CN110484429A - Microwave hydrolysis waste plant protein resource prepares compound amino acid syrup technique and equipment - Google Patents
Microwave hydrolysis waste plant protein resource prepares compound amino acid syrup technique and equipment Download PDFInfo
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Abstract
The invention discloses microwave hydrolysis waste plant protein resources to prepare compound amino acid syrup technique and equipment, including reacting can system, circulating pump system, feed can system, stir can system, return-flow system and Central Control Room control system, the right end of the Central Control Room control system is provided with return-flow system, the return-flow system and Central Control Room control system are electrically connected, by using the full-automatic acid material of PLC than control in the present invention, input and output material butterfly valve automatically switches, whole process only needs a people to operate in Central Control Room control system, the high degree of automation that can achieve in this way, reaction process does not generate any flammable and explosive substance, safety and stability, microwave hydrolysis system in the present invention uses synthesis under normal pressure, top setting is condensed back, production process is without any exhaust gas, the phenomenon that contaminated wastewater, and it is neutralized after the completion of hydrolyzing by addition potassium hydroxide PH is adjusted to six, and compounded amino acid mother liquor can be obtained through filtering.
Description
Technical field
The invention belongs to microwave hydrolysis system correlative technology fields, and in particular to the preparation of microwave hydrolysis waste plant protein resource is multiple
Close amino acid syrup technique and equipment.
Background technique
Amino acid is necessary base substance in human life movement.For compound amino acid there are many type, raw material is main
Dividing has plant type and animal-type.Plant type compound amino acid is using natural high-protein plant as raw material, using advanced Biochemical Engineering
Technology is extracted from plants, and separates a variety of amino acid and is refined.Animal-type compound amino acid is with various high protein animal bodies
For raw material, after microbial fermentation, acid and alkali hydrolysis processing, spray drying is process.
Existing compound amino acid syrup technology has the following problems: existing compound amino acid syrup technique into
When the preparation of row amino acid, not most is all to use manually to be fed and generated, such that the control ratio of charging
It is unreasonable and comparatively laborious in the process produced, need different workers to carry out different processes, and traditional answer
Close amino acid when being produced in production process it is possible that the phenomenon that exhaust gas, contaminated wastewater.
Summary of the invention
The purpose of the present invention is to provide microwave hydrolysis waste plant protein resources to prepare compound amino acid syrup technique and equipment,
To solve existing compound amino acid syrup technique mentioned above in the background art, generation step complexity is simultaneously when preparation
And it is possible that pollution the phenomenon that the problem of.
To achieve the above object, the invention provides the following technical scheme: microwave hydrolysis waste plant protein resource prepares compound ammonia
Base acid syrup technique and equipment, including reaction can system, circulating pump system, charging can system, stirring can system, return-flow system and
Central Control Room control system, the right end of the Central Control Room control system are provided with return-flow system, the return-flow system and Central Control Room control
System processed is electrically connected, and stirring can system, the stirring can system and middle control are provided on the downside of the right end of the return-flow system
Room control system is electrically connected, and the right end of the stirring can system is provided with charging can system, the charging can system and middle control
Room control system is electrically connected, and the left end of the charging can system is provided with circulating pump system, the circulating pump system and middle control
Room control system is electrically connected, and the left end of the circulating pump system is provided with reaction can system, the reaction can system and middle control
Room control system is electrically connected.
Preferably, the preparation step of the compound amino acid syrup technique is as follows:
Step 1: preparing raw material, and the raw material of preparation is fowl and animal excrement, prepares microwave, concentrated sulfuric acid catalyst;
Step 2: because reaction is to carry out under strong acid, and strong acid, highly basic and ultraviolet light can directly result in protein
Denaturation, any bacterium, virus and bacteria and virus are that unicellular organism will lead to cell dissolution under strong acid, can not be survived.
Fowl and animal excrement is converted to by animal feed, and toxicity caused by the substances such as heavy metal and toxic compounds safely can be in feed
Processing and making process in controlled;
Step 3: the raw material fowl and animal excrement of preparation is pumped into agitator tank, and opens the power switch of agitator tank;
Step 4: starting stirring, is passed through nitrogen protection, is slowly warming up to 200-250 by 60-80 revs/min of mixing speed
Degree reacts 8-12 hour;
Step 5: after completion of the reaction, fowl and animal excrement raw material is put into enzyme hydrolysis tank, manure of livestock and poultry is added into enzyme hydrolysis tank
Just the keratinase preparation of fowl and animal excrement raw material 0.5% is added into enzyme hydrolysis tank for the pure water of raw material 30%, controls enzyme hydrolysis
The internal temperature of tank is 50-60 degrees Celsius, is digested 2 hours;
Step 6: being added activated carbon block into the solution after enzymatic hydrolysis, and the ratio of solution and activated carbon block is 1: 40, and stirring is equal
It is even, go out activated carbon block with the strainer filtering of 50 mesh after storage one hour;
Step 7: by microwave machine continuing the solution after microwave hydrolysis to heat, and heats ten minutes, after making microwave hydrolysis
Solution is further concentrated, and the solution after concentration is filtered with the strainer of 800 mesh, filtered concentrate solution is put into very
It is dried in empty drying machine, obtains composite aminophenol powder;
Step 8: by being adjusted to 6 with PH in addition potassium hydroxide after the completion of hydrolysis, compound amino acid can be obtained through filtering
Mother liquor.Obtained after concentration high value compound amino acid syrup it is purified after can be sold towards feed market, can also directly make
It is externally sold for fertilizer containing amino acid liquid;
Step 9: and what is filtered down is precipitated as neutralizing obtained potassium sulfate and a small amount of ash content and amino acid, and sulfuric acid
Potassium itself is a kind of good potash fertilizer, and it is also a kind of good potash fertilizer that we can be used as the fertilizer of solid-state containing amino acid at this time;
Step 10: using the purposes after production as the industrial crops amino acid fertilizer such as tea, fruit and vegetable, animal feed addition
Agent, plant protection nutrient solution etc..
Compared with prior art, the present invention provides microwave hydrolysis waste plant protein resources to prepare compound amino acid syrup technique
And equipment, have it is following the utility model has the advantages that
(1), by using the full-automatic acid material ratio control of PLC in the present invention, input and output material butterfly valve automatically switches, and whole process is only
It needs a people to operate in Central Control Room control system, is assisted without more people, the high degree of automation that can achieve in this way, and react
Product is amino acid and glucose, and reaction process does not generate any flammable and explosive substance, safety and stability;
(2), the present invention in microwave hydrolysis system use synthesis under normal pressure, top setting be condensed back, production process without appoint
The phenomenon that exhaust gas, contaminated wastewater, and by that can be obtained through filtering in addition potassium hydroxide and PH is adjusted to six after the completion of hydrolyzing
To compounded amino acid mother liquor, the compound amino acid syrup of high value is obtained after concentration, to solve existing compound ammonia
Base acid syrup technique generation step when preparation is complicated and it is possible that the problem of the phenomenon that pollution.
Detailed description of the invention
Fig. 1 is three-dimensional model structure schematic diagram of the invention;
Fig. 2 is workflow structure schematic diagram of the invention;
In figure: 1, reacting can system;2, circulating pump system;3, feed can system;4, can system is stirred;5, return-flow system;
6, Central Control Room control system.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
The present invention provides technical solution referring to FIG. 1-2: microwave hydrolysis waste plant protein resource prepares compound amino acid syrup
Technique and equipment, including reaction can system 1, circulating pump system 2, charging can system 3, stirring can system 4, return-flow system 5 and in
Room control system 6 is controlled, the right end of Central Control Room control system 6 is provided with return-flow system 5, return-flow system 5 and Central Control Room control system 6
It is electrically connected, stirring can system 4, stirring can system 4 and Central Control Room control system 6 is provided on the downside of the right end of return-flow system 5
It is electrically connected, the right end of stirring can system 4 is provided with charging can system 3, and charging can system 3 and Central Control Room control system 6 are electrically
Connection, the left end of charging can system 3 are provided with circulating pump system 2, and circulating pump system 2 and Central Control Room control system 6 are electrically connected,
The left end of circulating pump system 2 is provided with reaction can system 1, and reaction can system 1 and Central Control Room control system 6 are electrically connected.
The preparation step of compound amino acid syrup technique is as follows:
Step 1: preparing raw material, and the raw material of preparation is fowl and animal excrement, prepares microwave, concentrated sulfuric acid catalyst;
Step 2: because reaction is to carry out under strong acid, and strong acid, highly basic and ultraviolet light can directly result in protein
Denaturation, any bacterium, virus and bacteria and virus are that unicellular organism will lead to cell dissolution under strong acid, can not be survived.
Fowl and animal excrement is converted to by animal feed, and toxicity caused by the substances such as heavy metal and toxic compounds safely can be in feed
Processing and making process in controlled;
Step 3: the raw material fowl and animal excrement of preparation is pumped into agitator tank, and opens the power switch of agitator tank;
Step 4: starting stirring, is passed through nitrogen protection, is slowly warming up to 200-250 by 60-80 revs/min of mixing speed
Degree reacts 8-12 hour;
Step 5: after completion of the reaction, fowl and animal excrement raw material is put into enzyme hydrolysis tank, manure of livestock and poultry is added into enzyme hydrolysis tank
Just the keratinase preparation of fowl and animal excrement raw material 0.5% is added into enzyme hydrolysis tank for the pure water of raw material 30%, controls enzyme hydrolysis
The internal temperature of tank is 50-60 degrees Celsius, is digested 2 hours;
Step 6: being added activated carbon block into the solution after enzymatic hydrolysis, and the ratio of solution and activated carbon block is 1: 40, and stirring is equal
It is even, go out activated carbon block with the strainer filtering of 50 mesh after storage one hour;
Step 7: by microwave machine continuing the solution after microwave hydrolysis to heat, and heats ten minutes, after making microwave hydrolysis
Solution is further concentrated, and the solution after concentration is filtered with the strainer of 800 mesh, filtered concentrate solution is put into very
It is dried in empty drying machine, obtains composite aminophenol powder;
Step 8: by being adjusted to 6 with PH in addition potassium hydroxide after the completion of hydrolysis, compound amino acid can be obtained through filtering
Mother liquor.Obtained after concentration high value compound amino acid syrup it is purified after can be sold towards feed market, can also directly make
It is externally sold for fertilizer containing amino acid liquid;
Step 9: and what is filtered down is precipitated as neutralizing obtained potassium sulfate and a small amount of ash content and amino acid, and sulfuric acid
Potassium itself is a kind of good potash fertilizer, and it is also a kind of good potash fertilizer that we can be used as the fertilizer of solid-state containing amino acid at this time;
Step 10: using the purposes after production as the industrial crops amino acid fertilizer such as tea, fruit and vegetable, animal feed addition
Agent, plant protection nutrient solution etc..
The working principle of the invention and process for using:
When to carry out producing the construction technology of the compound amino acid, at this moment pass through the microwave hydrolysis fowl and animal excrement system
The reaction principle of standby amino acid is the inverse process of protein dehydrating condensation, and principle is that the mode that amino acid molecular combines is by one
The hydroxyl of amino acid molecular and the amino of another amino acid molecular slough a molecular water simultaneously, and this combination is called dehydration
Condensation.Second for connecting the wherein left number of two amino acid moleculars is the chemical bond for being called peptide bond, has partial double bond property,
And the mixing in stirring can system 4 is carried out by fowl and animal excrement, and adds microwave, the concentrated sulfuric acid, water during stirring
By being adjusted to six with PH in addition potassium hydroxide after the completion of solution, compounded amino acid mother liquor can be obtained through filtering, obtained after concentration
It can be sold towards feed market after the compound amino acid syrup of high value is purified, it can also be directly as containing amino acid liquid fertilizer
Material is externally sold.And what is filtered down is precipitated as neutralizing obtained potassium sulfate and a small amount of ash content and amino acid, and potassium sulfate sheet
Body is a kind of good potash fertilizer.It is also a kind of good potash fertilizer, microwave hydrolysis that we can be used as the fertilizer of solid-state containing amino acid at this time
System uses synthesis under normal pressure, and top setting is condensed back, and production process is automatically sour using PLC without any exhaust gas, contaminated wastewater
Material automatically switches than control, input and output material butterfly valve, and whole process only needs a people to operate in Central Control Room control system 6, auxiliary without more people
It helps.High degree of automation, reaction product are amino acid and glucose, and reaction process does not generate any flammable and explosive substance, safety
Stablize, it is any because reaction is to carry out under strong acid, and strong acid, highly basic and ultraviolet light can directly result in protein denaturation
Bacterium, virus will lead to cell dissolution under strong acid, can not survive.Fowl and animal excrement is converted to by animal feed, weight
Toxicity caused by the substances such as metal and toxic compounds can be controlled safely in the processing and making process of feed, above
In examining report, we detect prepares in amino acid in bloom blue algae hydrolysis, detects that the ingredient of heavy metal lead is
0.0422mg/kg is far below country especially discharge standard 0.2mg/L.And national forage health standard minimum requirements 5mg/kg.
Microwave hydrolysis fowl and animal excrement adjusts PH through acid-base neutralization after completion of the reaction, using secondary filter, can be obtained and meets country
The amino acid and saccharide raw material of sanitary standard may be used as the industrial crops amino acid fertilizer such as tea, fruit and vegetable, animal feed addition
Agent, plant protection nutrient solution etc.;
Step 1: preparing raw material, and the raw material of preparation is fowl and animal excrement, prepares microwave, concentrated sulfuric acid catalyst;
Step 2: because reaction is to carry out under strong acid, and strong acid, highly basic and ultraviolet light can directly result in protein
Denaturation, any bacterium, virus and bacteria and virus are that unicellular organism will lead to cell dissolution under strong acid, can not be survived.
Fowl and animal excrement is converted to by animal feed, and toxicity caused by the substances such as heavy metal and toxic compounds safely can be in feed
Processing and making process in controlled;
Step 3: the raw material fowl and animal excrement of preparation is pumped into agitator tank, and opens the power switch of agitator tank;
Step 4: starting stirring, is passed through nitrogen protection, is slowly warming up to 200-250 by 60-80 revs/min of mixing speed
Degree reacts 8-12 hour;
Step 5: after completion of the reaction, fowl and animal excrement raw material is put into enzyme hydrolysis tank, manure of livestock and poultry is added into enzyme hydrolysis tank
Just the keratinase preparation of fowl and animal excrement raw material 0.5% is added into enzyme hydrolysis tank for the pure water of raw material 30%, controls enzyme hydrolysis
The internal temperature of tank is 50-60 degrees Celsius, is digested 2 hours;
Step 6: being added activated carbon block into the solution after enzymatic hydrolysis, and the ratio of solution and activated carbon block is 1: 40, and stirring is equal
It is even, go out activated carbon block with the strainer filtering of 50 mesh after storage one hour;
Step 7: by microwave machine continuing the solution after microwave hydrolysis to heat, and heats ten minutes, after making microwave hydrolysis
Solution is further concentrated, and the solution after concentration is filtered with the strainer of 800 mesh, filtered concentrate solution is put into very
It is dried in empty drying machine, obtains composite aminophenol powder;
Step 8: by being adjusted to 6 with PH in addition potassium hydroxide after the completion of hydrolysis, compound amino acid can be obtained through filtering
Mother liquor.Obtained after concentration high value compound amino acid syrup it is purified after can be sold towards feed market, can also directly make
It is externally sold for fertilizer containing amino acid liquid;
Step 9: and what is filtered down is precipitated as neutralizing obtained potassium sulfate and a small amount of ash content and amino acid, and sulfuric acid
Potassium itself is a kind of good potash fertilizer, and it is also a kind of good potash fertilizer that we can be used as the fertilizer of solid-state containing amino acid at this time;
Step 10: using the purposes after production as the industrial crops amino acid fertilizer such as tea, fruit and vegetable, animal feed addition
Agent, plant protection nutrient solution etc..
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (2)
1. microwave hydrolysis waste plant protein resource prepares compound amino acid syrup technique and equipment, including reaction can system (1), circulation
Pumping system (2), charging can system (3), stirring can system (4), return-flow system (5) and Central Control Room control system (6), feature exists
In: the right end of the Central Control Room control system (6) is provided with return-flow system (5), and the return-flow system (5) and Central Control Room control are
System (6) is electrically connected, and stirring can system (4), the stirring can system are provided on the downside of the right end of the return-flow system (5)
(4) it is electrically connected with Central Control Room control system (6), the right end of stirring can system (4) is provided with charging can system (3), institute
It states charging can system (3) and Central Control Room control system (6) is electrically connected, the left end of charging can system (3) is provided with circulation
Pumping system (2), the circulating pump system (2) and Central Control Room control system (6) are electrically connected, a left side for the circulating pump system (2)
End is provided with reaction can system (1), and the reaction can system (1) and Central Control Room control system (6) are electrically connected.
2. microwave hydrolysis waste plant protein resource according to claim 1 prepares compound amino acid syrup technique and equipment,
Be characterized in that: the preparation step of the compound amino acid syrup technique is as follows:
Step 1: preparing raw material, and the raw material of preparation is fowl and animal excrement, prepares microwave, concentrated sulfuric acid catalyst;
Step 2: because reaction is to carry out under strong acid, and strong acid, highly basic and ultraviolet light can directly result in protein denaturation,
Any bacterium, virus and bacteria and virus is that unicellular organism will lead to cell dissolution under strong acid, can not be survived.Manure of livestock and poultry
It is to be converted to by animal feed, toxicity caused by the substances such as heavy metal and toxic compounds safely can be in the processing of feed
It is controlled in manufacturing process;
Step 3: the raw material fowl and animal excrement of preparation is pumped into agitator tank, and opens the power switch of agitator tank;
Step 4: starting stirring 60-80 revs/min of mixing speed, is passed through nitrogen protection, is slowly warming up to 200-250 degree, instead
Answer 8-12 hour;
Step 5: after completion of the reaction, fowl and animal excrement raw material is put into enzyme hydrolysis tank, and it is former that fowl and animal excrement is added into enzyme hydrolysis tank
The keratinase preparation of fowl and animal excrement raw material 0.5% is added into enzyme hydrolysis tank for the pure water of material 30%, control enzyme hydrolysis tank
Internal temperature is 50-60 degrees Celsius, is digested 2 hours;
Step 6: being added activated carbon block into the solution after enzymatic hydrolysis, and the ratio of solution and activated carbon block is 1:40, stirs evenly,
Go out activated carbon block with the strainer filtering of 50 mesh after storage one hour;
Step 7: by microwave machine continuing the solution after microwave hydrolysis to heat, and heats ten minutes, the solution after making microwave hydrolysis
Further concentration, is filtered the solution after concentration with the strainer of 800 mesh, filtered concentrate solution is put into vacuum and is done
It is dried in dry machine, obtains composite aminophenol powder;
Step 8: by being adjusted to 6 with PH in addition potassium hydroxide after the completion of hydrolysis, compound amino acid mother can be obtained through filtering
Liquid.Obtained after concentration high value compound amino acid syrup it is purified after can be sold towards feed market, can also be directly as
Fertilizer containing amino acid liquid is externally sold;
Step 9: and what is filtered down is precipitated as neutralizing obtained potassium sulfate and a small amount of ash content and amino acid, and potassium sulfate sheet
Body is a kind of good potash fertilizer, and it is also a kind of good potash fertilizer that we can be used as the fertilizer of solid-state containing amino acid at this time;
Step 10: using the purposes after production as the industrial crops amino acid fertilizer such as tea, fruit and vegetable, animal feed additive, plant
Nutrition-retaining liquid etc..
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Cited By (4)
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CN111657300A (en) * | 2020-06-30 | 2020-09-15 | 安徽小溪生态科技发展有限公司 | Resource utilization method of livestock and poultry manure and straw and product |
CN112190595A (en) * | 2020-10-12 | 2021-01-08 | 安徽小溪生态科技发展有限公司 | Livestock and poultry excrement-based young animal immunomodulator and preparation method and application thereof |
CN113666590A (en) * | 2021-08-19 | 2021-11-19 | 安徽世绿环保科技有限公司 | Microwave sludge degradation system |
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CN111657300A (en) * | 2020-06-30 | 2020-09-15 | 安徽小溪生态科技发展有限公司 | Resource utilization method of livestock and poultry manure and straw and product |
CN112190595A (en) * | 2020-10-12 | 2021-01-08 | 安徽小溪生态科技发展有限公司 | Livestock and poultry excrement-based young animal immunomodulator and preparation method and application thereof |
CN113666590A (en) * | 2021-08-19 | 2021-11-19 | 安徽世绿环保科技有限公司 | Microwave sludge degradation system |
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