CN110464679B - Mud rubbing device and preparation method thereof - Google Patents
Mud rubbing device and preparation method thereof Download PDFInfo
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- CN110464679B CN110464679B CN201910843812.5A CN201910843812A CN110464679B CN 110464679 B CN110464679 B CN 110464679B CN 201910843812 A CN201910843812 A CN 201910843812A CN 110464679 B CN110464679 B CN 110464679B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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Abstract
The invention provides a mud rubbing device and a preparation method thereof. The mud rubbing device comprises the following components in percentage by weight: 0.05-2% of aloe vera leaf extract, 0.05-2% of pinus tomentosa extract, 0.4-1.1% of cutin exfoliating agent, 1.5-3% of thickening agent, 4-21% of humectant and the balance of water. The mud rubbing device is prepared by firstly mixing and homogenizing the thickening agent, the humectant, a part of the cutin peeling agent and water, and then adding the rest of the components and uniformly mixing. The mud rubbing device provided by the invention can quickly remove aged cutin without damaging skin, and has the advantages of quick mud rising, tender and smooth skin, no hair sticking and easiness in washing.
Description
Technical Field
The invention belongs to the technical field of washing and caring articles, and particularly relates to a mud rubbing device and a preparation method thereof.
Background
The human skin cells are continuously subjected to cycles of generation, aging and death, the aged and dead cells form cutin, and the newly generated cells gradually move to the cutin. The metabolism of the human skin is influenced by many factors such as diet, work and rest, mood, age, weather, etc. When the diet is unbalanced, the work and rest are irregular, or the skin is aged, the metabolism of skin cells is slowed down, and keratinocytes cannot normally fall off and are accumulated on the surface of the skin, so that the skin is rough and dull. In addition, when air dries, it also causes skin cells to be starved of water, accelerating the aging death and the keratin accumulation. Too thick stratum corneum will further affect the normal metabolism of the skin and exacerbate skin problems.
The mud rubbing device is also called mud rubbing bath device, is a washing and protecting cleaning article for removing aged cutin and dirt of skin, and can be smeared on the skin and gently rubbed to lead the aged cutin and the dirt to be gathered into mud scraps which are removed after being washed by water. CN 104546655A discloses a novel mud rubbing bathrobe, which is prepared from cumin plant mud-lifting factor, CHAMWHA composite essence, seaweed essence, mineral substances, vitamins and essential oil, wherein the cumin plant mud-lifting factor is extracted from the cumin cactus root sac in the Mexico desert. CN 104825345A discloses a mousse formula for removing dead skin, which consists of 30-60% of water agent and 40-70% of propellant; wherein the aqueous solution comprises: 1-10% of glycerol, 3-10% of sodium laureth sulfate, 3-5% of cocamidopropyl betaine, 1-3% of carbomer, 1-3% of behenyl trimethyl ammonium chloride and the balance of water; the product has a lot of fine and dense foams, and can deeply remove stratum corneum necrotic cells and promote skin metabolism.
However, the common mud rubbing device at present has the following disadvantages: 1. the mud is difficult to be generated by repeatedly kneading, and some mud is even not generated, and the generated mud is rare and the use feeling is poor; 2. the kneaded mud easily sticks to body hair, is difficult to wash, and has poor use feeling. Therefore, a mud rubbing product which has the advantages of quick mud lifting, no hair sticking and easy washing is to be developed to meet the market demand.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a mud rubbing device and a preparation method thereof. The mud rubbing device can quickly remove aged cutin without damaging skin, and has the advantages of quick mud lifting, tender and smooth skin, no hair sticking and easy washing.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the invention provides a mud rubbing device, which comprises the following components in percentage by weight:
0.05-2% of aloe vera leaf extract, 0.05-2% of pinus tomentosa extract, 0.4-1.1% of cutin exfoliating agent, 1.5-3% of thickening agent, 4-21% of humectant and the balance of water.
The aloe vera leaf extract contains active substance polysaccharide, amino acid, polypeptide, organic acid, vitamin and other water-soluble components, and can obviously enhance the water absorption performance of skin keratinized tissue; the codiales leptocembrae extract mainly comprises L-citrullinyl-L-arginine and galactosyl glycerol, can promote the synthesis of epidermal cell aquaporin-3, thereby enhancing the water circulation and the skin barrier function of the skin, has extremely strong water replenishing and moisturizing effects, can deeply permeate and moisturize from the surface layer, the middle layer and the deep layer of the skin, and naturally exfoliates through the permeation function.
According to the invention, the aloe barbadensis leaf extract and the pinus tomentosa extract are matched with each other, and the cutin stripping agent is combined, so that the removal of aged cutin can be obviously promoted, and the obtained mud rubbing device has the advantages of quick mud rising, no damage to skin, no hair sticking and easiness in washing.
In the present invention, the aloe vera leaf extract may be 0.05 to 2% by weight, for example, 0.05%, 0.06%, 0.07%, 0.08%, 0.09%, 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1%, 1.1%, 1.2%, 1.31%, 1.4%, 1.5%, 1.6%, 1.7%, 1.8%, 1.9%, or 2%. Preferably 0.8 to 1.5%.
The pinus hirsutus extract may be 0.05 to 2% by weight, for example, 0.05%, 0.06%, 0.07%, 0.08%, 0.09%, 0.1%, 0.2%, 0.3%, 0.4%, 0.5%, 0.6%, 0.7%, 0.8%, 0.9%, 1%, 1.1%, 1.2%, 1.31%, 1.4%, 1.5%, 1.6%, 1.7%, 1.8%, 1.9%, or 2%. Preferably 0.8 to 1.5%.
The exfoliating agent may be 0.4 to 1.1% by weight, for example, 0.4%, 0.45%, 0.5%, 0.55%, 0.6%, 0.65%, 0.7%, 0.75%, 0.8%, 0.85%, 0.9%, 0.95%, 1%, 1.05%, or 1.1%.
The thickener may be 1.5 to 3% by weight, for example, 1.5%, 1.6%, 1.7%, 1.8%, 1.9%, 2%, 2.1%, 2.2%, 2.3%, 2.4%, 2.5%, 2.6%, 2.7%, 2.8%, 2.9%, or 3% and the like.
The humectant may be present in an amount of 4-21% by weight, for example 4%, 5%, 6%, 7%, 8%, 9%, 10%, 12%, 13%, 15%, 16%, 18%, 20%, 21%, etc.
The following is a preferred technical solution of the present invention, but not a limitation to the technical solution provided by the present invention, and the object and advantageous effects of the present invention can be better achieved and achieved by the following preferred technical solution.
As a preferred technical scheme of the invention, the cutin peeling agent is behenyl trimethyl ammonium chloride.
As a preferred technical scheme, the thickening agent is carbomer.
Carbomer is acrylic acid crosslinked resin obtained by crosslinking pentaerythritol and the like with acrylic acid, is a very important rheology regulator, is an excellent gel matrix, has important purposes of thickening, suspending and the like, has simple process and good stability, and is widely applied to emulsion, cream and gel. Carbomers produce highly effective thickening at very low levels (0.25-0.5% of conventional levels) to produce emulsions, creams, gels and transdermal preparations of a wide range of viscosities and varying rheological properties.
As a preferred embodiment of the present invention, the humectant is selected from one or a combination of at least two of propylene glycol, glycerin or erythritol; typical but non-limiting examples of such combinations are: a combination of propylene glycol and glycerol, a combination of propylene glycol and erythritol, a combination of glycerol and erythritol, or a combination of propylene glycol, glycerol and erythritol.
Among them, erythritol has strong moisturizing and hygroscopic properties, and is useful as a moisturizing agent for cosmetics like glycerin, but does not have the greasy and sticky feeling of glycerin.
As a preferable technical scheme of the invention, the sludger also comprises 0.03-0.9% of solubilizer and 0.01-0.3% of aromatic.
Preferably, the solubilizer is hydrogenated castor oil.
Preferably, the hydrogenated castor oil is PEG-40 hydrogenated castor oil.
The fragrance may be a perfume.
Hydrogenated castor oil is a modified castor oil product, is a common high-efficiency solubilizer, and can uniformly disperse oily substances such as essence, essential oil and the like into water to form a stable and transparent solution. According to the difference of the epoxy group, it can be classified into PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PEG-80 hydrogenated castor oil, etc.
In a preferred embodiment of the present invention, the sticky candy further comprises 0.5-1% (e.g., 0.5%, 0.55%, 0.6%, 0.65%, 0.7%, 0.75%, 0.8%, 0.85%, 0.9%, 0.95%, or 1%) of a preservative.
Preferably, the preservative is selected from one or a combination of at least two of methyl hydroxybenzoate, phenoxyethanol or ethylhexyl glycerol; typical but non-limiting examples of such combinations are: methyl paraben in combination with phenoxyethanol, methyl paraben in combination with ethylhexylglycerin, phenoxyethanol in combination with ethylhexylglycerin, and the like.
As a preferred technical scheme of the invention, the mud rubbing device comprises the following components in percentage by weight:
0.8-1.5% of aloe vera leaf extract, 0.8-1.5% of pinus tomentosa extract, 0.4-1.1% of behenyl trimethyl ammonium chloride, 1.5-3% of carbomer, 1-10% of propylene glycol, 3-10% of glycerol, 0.1-1% of erythritol, 0.03-0.9% of PEG-40 hydrogenated castor oil, 0.01-0.3% of aromatic, 0.1-0.3% of methyl hydroxybenzoate, 0.35-0.5% of phenoxyethanol, 0.05-0.2% of ethylhexyl glycerol and the balance of water.
In a second aspect, the invention provides a preparation method of the mud rubbing device, which comprises the following steps:
(1) mixing thickener, humectant, 10-20% (such as 10%, 12%, 13%, 15%, 16%, 18% or 20%) cutin exfoliating agent and water, and homogenizing to obtain homogeneous solution;
(2) and (3) mixing the homogenized liquid obtained in the step (1) with the rest components to obtain the mud rubbing device.
As a preferable technical scheme of the invention, the temperature for mixing and homogenizing in the step (1) is 80-85 ℃, for example, 80 ℃, 81 ℃, 82 ℃, 83 ℃, 84 ℃ or 85 ℃ and the like; the time is 5-10min, such as 5min, 6min, 7min, 8min, 9min or 10 min.
Preferably, the mixing and homogenizing in the step (1) are carried out in a vacuum emulsifying pot.
Preferably, the temperature of the mixing in the step (2) is 40-45 ℃, for example, 40 ℃, 41 ℃, 42 ℃, 43 ℃, 44 ℃ or 45 ℃ and the like; the time is 5-10min, such as 5min, 6min, 7min, 8min, 9min or 10 min.
As a preferred technical scheme of the invention, the preparation method comprises the following steps:
(1) adding thickener, humectant, 10-20% cutin exfoliation agent and water into vacuum emulsifying pot, mixing and homogenizing at 80-85 deg.C for 5-10min to obtain homogeneous liquid;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 40-45 ℃, then adding the rest components, stirring and mixing for 5-10min, cooling to below 38 ℃, and discharging to obtain the pug device.
Compared with the prior art, the invention has the following beneficial effects:
the aloe vera leaf extract contains active substance polysaccharide, amino acid, polypeptide, organic acid, vitamin and other water-soluble components, and can obviously enhance the water absorption performance of skin keratinized tissue; the Pinus tomentosa extract mainly comprises L-citrulline-L-arginine and galactosyl glycerol, can promote synthesis of epidermal cell aquaporin-3, thereby enhancing water circulation and skin barrier function of skin, has extremely strong water replenishing and moisturizing effects, can deeply permeate and moisturize from the surface layer, the middle layer and the deep layer of the skin, and naturally removes cutin through the permeation function. According to the invention, the aloe barbadensis leaf extract and the pinus hirsutus extract are matched with each other, so that the synergy is realized, the effects of removing cutin and supplementing water of the aloe barbadensis leaf extract and the pinus hirsutus extract are improved, and the cutin remover is combined, so that the removal of aged cutin can be obviously promoted, and the effects of supplementing water, preserving moisture and tendering skin can be achieved. The obtained mud kneading device can quickly take out mud in 5-10 seconds, and a small amount of mud can be easily kneaded to obtain rich mud scraps; the skin care product is moist, fine and smooth, only old waste cutin is removed, the skin is not damaged, only dirt is cleaned, moisture is not taken away, and the skin becomes tender and smooth after the skin care product is used; the washing machine is free from hair sticking and easy to wash, can be washed after being rubbed with water, does not need external rubbing and washing, does not need secondary cleaning, and is easy and convenient to use.
Detailed Description
The technical solution of the present invention is further illustrated by the following specific examples. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
Example 1
The embodiment provides a mud rubbing device which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, 1/10 cutin exfoliant and water into vacuum emulsifying pan, mixing and homogenizing at 80 deg.C for 10min to obtain homogenized solution;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 45 ℃, then adding the rest components, stirring and mixing for 10min, cooling to 38 ℃, and discharging to obtain the mud rubbing device.
Example 2
The embodiment provides a mud rubbing device which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, cutin remover 1/10 and water into vacuum emulsifying pan, mixing and homogenizing at 85 deg.C for 5min to obtain homogeneous solution;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 40 ℃, then adding the rest components, stirring and mixing for 10min, cooling to 38 ℃, and discharging to obtain the mud rubbing device.
Example 3
The embodiment provides a mud rubbing device, which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, cutin remover 1/10 and water into vacuum emulsifying pot, mixing and homogenizing at 83 deg.C for 8min to obtain homogeneous solution;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 42 ℃, then adding the rest components, stirring and mixing for 8min, cooling to 38 ℃, and discharging to obtain the mud rubbing device.
Example 4
The embodiment provides a mud rubbing device which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, 1/10 cutin exfoliant and water into vacuum emulsifying pan, mixing and homogenizing at 85 deg.C for 10min to obtain homogenized solution;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 45 ℃, then adding the rest components, stirring and mixing for 10min, cooling to 38 ℃, and discharging to obtain the mud rubbing device.
Example 5
The embodiment provides a mud rubbing device which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, cutin remover 1/10 and water into vacuum emulsifying pot, mixing and homogenizing at 85 deg.C for 10min to obtain homogeneous solution;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 45 ℃, then adding the rest components, stirring and mixing for 10min, cooling to 38 ℃, and discharging to obtain the mud rubbing device.
Example 6
The embodiment provides a mud rubbing device, which comprises the following components in percentage by weight:
the preparation method of the mud rubbing device comprises the following steps:
(1) adding thickener, humectant, cutin remover 1/10 and water into vacuum emulsifying pot, mixing and homogenizing at 85 deg.C for 10min to obtain homogeneous solution;
(2) and (2) cooling the homogeneous liquid obtained in the step (1) to 45 ℃, then adding the rest components, stirring and mixing for 10min, cooling to 38 ℃, and discharging to obtain the slub paste.
Example 7
The difference between the mud rubbing agent and the mud rubbing agent in example 6 is that the weight percentage of the aloe barbadensis leaf extract is 0.05%, the weight percentage of the codium tomentosum extract is 1.95%, and other components and preparation methods are the same as those in example 6.
Example 8
The difference between the mud rubbing agent and the mud rubbing agent in example 6 is that the weight percentage of the aloe barbadensis leaf extract is 1.95%, the weight percentage of the codium tomentosum extract is 0.05%, and other components and preparation methods are the same as those in example 6.
Comparative example 1
The difference between the mud rubbing agent and the mud rubbing agent in example 6 is that the mud rubbing agent does not contain the aloe barbadensis leaf extract, the weight percentage of the codium tomentosum extract is 2%, and other components and the preparation method are the same as those in example 6.
Comparative example 2
The difference between the mud rubbing agent and the mud rubbing agent in example 6 is that the aloe barbadensis leaf extract accounts for 2 wt%, the aloe barbadensis leaf extract does not contain the codium tomentosum extract, and other components and preparation methods are the same as those in example 6.
Comparative example 3
The difference between the mud rubbing device and the mud rubbing device in example 6 is that the weight percentage of the cutin peeling agent is 0.3 percent, and other components and the preparation method are the same as those in example 6.
Comparative example 4
The difference between the mud rubbing agent and the mud rubbing agent in example 6 is that the weight percentage of the thickening agent is 1%, and other components and the preparation method are the same as those in example 6.
Performance evaluation:
(1) skin irritation test:
the swab packs provided in examples 1 to 8 were diluted to 10mg/mL with 20mmol/L PBS solution and used as sample solutions. 180 volunteers between the ages of 30-40 were selected as subjects and randomized into 9 groups of 20 individuals each. 0.05mL of the sample solution was taken by syringe and placed in a chamber of a spot test tape (PBS solution as a blank control), and the spot test tape with the sample solution was immediately stuck to the normal skin of the left forearm of the subject from the lower part thereof in the longitudinal direction while gently pressing the chamber one by one to remove air and to distribute the sample uniformly. The test site is marked for easy observation. The patch was applied every 24 hours and then removed for a second half hour and examined according to the CTFA guidelines for a total of 5 patch tests. On day 6 after completion of skin application, additional examination was performed to observe delayed reactions.
The criteria for the skin irritation test are shown in table 1 below:
TABLE 1
The results of the skin irritation test are shown in table 2 below:
TABLE 2
As can be seen from the results in table 2, the skin reactions of the subjects were all negative for the mud rub strips provided in examples 1 to 8, indicating that the mud rub strips provided by the present invention are non-irritating to human skin.
(2) Erythrocyte hemolysis experiment:
preparation of erythrocyte suspension: selecting healthy rabbits, taking 9mL of blood from heart, adding 1mL of 2% potassium oxalate solution, centrifuging, discarding supernatant, diluting the precipitate to 20mL with 20mmol/L PBS solution, and storing at 4 ℃ for later use.
Hemolysis experiment:
the strips provided in examples 1-8 were selected and diluted to different concentrations with PBS solution, with 5 concentration gradients set for each sample. Taking 10mL of a dilution of a sample to be detected, adding 200 μ L of the erythrocyte suspension (controlling the final concentration of the sample to be 5, 10, 20, 50 and 100mg/mL respectively), using distilled water as a full-blood-soluble control and PBS solution as a negative control, gently mixing, incubating at 37 ℃ for 30min, centrifuging at 2000r/min for 10min, taking the supernatant, and testing the absorbance (A) at 560nm by using a spectrophotometer560) Calculating the hemolysis rate according to the following formula;
a standard curve of hemolysis rate vs. sample concentration was plotted, and the sample concentration at which hemolysis occurred in 50% erythrocytes (HD) was calculated50)。
Protein denaturation experiments:
diluting the Mianbao provided in examples 1-8 to 10g/L with PBS, taking 10mL of the dilution of the sample to be tested, adding 200 μ L of the erythrocyte suspension, taking distilled water as a blank control and 1mg/mL of Sodium Dodecyl Sulfate (SDS) solution as a positive control, mixing gently, incubating at 37 ℃ for 30min, centrifuging at 2000r/min for 10min, taking the supernatant, and testing the absorbance A at 540nm and 575nm respectively with a spectrophotometer540And A575Calculating a protein Denaturation Index (DI) according to the following formula;
wherein R is1Blank control group a575Blank control group A540,R2Experimental group a575Experimental group A540,R3Positive control group A575Positive control group A540。
Evaluating the irritation of the sample to be tested according to the L/D value, wherein the L/D value is HD50DI, erythrocyte hemolysis assay irritation grading criteria are shown in Table 3 below:
TABLE 3
L/D | Grading |
﹥100 | Has no irritation |
10﹤L/D≤100 | Micro-stimulation property |
1﹤L/D≤10 | Mild irritation |
0.1﹤L/D≤1 | Moderate irritation |
L/D≤0.1 | Severe irritation |
The results of the above-described experiments for hemolysis of erythrocytes are shown in table 4 below:
TABLE 4
Test sample | HD50(mg/L) | DI(%) | L/D | Evaluation of |
Example 1 | 12725 | 0.76 | ﹥100 | Has no irritation |
Example 2 | 4984 | 1.38 | ﹥100 | Has no irritation |
Example 3 | 6326 | 1.15 | ﹥100 | Has no irritation |
Example 4 | 5357 | 1.24 | ﹥100 | Has no irritation |
Example 5 | 5472 | 1.27 | ﹥100 | Has no irritation |
Example 6 | 6639 | 0.93 | ﹥100 | Has no irritation |
Example 7 | 5785 | 1.17 | ﹥100 | Has no irritation |
Example 8 | 5661 | 1.22 | ﹥100 | Has no irritation |
As can be seen from the results in Table 4, the samples of examples 1-8 all provided clay liners having L/D values greater than 100, and were non-irritating.
(2) And (3) a mud-forming effect test:
120 female volunteers between the ages of 30-40 were selected as subjects, randomized into 12 groups of 10 people each. Test areas of 3cm × 3cm were drawn on the left and right sides of the face of the subject, 0.5mL of the mud pads provided in examples 1 to 8 and comparative examples 1 to 4 were uniformly applied to the test areas, respectively, and the subject gently rubbed the left side of the face with the left hand and gently rubbed the right side of the face with the right hand, and the time to start mud-up was recorded, and the results are shown in the following table 5:
TABLE 5
As can be seen from the results in Table 5, the mud rubbings provided in examples 1-8 were faster to be slimed within 5-10s by compounding the aloe barbadensis leaf extract and the codium tomentosum extract with the exfoliating agent. In addition, since the ratio of the aloe vera leaf extract to the codium tomentosum extract in the pugmo provided in example 7 is small, and the ratio of the aloe vera leaf extract to the codium tomentosum extract in the pugmo provided in example 8 is large, the cooperation effect of the aloe vera leaf extract and the codium tomentosum extract is not sufficiently exerted, the mud lifting time of the pugmo provided in examples 7 and 8 is longer than that of example 6.
Comparative example 1 the aloe vera leaf extract was not contained, and comparative example 2 the pinus tomentosa extract was not contained, and the compounding relationship between the aloe vera leaf extract and the pinus tomentosa extract was broken; comparative example 3 the obtained mud rub has a low mud rising speed and a small mud rising amount because the addition amount of the cutin peeling agent is small and the capability of removing aged cutin is insufficient. Comparative example 4 the same is slower in the mud-lifting speed because the thickener is less added, the viscosity of the mud-rolling device is lower, and the aging cutin and dirt aggregation are not facilitated.
(3) Skin moisturizing effect test
Selecting 15 females and 15 males as test objects, drawing test areas with the size of 3cm multiplied by 3cm on the inner sides of the left forearm and the right forearm of the test objects respectively, and testing the moisture content of the skin of the test areas of the test objects by using a skin moisture tester; then 0.5mL of the mud rub strips provided in examples 1-8 and comparative examples 1-4 were uniformly applied to the test area of the left arm of the subject, the test area of the right arm was applied with placebo cream as a blank control, after 30min, the mud rub strips in the test area of the left arm were wiped off, the skin moisture content in the test area was again measured with a skin moisture tester, and the variation value of the skin moisture content was calculated, and the evaluation criteria and the test results of the skin moisturizing effect were respectively shown in the following tables 6 and 7:
TABLE 6
Grade of moisturizing effect | Is on the low side | Medium grade | Is good | Is excellent in |
2h change in Water content | ≤10% | 10-20% | 20-30% | ≥30% |
TABLE 7
As can be seen from the results in table 7, the mud rub provided by the present invention has moderate moisturizing effect, and helps to keep skin tender and smooth by cleaning dirt without moisture. Examples 7 and 8 the skin moisture content was less increased because the ratio of aloe vera leaf extract to pinus tomentosa extract was either smaller or larger, respectively, which is detrimental to the combination of moisturizing effect of both. Comparative examples 1 and 2 have a low moisturizing effect because only one of the extracts exerts a moisturizing effect without the aloe vera leaf extract and the pinus tomentosa extract, respectively, and the compounding relationship between the aloe vera leaf extract and the pinus tomentosa extract is broken.
The applicant declares that the above description is only a specific embodiment of the present invention, but the scope of the present invention is not limited thereto, and it should be understood by those skilled in the art that any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are within the scope and disclosure of the present invention.
Claims (6)
1. The mud rubbing device is characterized by comprising the following components in percentage by weight:
0.8-1.5% of aloe barbadensis leaf extract, 0.8-1.5% of pinus hirsutus extract, 0.4-1.1% of behenyl trimethyl ammonium chloride, 1.5-3% of carbomer, 1-10% of propylene glycol, 3-10% of glycerol, 0.1-1% of erythritol, 0.03-0.9% of PEG-40 hydrogenated castor oil, 0.01-0.3% of aromatic, 0.1-0.3% of methylparaben, 0.35-0.5% of phenoxyethanol, 0.05-0.2% of ethylhexyl glycerol and the balance of water;
wherein, the behenyl trimethyl ammonium chloride is a cutin peeling agent, the carbomer is a thickening agent, and the propylene glycol, the glycerol and the erythritol are humectants.
2. The mud scraper preparation method according to claim 1, wherein the preparation method comprises the following steps:
(1) mixing and homogenizing a thickening agent, a humectant, 10-20% of a cutin peeling agent and water to obtain a homogenized liquid;
(2) and (2) mixing the homogenized liquid obtained in the step (1) with the rest components to obtain the sludger.
3. The method according to claim 2, wherein the temperature for mixing and homogenizing in step (1) is 80-85 ℃ and the time is 5-10 min.
4. The method according to claim 2, wherein the mixing and homogenizing in the step (1) are performed in a vacuum emulsifying kettle.
5. The method according to claim 2, wherein the mixing in the step (2) is carried out at a temperature of 40 to 45 ℃ for 5 to 10 min.
6. The method of claim 2, comprising the steps of:
(1) adding thickener, humectant, 10-20% cutin exfoliation agent and water into vacuum emulsifying pot, mixing and homogenizing at 80-85 deg.C for 5-10min to obtain homogeneous liquid;
(2) and (2) cooling the homogenized liquid obtained in the step (1) to 40-45 ℃, then adding the rest components, stirring and mixing for 5-10min, cooling to below 38 ℃, and discharging to obtain the pug device.
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