CN110591826B - Foaming cup wax and production method thereof - Google Patents
Foaming cup wax and production method thereof Download PDFInfo
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- CN110591826B CN110591826B CN201910894096.3A CN201910894096A CN110591826B CN 110591826 B CN110591826 B CN 110591826B CN 201910894096 A CN201910894096 A CN 201910894096A CN 110591826 B CN110591826 B CN 110591826B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
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Abstract
The invention discloses a foaming cup wax and a production method thereof, belonging to the technical field of candles. The invention comprises the following raw materials in parts by weight: 5-20 parts of soybean wax, 15-35 parts of palm wax, 0-10 parts of soft wax, 28-80 parts of paraffin and 0-7 parts of essence; the invention also provides a preparation method of the foaming cup wax, which comprises the steps of respectively dissolving the soybean wax, the palm wax, the soft wax and the paraffin wax, mixing the materials step by step, controlling the mixing temperature and the essence adding time, and foaming to obtain the foaming cup wax. The formula of the foaming cup wax is adjusted, the reasonable matching and the scientific design are realized, the plant wax proportion is improved, the dosage of the paraffin wax is reduced, the consumption of the paraffin wax is reduced, and the petroleum resource is saved; the process flow is short, the control is convenient, the obtained foam cupcandle has compact and uniform bubbles, the density of the candle is reduced, the combustion performance is good, the self-extinguishing phenomenon can not occur, the combustion is stable, and the problems that the traditional foam candle is easy to collapse and the flame is suddenly high and suddenly low at high temperature are solved.
Description
Technical Field
The invention belongs to the technical field of candles, and particularly relates to foamed cupcandle and a production method thereof.
Background
At present, most of cup waxes in the market are directly filled after raw materials (paraffin, plant wax and the like) are mixed and melted, and the cup waxes filled in the mode are called solid waxes; the wax is generally of a solid structure, the structure is compact, the material consumption is increased, and the cost is increased. Moreover, as the cooling shrinkage is large in the production process, the interior of the wax column is often provided with a plurality of recesses, tunnels and other heterogeneous structures, and the structures can have adverse effects on the fragrance volatilization and the thermal stability of the wax column, such as: the phenomena of unstable flame, incomplete volatilization of fragrance, oil discharge and the like occur in the combustion process.
The foaming wax is a candle prepared by a foaming process technology, and specifically refers to a candle which is prepared by mixing and melting raw materials, stirring, introducing air into a solution, uniformly dispersing to realize a large contact surface of liquid and gas, and cooling to obtain a wax block with a loose structure. Compared with the homogeneous wax body structure of the foaming cup wax manufactured by the foaming process technology, the foaming cup wax manufactured by the foaming process technology has the advantage that the wax weight is reduced due to the special average value, loose structure and uniform bubble distribution. According to statistics, compared with common cup wax, the cup wax has the advantages that the weight of the foaming wax can be saved by at least 15%, the combustion is stable, the combustion is not affected, meanwhile, the fragrance is thoroughly volatilized, and the problems of oil production, melting pits and the like are solved.
However, in the foaming cup wax in the prior art, due to the fact that the paraffin content in the formula is high, the process is unstable, bubbles are different in size and are not distributed uniformly, the bubbles at the lower part are few, the bubbles at the top part are large, meanwhile, the risk of collapse is accompanied, the flame is suddenly high and suddenly low, even self-extinguishes, and the combustion and stability performance are seriously affected.
Disclosure of Invention
The invention aims to provide a foaming cup wax and a production method thereof, and solves the problem that the combustibility and stability of the foaming cup wax are seriously influenced due to the fact that bubbles in the foaming cup wax are different in size and distribution in the prior art.
In order to solve the technical problems, the invention is mainly realized by the following technical scheme:
in one aspect, the foaming cup wax provided by the invention comprises the following raw materials in parts by weight:
the formula of the foaming cup wax is adjusted, the soybean wax, the palm wax, the soft wax and the paraffin wax are reasonably matched, the design is scientific, the proportion of the vegetable wax is improved, the using amount of the paraffin wax is reduced, the consumption of the paraffin wax is reduced, and the petroleum resource is saved; the foaming cup wax disclosed by the invention is small in bubbles, uniform in size and uniform in distribution, the collapse of the bubbles is not worried about, the density of the candle is reduced, the condition that the bubbles at the lower part are few and the bubbles at the top are large in the foaming process in the traditional method is avoided, the combustion performance is good, the self-extinguishing phenomenon cannot occur, the combustion is stable, and the problems that the collapse, the high and low flame and the poor combustion stability are easy to occur in the traditional foaming candle at high temperature are solved.
As a preferred embodiment, the feed comprises the following raw materials in parts by weight:
the invention can further adjust the proportion of the soybean wax, the palm wax, the soft wax and the paraffin wax, further reduce the dosage of the paraffin wax, improve the dosage of the vegetable wax including the soybean wax, the palm wax and the soft wax, further optimize the proportion of all the raw materials, and more easily obtain the foaming cup wax with compact and uniform bubbles, good combustion performance and stable performance.
As a preferred embodiment, the feed comprises the following raw materials in parts by weight:
the invention can also continuously adjust the proportion of the soybean wax, the palm wax, the soft wax and the paraffin wax, further reduce the dosage of the paraffin wax, improve the dosage of the vegetable wax including the soybean wax, the palm wax and the soft wax, reduce the dosage of the paraffin wax, reduce the consumption of the paraffin wax and save petroleum resources; the raw materials with the proportion can more easily obtain the foamed cupcandle with compact and uniform bubbles, good combustion performance and stable performance.
The invention relates to a production method of foaming cup wax, which comprises the following steps:
1) Dissolving paraffin at 100-120 deg.C to obtain paraffin liquid;
2) Dissolving soybean wax and palm wax at 65-85 deg.C respectively to obtain soybean wax solution and palm wax solution;
3) Melting soft wax at 85-105 deg.C to obtain soft wax solution;
4) Mixing the paraffin liquid obtained in the step 1) and the palm wax liquid and the soybean wax liquid obtained in the step 2) at 75-85 ℃, and stirring for 15-25min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid;
5) Mixing the mixed solution obtained in the step 4) and the soft wax solution obtained in the step 3) at the temperature of 80-90 ℃, and stirring for 15-25min to obtain a foaming solution;
6) Taking essence, and adding the essence at 75-85 ℃ within 20-30min before foaming the foaming liquid obtained in the step 5) to obtain wax liquid;
7) Adding the wax liquid obtained in the step 6) into a foaming machine at 75-85 ℃, foaming, and circulating for 3-10min at 70-85 ℃;
8) Filling into a cup to obtain the foaming cup wax.
The soybean wax, the palm wax, the soft wax and the paraffin wax are respectively dissolved, then are gradually mixed, the adding time and the adding temperature of the essence are controlled, and foaming is carried out in a foaming machine, so that the production method has the advantages of short process flow, convenience in control, no special requirement on equipment and easiness in realizing industrialization; the obtained foaming cup wax has small bubbles, uniform bubble sizes and even distribution, does not worry about the collapse of the bubbles, reduces the density of the candle, avoids the condition that the bubbles at the lower part are few and the bubbles at the top are big bubbles easily formed in the foaming process of the traditional method, has good combustion performance, can not self-extinguish, has stable combustion, and solves the problems that the traditional foaming candle is easy to collapse, has suddenly high and suddenly low flame, has poor combustion stability and the like at high temperature.
In a preferred embodiment, in step 1), the paraffin is further purged under stirring for at least 30min after being melted. The invention can remove trace benzene, toluene and other harmful substances in the paraffin by blowing, so that the obtained foaming cup wax is safer and more environment-friendly.
As a preferred embodiment, in the step 1), the stirring speed is 100 to 500r/min. The stirring speed is controlled during stirring, so that on one hand, energy consumption is saved, and on the other hand, all trace harmful substances such as benzene, toluene and the like in paraffin can be purged out.
In a preferred embodiment, in step 1), nitrogen is used for purging. The invention can adopt various inert gases during purging, and nitrogen is preferably used for purging because of wide sources, low cost and large amount in air.
In a preferred embodiment, in the step 8), the density of the foaming cup wax is 600-800g/L. The foamed cupcandle obtained by the invention has the advantages of low density, light weight and convenient use.
As a preferred embodiment, in the step 4), the stirring speed is 100 to 500r/min. The invention controls the stirring speed of the paraffin liquid, the palm wax liquid and the soybean wax liquid during mixing, so that the three are fully mixed, and the interaction among the three is promoted.
As a preferred embodiment, in the step 5), the stirring speed is 100 to 500r/min. The invention also controls the stirring speed of the mixed liquid of the soft wax liquid and the paraffin liquid, the palm wax liquid and the soybean wax liquid during mixing, so that the soft wax liquid and the paraffin liquid are fully mixed, and the interaction between the soft wax liquid and the soybean wax liquid is promoted.
Compared with the prior art, the invention has the beneficial effects that: the formula of the foaming cup wax is adjusted, the soybean wax, the palm wax, the soft wax and the paraffin wax are reasonably matched, the design is scientific, the proportion of the vegetable wax is improved, the using amount of the paraffin wax is reduced, the consumption of the paraffin wax is reduced, and the petroleum resource is saved; the production process is short in flow, convenient to control, free of special requirements on equipment and easy to realize industrialization; the obtained foaming cup candle is small in bubbles, uniform in size, uniform in distribution, compact and uniform in bubbles, free of worrying about collapse of the bubbles, good in combustion performance, free of self-extinguishing phenomenon and stable in combustion, avoids the problem that the conventional foaming candle is easy to collapse, has little bubbles at the lower part and large bubbles at the top in the foaming process, and solves the problems that the conventional foaming candle is easy to collapse, has little flame and poor combustion stability at high temperature.
Drawings
FIG. 1 is a photograph of a foamed cupwax made in accordance with one embodiment of the present invention;
FIG. 2 is a top plan photographic view of FIG. 1;
FIG. 3 is a photograph showing a real image of a conventional commercially available foaming wax;
fig. 4 is a top plan photograph of fig. 3.
Detailed Description
The technical solutions of the present invention will be described clearly and completely with reference to specific embodiments of the present invention, and it should be understood that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention relates to foaming cup wax which comprises the following raw materials in parts by weight:
preferably, the feed comprises the following raw materials in parts by weight:
further, the feed comprises the following raw materials in parts by weight:
the invention relates to a production method of foaming cup wax, which comprises the following steps:
1) Dissolving paraffin at 100-120 deg.C to obtain paraffin solution;
2) Dissolving soybean wax and palm wax at 65-85 deg.C respectively to obtain soybean wax solution and palm wax solution;
3) Melting soft wax at 85-105 deg.C to obtain soft wax solution;
4) Mixing the paraffin liquid obtained in the step 1) and the palm wax liquid and the soybean wax liquid obtained in the step 2) at 75-85 ℃, and stirring for 15-25min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid;
5) Mixing the mixed solution obtained in the step 4) and the soft wax solution obtained in the step 3) at the temperature of 80-90 ℃, and stirring for 15-25min to obtain a foaming solution;
6) Taking essence, and adding the essence at 75-85 ℃ within 20-30min before foaming the foaming liquid obtained in the step 5) to obtain wax liquid;
7) Adding the wax liquid obtained in the step 6) into a foaming machine at 75-85 ℃, foaming, and circulating for 3-10min at 70-85 ℃;
8) Filling into a cup to obtain the foaming cup wax.
Preferably, in the step 1), the paraffin is further purged for at least 30min under stirring after being dissolved.
Further, in the step 1), the stirring speed is 100-500r/min.
Specifically, in the step 1), nitrogen is used for purging during purging.
Still preferably, in the step 8), the density of the foamed cupwax is 600-800g/L.
Still further, in the step 4), the stirring speed is 100-500r/min.
More specifically, in the step 5), the stirring speed is 100-500r/min.
Example one
The invention relates to a production method of foaming cup wax, which comprises the following steps:
1) Weighing the following raw materials in parts by weight: 20 parts of soybean wax; 25 parts of palm wax; 10 parts of soft wax; 28 parts of paraffin;
2) Dissolving paraffin at 100 deg.C to obtain paraffin solution;
3) Dissolving soybean wax and palm wax at 65 deg.C and 75 deg.C respectively to obtain soybean wax solution and palm wax solution;
4) Melting soft wax at 85 deg.C to obtain soft wax solution;
5) Mixing the paraffin liquid obtained in the step 2) and the palm wax liquid and the soybean wax liquid obtained in the step 3) at 75 ℃, and stirring for 25min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid;
6) Mixing the mixed solution obtained in the step 5) with the soft wax solution obtained in the step 4) at 80 ℃, and stirring for 25min to obtain a foaming solution;
7) Adding the wax liquid obtained in the step 6) into a foaming machine at 75 ℃, foaming, and circulating for 10min at 70 ℃;
8) And filling the mixture into a cup after the foaming machine finishes foaming to obtain the foaming cup wax.
Example two
The invention relates to a production method of foaming cup wax, which comprises the following steps:
1) Weighing the following raw materials in parts by weight: 15 parts of soybean wax; 15 parts of palm wax; 7 parts of soft wax; 60 parts of paraffin; 3 parts of essence;
2) Dissolving paraffin at 105 deg.C, starting benzene removal device, continuously stirring and blowing, and maintaining for 40min to obtain paraffin liquid;
3) Respectively dissolving soybean wax and palm wax at 75 deg.C to obtain soybean wax solution and palm wax solution;
4) Dissolving soft wax at 100 deg.C to obtain soft wax solution;
5) Mixing the paraffin liquid obtained in the step 2) and the palm wax liquid and the soybean wax liquid obtained in the step 3) at 80 ℃, and stirring for 22min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid;
6) Mixing the mixed solution obtained in the step 5) with the soft wax solution obtained in the step 4) at 82 ℃, and stirring for 21min to obtain a foaming solution;
7) Taking essence, and adding the essence at 81 ℃ within 28min before foaming the foaming liquid obtained in the step 6) to obtain wax liquid;
8) Transferring the wax liquid obtained in the step 7) to a foaming machine, keeping the temperature at 80 ℃, starting the foaming machine, keeping the temperature at 80 ℃, and circulating for 6min;
9) And filling the mixture into a cup after the foaming machine finishes foaming to obtain the foaming cup wax.
EXAMPLE III
The invention relates to a production method of foaming cup wax, which comprises the following steps:
1) Weighing the following raw materials in parts by weight: 5 parts of soybean wax; 35 parts of palm wax; 80 parts of paraffin; 7 parts of essence;
2) Dissolving paraffin at 120 deg.C, starting benzene removal device, stirring, and purging with nitrogen gas for 60min to obtain paraffin solution;
3) Dissolving soybean wax and palm wax at 85 deg.C respectively to obtain soybean wax solution and palm wax solution;
4) Dissolving soft wax at 105 deg.C to obtain soft wax solution;
5) Mixing the paraffin liquid obtained in the step 2) and the palm wax liquid and the soybean wax liquid obtained in the step 3) at 85 ℃, and stirring for 15min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid;
6) Mixing the mixed solution obtained in the step 5) with the soft wax solution obtained in the step 4) at 90 ℃, and stirring for 15min to obtain a foaming solution;
7) Taking essence, and adding the essence at 85 ℃ within 20min before foaming the foaming liquid obtained in the step 6) to obtain wax liquid;
8) Transferring the wax liquid obtained in the step 7) to a foaming machine, keeping the temperature at 85 ℃, starting the foaming machine, foaming, keeping the temperature at 85 ℃, and circulating for 3min;
9) Filling into a cup to obtain the foaming cup wax.
Four foamed cup waxes obtained in the first to third examples were prepared, four commercially available foamed cup waxes were prepared as control samples, performance test experiments were performed, and the total weight, the wax weight, the burning time, the residual wax amount, the wall temperature of the foamed cup wax during burning, the flame height, the residual smoke, and the candle consumption were measured, wherein the wall temperature, the flame height, and the residual smoke were measured as the minimum and maximum values, and the experimental results are shown in table 1.
The foamed cup wax obtained in the first embodiment of the invention and the comparison sample are photographed by using cameras respectively, and as can be seen from fig. 1 and fig. 2, the foamed cup wax has compact and uniform bubbles, small bubbles, consistent bubble size and uniform distribution; however, as can be seen from fig. 3 and 4, the bubbles of the comparative example are not uniform in size and are not uniformly distributed, and a large bubble appears.
As can be seen from Table 1, the burning time of the foamed cupcandle produced by the method of the invention is 42-46h, which is much longer than that of the control sample; the minimum value of the flame height of the foaming cupcandle produced by the method is about 24mm, and the maximum value of the flame height is about 27mm, which are respectively higher than the minimum value and the maximum value of the flame height of a control sample during combustion; the minimum value of the remaining smoke retention time after the combustion of the foamed cupule wax produced by the method of the invention is about 8s, and the maximum value of the remaining smoke retention time is about 12s, which are respectively shorter than the minimum value and the maximum value of the remaining smoke retention time after the combustion of the control sample; the candle consumption after burning of the foamed cupcandle produced by the process of the present invention was about 84%, which is significantly higher than the candle consumption of the control after burning. In addition, the foaming cupola wax produced by the method has good combustion performance, no self-extinguishing phenomenon, stable combustion and no collapse or low-high flame phenomenon in the combustion process.
TABLE 1 Performance test results for different foaming waxes
Therefore, compared with the prior art, the invention has the beneficial effects that: the formula of the foaming cup wax is adjusted, the soybean wax, the palm wax, the soft wax and the paraffin wax are reasonably matched, the design is scientific, the proportion of the vegetable wax is improved, the using amount of the paraffin wax is reduced, the consumption of the paraffin wax is reduced, and the petroleum resource is saved; the production process is short in flow, convenient to control, free of special requirements on equipment and easy to realize industrialization; the obtained foaming cup candle is small in bubbles, uniform in size, uniform in distribution, compact and uniform in bubbles, free of worrying about collapse of the bubbles, good in combustion performance, free of self-extinguishing phenomenon and stable in combustion, avoids the problem that the traditional foaming candle is easy to collapse, the flame is suddenly high and suddenly low, the combustion stability is poor and the like due to the fact that the bubbles at the lower part are few and the bubbles at the top are all large in the foaming process in the traditional method.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (7)
1. A foaming cup wax is characterized in that:
the foaming cup wax comprises the following raw materials in parts by weight:
10-20 parts of soybean wax;
25-30 parts of palm wax;
5-10 parts of soft wax;
30-40 parts of paraffin;
1-5 parts of essence;
the production method of the foaming cup wax comprises the following steps: 1) Dissolving paraffin at 100-120 deg.C to obtain paraffin liquid; 2) Dissolving soybean wax and palm wax at 65-85 deg.C respectively to obtain soybean wax solution and palm wax solution; 3) Melting soft wax at 85-105 deg.C to obtain soft wax solution; 4) Mixing the paraffin liquid obtained in the step 1) and the palm wax liquid and the soybean wax liquid obtained in the step 2) at 75-85 ℃, and stirring for 15-25min to completely mix the paraffin liquid and the soybean wax liquid to obtain a mixed liquid; 5) Mixing the mixed solution obtained in the step 4) and the soft wax solution obtained in the step 3) at the temperature of 80-90 ℃, and stirring for 15-25min to obtain a foaming solution; 6) Taking essence, and adding the essence at 75-85 ℃ within 20-30min before foaming the foaming liquid obtained in the step 5) to obtain wax liquid; 7) Adding the wax liquid obtained in the step 6) into a foaming machine at 75-85 ℃, foaming, and circulating for 3-10min at 70-85 ℃; 8) Filling into a cup to obtain the foaming cup wax.
2. The foamed cupwax of claim 1, wherein:
in the step 1), the paraffin is required to be blown for at least 30min under stirring after being dissolved.
3. The foamed cupwax of claim 2, wherein:
in the step 1), the stirring speed is 100-500r/min.
4. The foamed cupwax of claim 2, wherein:
in the step 1), nitrogen is adopted for purging during purging.
5. The foamed cupwax of any one of claims 1-4, wherein:
in the step 8), the density of the foaming cup wax is 600-800g/L.
6. The foamed cupwax of claim 1, wherein:
in the step 4), the stirring speed is 100-500r/min.
7. The foamed cupwax of claim 1, wherein:
in the step 5), the stirring speed is 100-500r/min.
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