent to that a plurality of bombs explode in the inside, the damage action time to the material is very short, and the treatment efficiency is very high. The temperature of the treatment method is controllable, and the material performance can be retained to the greatest extent according to requirements.
In another aspect, the embodiments of the present invention provide a plant beverage using dendrobium as a main raw material, wherein the plant material is processed by the material processing method. The dendrobium has various bioactive components, and various components of the dendrobium can be squeezed out completely as possible by using the material treatment method and the bioactivity can be kept.
The plant beverage also comprises sword bean, common fennel fruit, Chinese yam, hawthorn fruit, purslane, zaocys dhumnade, dark plum fruit, pawpaw, fructus cannabis, seville orange flower, fragrant solomonseal rhizome, liquorice root, angelica dahurica, ginkgo seed, white hyacinth bean, dried longan pulp, cassia seed, lily bulb, nutmeg, cinnamon, emblic leafflower fruit, finger citron, almond, sea buckthorn, oyster, gordon euryale seed, red bean, donkey-hide gelatin, chicken's gizzard-membrane, malt, kelp, jujube, momordica grosvenori, bunge cherry seed, honeysuckle flower, Chinese olive, heartleaf houttuynia herb, ginger, semen hoveniae, medlar, gardenia, amomum fruit, scaphium scaphigerum, tuckahoe, citron, elsholtzia, peach seed, mulberry leaf, mulberry red, platycodon root, sharpleaf galangal fruit, lotus leaf, radish seed, lotus seed, galangal, lophatherum gracile, fermented soybean, chrysanthemum flower, chicory, yellow mustard seed, sealwort, perilla seed, kudzuvine root, Fresh lalang grass rhizome, fresh rhizoma phragmitis, pallas pit viper, orange peel, mint, coix seed, allium macrostemon, raspberry, wrinkled gianthyssop, ginseng leaf, ginseng fruit, pseudo-ginseng, glabrous greenbrier rhizome, Japanese thistle herb, glossy privet fruit, dogwood fruit, medicinal cyathula root, unibract fritillary bulb, szechuan lovage rhizome, red deer fetus, hairy antler, red deer bone, salvia miltiorrhiza, cortex acanthopanacis, Chinese magnoliavine fruit, largetrifolious bugbane rhizome, cochinchnese asparagus root, tall gastrodia tuber, heterophylly falsestarwort root, morinda officinalis, costustoot, common scouring rush fruit, great burdock achene root, plantain seed, coastal glehnia root, fritillaria thunbergii, figwort root, raw polygonum multiflorum, bletilla, white atractylodes rhizome, white paeony root, cardamom, abalone shell, cortex lycii radicis, Chinese angelica, bamboo, safflower, rhodiola rosea, American ginseng, evodia rutaecarpa, achyranthes bidentata, Acanthopanax, rose hip, eupatorium japonicum, rhizoma alismatis, rose, roselle, rhizoma anemarrhenae, apocynum venetum, broadleaf holly leaf, wild buckwheat rhizome, cherokee rose fruit, green tangerine peel, mangnolia officinalis, magnolia officinalis, turmeric, bitter orange, immature bitter orange, platycladi seed, pearl, gynostemma pentaphylla, fenugreek, madder, long pepper, Chinese chive seed, vine of multiflower knotweed, nutgrass galingale rhizome, drynaria rhizome, codonopsis pilosula, white mulberry root-bark, mulberry twig, thunberg fritillary bulb, motherwort, centella, epimedium herb, south dodder seed, wild chrysanthemum flower, ginkgo leaf, astragalus, Hubei fritillary bulb, senna leaf, gecko, cowberry fruit, sophora fruit, cattail pollen, puncturevine, propolis, tamarind fruit, eclipta, cooked rhubarb, prepared rehmannia root. The dendrobium nobile has rich active functional components, and the raw materials are further added, so that the effect of the plant beverage can be enhanced and enriched by the material treatment method.
The plant beverage comprises at least one of flavonoids, saponins, polysaccharides, alkaloids, amino acids, microelements, phenols, phenanthrene compounds, wine, water and vinegar. These are only bioactive components in dendrobium, and according to a specific formula, the ingredients can be richer after being selected.
In conclusion, the plant beverage adopts the material treatment method, and the effective components can be uniformly and efficiently squeezed by utilizing the hole effect internal blasting; in addition, the biological active ingredients which are high in temperature and easy to oxidize can be further protected through low-temperature control; the dispersion plasmid in the dispersion liquid obtained by final treatment has small diameter and is favorable for absorption, and acetic acid, water or alcohol is used as a solvent to dissolve part of components, so that a functional drink with rich nutrition is finally formed.
The invention is further illustrated below with reference to specific embodiments and the accompanying drawings.
Example 1
Method for treating plant material
The first step of pretreatment: herba Dendrobii is used as main raw material and added with semen Canavaliae, fructus Foeniculi, rhizoma Dioscoreae, fructus crataegi, herba Portulacae, Zaocys, mume fructus, fructus Chaenomelis, fructus Cannabis, bitter orange flower, rhizoma Polygonati Odorati, Glycyrrhrizae radix, radix Angelicae Dahuricae, semen Ginkgo, semen lablab album, arillus longan (arillus longan), semen Cassiae, Bulbus Lilii, semen Myristicae, cortex Cinnamomi, fructus Phyllanthi, fructus Citri Sarcodactylis, semen Armeniacae amarum (sweet, fructus Hippophae, Concha Ostreae, semen euryales, semen Phaseoli, colla Corii Asini, endothelium corneum Gigeriae Galli, fructus Hordei Germinatus, thallus laminariae, fructus Jujubae (fructus Jujubae, Ziziphi Spinosae, fructus Jujubae), fructus Siraitiae Grosvenorii, semen Pruni, flos Lonicerae, fructus Canarii albi, herba Houttuyniae, rhizoma Zingiberis recens (rhizoma Zingiberis recens, fructus Hoveniae, fructus Lycii, fructus Gardeniae, fructus Amomi, semen Scaphii, Poria, fructus Citri, herba Moslae chinensis, semen Persicae, semen Nelumbinis, rhizoma Alpiniae Officinarum, folium Bambusae, semen Sojae Preparatum, black pepper, sophora flower bud, sophora flower, dandelion, honey, Chinese torreya seed, spina date seed, fresh lalang grass rhizome, fresh reed rhizome, viper, orange peel, mint, coix seed, allium macrostemon, raspberry, wrinkled gianthyssop herb, ginseng leaf, ginseng fruit, pseudo-ginseng, glabrous greenbrier rhizome, Japanese thistle herb, glossy privet fruit, dogwood fruit, medicinal cyathula root, unibract fritillary bulb, szechuan lovage rhizome, red deer fetus, red deer antler, red deer bone, salvia miltiorrhiza, acanthopanax bark, Chinese magnoliavine fruit, largetrifolioliolious bugbane rhizome, cochinchnese asparagus root, tall gastrodia tuber, heterophylly falsestarwort root, costus root, common scouring rush herb, great burdock achene root, plantain seed, coastal glehnia root, fritillaria bulb, figwort root, dried rehmannia root, raw tuber fleeceflower root, bletilla, white atractylodes rhizome, white paeony root, cardamon, sea-ear shell, dendrobium, One or more of fructus psoraleae, myrobalan, red paeony root, polygala tenuifolia, dwarf lilyturf tuber, tortoise shell, eupatorium fortunei, cacumen biotae, prepared rhubarb, prepared fleece-flower root, acanthopanax senticosus, rose hip, herba lycopi, rhizoma alismatis, rose hip, rhizoma anemarrhenae, apocynum venetum, broadleaf holly leaf, wild buckwheat rhizome, cherokee rose fruit, green tangerine peel, magnolia officinalis flower, turmeric, bitter orange, immature bitter orange, platycladi seed, pearl, gynostemma pentaphylla, fenugreek, madder, long pepper, Chinese chive seed, vine of multiflower knotweed, rhizoma cyperi, rhizoma drynariae, codonopsis pilosula, white mulberry bark, mulberry twig, thunberg fritillary bulb, motherwort, centella, epimedium, semen cuscutae, wild chrysanthemum flower, ginkgo leaf, astragalus mongholicus, Hubei fritillary bulb, senna leaf, gecko, cowberry fruit, sophora fruit, cattail pollen, caltrop, propolis, tamarind fruit. Wherein the content of the dendrobium is 15 percent, the content of other raw materials is 1 percent, and the content of the solvent is 84 percent.
And a second step of dispersion: dissolving the treated plant material in Chinese liquor, red wine or fruit vinegar;
thirdly, sending the mixture into high-pressure nanometer equipment: mixing at 0 deg.C under 100MPa to obtain a homogeneous dispersion system, spraying at 200MPa, and collecting in a container to obtain a dispersion system with particle size of 30-50 nm;
and fourthly, filtering treatment: filtering the dispersion system to remove impurities such as cellulose which are difficult to process, on one hand, the uniform particle size can be ensured, on the other hand, the impurities can be removed, and finally the plant material-containing beverage is obtained.
Example 2
Processing method for multilayer graphene
The first step is to crush the graphite to 150-;
secondly, adding the graphite obtained by treatment into water, wherein the mass concentration of the graphite is 15-30%, adding 0.5% of polyethylene glycol, and selectively adding maleic anhydride according to the requirement of conductivity of the prepared graphene;
thirdly, adding the dispersion liquid into ultrahigh pressure nano equipment, mixing under 100Mpa, then spraying under 200Mpa, and collecting in a container to obtain the dispersion liquid; the pore size of the filter screen can be selected according to different requirements of customers, so that an ideal nanometer product is obtained.
As shown in fig. 1, 2 and 3, the images are scanning electron micrographs of the multilayer graphene at different multiples, and the formed multilayer graphene has a clear structure and uniform particle size.
The particle size was 37.2nm as indicated by data D50 obtained using a Malvern 2000 particle size tester as shown in FIG. 4.
Example 3
Method for treating coating
Firstly, pre-treating the pigment (such as titanium dioxide) to 150-200 μm;
secondly, dispersing 1-5% of polyvinyl alcohol, 10% of auxiliary agent, 0.5% of polyethylene glycol and 10% -20% of treated pigment (such as titanium dioxide) in water;
and thirdly, adding the dispersion liquid into ultrahigh pressure nano equipment, mixing under 100Mpa, then spraying under 200Mpa, and collecting in a container to obtain the dispersion liquid with the particle size of 30-50 nm.

Claims (10)

1. A method of material processing, comprising the steps of:
crushing and pretreating the material to the particle size of 150-200 μm;
dispersing the pretreated material powder in a solvent to form a dispersion system;
and processing the dispersion system by ultrahigh pressure nano equipment until the particle size is 1nm-100 nm.
2. The material processing method as claimed in claim 1, further comprising the steps of: and filtering the powder after passing through the ultrahigh-pressure nano equipment.
3. The material processing method according to claim 1, characterized in that: the ultrahigh pressure nanocrystallization equipment treatment comprises at least one of high pressure treatment and mixing treatment.
4. The material processing method according to claim 1, characterized in that: the working pressure range of the ultrahigh pressure nanometer equipment is 100MPa-250 MPa.
5. The material processing method according to claim 1, characterized in that: the processing temperature of the ultrahigh pressure nanocrystallization equipment is more than or equal to-6 ℃.
6. The material processing method according to claim 1, characterized in that: the processing speed of the ultrahigh pressure nano equipment is 20-40L/h.
7. The material processing method according to claim 1, characterized in that: the material comprises any one or more of plant materials, metal materials, heat conduction materials, stone materials, chemical materials, semiconductor materials and two-dimensional materials.
8. A plant beverage taking dendrobium as a main material is characterized in that: wherein the plant material is treated by a material treatment process as claimed in any one of claims 1 to 7.
9. The plant drink according to claim 8, characterized in that: the plant beverage also comprises sword bean, common fennel fruit, Chinese yam, hawthorn fruit, purslane, zaocys dhumnade, dark plum fruit, pawpaw, fructus cannabis, seville orange flower, fragrant solomonseal rhizome, liquorice root, angelica dahurica, ginkgo seed, white hyacinth bean, dried longan pulp, cassia seed, lily bulb, nutmeg, cinnamon, emblic leafflower fruit, finger citron, almond, sea buckthorn, oyster, gordon euryale seed, red bean, donkey-hide gelatin, chicken's gizzard-membrane, malt, kelp, jujube, momordica grosvenori, bunge cherry seed, honeysuckle flower, Chinese olive, heartleaf houttuynia herb, ginger, semen hoveniae, medlar, gardenia, amomum fruit, scaphium scaphigerum, tuckahoe, citron, elsholtzia, peach seed, mulberry leaf, mulberry red, platycodon root, sharpleaf galangal fruit, lotus leaf, radish seed, lotus seed, galangal, lophatherum gracile, fermented soybean, chrysanthemum flower, chicory, yellow mustard seed, sealwort, perilla seed, kudzuvine root, Fresh lalang grass rhizome, fresh rhizoma phragmitis, pallas pit viper, orange peel, mint, coix seed, allium macrostemon, raspberry, wrinkled gianthyssop, ginseng leaf, ginseng fruit, pseudo-ginseng, glabrous greenbrier rhizome, Japanese thistle herb, glossy privet fruit, dogwood fruit, medicinal cyathula root, unibract fritillary bulb, szechuan lovage rhizome, red deer fetus, hairy antler, red deer bone, salvia miltiorrhiza, cortex acanthopanacis, Chinese magnoliavine fruit, largetrifolious bugbane rhizome, cochinchnese asparagus root, tall gastrodia tuber, heterophylly falsestarwort root, morinda officinalis, costustoot, common scouring rush fruit, great burdock achene root, plantain seed, coastal glehnia root, fritillaria thunbergii, figwort root, raw polygonum multiflorum, bletilla, white atractylodes rhizome, white paeony root, cardamom, abalone shell, cortex lycii radicis, Chinese angelica, bamboo, safflower, rhodiola rosea, American ginseng, evodia rutaecarpa, achyranthes bidentata, Acanthopanax, rose hip, eupatorium japonicum, rhizoma alismatis, rose, roselle, rhizoma anemarrhenae, apocynum venetum, broadleaf holly leaf, wild buckwheat rhizome, cherokee rose fruit, green tangerine peel, mangnolia officinalis, magnolia officinalis, turmeric, bitter orange, immature bitter orange, platycladi seed, pearl, gynostemma pentaphylla, fenugreek, madder, long pepper, Chinese chive seed, vine of multiflower knotweed, nutgrass galingale rhizome, drynaria rhizome, codonopsis pilosula, white mulberry root-bark, mulberry twig, thunberg fritillary bulb, motherwort, centella, epimedium herb, south dodder seed, wild chrysanthemum flower, ginkgo leaf, astragalus, Hubei fritillary bulb, senna leaf, gecko, cowberry fruit, sophora fruit, cattail pollen, puncturevine, propolis, tamarind fruit, eclipta, cooked rhubarb, prepared rehmannia root.
10. The plant drink according to claim 8 or 9, characterized in that: the plant beverage comprises at least one of flavonoids, saponins, polysaccharides, alkaloids, amino acids, microelements, phenols, phenanthrene compounds, wine, water and vinegar.
CN201910892541.2A 2019-09-20 2019-09-20 Material treatment method and application thereof Pending CN110637956A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111690284A (en) * 2020-06-30 2020-09-22 浙江喜盈门家居科技股份有限公司 Preparation process of biomass-based nano material
WO2023074459A1 (en) * 2021-10-28 2023-05-04 住友化学株式会社 Composition for preventing, improving or alleviating symptoms relating to phlegm and dampness
ES2951198A1 (en) * 2022-03-11 2023-10-18 Xuehe Huang A TRADITIONAL CHINESE MEDICINE (Machine-translation by Google Translate, not legally binding)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103070393A (en) * 2013-01-08 2013-05-01 浙江工业大学 Preparation method for nano-bone meal
CN104271228A (en) * 2012-03-09 2015-01-07 株式会社赛勒芙特 Nanoparticle dispersion, nanoparticle-carrying powder, and processes for manufacturing same
CN105655570A (en) * 2016-04-01 2016-06-08 四川创能新能源材料有限公司 Refining preparation method of nanoscale silicon powder material

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104271228A (en) * 2012-03-09 2015-01-07 株式会社赛勒芙特 Nanoparticle dispersion, nanoparticle-carrying powder, and processes for manufacturing same
CN103070393A (en) * 2013-01-08 2013-05-01 浙江工业大学 Preparation method for nano-bone meal
CN105655570A (en) * 2016-04-01 2016-06-08 四川创能新能源材料有限公司 Refining preparation method of nanoscale silicon powder material

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
和段琪著: "《云南生物产业创新驱动发展研究》", 31 October 2015, 冶金工业出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111690284A (en) * 2020-06-30 2020-09-22 浙江喜盈门家居科技股份有限公司 Preparation process of biomass-based nano material
WO2023074459A1 (en) * 2021-10-28 2023-05-04 住友化学株式会社 Composition for preventing, improving or alleviating symptoms relating to phlegm and dampness
ES2951198A1 (en) * 2022-03-11 2023-10-18 Xuehe Huang A TRADITIONAL CHINESE MEDICINE (Machine-translation by Google Translate, not legally binding)

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