CN110501284A - A device and method for testing the bonding strength of composite pipes under thermal loading conditions - Google Patents

A device and method for testing the bonding strength of composite pipes under thermal loading conditions Download PDF

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CN110501284A
CN110501284A CN201910815840.6A CN201910815840A CN110501284A CN 110501284 A CN110501284 A CN 110501284A CN 201910815840 A CN201910815840 A CN 201910815840A CN 110501284 A CN110501284 A CN 110501284A
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insulation box
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王守泽
徐滨士
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Beijing University of Technology
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N19/00Investigating materials by mechanical methods
    • G01N19/04Measuring adhesive force between materials, e.g. of sealing tape, of coating

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Abstract

一种测试热加载条件下复合管结合强度的装置及方法,属于复合管结合强度性能测试技术领域。包括高强度承压框架、压力系统、加热保温箱、可调节支架;压力系统固定在高强度承压框架内;变径压头插入加热保温箱,将待测试的复合管放置于变径压头上,变径压头的上端面只与待测试复合管的内管下端面接触,加热保温箱箱体高度与测试管段上端面基本平齐,盖上加热保温箱上盖,加热保温箱上盖与高强度框架接触,加热保温箱上盖的下表面只与待测试复合管的外管上端面接触;打开加热保温箱电源,升温至所需的测试温度,温度稳定后保温,加载压力,观察压力变化,当压力达到最大值开始明显下降时,说明复合管已经发生了剪切破坏,记录此过程的压力值。The invention relates to a device and method for testing the bonding strength of composite pipes under thermal loading conditions, belonging to the technical field of bonding strength performance testing of composite pipes. Including high-strength pressure-bearing frame, pressure system, heating insulation box, and adjustable bracket; the pressure system is fixed in the high-strength pressure-bearing frame; the variable-diameter indenter is inserted into the heating insulation box, and the composite pipe to be tested is placed on the variable-diameter indenter The upper end surface of the variable diameter indenter is only in contact with the lower end surface of the inner tube of the composite pipe to be tested. The height of the heating insulation box is basically the same as the upper end surface of the test pipe section. In contact with the high-strength frame, the lower surface of the upper cover of the heating insulation box is only in contact with the upper end surface of the outer tube of the composite pipe to be tested; turn on the power supply of the heating insulation box, raise the temperature to the required test temperature, keep warm after the temperature is stable, load the pressure, and observe Pressure changes. When the pressure reaches the maximum value and begins to drop significantly, it indicates that the composite pipe has undergone shear failure, and the pressure value of this process is recorded.

Description

一种测试热加载条件下复合管结合强度的装置及方法A device and method for testing the bonding strength of composite pipes under thermal loading conditions

技术领域technical field

本发明涉及复合管结合强度性能测试技术领域,特别涉及一种测试热加载条件下复合管结合强度的装置及方法。The invention relates to the technical field of composite pipe bonding strength performance testing, in particular to a device and method for testing the bonding strength of composite pipes under thermal loading conditions.

背景技术Background technique

复合管是由两种或两种以上不同性能的材料构成的具有双层或者多层结构的复合管材,工程应用中可以根据应用的环境和对管材的性能要求进行复合管材料体系和生产工艺的选择和设计,能够最大限度地实现材料的优势互补,在保证管道基本性能的基础上,提高管道的耐腐蚀性,延长管道的使用寿命,降低工程费用,往往能够替代纯不锈钢管、铜管或其他昂贵的合金管。目前各种复合管已在石油开发、化工、冶金、船舶、矿山、军工等领域取得大量应用。The composite pipe is a composite pipe with a double-layer or multi-layer structure composed of two or more materials with different properties. In engineering applications, the material system and production process of the composite pipe can be selected according to the application environment and the performance requirements of the pipe. The selection and design can maximize the complementary advantages of materials. On the basis of ensuring the basic performance of the pipeline, it can improve the corrosion resistance of the pipeline, prolong the service life of the pipeline, and reduce the engineering cost. It can often replace pure stainless steel pipes, copper pipes or Other expensive alloy tubes. At present, various composite pipes have been widely used in petroleum development, chemical industry, metallurgy, shipbuilding, mining, military industry and other fields.

结合强度是评价复合管性能的最重要的一项技术指标。目前,在不同类别的复合管的相关标准中已经给出了结合强度的具体要求和测试方法,比如在GB/T28897《钢塑复合管》,SY/T 6855《含H2S/CO2天然气田集输管网用双金属复合管》,SY/T 6662.8-2016《陶瓷内衬管及管件》等标准中均对复合管的结合强度做了要求并给出了试验的示意图。这些标准都是对室温下的复合管的结合强度进行要求,忽略了温度对由不同热膨胀系数材料体系构成的复合管造成的结合强度的影响,对指导复合管在热加载工况下的应用存在不足之处,易造成生产事故和安全隐患。Bonding strength is the most important technical index for evaluating the performance of composite pipes. At present, the specific requirements and test methods for the bonding strength have been given in the relevant standards of different types of composite pipes, such as in GB/T28897 "Steel-Plastic Composite Pipes", SY/T 6855 "Containing H 2 S/CO 2 Natural Gas Bimetal Composite Pipes for Field Gathering Pipeline Networks", SY/T 6662.8-2016 "Ceramic Lined Pipes and Fittings" and other standards have made requirements for the bonding strength of composite pipes and given a schematic diagram of the test. These standards all require the bonding strength of composite pipes at room temperature, ignoring the influence of temperature on the bonding strength of composite pipes composed of material systems with different thermal expansion coefficients, which have problems in guiding the application of composite pipes under thermal loading conditions. Inadequacies can easily cause production accidents and hidden safety hazards.

发明内容Contents of the invention

为解决上述不足,本发明提供了一种能够测试热加载条件下复合管结合强度的实验装置及方法,实验方法简单,实验装置结构简单、操作灵活、测试快速直观。In order to solve the above shortcomings, the present invention provides an experimental device and method capable of testing the bonding strength of composite pipes under thermal loading conditions. The experimental method is simple, the experimental device has simple structure, flexible operation, and quick and intuitive testing.

为达到上述目的,本发明通过以下技术方案实现:In order to achieve the above object, the present invention is achieved through the following technical solutions:

一种测试热加载条件下复合管结合强度的装置,分为四个部分:高强度承压框架(1),压力系统(2),加热保温箱(3),可调节支架(4);A device for testing the bonding strength of composite pipes under thermal loading conditions, which is divided into four parts: a high-strength pressure-bearing frame (1), a pressure system (2), a heating insulation box (3), and an adjustable support (4);

高强度承压框架(1)用于承受整个测试系统的负载,高强度承压框架为箱体结构,上部开有通孔(1-2),用于观察实验过程,还可用于调整试样位置;The high-strength pressure-bearing frame (1) is used to bear the load of the entire test system. The high-strength pressure-bearing frame is a box structure with through holes (1-2) on the upper part for observing the experimental process and also for adjusting the sample. Location;

压力系统(2)底部固定在高强度承压框架1内的底部部,用于产生和输出测试结合强度的压力;压力系统自上而下依次包括部件变径压头(2-2)、压头(2-3)、能施加压力的缸体(2-4)、底座(2-5),底座(2-5)固定在压力系统2的底部上,缸体(2-4)设有高精度数字显示压力表(2-6)及加载控制器(2-7);变径压头(2-2)为圆柱结构,上部端面直径相对较小,下部端面直径相对较大,根据复合管尺寸选取合适的变径压头尺寸,其上部端面直接与复合管试件的内管端面接触,用于对内管加载压力,变径压头(2-2)下部端面设有圆柱形引导面凹槽(2-8),用于与圆柱形的压头(2-3)稳定配合;圆柱形的压头(2-3)顶部与变径压头的圆柱形引导面凹槽(2-8)配合,用于传导压力到试件,压头(2-3)顶部与变径压头接触的结合面处设有隔热垫片(2-9),用于降低热量损失,降低传递到压力系统的热量,保护压力系统;高精度数字显示压力表(2-6),用于快速直观的读取压力系统传递的压力数值,其读数单位为MPa、Psi、KN等。The bottom of the pressure system (2) is fixed on the bottom part of the high-strength pressure-bearing frame 1, and is used to generate and output the pressure for testing the bonding strength; Head (2-3), cylinder body (2-4) capable of applying pressure, base (2-5), base (2-5) is fixed on the bottom of pressure system 2, and cylinder body (2-4) is provided with High-precision digital display pressure gauge (2-6) and loading controller (2-7); variable diameter pressure head (2-2) is a cylindrical structure, the diameter of the upper end face is relatively small, and the diameter of the lower end face is relatively large Select the appropriate size of the variable diameter indenter for the pipe size, and its upper end surface is directly in contact with the inner tube end surface of the composite pipe test piece, which is used to apply pressure to the inner tube. The lower end surface of the variable diameter indenter (2-2) is provided with a cylindrical guide Surface groove (2-8), used for stable cooperation with cylindrical indenter (2-3); the top of cylindrical indenter (2-3) and the cylindrical guide surface groove (2 -8) Fitting, used to transfer pressure to the test piece, heat insulating gasket (2-9) is provided at the joint surface where the top of the indenter (2-3) is in contact with the variable diameter indenter, to reduce heat loss and reduce The heat transmitted to the pressure system protects the pressure system; the high-precision digital display pressure gauge (2-6) is used to quickly and intuitively read the pressure value transmitted by the pressure system, and the reading unit is MPa, Psi, KN, etc.

加热保温箱(3)位于高强度承压框架(1)内部上端,用于将待测试复合管段加热至指定温度,并在此温度下完成测试;包括加热保温箱箱体(3-2)、加热元件(3-3)、隔热保温层(3-4)、加热保温箱上盖(3-5)、温度传感器(3-6)、数字显示温度计及控温装置(3-7),加热保温箱电源(3-8);加热保温箱箱体(3-2)用于承载加热保温箱的其它部件,加热保温箱箱体(3-2)下部置于在可调节支架(4)上,用于固定加热保温箱,可调节支架(4)位于高强度承压框架(1)内;隔热保温层(3-4)设置在加热保温箱箱体内表面,用于防止热量散失,保持箱体内部温度;加热元件(3-3)位于加热保温箱箱体(3-2)内部用于加温;加热保温箱上盖(3-5)采样上盖连接销(3-10)与加热保温箱箱体上端口进行配合,加热保温箱上盖(3-5)上表面与高强度承压框架贴合,用于承载测试时试样上部外层管端面产生的压力,加热保温箱上盖(3-5)开有通孔(3-13),不同尺寸的试样选择不同通孔尺寸的加热保温箱上盖,加热保温箱上盖通孔(3-13)处设有隔热保温的通孔塞(3-11),用于密封上盖,避免热量损失;加热保温箱箱体(3-2)内设有温度传感器(3-6),数字显示温度计及自动控温装置(3-7)与温度传感器(3-6)和加热元件(3-3)连接和配合,用于直观的读取加热保温箱内的温度,当温度达到设定温度时,控温装置控制加热元件自动断电,温度降低时自动加热,保证箱内温度恒定;The heating insulation box (3) is located at the upper end of the high-strength pressure-bearing frame (1), and is used to heat the composite pipe section to be tested to a specified temperature, and complete the test at this temperature; it includes the heating insulation box body (3-2), heating element (3-3), heat insulation layer (3-4), heating insulation box upper cover (3-5), temperature sensor (3-6), digital display thermometer and temperature control device (3-7), Heating and incubating box power supply (3-8); heating and incubating box body (3-2) is used to carry other parts of heating and incubating box, and the lower part of heating and incubating box body (3-2) is placed on adjustable support (4) On the top, it is used to fix the heating and incubating box. The adjustable bracket (4) is located in the high-strength pressure-bearing frame (1); the heat insulation layer (3-4) is arranged on the inner surface of the heating and incubating box to prevent heat loss. Maintain the internal temperature of the box; the heating element (3-3) is located inside the heating incubator box (3-2) for heating; the upper cover of the heating incubator (3-5) samples the upper cover connection pin (3-10) Cooperate with the upper port of the heating and incubating box, and the upper surface of the heating and incubating box (3-5) is attached to the high-strength pressure-bearing frame, which is used to bear the pressure generated by the end surface of the upper outer layer of the sample during the test, heating and insulating The upper cover of the box (3-5) has a through hole (3-13). For samples of different sizes, choose the upper cover of the heating and incubating box with different through hole sizes. The through-hole plug (3-11) of heat insulation is used for sealing the upper cover to avoid heat loss; the heating insulation box body (3-2) is provided with a temperature sensor (3-6), a digital display thermometer and an automatic control The temperature device (3-7) is connected and cooperated with the temperature sensor (3-6) and the heating element (3-3), and is used for visually reading the temperature in the heating incubator. When the temperature reaches the set temperature, the temperature control The device controls the heating element to automatically cut off the power, and automatically heats up when the temperature drops to ensure a constant temperature in the box;

所述加热保温箱3底部开有通孔(3-12),用于变径压头上端伸入到加热保温箱内;通孔(3-12)内侧壁设有一层柔性隔热保温材料(3-9),用于密封变径压头与加热保温箱体的间隙,柔性隔热保温材料应能适应不同变径压头的尺寸,防止热量从变径压头与孔的间隙散失,并且不会影响测试结果;The bottom of the heating insulation box 3 has a through hole (3-12), which is used for the upper end of the variable diameter pressure head to extend into the heating insulation box; the inner wall of the through hole (3-12) is provided with a layer of flexible heat insulation material ( 3-9), used to seal the gap between the variable-diameter indenter and the heating insulation box, the flexible thermal insulation material should be able to adapt to the size of different variable-diameter indenters, to prevent heat from being lost from the gap between the variable-diameter indenter and the hole, and will not affect the test results;

高强度承压框架(1)上部设有通孔,高强度承压框架(1)上部的通孔直径不小于加热保温箱上盖通孔(3-13)且两者同轴;加热保温箱上盖通孔(3-13)的直径大于待测复合管的外管内直径小于外管外直径;变径压头(2-2)上部端面直径大于待测复合管的内管内直径小于内管外直径。The upper part of the high-strength pressure-bearing frame (1) is provided with a through hole, and the diameter of the through-hole on the upper part of the high-strength pressure-bearing frame (1) is not smaller than the through hole (3-13) on the upper cover of the heating and incubating box, and the two are coaxial; the heating and incubating box The diameter of the upper cover through hole (3-13) is larger than the inner diameter of the outer tube of the composite tube to be tested and smaller than the outer diameter of the outer tube; Outer diameter.

可调节支架4固定在高强度承压框架1内部,用于以可调节高度的方式支撑和固定加热保温箱(3)。The adjustable bracket 4 is fixed inside the high-strength pressure-bearing frame 1, and is used to support and fix the heating and incubating box (3) in a height-adjustable manner.

压头(2-3)用于调节高度,缸体(2-4)为能够沿变径压头(2-2)轴线方向持续增加压力装置。The pressure head (2-3) is used to adjust the height, and the cylinder body (2-4) is a device capable of continuously increasing the pressure along the axial direction of the variable diameter pressure head (2-2).

实验方法如下:压力系统固定在高强度承压框架内,根据待测试的复合管尺寸选择适用的变径压头;通过加热保温箱下孔将变径压头插入加热保温箱,将待测试的复合管放置于变径压头上并调整好,使得变径压头与待测试的复合管同轴,变径压头的上端面只与待测试复合管的内管下端面接触,调整加热保温箱支架高度使加热保温箱箱体高度与测试管段上端面基本平齐,盖上加热保温箱上盖,上盖固定销嵌入销孔内,缓慢升高压力系统的压头高度,至加热保温箱上盖与高强度框架轻轻接触,同时加热保温箱上盖的下表面只与待测试复合管的外管上端面接触;调整加热保温箱支架高度使其支撑加热保温箱;打开加热保温箱电源,匀速升温至所需的测试温度,温度稳定后保温15-30分钟,压力系统开始缓慢向上加载压力,观察压力变化,当压力达到最大值开始明显下降时,说明复合管已经发生了剪切破坏,记录此过程的压力值,通过最大值计算复合管的结合力。The experimental method is as follows: the pressure system is fixed in a high-strength pressure-bearing frame, and the applicable variable-diameter indenter is selected according to the size of the composite pipe to be tested; the variable-diameter indenter is inserted into the heating incubator through the lower hole of the heating incubator, and the test The composite pipe is placed on the variable-diameter indenter and adjusted so that the variable-diameter indenter is coaxial with the composite pipe to be tested, and the upper end surface of the variable-diameter indenter is only in contact with the lower end surface of the inner tube of the composite pipe to be tested. Adjust the heating and heat preservation The height of the box support makes the height of the heating and incubating box basically flush with the upper end surface of the test pipe section. Cover the heating and incubating box, and insert the fixing pin of the upper cover into the pin hole. Slowly increase the height of the pressure head of the pressure system to the heating and incubating box. The upper cover is in light contact with the high-strength frame, and at the same time, the lower surface of the upper cover of the heating incubator is only in contact with the upper end surface of the outer tube of the composite tube to be tested; adjust the height of the bracket of the heating incubator to support the heating incubator; turn on the power of the heating incubator , heat up to the required test temperature at a uniform speed, keep the temperature stable for 15-30 minutes, the pressure system begins to slowly increase the pressure, observe the pressure change, when the pressure reaches the maximum value and begins to drop obviously, it means that the composite pipe has shear damage , record the pressure value of this process, and calculate the binding force of the composite pipe through the maximum value.

所述压力系统压头经过热处理工艺,获得较高的硬度和韧性,确保施压过程中不会变形和破裂。The pressure head of the pressure system has undergone a heat treatment process to obtain high hardness and toughness, so as to ensure that it will not be deformed and broken during the pressure application process.

所述压力系统安装有高精度数字显示压力表,能够快速直观的读取压力数值,压力表可以调整读数单位为MPa、Psi、KN等,满足不同读数需求。The pressure system is equipped with a high-precision digital display pressure gauge, which can quickly and intuitively read the pressure value. The pressure gauge can be adjusted to MPa, Psi, KN, etc. to meet different reading requirements.

所述变径压头可以根据复合管尺寸选取,变径压头底部设有圆柱形引导面,保证变径压头与压头的稳定配合,确保实验的准确性。The variable-diameter indenter can be selected according to the size of the composite pipe. The bottom of the variable-diameter indenter is provided with a cylindrical guide surface to ensure the stable cooperation between the variable-diameter indenter and the indenter, and to ensure the accuracy of the experiment.

所述压头顶部与变径压头接触的结合面设有隔热垫片,降低保温箱的热量损失,保护压力系统。The junction surface of the top of the indenter in contact with the variable diameter indenter is provided with a thermal insulation gasket to reduce the heat loss of the incubator and protect the pressure system.

所述加热保温箱设有自动控温装置,内部设有加热元件,箱内设有温度传感器,当温度达到设定温度时,加热元件自动断电,温度降低时自动加热,保证箱内温度恒定。The heating and incubating box is equipped with an automatic temperature control device, a heating element is installed inside, and a temperature sensor is installed inside the box. When the temperature reaches the set temperature, the heating element is automatically powered off, and it is automatically heated when the temperature drops to ensure a constant temperature in the box. .

所述加热保温箱温度可在室温至1000℃内调节,涵盖目前工程应用的绝大部分工况条件。The temperature of the heating and incubating box can be adjusted from room temperature to 1000°C, covering most of the working conditions of current engineering applications.

所述加热保温箱设有数字显示温度计,可以直观的读取箱内的温度。The heating and incubating box is provided with a digital display thermometer, which can intuitively read the temperature in the box.

所述加热保温箱设有销连接的活动上盖,方便安装测试管段及设备维修,上盖开有通孔,并配套隔热保温的通孔塞,上盖通孔的尺寸与测试管段密切相关,不同的测试管段要选择不同的上盖。The heating and incubating box is equipped with a pin-connected movable upper cover, which is convenient for installing test pipe sections and equipment maintenance. The upper cover has a through hole, and is equipped with a through hole plug for heat insulation. The size of the through hole of the upper cover is closely related to the test pipe section. , Different test pipe sections should choose different upper covers.

所述加热保温箱内壁设有一层隔热保温材料,避免箱内热量损失。The inner wall of the heating and incubating box is provided with a layer of thermal insulation material to avoid heat loss in the box.

所述加热保温箱底部开有通孔,孔内壁设有一层柔性隔热保温材料,能够适应不同变径压头的尺寸,防止热量从变径压头与孔的间隙散失,并且不会影响测试结果。There is a through hole at the bottom of the heating and incubating box, and a layer of flexible heat insulation material is provided on the inner wall of the hole, which can adapt to the size of different indenters, prevent heat loss from the gap between the indenter and the hole, and will not affect the test result.

所述高强度承压框架采用高强度合金钢焊接而成,能承受较大压力不变形。The high-strength pressure-bearing frame is welded by high-strength alloy steel, which can withstand relatively large pressure without deformation.

所述加热保温箱支架能够任意调节高度,为加热保温箱提供稳定支撑。The height of the heating and incubating box support can be adjusted arbitrarily to provide stable support for the heating and incubating box.

所述高强度承压框架采用高强度合金钢焊接而成,能承受较大压力不变形。The high-strength pressure-bearing frame is welded by high-strength alloy steel, which can withstand relatively large pressure without deformation.

所述压力系统压头(2-3)与变径压头(2-2)配合用于传递测试压力,需经过热处理等工艺处理,用以获得较高的硬度和韧性。The pressure system indenter (2-3) cooperates with the variable diameter indenter (2-2) to transmit test pressure, and needs to undergo heat treatment and other processes to obtain higher hardness and toughness.

本发明的有益效果如下:The beneficial effects of the present invention are as follows:

1.本发明测试方法充分考虑到了复合管材的实际应用工况,测试结果对于指导复合管材的工程应用具有现实意义。1. The test method of the present invention has fully considered the actual application conditions of the composite pipe, and the test results have practical significance for guiding the engineering application of the composite pipe.

2.本发明温度控制范围大,覆盖目前工程应用的绝大部分工况条件。2. The temperature control range of the present invention is large, covering most of the working conditions of current engineering applications.

3.本发明填补了热加载条件下复合管结合强度测试的空白。3. The present invention fills up the gap in the bond strength test of composite pipes under thermal loading conditions.

附图说明Description of drawings

附图1是测试热加载条件下复合管结合强度装置的结构示意图Accompanying drawing 1 is the structural schematic diagram of the device for testing the bonding strength of composite pipes under thermal loading conditions

附图2是高强度承压框架俯视图Accompanying drawing 2 is the top view of the high-strength pressure-bearing frame

附图3是未安装管件的加热保温箱俯视图Accompanying drawing 3 is the top view of the heating insulation box without pipe fittings

1.高强度承压框架;1-2.承压框架通孔;2.压力系统;2-2.变径压头;2-3.压头;2-4.缸体;2-5.底座;2-6.高精度数字显示压力表;2-7.加载控制器;2-8.圆柱形引导面凹槽;2-9.隔热垫片;3.加热保温箱;3-2.加热保温箱箱体;3-3.加热元件;3-4.隔热保温层;3-5.加热保温箱上盖;3-6.温度传感器;3-7.温度计及控温装置;3-8.加热保温箱电源;3-9.柔性保温隔热材料;3-10.上盖连接销;3-11.上盖保温通孔塞;3-12.加热保温箱下通孔;3-13.加热保温箱上通孔;4.可调节支架;5.测试复合管段外管(层);6.测试复合管段内管(层)。1. High-strength pressure bearing frame; 1-2. Through hole of pressure bearing frame; 2. Pressure system; 2-2. Variable diameter pressure head; 2-3. Pressure head; 2-4. Cylinder body; 2-5. Base; 2-6. High-precision digital display pressure gauge; 2-7. Loading controller; 2-8. Cylindrical guide surface groove; 2-9. Heat insulation gasket; 3. Heating insulation box; 3-2 .Heating insulation box body; 3-3. Heating element; 3-4. Heat insulation layer; 3-5. Heating insulation box upper cover; 3-6. Temperature sensor; 3-7. Thermometer and temperature control device; 3-8. Power supply for heating and incubating box; 3-9. Flexible thermal insulation material; 3-10. Upper cover connection pin; 3-11. Upper cover insulation through hole plug; 3-13. Through hole on the heating insulation box; 4. Adjustable bracket; 5. Test the outer tube (layer) of the composite pipe section; 6. Test the inner pipe (layer) of the composite pipe section.

具体实施方式Detailed ways

下面结合附图和具体实施方式对本发明做进一步说明。The present invention will be further described below in conjunction with the accompanying drawings and specific embodiments.

如图1所示,本发明采用的试验装置包括高强度承压框架1;压力系统2,具体包括变径压头2-2、压头2-3、缸体2-4、底座2-5、高精度数显压力表2-6、加载控制器2-7、隔热垫片2-9;加热保温箱3,具体包括加热保温箱箱体3-2、加热元件3-3、隔热保温层3-4、加热保温箱上盖3-5、温度传感器3-6、温度计及控温装置3-7、加热保温箱电源3-8、、柔性保温隔热材料3-9、上盖连接销3-10、上盖保温通孔塞3-11;可调节支架4等组成。As shown in Figure 1, the test device adopted in the present invention includes a high-strength pressure-bearing frame 1; a pressure system 2, specifically including a variable-diameter indenter 2-2, an indenter 2-3, a cylinder body 2-4, and a base 2-5 , high-precision digital display pressure gauge 2-6, loading controller 2-7, heat insulation gasket 2-9; heating insulation box 3, specifically including heating insulation box body 3-2, heating element 3-3, heat insulation Insulation layer 3-4, heating insulation box upper cover 3-5, temperature sensor 3-6, thermometer and temperature control device 3-7, heating insulation box power supply 3-8, flexible thermal insulation material 3-9, upper cover Connecting pin 3-10, loam cake insulation through-hole plug 3-11; Adjustable support 4 etc. are formed.

高强度承压框架1用于承受整个测试系统的负载,承压框架上部开有通孔1-2,用于观察实验过程,还可用于调整试样位置。压力系统2底部固定在高强度承压框架1下部,用于产生和输出测试结合强度的压力。根据测试试件的参数选择适用的变径压头2-2;通过加热保温箱下孔3-12将变径压头2-2插入加热保温箱3内,将测试复合管段放置于变径压头2-2上并调整好测试管段中心,调整可调节支架4高度使加热保温箱箱体3-2高度与测试管段上端面基本平齐,盖上加热保温箱上盖3-5,上盖固定销3-10嵌入销孔内,缓慢升高压头2-3高度,至加热保温箱上盖3-5与高强度框架1轻轻接触,调整可调节支架4高度使其支撑加热保温箱;打开加热保温箱电源3-8,升温至所需的测试温度,温度稳定后保温15-30分钟,控制加载控制器2-7开始缓慢加载,观察压力表2-6读数变化,当压力达到最大值并突然下降时,说明复合管已经发生了剪切破坏,记录此过程的压力值。The high-strength pressure-bearing frame 1 is used to bear the load of the whole test system, and the upper part of the pressure-bearing frame is provided with through holes 1-2, which are used for observing the experiment process and can also be used for adjusting the position of the sample. The bottom of the pressure system 2 is fixed on the lower part of the high-strength pressure-bearing frame 1, and is used to generate and output pressure for testing the bonding strength. Select the applicable variable-diameter indenter 2-2 according to the parameters of the test piece; insert the variable-diameter indenter 2-2 into the heating incubator 3 through the lower hole 3-12 of the heating incubator, and place the test composite pipe section in the variable-diameter indenter. Put on the head 2-2 and adjust the center of the test pipe section, adjust the height of the adjustable bracket 4 so that the height of the heating incubator box 3-2 is basically flush with the upper end surface of the test pipe section, cover the heating incubator cover 3-5, the upper cover The fixed pin 3-10 is embedded in the pin hole, and the height of the pressure head 2-3 is slowly raised until the upper cover 3-5 of the heating insulation box is in light contact with the high-strength frame 1, and the height of the adjustable bracket 4 is adjusted to support the heating insulation box; Turn on the power supply 3-8 of the heating and incubating box, raise the temperature to the required test temperature, keep it warm for 15-30 minutes after the temperature is stable, control the loading controller 2-7 to start loading slowly, observe the changes in the readings of the pressure gauge 2-6, when the pressure reaches the maximum When the value drops suddenly, it indicates that the composite pipe has undergone shear failure, and the pressure value of this process is recorded.

所述压力系统2包括变径压头2-2、压头2-3、缸体2-4、底座2-5、及高精度数显压力表2-6及加载控制器2-7。The pressure system 2 includes a variable-diameter pressure head 2-2, a pressure head 2-3, a cylinder body 2-4, a base 2-5, a high-precision digital display pressure gauge 2-6, and a loading controller 2-7.

所述压力系统2中的变径压头2-2及压头2-3用于直接对测试试样加载压力,要进行相应处理,获得高硬度和高韧性,确保施压过程中不会变形和破裂。The variable-diameter indenter 2-2 and indenter 2-3 in the pressure system 2 are used to directly apply pressure to the test sample, and corresponding treatment should be carried out to obtain high hardness and high toughness, so as to ensure that it will not be deformed during the pressure application process and burst.

所述压力系统2中的高精度数字显示压力表2-6,用于快速直观的读取压力数值,压力表可以调整读数单位为MPa、Psi、KN等,满足不同读数需求,还可通过压力值、压头的面积等参数,实现不同单位数值的换算,以满足不同的计算需求。The high-precision digital display pressure gauge 2-6 in the pressure system 2 is used to read the pressure value quickly and intuitively. The pressure gauge can adjust the reading unit to MPa, Psi, KN, etc. to meet different reading requirements. Value, the area of the indenter and other parameters, realize the conversion of different unit values to meet different calculation needs.

所述变径压头2-2可以根据测试试件尺寸选取,变径压头2-2底部设有圆柱形引导面2-8,用于引导变径压头与压头的配合,确保实验的准确性。The variable-diameter indenter 2-2 can be selected according to the size of the test piece, and the bottom of the variable-diameter indenter 2-2 is provided with a cylindrical guide surface 2-8, which is used to guide the cooperation of the variable-diameter indenter and the indenter to ensure that the test accuracy.

所述压头2-3顶部与变径压头2-2接触的结合面设有隔热垫片2-9,用于降低保温箱的热量损失,降低传递到压力系统的热量,保护压力系统。A thermal insulation gasket 2-9 is provided on the joint surface where the top of the indenter 2-3 is in contact with the variable diameter indenter 2-2, which is used to reduce the heat loss of the incubator, reduce the heat transferred to the pressure system, and protect the pressure system .

所述加热保温箱3设有数字显示温度计及自动控温装置(3-7),内部设有加热元件3-3,箱内设有温度传感器3-6,用于直观的读取箱内的温度,及当温度达到设定温度时,控温装置能够控制加热元件自动断电,温度降低时控温装置能够控制加热元件自动加热,保证箱内温度恒定。The heating and incubating box 3 is provided with a digital display thermometer and an automatic temperature control device (3-7), and a heating element 3-3 is arranged inside, and a temperature sensor 3-6 is provided in the box for visually reading the temperature in the box. temperature, and when the temperature reaches the set temperature, the temperature control device can control the heating element to automatically power off, and when the temperature drops, the temperature control device can control the heating element to automatically heat to ensure a constant temperature in the box.

所述加热保温箱3设有销3-10连接的活动上盖3-5,用于承载压力、方便安装测试管段及设备维修,上盖开有通孔3-13,用于观察测试管段位置和测试状态,上盖通孔3-13配有隔热保温的通孔塞3-11,用于加温及保温过程中密封上盖,避免热量损失。上盖通孔3-13的尺寸与测试管段密切相关,不同的测试管段要选择不同的上盖3-5。The heating and incubating box 3 is provided with a movable upper cover 3-5 connected by pins 3-10, which is used to carry pressure, facilitate the installation of the test pipe section and equipment maintenance, and the upper cover has a through hole 3-13 for observing the position of the test pipe section And test state, upper cover through hole 3-13 is equipped with heat insulation through hole plug 3-11, is used for sealing upper cover in heating and heat preservation process, avoids heat loss. The size of the upper cover through hole 3-13 is closely related to the test pipe section, and different upper cover 3-5 should be selected for different test pipe sections.

所述加热保温箱3内壁设有一层隔热保温材料3-4,用于避免箱内热量损失。The inner wall of the heating and incubating box 3 is provided with a layer of thermal insulation material 3-4 to avoid heat loss in the box.

所述加热保温箱3底部开有通孔3-12,孔内壁设有一层柔性隔热保温材料3-9,用于适应不同变径压头的尺寸,防止热量从变径压头与孔的间隙散失,并且不会影响测试结果。The bottom of the heating and incubating box 3 is provided with a through hole 3-12, and the inner wall of the hole is provided with a layer of flexible thermal insulation material 3-9, which is used to adapt to the size of different variable-diameter indenters, and prevent heat from passing between the variable-diameter indenters and the hole. Gaps are lost and do not affect test results.

所述高强度承压框架1采用高强度合金钢焊接而成,能承受较大压力不变形。The high-strength pressure-bearing frame 1 is welded by high-strength alloy steel, which can withstand relatively large pressure without deformation.

所述加热保温箱支架4能够任意调节高度,为加热保温箱提供稳定支撑。The heating and incubating box support 4 can be adjusted in height arbitrarily to provide stable support for the heating and incubating box.

本发明整套试验装置重量仅几十公斤,可随意搬运,只要有电源的地方均可操作,满足不同试验需求。The weight of the whole test device of the present invention is only tens of kilograms, and it can be transported at will, and can be operated wherever there is a power supply, so as to meet different test requirements.

实施例1:测试双金属复合管在300℃条件下的结合强度Example 1: Test the bonding strength of the bimetal composite pipe at 300°C

(1)试验管段准备:截取20mm长,51mm碳钢管复合3mm不锈钢管的双金属复合管,复合管内径为56mm,复合管结合面直径为62mm。(2)试验配件选取:选取直径60mm的变径压头;(3)试验组装:将变径压头与压头组装,中间垫隔热垫片;将变径压头与加热保温箱通过底部通孔组装;将试验管段调整好中心,放置于变径压头上,保证不锈钢层均匀地落在变径压头上;调整加热保温箱高度使箱体上缘与管段上端面平齐;盖上保温箱上盖,上盖固定销嵌入销孔内;缓慢升高压头高度,至加热保温箱上盖与高强度框架轻轻接触,调整加热保温箱支架高度使其支撑加热保温箱;确认测试管段位置无偏移后,塞上上盖保温通孔塞;(4)试验升温:打开加热保温箱电源,匀速升温至300℃,温度稳定后保温20分钟;(5)压力试验:调整压力表读数单位,缓慢加载,观察压力变化,当压力达到最大值开始明显下降时,说明复合管已经发生了剪切破坏,记录此过程的压力值(6)试验结束:拆卸设备,取出试验管段,测量和记录相关数据,留取照片或视频资料,根据相关标准计算复合管结合强度。(1) Test pipe section preparation: cut 20mm long, 51mm carbon steel pipe combined with 3mm stainless steel pipe is a bimetal composite pipe, the inner diameter of the composite pipe is 56mm, and the diameter of the joint surface of the composite pipe is 62mm. (2) Selection of test accessories: Select a variable-diameter indenter with a diameter of 60mm; (3) Test assembly: Assemble the variable-diameter indenter with the indenter, and place a heat-insulating gasket in the middle; pass the variable-diameter indenter and the heating insulation box through the bottom Through-hole assembly; adjust the center of the test pipe section and place it on the variable-diameter indenter to ensure that the stainless steel layer falls evenly on the variable-diameter indenter; adjust the height of the heating insulation box so that the upper edge of the box body is flush with the upper end surface of the pipe section; cover Put the upper cover of the incubator on, and the fixing pin of the upper cover is embedded in the pin hole; slowly raise the height of the pressure head until the upper cover of the heating incubator touches the high-strength frame lightly, adjust the height of the bracket of the heating incubator to support the heating incubator; confirm the test After the position of the pipe section has no deviation, plug the heat preservation through hole plug of the upper cover; (4) test temperature rise: turn on the power of the heating incubator, raise the temperature to 300°C at a uniform speed, and keep the temperature for 20 minutes after the temperature is stable; (5) pressure test: adjust the pressure gauge Reading unit, load slowly, observe the pressure change, when the pressure reaches the maximum value and begins to drop obviously, it indicates that the composite pipe has shear failure, record the pressure value of this process (6) end of the test: disassemble the equipment, take out the test pipe section, measure And record relevant data, keep photos or video materials, and calculate the bonding strength of composite pipes according to relevant standards.

具体测试中可重复上述试验,取多次平均值作为最终测试结果。In the specific test, the above test can be repeated, and the average value of multiple times can be taken as the final test result.

实施例2:测试金属陶瓷复合油管在500℃条件下的结合强度Example 2: Testing the bonding strength of metal-ceramic composite oil pipes at 500°C

(1)试验管段准备:截取20mm长,碳钢管复合3mm金属陶瓷层的金属陶瓷复合管,复合管内径为70mm,复合管结合面直径为76mm。(2)试验配件选取:选取直径75mm的变径压头;(3)试验组装:将变径压头与压头组装,中间垫隔热垫片;将变径压头与加热保温箱通过底部通孔组装;将试验管段调整好中心,放置于变径压头上,保证陶瓷层均匀地落在变径压头上;调整加热保温箱高度使箱体上缘与管段上端面平齐;盖上保温箱上盖,上盖固定销嵌入销孔内;缓慢升高压头高度,至加热保温箱上盖与高强度框架轻轻接触,调整加热保温箱支架高度使其支撑加热保温箱;确认测试管段位置无偏移后,塞上上盖保温通孔塞;(4)试验升温:打开加热保温箱电源,匀速升温至500℃,温度稳定后保温30分钟;(5)压力试验:调整压力表读数单位,缓慢加载,观察压力变化,当压力达到最大值开始明显下降时,说明复合管已经发生了剪切破坏,记录此过程的压力值;(6)试验结束:拆卸设备,取出试验管段,测量和记录相关数据,留取照片或视频资料,根据相关标准计算复合管结合强度。(1) Test pipe section preparation: cut 20mm long, The cermet composite pipe with carbon steel pipe and 3mm cermet layer, the inner diameter of the composite pipe is 70mm, and the diameter of the joint surface of the composite pipe is 76mm. (2) Selection of test accessories: Select a variable-diameter indenter with a diameter of 75mm; (3) Test assembly: Assemble the variable-diameter indenter with the indenter, and place a heat-insulating gasket in the middle; pass the variable-diameter indenter and the heating insulation box through the bottom Through-hole assembly; adjust the center of the test pipe section and place it on the variable-diameter indenter to ensure that the ceramic layer falls evenly on the variable-diameter indenter; adjust the height of the heating insulation box so that the upper edge of the box body is flush with the upper end surface of the pipe section; cover Put the upper cover of the incubator on, and the fixing pin of the upper cover is embedded in the pin hole; slowly raise the height of the pressure head until the upper cover of the heating incubator touches the high-strength frame lightly, adjust the height of the bracket of the heating incubator to support the heating incubator; confirm the test After there is no deviation in the position of the pipe section, plug the insulation through-hole plug of the upper cover; (4) Test temperature rise: turn on the power of the heating incubator, raise the temperature to 500°C at a uniform speed, and keep the temperature for 30 minutes after the temperature is stable; (5) Pressure test: Adjust the pressure gauge Reading unit, load slowly, observe the pressure change, when the pressure reaches the maximum value and begins to drop obviously, it indicates that the composite pipe has undergone shear failure, record the pressure value of this process; (6) End of the test: disassemble the equipment, take out the test pipe section, Measure and record relevant data, keep photos or video materials, and calculate the bonding strength of composite pipes according to relevant standards.

具体测试中可重复上述试验,取多次平均值作为最终测试结果。In the specific test, the above test can be repeated, and the average value of multiple times can be taken as the final test result.

Claims (7)

1. a kind of device for testing multiple tube bond strength under hot loading environment, which is characterized in that be divided into four parts: high-intensitive Pressure-bearing frame (1), pressure system (2), heater incubator (3), adjustable support (4);
High-intensitive pressure-bearing frame (1) is used to bear the load of entire test macro, and high-intensitive pressure-bearing frame is body structure, top It is provided with through-hole (1-2), is used for observation experiment process, it may also be used for adjustment sample position;
Pressure system (2) bottom is fixed on the base portion in high-intensitive pressure-bearing frame (1), combines by force for producing and exporting test The pressure of degree;Pressure system includes successively from top to bottom component variable diameter pressure head (2-2), pressure head (2-3), can apply stressed cylinder body (2-4), pedestal (2-5), pedestal (2-5) are fixed on the bottom of pressure system 2, and cylinder body (2-4) is equipped with high accuracy number and shows Pressure gauge (2-6) and load controller (2-7);Variable diameter pressure head (2-2) is cylindrical structure, and upper end diameter is relatively small, under End surface diameter is relatively large, according to the suitable variable diameter indenter size of multiple tube selection of dimension, thereon end surface directly with it is compound The inner tube end face of pipe test specimen contacts, for inner tube on-load pressure, variable diameter pressure head (2-2) lower end surface to be equipped with cylindrical guide sur-face Groove (2-8) cooperates for stablizing with cylindrical pressure head (2-3);The circle at cylindrical pressure head (2-3) top and variable diameter pressure head Cylindricality guide surface groove (2-8) cooperation is used for the combination that conducting pressure is contacted to test specimen, pressure head (2-3) top and variable diameter pressure head It is equipped with heat insulating mattress (2-9) at face, for reducing thermal loss, the heat for being transmitted to pressure system is reduced, protects pressure system; High accuracy number shows pressure gauge (2-6), the pressure value for reading pressure system transmitting for quicklook;
Heater incubator (3) is located at high-intensitive pressure-bearing frame (1) inner upper end, for Compound pipe to be tested to be heated to specifying Temperature, and test is completed at this temperature;Including heating and thermal insulation box body (3-2), heating element (3-3), insulating (3- 4), heating and thermal insulation box cover (3-5), temperature sensor (3-6), digital display thermometer and temperature regulating device (3-7), heating and thermal insulation Case power supply (3-8);Heating and thermal insulation box body (3-2) is used to carry other components of heater incubator, heating and thermal insulation box body (3- 2) lower part is placed on adjustable support (4), and for fixing heater incubator, adjustable support (4) is located at high-intensitive pressure-bearing frame In frame (1);Insulating (3-4) setting is kept in cabinet in heater incubator interior for preventing heat loss Portion's temperature;Heating element (3-3) is located inside heating and thermal insulation box body (3-2) for heating;Heating and thermal insulation box cover (3-5) is adopted Sample upper cover connecting pin (3-10) is cooperated with heating and thermal insulation box body upper port, the heating and thermal insulation box cover upper surface (3-5) with High-intensitive pressure-bearing frame fitting, the pressure that sample upper outer layer end surfaces generate when for bearing test, heating and thermal insulation box cover (3-5) is provided with through-hole (3-13), and various sizes of sample selects the heating and thermal insulation box cover of different clear size of opening, heater incubator Through hole plug (3-11) at upper cover through-hole (3-13) equipped with heat-insulation and heat-preservation avoids thermal loss for sealing upper cover;Heating and thermal insulation Temperature sensor (3-6), digital display thermometer and automatic temp controller (3-7) and temperature sensing are equipped in box body (3-2) Device (3-6) and heating element (3-3) connection and cooperation, for intuitively reading the temperature in heater incubator, when temperature reaches When set temperature, temperature regulating device control heating element is automatically powered off, and temperature heats automatically when reducing, and guarantees that the temperature inside the box is constant;
3 bottom of heater incubator is provided with through-hole (3-12), extend into heater incubator for variable diameter pressure head upper end;Through-hole (3-12) inner sidewall is equipped with one layer of flexible heat-insulating heat-preserving material (3-9), for sealing between variable diameter pressure head and heating and thermal insulation cabinet Gap, flexible heat-insulating heat-preserving material should be able to adapt to the size of different variable diameter pressure heads, prevent heat from dissipating from the gap in variable diameter pressure head and hole It loses, and will not influence test result;
High-intensitive pressure-bearing frame (1) top is equipped with through-hole, and the through-hole diameter on high-intensitive pressure-bearing frame (1) top is protected not less than heating Incubator upper cover through-hole (3-13) and the two is coaxial;The diameter of heating and thermal insulation box cover through-hole (3-13) is greater than the outer of multiple tube to be measured Pipe interior diameter is less than outer tube overall diameter;The inner tube interior diameter that variable diameter pressure head (2-2) upper end diameter is greater than multiple tube to be measured is small In inner tube overall diameter.
2. a kind of device for testing multiple tube bond strength under hot loading environment described in accordance with the claim 1, which is characterized in that Adjustable support 4 is fixed on inside high-intensitive pressure-bearing frame 1, for supporting and fixing heating and thermal insulation in a manner of height-adjustable Case (3).
3. a kind of device for testing multiple tube bond strength under hot loading environment described in accordance with the claim 1, which is characterized in that Pressure head (2-3) is that can continue to increase pressure apparatus along variable diameter pressure head (2-2) axis direction for adjusting height, cylinder body (2-4).
4. a kind of device for testing multiple tube bond strength under hot loading environment described in accordance with the claim 1, which is characterized in that The heater incubator is equipped with automatic temp controller, and inside is equipped with heating element, temperature sensor is equipped in case, when temperature reaches When set temperature, heating element is automatically powered off, and temperature heats automatically when reducing, and guarantees that the temperature inside the box is constant.
5. a kind of device for testing multiple tube bond strength under hot loading environment described in accordance with the claim 1, which is characterized in that The heater incubator temperature can cover most working conditions of current engineer application in room temperature to adjusting in 1000 DEG C.
6. a kind of device for testing multiple tube bond strength under hot loading environment described in accordance with the claim 1, which is characterized in that The high intensity pressure-bearing frame is welded using high strength alloy steel.
7. using the method for device to test multiple tube bond strength described in any one of claims 1-6, which is characterized in that experiment Method is as follows: pressure system is fixed in high-intensitive pressure-bearing frame, the variable diameter being applicable according to multiple tube size selection to be tested Pressure head;Variable diameter pressure head is inserted into heater incubator by heater incubator lower opening, multiple tube to be tested is placed in variable diameter pressure On head and adjust so that variable diameter pressure head and multiple tube to be tested are coaxial, the upper surface of variable diameter pressure head only with it is to be tested compound The inner tube lower end face contact of pipe, adjustment heater incubator support height make heater incubator box height and test pipeline section upper surface It being substantially flush, covers heating and thermal insulation box cover, upper cover fixed pin is embedded in pin hole, the fall head of pressure system is slowly increased, Gently contacted to heating and thermal insulation box cover with high strength frame, at the same the lower surface of heating and thermal insulation box cover only with it is to be tested compound The outer tube upper end face contact of pipe;Adjustment heater incubator support height makes it support heater incubator;Open heater incubator electricity Source is at the uniform velocity warming up to required test temperature, and temperature keeps the temperature 15-30 minutes after stablizing, and pressure system starts slowly load upwards Pressure observes pressure change, when pressure, which reaches maximum value, to be started to be decreased obviously, illustrates that multiple tube has occurred that shearing is broken It is bad, the pressure value of this process is recorded, the bond strength of maximum value calculation multiple tube is passed through.
CN201910815840.6A 2019-08-30 2019-08-30 A device and method for testing the bonding strength of composite pipes under thermal loading conditions Active CN110501284B (en)

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