CN110527339A - The production method for inducing the woodcare paint and its functional powders and auxiliary agent of negative oxygen ion - Google Patents
The production method for inducing the woodcare paint and its functional powders and auxiliary agent of negative oxygen ion Download PDFInfo
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- CN110527339A CN110527339A CN201910861792.4A CN201910861792A CN110527339A CN 110527339 A CN110527339 A CN 110527339A CN 201910861792 A CN201910861792 A CN 201910861792A CN 110527339 A CN110527339 A CN 110527339A
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- negative oxygen
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/08—Polyesters modified with higher fatty oils or their acids, or with natural resins or resin acids
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/03—Powdery paints
- C09D5/033—Powdery paints characterised by the additives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses the production methods of a kind of woodcare paint for inducing negative oxygen ion and its functional powders and auxiliary agent, and wherein the production method of negative oxygen ion function powder is the following steps are included: bake drying for ion adsorption type rare earth ore stone, rich magnesium fibrous silicate and hydrous magnesium silicate；The rich magnesium fibrous silicate and ion adsorption type rare earth ore stone that bake after drying are extracted using acidic extractant, high-temperature baking is carried out after extraction, removes radioactive element；Amorphous silica is heated, soluble silicon acid content therein is reduced；It by hydrous magnesium silicate, rich magnesium fibrous silicate, ion adsorption type rare earth ore stone and silica, crushes and is uniformly mixed, obtain negative oxygen ion function powder.The cost of material of the present invention, negative oxygen ion function auxiliary agent are low, the woodcare paint for the negative oxygen ion produced, and constantly induce negative oxygen ion to space ionization, purify air and environment, while will not change the original quality of woodcare paint, have the characteristics that stable.
Description
Technical field
The present invention relates to woodcare paint production fields, and in particular to a kind of woodcare paint and its functional powders for inducing negative oxygen ion
With the production method of auxiliary agent.
Background technique
Woodcare paint refers to a kind of lacquer type organic coating on woodwork, there is polyester, polyurethane paint etc..Aqueous woodware paint is made with water
For diluent, no any harmful volatilization, has the characteristics that safety and environmental protection.With the increase of people's health consciousness and environmental consciousness,
Negative oxygen ion woodcare paint is more and more welcomed by the people.However, common negative oxygen ion woodcare paint is influenced by processing technology on the market,
The disadvantages of small, at high cost there are negative oxygen ion burst size.Existing negative oxygen ion function auxiliary agent mostly uses with hydrous magnesium silicate, contains
Water silicate clay and amorphous silicas are basic material, and addition Tourmaline stone, rare earth and tourmaline synthesize negative oxygen ion
The mode of occurring source, material requested type is complicated, and material cost is high, there are the negative oxygen ion function auxiliary agent radioactivity of preparation compared with
By force.
In view of this, being badly in need of improving the production method of existing negative oxygen ion woodcare paint, to improve negative oxygen ion wood
The negative oxygen ion burst size of device paint reduces production cost.
Summary of the invention
The technical problem to be solved by the present invention is to existing negative oxygen ion woodcare paint negative oxygen ion burst sizes small, production cost
High problem.
In order to solve the above-mentioned technical problem, the technical scheme adopted by the invention is that providing a kind of negative oxygen ion function powder
Production method, comprising the following steps:
Ion adsorption type rare earth ore stone, rich magnesium fibrous silicate and hydrous magnesium silicate are baked into drying；
The rich magnesium fibrous silicate and ion adsorption type rare earth ore stone that bake after drying are carried out using acidic extractant
Extraction carries out high-temperature baking after extraction, remove radioactive element；
Amorphous silica is heated, soluble silicon acid content therein is reduced；
By hydrous magnesium silicate of the baking after dry, the rich magnesium fibrous silicate and ion after removal radioactive element
Absorbent-type rare earth ore and silica are crushed and are uniformly mixed, and obtain negative oxygen ion function powder.
In the above-mentioned methods, the hydrous magnesium silicate, rich magnesium fibrous silicate, ion adsorption type rare earth ore stone and dioxy
The weight fraction ratio of SiClx is 3:(3-6): (4-8): (1-2.5).
In the above-mentioned methods, the hydrous magnesium silicate, rich magnesium fibrous silicate, ion adsorption type rare earth ore stone and dioxy
The weight fraction ratio of SiClx is 3:6:5:1.
In the above-mentioned methods, the negative oxygen ion function powder mixed with neutral water soluble auxiliary agent and resin, stirred, made
Three is sufficiently mixed as white gum object, obtains negative oxygen ion function auxiliary agent, and the weight fraction ratio of three is (3-5): (20-
30): (80-92).
In the above method, in the silica of lenticular, soluble silicon acid content is 30% or less.
In the above-mentioned methods, using acidic extractant to the rich magnesium fibrous silicate and ion type after baking drying
When rare earth ore is extracted, the quality of acidic extractant used is rich magnesium fibrous silicate and ion adsorption type rare earth ore stone
3-5 times of quality sum, and the concentration of acidic extractant is 5-15wt%.
In the above-mentioned methods, the radioactivity member after extraction, in rich magnesium fibrous silicate and ion adsorption type rare earth ore stone
The removal rate of element is 80% or more.
The present invention also provides a kind of production methods of woodcare paint for inducing negative oxygen ion:
Woodenware raw materials for varnish is mixed according to a conventional method, and according to the density of woodcare paint, addition produces negative according to the method described above
Oxonium ion function additive.
In the above-mentioned methods, density is the woodcare paint of 1:1.15~1.2, the weight ratio of negative oxygen ion function auxiliary agent addition
It is 2%；Density is the woodcare paint of 1:1.25~1.35, and the weight ratio of negative oxygen ion function auxiliary agent addition is 3.5%；Density is
The woodcare paint of 1:1.4~1.5, the weight ratio of negative oxygen ion function auxiliary agent addition are 4%.
Compared with prior art, negative oxygen ion function auxiliary agent provided by the invention uses ion adsorption type rare earth ore stone, richness
Fibrous magnesium silicate, hydrous magnesium silicate and silica prepare, and raw material easily obtains, and reduce production cost.By above-mentioned
The white jelly of negative oxygen ion function auxiliary agent of method preparation, has certain viscosity, has good adhesion.
In the present invention negative oxygen ion function auxiliary agent is added into woodcare paint according to the density of woodcare paint in proportion, guaranteed different
Persistently ionization induces negative oxygen ion to the woodcare paint of density all under air vibration effect, to meet woodcare paint under different situations
Requirement.
Detailed description of the invention
Fig. 1 is the production method flow chart of negative oxygen ion function auxiliary agent in the present invention；
Fig. 2 is the production method process that the woodcare paint of negative oxygen ion is induced in the present invention.
Specific embodiment
The present invention provides the production method of a kind of woodcare paint for inducing negative oxygen ion and its functional powders and auxiliary agent, productions
Woodcare paint can air vibration effect under constantly induce negative oxygen ion, ensure the respiratory health of people.Below with reference to explanation
Book the drawings and specific embodiments are described in detail the present invention.
In order to make more clearly explanation and illustration to technical solution of the present invention and implementation, realization introduced below is originally
Several preferred specific embodiments of inventive technique scheme.Obviously, specific embodiment discussed below is only of the invention one
Section Example, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not doing
Every other embodiment obtained under the premise of creative work out, shall fall within the protection scope of the present invention.
Negative oxygen ion function auxiliary agent is the prerequisite of negative oxygen ion woodcare paint production, the quality of negative oxygen ion function auxiliary agent
Determine whether woodcare paint can satisfy country and test the detection of negative oxygen ion woodcare paint, especially with respect to the prison of radiant quantity
It surveys and requires.
The production method of negative oxygen ion function powder and auxiliary agent provided by the invention, as shown in Figure 1, comprising the following steps:
Step 110: by ion adsorption type rare earth ore stone, rich magnesium fibrous silicate (such as sepiolite) and hydrous magnesium silicate
(such as talcum) carries out baking drying process.
The specific practice is: above-mentioned three kinds of raw materials being put into drying oven or dryer and carry out baking drying process, bake temperature
Degree is 60 degree, bakes and banks up with earth the time not less than 24 hours, dries three kinds of raw materials thoroughly.
Step 120: using acidic extractant to the rich magnesium fibrous silicate and ion adsorption type re after baking drying
Ore is extracted, and high-temperature baking is carried out after extraction, removes radioactive element, such as radium, thorium, potassium radioactive element.
Specific method is: the rich magnesium obtained using middle strong acidity extractant (dissociation constant (Ka ≈ 10)) to step 110 is fine
Dimension shape silicate and ion adsorption type rare earth ore stone are extracted, and the quality of acidic extractant used is rich magnesium fibrous silicate
With 3-5 times of ion adsorption type rare earth ore stone quality sum, sour concentration be 5-15wt% (Weight percent, quality hundred
Divide ratio), extraction time is not less than 5 hours, so that rich magnesium fibrous silicate and ion adsorption type rare earth ore stone divide in the solution
Dissipating becomes graininess, after other impurities precipitating, then by pure rich magnesium fibrous silicate and ion adsorption type rare earth ore stone
It takes out, carries out high-temperature baking, temperature is not less than 180 degree, and baking time is no less than 24 hours, becomes canescence.
By above-mentioned extraction processing, the removal rate of the radioactive elements such as radium, thorium, potassium can be made to reach 80% or more.
Step 130: amorphous silica being heated, the content of mensuration dissolubility silicic in silica is reduced.
The specific practice is: amorphous silicas heated, such as is warmed to 300 degree or 350 degree, silica at this time
It is neutral, nontoxic with pH value, the advantages that suspendability is good, and absorption property is strong, while having to Alpha-ray radioactive ray good
It is comprehensive, increase its half-life period 45%.
Step 140: will bake it is dry after hydrous magnesium silicate, the rich magnesium fibrous silicate after removal radioactive element and
Ion adsorption type rare earth ore stone and silica are crushed and are uniformly mixed, and obtain negative oxygen ion function powder.Negative oxygen ion function
The granularity of energy powder is not less than 1500 mesh.
Wherein, in preferred embodiment, hydrous magnesium silicate, rich magnesium fibrous silicate, ion adsorption type rare earth ore stone and
The weight fraction ratio of silica is 3:(3-6): (4-8): (1-2.5).
The following are typical specific embodiments:
Specific embodiment 1.
Water magnesium silicate, 3；
Rich magnesium fibrous silicate, 5.5；
Ion adsorption type rare earth ore stone, 4；
Silica, 2.5.
Specific embodiment 2.
Water magnesium silicate, 3；
Rich magnesium fibrous silicate, 3；
Ion adsorption type rare earth ore stone, 8；
Silica, 1.
Specific embodiment 3.
Water magnesium silicate, 3；
Rich magnesium fibrous silicate, 3.5；
Ion adsorption type rare earth ore stone, 7；
Silica, 1.5.
Specific embodiment 4.
Water magnesium silicate, 3；
Rich magnesium fibrous silicate, 4；
Ion adsorption type rare earth ore stone, 6；
Silica, 2.
Specific embodiment 5.
Water magnesium silicate, 3；
Rich magnesium fibrous silicate, 6；
Ion adsorption type rare earth ore stone, 5；
Silica, 1.
Preferably, step 150: negative oxygen ion function powder, neutral water soluble auxiliary agent being mixed with resin, stirred, makes three
Person is sufficiently mixed as white gum object, obtains negative oxygen ion function auxiliary agent.
In the step, mixing time is not less than 1 hour, 800 revs/min of stirring rate, does not have sediment within static 24 hours
For qualification.
Negative oxygen ion function powder, neutral water soluble auxiliary agent and the heavy portion rate of resin three are (3-5): (20-30):
(80-92)。
The following are typical specific embodiments:
Specific embodiment 1.
Negative oxygen ion function powder, 5；
Neutral water soluble auxiliary agent, 30；
Resin, 80.
Specific embodiment 2.
Negative oxygen ion function powder, 5；
Neutral water soluble auxiliary agent, 30；
Resin, 80.
Specific embodiment 3.
Negative oxygen ion function powder, 4；
Neutral water soluble auxiliary agent, 26；
Resin, 85.
Specific embodiment 4.
Negative oxygen ion function powder, 4；
Neutral water soluble auxiliary agent, 28；
Resin, 83.
Specific embodiment 5.
Negative oxygen ion function powder, 3；
Neutral water soluble auxiliary agent, 20；
Resin, 92.
Specific embodiment 6.
Negative oxygen ion function powder, 5；
Neutral water soluble auxiliary agent, 22；
Resin, 88.
In the above scheme, ion adsorption type rare earth ore stone is also known as weathering crust remnants type Rare Earth Mine, is containing rare earth granite
Or volcanic rock forms clay mineral through many years weathering, the rare earth ion dissociateed is adsorbed on hydrated ion or hydroxyl hydrated ion
On clay mineral.Ore is mostly in hilly country, and for loose husky clay, color has white, grey, red, yellow.Density is
2.0~2.5g/cm3.Rare earth element 80%~90% in ore is adsorbed on kaolin, galapectite and water cloud in ionic condition
On the clay minerals such as mother；The rare-earth cation being adsorbed on clay mineral is not soluble in water or ethyl alcohol, but in strong electrolytic solution
Ion exchange can occur and enter solution and there is reversible reaction.It is mainly distributed on China Jiangxi, Guangdong, Hunan, Guangxi, Fujian
Etc. ground.
Ion adsorption type rare earth ore stone contains rare earth element, rare earth element due to itself energy with higher, with sky
It, can be with inducing negative air ion when gas contacts.In addition, the complex salt in rare earth also has the function of the molecular ionization in air
Can, to increase the concentration of anion in air.However, rare earth element also has stronger radioactivity simultaneously, human body can be made
At certain injury.Therefore, negative oxygen ion occurring source in the prior art is all that the additions such as tourmaline, Tourmaline stone are a small amount of
Rare earth progress is composite modified, and still, the exceeded problem of radioactive radiation can not efficiently solve always.
In the application, ion adsorption type rare earth ore stone is extracted by using middle strong acidity extractant, keeps penetrating property first
The removal rate of element reaches 80% or more, thus, application scheme directly can induce negative oxygen ion using rare earth, without making again
With other raw materials such as tourmaline, Tourmaline stones, reduces the type selecting and dosage of raw material, simplify production technology, reduce costs.
The present invention also provides a kind of production methods of woodcare paint for inducing negative oxygen ion, as shown in Fig. 2, including following step
It is rapid:
Step 210: woodcare paint is prepared using mixing method.
By woodenware raw materials for varnish such as alkyd based resin or acrylic emulsion, with water and other additive dispersion and emulsions, preparation
Woodcare paint.
Step 220: step 150 is added into woodcare paint in proportion and is made for the density of the woodcare paint according to made from step 210
Negative oxygen ion function auxiliary agent.
The brushing surface painted and brushing technique and the brushing number of plies are considered, in the woodcare paint that density is 1:1.15~1.2
In, 2% negative oxygen ion function auxiliary agent is added, so that every square metre of brushing weight in 0.08KG, is brushed or one liang of spraying
It is secondary to be advisable；
In the woodcare paint that density is 1:1.25~1.35, the brushing surface painted and brushing technique and brush are considered
Number, adds 3.5% negative oxygen ion function auxiliary agent.So that every square metre of brushing weight in 0.15KG, is brushed or spraying one
It is advisable twice.
In the woodcare paint that density is 1:1.4~1.5, the brushing surface painted and brushing technique and brush are considered
Number, adds 4% negative oxygen ion function auxiliary agent.So that every square metre of brushing weight in 0.23KG, is brushed or one liang of spraying
It is secondary to be advisable.
The woodcare paint produced according to the method described above, can be under air vibration effect, and into space, constantly ionization is induced
Negative oxygen ion, according to detection, the amount of inducing of woodcare paint is 1200-2500/cubic centimetre, can effectively improve living environment,
Ensure people's respiratory health.Meanwhile negative oxygen ion function auxiliary agent and woodcare paint are simple physical mixed, and it is anti-that chemistry does not occur
It answers, the original quality of woodcare paint will not be changed, there is stable characteristic.
The existing material for inducing negative oxygen ion or fabric production technology are usually all that negative oxygen ion function powder is direct
Addition uses, and such usage mode, the wellability and adhesion of negative oxygen ion function powder are lower, therefore, the production produced
The amount of inducing of product, negative oxygen ion is relatively low.
In application scheme, negative oxygen ion function powder, neutral water soluble auxiliary agent are mixed with resin first, stirred, is made
Three is sufficiently mixed as white gum object, obtains negative oxygen ion function auxiliary agent.Then in subsequent production technology, using negative
Oxonium ion function additive, rather than negative oxygen ion function powder is directly used, due to have passed through and neutral water soluble auxiliary agent and tree
The viscosity of rouge and mixed processing, negative oxygen ion function auxiliary agent increases, and the dispersibility and suspension of negative oxygen ion function powder are more preferable,
Therefore the wellability on product and adhesion greatly improve, to substantially increase the amount of inducing of negative oxygen ion and use the longevity
Life.
In addition, silica used in the prior art, usually untreated decrystallized silica, this two
Raw silicon oxide material, either sedimentation prepare or vapor phase method prepares, and product all can be weakly acidic, containing few
The mensuration dissolubility silicic of amount.In this way, the negative oxygen ion function powder prepared can make solution in weak after being added in solution
Acidity, regardless of being material producing process or fabric production technology, faintly acid can all generate certain influence to product quality,
And the ionization that can reduce finished material, reduces the amount of inducing of negative oxygen ion.
And application scheme, it has carried out heat treatment first for starting silica, has reduced solvable in silica
The content of property silicic acid, guarantees that auxiliary agent is in neutrality, to improve the quality of negative oxygen ion function auxiliary agent, ensure that product can be steady
Surely negative oxygen ion continuously is induced to space ionization.
The production method of the woodcare paint provided by the invention for inducing negative oxygen ion, has the advantages that following prominent:
(1) using magnesium silicate, rich magnesium silicate, ion adsorption type rare earth ore stone and silica as primary raw material, raw material at
This is low, and the amount of inducing of negative oxygen ion is big, and radiant quantity is low.
(2) manufacture craft is simple, simplifies raw material type, reduces production cost.
(3) the negative oxygen ion woodcare paint produced using the method for the present invention can be induced continuously to space ionization
Negative oxygen ion, the amount of inducing are 1200-2500/cm3, people's lives space can be improved, purify air and environment.
The invention is not limited to above-mentioned preferred forms, and anyone should learn that is made under the inspiration of the present invention
Structure change, the technical schemes that are same or similar to the present invention are fallen within the scope of protection of the present invention.
Claims (9)
1. a kind of production method of negative oxygen ion function powder, which comprises the following steps:
Ion adsorption type rare earth ore stone, rich magnesium fibrous silicate and hydrous magnesium silicate are baked into drying；
The rich magnesium fibrous silicate and ion adsorption type rare earth ore stone that bake after drying are extracted using acidic extractant,
High-temperature baking is carried out after extraction, removes radioactive element；
Amorphous silica is heated, soluble silicon acid content therein is reduced；
By hydrous magnesium silicate of the baking after dry, the rich magnesium fibrous silicate after removal radioactive element and ionic adsorption
Type rare earth ore and silica are crushed and are uniformly mixed, and obtain negative oxygen ion function powder.
2. the method according to claim 1, wherein the hydrous magnesium silicate, rich magnesium fibrous silicate, ion
The weight fraction ratio of absorbent-type rare earth ore and silica is 3:(3-6): (4-8): (1-2.5).
3. the method according to claim 1, wherein the hydrous magnesium silicate, rich magnesium fibrous silicate, ion
The weight fraction ratio of absorbent-type rare earth ore and silica is 3:6:5:1.
4. the method according to claim 1, wherein the negative oxygen ion function powder is helped with neutral water soluble
Agent and resin mixing, stirring, are sufficiently mixed three as white gum object, obtain negative oxygen ion function auxiliary agent, the weight of three
Measuring portion rate is (3-5): (20-30): (80-92).
5. the method according to claim 1, wherein in the silica of lenticular, soluble silicon acid content is
30% or less.
6. the method according to claim 1, wherein using acidic extractant to the rich magnesium fiber after baking drying
When shape silicate and ion adsorption type rare earth ore stone are extracted, the quality of acidic extractant used is rich magnesium fibrous silicate
With 3-5 times of ion adsorption type rare earth ore stone quality sum, and the concentration of acidic extractant be 5-15wt%.
7. the method according to claim 1, wherein extraction after, rich magnesium fibrous silicate and ion type
The removal rate of radioactive element in rare earth ore is 80% or more.
8. a kind of production method for the woodcare paint for inducing negative oxygen ion, which comprises the following steps:
Mixing method prepares woodcare paint；
According to the density of the woodcare paint of preparation, negative oxygen ion function obtained by the above method is added into woodcare paint obtained and helps
Agent.
9. according to the method described in claim 8, it is characterized in that, density is the woodcare paint of 1:1.15~1.2, negative oxygen ion function
The weight ratio of energy auxiliary agent addition is 2%；Density is the woodcare paint of 1:1.25~1.35, the weight of negative oxygen ion function auxiliary agent addition
Amount ratio is 3.5%；Density is the woodcare paint of 1:1.4~1.5, and the weight ratio of negative oxygen ion function auxiliary agent addition is 4%.
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| CN110396324A (en) * | 2019-09-12 | 2019-11-01 | 河北森雅环保新材料科技有限公司 | The production method for inducing the water paint and its functional powders and auxiliary agent of negative oxygen ion |
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Application publication date: 20191203 |