CN1104906C - Tibetan-medicinal bath for treating rheumatism and its preparing process - Google Patents
Tibetan-medicinal bath for treating rheumatism and its preparing process Download PDFInfo
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- CN1104906C CN1104906C CN99127556A CN99127556A CN1104906C CN 1104906 C CN1104906 C CN 1104906C CN 99127556 A CN99127556 A CN 99127556A CN 99127556 A CN99127556 A CN 99127556A CN 1104906 C CN1104906 C CN 1104906C
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Abstract
The present invention relates to a Tibetan medicinal bath for treating rheumatism and a preparation process thereof. After six kinds of Tibetan medicines of rhododendron, garden cypress, artemisia sieversiana, myricaria germanica, yellow horn wood, ephedra, etc. are cleaned, dried, decocted in water and fermented, first, volatile oil components in the rhododendron, the myricaria germanica, the garden cypress and the artemisia sieversiana are enriched by a vapor distillation method; second, the ephedra and the yellow horn wood are added, and 30 to 70% of ethanol or water is used for backflow extraction; third, impurities of pigment, etc. are removed in a cryoprecipitation or molecular retention mode after concentration; finally, the volatile oil components are respectively prepared into a water agent, a granule and paste. The Tibetan medicinal bath of the present invention is mainly used for a vapor bath and a bath, and has obvious therapeutic effects for the treatment of the intractable diseases of intractable rheumatic arthritis, rheumatoid arthritis, chronic waist and leg pain, skin disease, etc.
Description
The invention belongs to the rheumatism dipping, especially relate to a kind of treatment rheumatism, rheumatoid arthritis, chronic lambago and skelalgia, dermopathic Tibetan medicine dipping and preparation method thereof.
Rheumatism, especially diseases such as rheumatism, rheumatoid arthritis, lumbago and skelalgia bring inconvenience for many patients' life, though multiple pharmaceutical dosage form is arranged at present, comprising for oral administration and external treatment, serves as main carry out dipping and steam bath to treat above-mentioned curative effect of disease remarkable with the decoction with famous Tibetan medicine dipping proved recipe five tastes manna soup especially.But because this decoction appearance character is poor, should not carries and should go mouldy and wait deficiency, use and promoting and caused inconvenience.
The object of the present invention is to provide the rheumatism Tibetan medicine dipping of diseases such as treatment rheumatism.
Another object of the present invention also is to provide the preparation technology of the Tibetan medicine dipping of simple, the reliable and stable treatment rheumatism of a kind of technology.
The objective of the invention is to realize by following measure: a kind of material content for the treatment of the Tibetan medicine dipping of rheumatism is; Rhododendron 80-600 gram, garden cypress 80-600 gram, Artemisia sieversiana Willd. 80-600 gram, Cacumen Myricariae Germanicae 80-600 gram, wood of shiny-leaved yellowhorn 80-600 gram, Herba Ephedrae 80-600 gram.
The preparation technology of the Tibetan medicine dipping of described treatment rheumatism: get Rhododendron, the garden cypress, Cacumen Myricariae Germanicae, Artemisia sieversiana Willd., wood of shiny-leaved yellowhorn, Herba Ephedrae, clean, dry, decocting boils, taking-up is put in the installation for fermenting, add 2 kilograms distillers yeast ratio and add 2-3 kilogram Chinese liquor ratio in per 100 kilograms of raw materials and add in the installation for fermenting and mix thoroughly in per 100 kilograms of raw materials, insulation is 48 hours under 37-40 ℃ of temperature, dry after the taking-up, take out Rhododendron again, Cacumen Myricariae Germanicae, the garden cypress, Artemisia sieversiana Willd. steam distillation enrichment volatile oil composition wherein, add Herba Ephedrae again, wood of shiny-leaved yellowhorn, with the ethanol of 30-70% or water reflux, extract, three times, each 2 hours, behind the merge extractive liquid,, concentrate and reclaim ethanol or water, when volume and rate of charge are 1: 1, Cryoprecipitation 48 hours, remove by filter impurity, the clear liquid part is the ultrafiltration post filtration of 2-4 ten thousand molecular weight through molecular sieve, or the 30-90% ethanol elution part after macroporous resin separates, be condensed into certain volume by the preparation specification, add the volatile oil part that has proposed, add 0.1～2% ethanol or tween again and increase liquid, stir evenly, be water preparation.
Get above-mentioned molecular sieve or the filtering clear liquid part of macroporous resin crossed, vacuum concentration to gravity Baume is more than 1.3, carry out centrifugal spray or vacuum drying, an amount of excipient is pulverized, sieved, adds to dried product, make granule, treat particle drying after, press the prescription proportion scale and add the volatile oil part, sealing is granule immediately.
Get the clear liquid part of above-mentioned molecular sieve or macroporous resin, vacuum concentration adds an amount of excipient to thick paste, and the dermal osmosis lubricant is made the ointment shape, is unguentum.
The gold that adopts the present invention to make is scolded manna body lotion dosage form, can treat pertinacious diseases such as the prolonged rheumatism that does not heal, rheumatoid arthritis, chronic lambago and skelalgia, dermatosis.It is mainly used in dipping and steam bath, has characteristics such as easy to carry, that cure rate is high, have no side effect.
The invention will be further described below in conjunction with embodiment.
Get: Rhododendron 280 grams, garden cypress branch 280 grams, Artemisia sieversiana Willd. 280 grams, Cacumen Myricariae Germanicae 280 grams, wood of shiny-leaved yellowhorn 280 grams, Herba Ephedrae 280 grams, clean, dry, decocting boiled 3 minutes, taking-up is put in the installation for fermenting, to add 2 kilograms of Chinese liquor ratios and add 2 kilograms of Chinese liquor ratios in per 100 kilograms of raw materials and add in the installation for fermenting and mix thoroughly with raw material in per 100 kilograms of raw materials, insulation is 48 hours under 40 ℃ of temperature, dry after taking out again, get Rhododendron, Cacumen Myricariae Germanicae, the garden cypress, Artemisia sieversiana Willd. steam distillation enrichment volatile oil component wherein, add Herba Ephedrae again, wood of shiny-leaved yellowhorn, be used for 50% alcohol reflux three times, each 2 hours, behind the merge extractive liquid,, concentrate and reclaim ethanol, to volume and rate of charge be 1: 1 o'clock, Cryoprecipitation 48 hours, remove by filter impurity, the clear liquid part is annotated through the ultrafiltration of molecular sieve 30,000 molecular weight and is filtered, or 50% ethanol elution part after macroporous resin separates, press preparation specification simmer down to certain volume, add the volatile oil part that has proposed, add 0.5% ethanol or tween again and increase liquid, stir evenly, be water preparation.
Get above-mentioned molecular sieve or the filtering clear liquid part of macroporous resin crossed, vacuum concentration to gravity Baume is more than 1.3, carry out centrifugal spray or vacuum drying, an amount of excipient is pulverized, sieved, adds to dried product, make granule, treat particle drying after, press the prescription proportion scale and add the volatile oil part, sealing is granule immediately.
Get the above-mentioned clear liquid part of crossing molecular sieve or crossing macroporous resin, vacuum concentration adds an amount of excipient to thick paste, and dermal osmosis lubricant etc. are made the ointment shape, are unguentum.
It is on existing Tibetan medicine dipping basis that gold of the present invention is scolded manna liquor type, help formulated with Tibetan medicine and Chinese medicine, thereby traditional drugs is developed.
Rhododendron: mainly contain volatile oil and water solublity two constituents, volatile oil contains r-selinene, Cuculus polioephalus alkene, Cuculus polioephalus time alkene, d-selinene, k-celery in compositions such as alkene, yak ketone, Chinese juniper brain, benzylacetones, has relieving cough and expelling phlegm, bacteriostasis.Water-soluble components contains compositions such as multiple flavone compounds such as Quercetin, quercitrin, gossypetin, hyperin, 8 one methoxyl group Quercetins and organic acid, tannin, and its total flavones partly has the effect of cardiovascular system pharmacology.
Garden cypress: mainly contain australene, nopinene, limonene, carene-3, absinthol, terpineol, δ-Cuculus polioephalus alkene, earthen table in the volatile oil and cling to chemical constituents such as rare alcohol, water-soluble components contains Huang, phenols, reducing sugar, organic acid etc., and wherein limonene has antitussive effect.
Artemisia sieversiana Willd.: main component is 1 in the volatile oil), 8-presses leaf oil element, Camphora, Borneolum Syntheticum, piperitone.2), 2-methyl acid Herba Pelargonii Graveolentis fat, 2-Methyl Butyric Acid Herba Pelargonii Graveolentis fat, α-selinene, Flos Matricariae chamomillae, burning that the treatment ultraviolet radiation causes arranged.Water-soluble components mainly contains sieversinin, sieversin, Absinthium lactone, acid, alkaloid etc., has stronger antibiotic and antiinflammation, inflammation is oozed out vascular permeability strengthen, and Ovum Gallus domesticus album, formaldehyde swollen joint etc. all has significant inhibitory effect.
Cacumen Myricariae Germanicae: Main Ingredients and Appearance is volatile oil, phenols, organic acid etc.
Wood of shiny-leaved yellowhorn: Main Ingredients and Appearance is flavone compound, coumarin, sugar and tannin classes such as myricetin.Have eliminating phlegm and stopping cough and diuresis.
Herba Ephedrae: Main Ingredients and Appearance is ephedrine, pseudoephedrine, flavonoid glycoside, tannin, dextrin, inulin, starch, pectin, cellulose, glucose etc.Buffering bronchial asthma attack and prevention outbreak are arranged, multiple diseases such as anti-skin, mucosa, treatment myasthenia gravis, analgesic, antiviral etc.
Claims (4)
1, a kind of Tibetan medicine dipping for the treatment of rheumatism is characterized in that its prescription is: Rhododendron 80-600 gram, garden cypress 80-600 gram, Artemisia sieversiana Willd. 80-600 gram, Cacumen Myricariae Germanicae 80-600 gram, wood of shiny-leaved yellowhorn 80-600 gram, Herba Ephedrae 80-600 gram.
2, the preparation technology of the Tibetan medicine dipping of the described treatment rheumatism of a kind of claim 1 is characterized in that this technology contains following step; Get Rhododendron, the garden cypress, Cacumen Myricariae Germanicae, big seed punt-pole, wood of shiny-leaved yellowhorn, Herba Ephedrae, clean, dry, decocting boils, taking-up is put in the installation for fermenting, add 2 kilograms distillers yeast ratio and add in the installation for fermenting in per 100 kilograms of raw materials and mix thoroughly in the ratio that per 100 kilograms of raw materials add 2-3 kilogram grain neutral spirit, insulation is 48 hours under 37-40 ℃ of temperature, dry after the taking-up, take out Rhododendron again, Cacumen Myricariae Germanicae, the garden cypress, Artemisia sieversiana Willd. steams slide method enrichment volatile oil composition wherein with steam, add Herba Ephedrae again, wood of shiny-leaved yellowhorn, the ethanol of usefulness 30-70% or water reflux, extract, three times, each 2 hours, behind the merge extractive liquid,, concentrate to reclaim ethanol or water, when volume and rate of charge are 1: 1, Cryoprecipitation 48 hours, remove by filter impurity, clear liquid partly is the ultrafiltration post filtration of 2-4 ten thousand molecular weight through molecular sieve, or the 30-90% ethanol elution part after macroporous resin separates, and is condensed into certain volume by the preparation specification, add the volatile oil part that has proposed, add 0.1～2% ethanol or tween again and increase liquid, stir evenly, be water preparation.
3, the preparation technology of the Tibetan medicine dipping of treatment rheumatism according to claim 2, it is characterized in that the filtering clear liquid part of described filtration molecular sieve or macroporous resin, vacuum concentration to gravity Baume is counted more than 1.3, carries out centrifugal spray or vacuum drying, and dried product is pulverized, sieve, add an amount of excipient, make granule, treat particle drying after, press the prescription proportion scale and add the volatile oil part, be granule.
4, the preparation technology of rheumatism Tibetan medicine according to claim 2 dipping is characterized in that: the filtering clear liquid part of described filtration molecular sieve or macroporous resin, and vacuum concentration is to thick educating, add an amount of excipient, the dermal osmosis lubricant is made the ointment shape, is unguentum.
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| Application Number | Priority Date | Filing Date | Title |
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| CN99127556A CN1104906C (en) | 1999-12-29 | 1999-12-29 | Tibetan-medicinal bath for treating rheumatism and its preparing process |
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| Application Number | Priority Date | Filing Date | Title |
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| CN99127556A CN1104906C (en) | 1999-12-29 | 1999-12-29 | Tibetan-medicinal bath for treating rheumatism and its preparing process |
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| Publication Number | Publication Date |
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| CN1263777A CN1263777A (en) | 2000-08-23 |
| CN1104906C true CN1104906C (en) | 2003-04-09 |
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| CN99127556A Expired - Fee Related CN1104906C (en) | 1999-12-29 | 1999-12-29 | Tibetan-medicinal bath for treating rheumatism and its preparing process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100434084C (en) * | 2005-08-23 | 2008-11-19 | 兰州和盛堂制药有限公司 | Pharmaceutical composition for treating rheumatic and rheumatoid diseases and its preparation process |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100382781C (en) * | 2005-01-21 | 2008-04-23 | 西藏宇妥藏药研究有限公司 | Method for preparing bath powder of Tibet medicine and its quality control method |
| CN100341529C (en) * | 2005-01-21 | 2007-10-10 | 西藏宇妥藏药研究有限公司 | Combination of Tibet medicine of containing salt and possessing medicinal effect health care, and preparation metohd |
| CN100387217C (en) * | 2005-04-01 | 2008-05-14 | 吴玉仁 | Enzyme body building bath powder and its preparation method |
| TWI481374B (en) * | 2012-10-31 | 2015-04-21 | Yuding Energy Technology Co Ltd | Method for manufacturing energy saving pot |
| CN106309849A (en) * | 2016-11-04 | 2017-01-11 | 山东金诃药物研究开发有限公司 | Tibetan medicine compound for foot bath and application thereof |
| CN107569533A (en) * | 2017-09-18 | 2018-01-12 | 次旺 | Composition and its application, preparation method with enhancing bone density effect |
| CN110129057B (en) * | 2019-05-06 | 2021-01-15 | 中国科学院西北高原生物研究所 | Rhododendron anthopogonoides extract and its extraction method and application |
| CN112168929A (en) * | 2020-09-28 | 2021-01-05 | 西藏奇正藏药股份有限公司 | Pharmaceutical composition and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1109778A (en) * | 1995-01-11 | 1995-10-11 | 隋文方 | "Shenqikang" bathing powder |
| CN1131035A (en) * | 1995-12-05 | 1996-09-18 | 廖利平 | Chinese herbal medicine composition |
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1999
- 1999-12-29 CN CN99127556A patent/CN1104906C/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1109778A (en) * | 1995-01-11 | 1995-10-11 | 隋文方 | "Shenqikang" bathing powder |
| CN1131035A (en) * | 1995-12-05 | 1996-09-18 | 廖利平 | Chinese herbal medicine composition |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100434084C (en) * | 2005-08-23 | 2008-11-19 | 兰州和盛堂制药有限公司 | Pharmaceutical composition for treating rheumatic and rheumatoid diseases and its preparation process |
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| Publication number | Publication date |
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| CN1263777A (en) | 2000-08-23 |
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