CN110464659A - A kind of anhydrous muffin and preparation method thereof - Google Patents
A kind of anhydrous muffin and preparation method thereof Download PDFInfo
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- CN110464659A CN110464659A CN201910678365.2A CN201910678365A CN110464659A CN 110464659 A CN110464659 A CN 110464659A CN 201910678365 A CN201910678365 A CN 201910678365A CN 110464659 A CN110464659 A CN 110464659A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The present invention provides a kind of anhydrous muffins and preparation method thereof, belong to daily cosmetics field, including A phase, B phase and C phase, wherein A phase includes mica, talcum powder and titanium dioxide, B phase includes iron oxide yellow and iron oxide red, and C phase includes sad certain herbaceous plants with big flowers acid glycerol three ester, galam butter, pentaerythritol tetraoctyl stearate and Phenoxyethanol；By the component in high speed dispersion A phase, the component of exquisiteness B phase is then ground, then mixes the component in A phase and B phase, disposable C phase of spraying is last all to carry out moderate-speed mixer, compacting, molding, demoulding, finished product into the A phase and B phase mixed.The present invention has the function of that face is repaired in concealing, select the ingredient of mild pro-skin and nourishing, mix suitable facial skin pH, and the anhydrous muffin long naturally with adornment effect is held with makeup, preparation method by simplifying simultaneously, reach and effectively keep the activity of ingredient, be uniformly dispersed, and reduce dust, to drop low-loss effect.
Description
Technical field
The present invention relates to daily cosmetics field, a kind of anhydrous muffin and preparation method thereof is particularly belonged to.
Background technique
Muffin is cosmetics indispensable in people's daily life, by a variety of powder materials and adhesive by mixing, compacting
Made of cake solids beautification product, have the function of covering, attachment, Tu Zhan, colouration and modification.And muffin is as color make-up system
Column, traditional ingredient and manufacture craft cause it that can only tentatively cover in certain defects on skin, flaw and the modification colour of skin
The problem of, but do not have reparation and protect the effect of skin, moreover, could not also cater to the characteristic of skin in the market, produce mild
The muffin of pro-skin and suitable skin ph, muffin in the market can only cover flaw for the moment, the quality of skin but allowed to cannot get
Improve, or even worse and worse.
Meanwhile if be easy to be condensed into blocks when the muffin of commercial type adds water, dispersion effect it is poor, without adding
The muffin adhesiveness of moisture is poor, silty is dry, can especially form striped after absorbing sweat on the skin, leads to makeup and holds adornment effect
Fruit is poor, not enough naturally.
In addition, traditional anhydrous muffin preparation process is that direct pressing forms after dispersion stirring, silty is loose, powder
Dirt is larger, and more and more difficult compression moulding is lost.
Therefore it provides going out a kind of while there is concealing effect, it is suitble to skin pH value, preferably repairs and nourish human body
Skin, and with makeup naturally and hold the long anhydrous muffin and preparation method thereof of adornment effect be field technical staff there is an urgent need to
It solves the problems, such as.
Summary of the invention
For the problems of background technique, the present invention provides a kind of anhydrous muffins and preparation method thereof, have and hide
The flaw repairs the effect of face, and the ingredient of mild pro-skin and nourishing is selected to mix suitable facial skin pH according to the pH value of skin,
With the anhydrous muffin that makeup is long naturally with adornment effect is held, while passing through the preparation method simplified, effectively keep the activity of ingredient,
Reach and be uniformly dispersed and reduce dust, reduces the effect of loss.
To achieve the above object, the present invention is achieved by the following scheme:
A kind of anhydrous muffin and preparation method thereof, is made of A phase, B phase and C phase, and the A phase includes below according to weight
Measure the component of number:
Mica: 42-47 parts；
Talcum powder: 33-38 parts；
Titanium dioxide: 8-10 parts；
The B phase includes following component according to parts by weight:
Iron oxide yellow: 0.26-0.34 parts；
Iron oxide red: 0.08-0.12 parts；
The C phase includes following component according to parts by weight:
Sad certain herbaceous plants with big flowers acid glycerol three ester: 2.9-3.3 parts；
Natural oil: 2.7--3.2 parts；
Pentaerythritol tetraoctyl stearate: 3.6-4.1 parts；
Phenoxyethanol: 0.3-0.4 parts.
The measure further taken is: the mica is that silicon handles mica, and wet-milling calcinated type mica is selected to be answered
Silicon cladding and surface-catalyzed reactions are closed, surface is smooth, and powder high resilience has the fabulous transparency, and particle diameter distribution is uniform, so that
The more aobvious soft and silk of skin feel is sliding.
The measure further taken is: the talcum powder is that silicon handles talcum powder, and subtle talcum powder is selected to be answered
Close silicon cladding and surface-catalyzed reactions so that powder have superior coating, briquettability and hydrophobicity, even particle size distribution,
Whiteness is high, the smooth exquisiteness of feel, good fluidity, has good dispersibility and the intermiscibility in oily phase, keeps dressing lasting, and
It is effectively improved the suppression performance of product, has more texture.
The measure further taken is: the natural oil includes animal fat and vegetable fat, specially wool
One of rouge, galam butter, olive oil, grape seed oil or several components mixed.Wherein, lanolin originates in Australia
Continent, by Refining, purity has the effect of excellent moisturizing, emulsification, stabilization, moist and compatibility 99% or more；Ox
The ingredients such as oily fruit oil vitamin rich in, sterol, lecithin to skin safe, have good nutrition, moisten and its seep
Effect thoroughly, skin and muscles are fair, careful glossy for order；Olive oil is rich in the squalene splendid with skin affinity and rouge needed by human
Fat acid, absorption rapidly, effectively keep skin elasticity and moisten, it is anti-that there are also monounsaturated fatty acids abundant, vitamin and phenols
Oxidation material, the effect of facial wrinkles can be eliminated, skin aging is prevented, resist ultraviolet light and nourish skin care；Grape seed oil is rich in
Linolenic oil and proanthocyanidin can resist free radical, and anti-aging, prevention melanin deposition, penetration are strong, while nutrition and profit
The effect of damp skin.
The sad certain herbaceous plants with big flowers acid glycerol three ester of selection is high-purity grease, has good spreadability, while keeping skin moisturizing soft
With, glossy, stable and smooth but not greasy effect.
The pentaerythritol tetraoctyl stearate of selection clearly moistens and non-greasy, the pH value of silty is adjusted, general powder
Cake pH value 8-9 is adjusted and is arrived pH value 7.2-7.8, while keeping silty soft, not loose, is preferably adhered to skin and is held adornment effect
More preferably.
The second object of the present invention is to provide a kind of preparation method of anhydrous muffin, does not need complicated technique production,
Complicated technology bring operational risk is effectively reduced, uses manpower and material resources sparingly, while various components being allowed to be sufficiently mixed, does not damage beneficial
The factor and component characteristic, there is the anhydrous muffin prepared of cooperation this method good concealing, protection effect and nutrition to moisten,
Improve skin quality, anti-aging and mild safe effect.
For this purpose, the present invention also provides a kind of preparation methods of anhydrous muffin, comprising the following steps:
1) in agitated kettle, it is put into each component for corresponding to number in A phase one by one, carries out high speed dispersion, revolving speed 2000-
3000 revs/min, the time is 20-50 seconds, then stops stirring, clears up pot side and upper cover powder, repeats the primary high speed point of progress
Dissipate and clear up pot side and upper cover powder；
2) scattered A phase 200g is taken out from pot, and is put into togerther pulverizer with each component for corresponding to number in B phase
In, it carries out grinding dispersion and grinding is fine and smooth；
3) it takes out the good component of ground and mixed in step 2) and is reentered into the agitated kettle of A phase, each part will be corresponded in C phase
Several groups are distributed into spout pouring pot, and the oil-blast switch of spout pouring pot is connected to the agitated kettle of A phase, and starting agitated kettle carries out high speed
Oil-blast switch is opened while stirring, the component of C phase is disposably sprayed into agitated kettle and is sufficiently mixed with A phase and B phase, closes oil spout
Switch；
4) revolving speed in agitated kettle is adjusted to 500-1500 revs/min of middling speed, stirring is closed after 10-20 seconds, is then cleared up
Pot side and upper cover powder continue 500-1500 revs/min of middling speed, stir 10-20 seconds, form D phase, stop stirring；
5) discharging is put into D phase in full-automatic pressure mill and carries out press-powder, and first precompressed 2-3 seconds, pressure 20-40MPa, then
Pressure maintaining, the molding, demoulding for carrying out 4-6 seconds, obtain finished product.
Through the above technical solutions, compared with prior art, the present invention possessed have the beneficial effect that:
1, the present invention not only has concealing effect, and mildly safety, nutritional ingredient therein can provide needed for skin component
Nutrition, and also have the function of moisturizing, anti-aging and antiultraviolet；
2, the present invention is deployed according to the pH value of human skin, so that the pH value of silty complies fully with the pH of human skin
Value keeps skin vigor, and the makeup effect lasting with nature to not destroy the acid-base balance of skin；
3, the present invention is whole does not add water, by oil, ester it is reasonably combined, enhance the adhesiveness of silty, so that silty is soft
With exquisiteness；
4, the present invention is effectively reduced in the operational risk and production process of complicated technology and is generated by the technique production simplified
Dust, use manpower and material resources sparingly, and can effective protection Ingredients Active, filled while not damaging beneficial agents and substance characteristics
Divide the interaction increased between substance, to play the beneficial effect of formula to greatest extent.
Specific embodiment
In order to better understand the technical solution adopted in the present invention, the preferred embodiment of the present invention is said below
It is bright, it should be understood that embodiment described herein is only for the purpose of illustrating and explaining the present invention and is not intended to limit the present invention.
Embodiment 1: a kind of anhydrous muffin is made of A phase, B phase and C phase, and the A phase includes below according to parts by weight
Several components:
Mica: 45.41 parts；
Talcum powder: 35.00 parts；
Titanium dioxide: 9.00 parts；
The B phase includes following component according to parts by weight:
Iron oxide yellow: 0.29 part；
Iron oxide red: 0.10 part；
The C phase includes following component according to parts by weight:
Sad certain herbaceous plants with big flowers acid glycerol three ester: 3.10 parts；
Galam butter: 2.90 parts；
Pentaerythritol tetraoctyl stearate: 3.80 parts；
Phenoxyethanol: 0.40 part.
And it is prepared by following steps:
1) in agitated kettle, it is put into each component for corresponding to number in A phase one by one, carries out high speed dispersion, revolving speed 2000-
3000 revs/min, the time is 20-50 seconds, then stops stirring, clears up pot side and upper cover powder, repeats the primary high speed point of progress
Dissipate and clear up pot side and upper cover powder；
2) scattered A phase 200g is taken out from pot, and is put into togerther pulverizer with each component for corresponding to number in B phase
In, it carries out grinding dispersion and grinding is fine and smooth；
3) it takes out the good component of ground and mixed in step 2) and is reentered into the agitated kettle of A phase, each part will be corresponded in C phase
Several groups are distributed into spout pouring pot, and the oil-blast switch of spout pouring pot is connected to the agitated kettle of A phase, and starting agitated kettle carries out high speed
Oil-blast switch is opened while stirring, the component of C phase is disposably sprayed into agitated kettle and is sufficiently mixed with A phase and B phase, closes oil spout
Switch；
4) revolving speed in agitated kettle is adjusted to 500-1500 revs/min of middling speed, stirring is closed after 10-20 seconds, is then cleared up
Pot side and upper cover powder continue 500-1500 revs/min of middling speed, stir 10-20 seconds, form D phase, stop stirring；
5) discharging is put into D phase in full-automatic pressure mill and carries out press-powder, and first precompressed 2-3 seconds, pressure 20-40MPa, then
Pressure maintaining, the molding, demoulding for carrying out 4-6 seconds, obtain finished product.
Anhydrous muffin 1 has been prepared with method and step by being formulated above.
Embodiment 2: a kind of anhydrous muffin is made of A phase, B phase and C phase, and the A phase includes below according to parts by weight
Several components:
Mica: 43.00 parts；
Talcum powder: 37.22 parts；
Titanium dioxide: 9.00 parts；
The B phase includes following component according to parts by weight:
Iron oxide yellow: 0.26 part；
Iron oxide red: 0.12 part；
The C phase includes following component according to parts by weight:
Sad certain herbaceous plants with big flowers acid glycerol three ester: 3.3 parts；
Lanolin+olive oil: 2.70 parts；
Pentaerythritol tetraoctyl stearate: 4.10 parts；
Phenoxyethanol: 0.30 part.
And it is prepared by following steps:
1) in agitated kettle, it is put into each component for corresponding to number in A phase one by one, carries out high speed dispersion, revolving speed 2000-
3000 revs/min, the time is 20-50 seconds, then stops stirring, clears up pot side and upper cover powder, repeats the primary high speed point of progress
Dissipate and clear up pot side and upper cover powder；
2) scattered A phase 200g is taken out from pot, and is put into togerther pulverizer with each component for corresponding to number in B phase
In, it carries out grinding dispersion and grinding is fine and smooth；
3) it takes out the good component of ground and mixed in step 2) and is reentered into the agitated kettle of A phase, each part will be corresponded in C phase
Several groups are distributed into spout pouring pot, and the oil-blast switch of spout pouring pot is connected to the agitated kettle of A phase, and starting agitated kettle carries out high speed
Oil-blast switch is opened while stirring, the component of C phase is disposably sprayed into agitated kettle and is sufficiently mixed with A phase and B phase, closes oil spout
Switch；
4) revolving speed in agitated kettle is adjusted to 500-1500 revs/min of middling speed, stirring is closed after 10-20 seconds, is then cleared up
Pot side and upper cover powder continue 500-1500 revs/min of middling speed, stir 10-20 seconds, form D phase, stop stirring；
5) discharging is put into D phase in full-automatic pressure mill and carries out press-powder, and first precompressed 2-3 seconds, pressure 20-40MPa, then
Pressure maintaining, the molding, demoulding for carrying out 4-6 seconds, obtain finished product.
Anhydrous muffin 2 has been prepared with method and step by being formulated above.
In addition, the present invention has purchased muffin conventional on the market, and the nothing produced respectively with embodiment 1 and embodiment 2
Pigment cake 1 and anhydrous muffin 2 have carried out following tests.
Test method: 200 people of the 18-30 years old healthy women in areal is randomly selected as subject, the face of subject
Portion's no inflammation or allergic symptom, but face has slightly dry symptom, are then randomly assigned into 4 groups, code set 1 to 4, often
50 people of group.Subject's every morning is primary and afternoon is primary, using the sample uniform application of distribution in face, and after use 5
Effect and impression feedback are carried out in hour, and records one month service condition and carries out data summarization analysis, as a result such as the following table 1
With table 2:
Table 1: the result that muffin 1 compares experiment with conventional muffin counts
Table 2: the result that muffin 2 compares experiment with conventional muffin counts
By two above experiment, four groups of data compare and induction and conclusion, it can be clearly seen that, the present invention prepares
Anhydrous muffin have the effect of preferably nourishing, protect skin and hold adornment compared to common muffin in the market.
The above is only used to illustrate the technical scheme of the present invention and not to limit it, and ordinary people in the field is to of the invention
Other modifications or equivalent replacement that technical solution is made as long as it does not depart from the spirit and scope of the technical scheme of the present invention should all
It is included within the scope of the claims of the present invention.
Claims (5)
1. a kind of anhydrous muffin, which is characterized in that be made of A phase, B phase and C phase, the A phase includes below according to weight
The component of number:
Mica: 42-47 parts；
Talcum powder: 33-38 parts；
Titanium dioxide: 8-10 parts；
The B phase includes following component according to parts by weight:
Iron oxide yellow: 0.26-0.34 parts；
Iron oxide red: 0.08-0.12 parts；
The C phase includes following component according to parts by weight:
Sad certain herbaceous plants with big flowers acid glycerol three ester: 2.9-3.3 parts；
Natural oil: 2.7--3.2 parts；
Pentaerythritol tetraoctyl stearate: 3.6-4.1 parts；
Phenoxyethanol: 0.3-0.4 parts.
2. a kind of anhydrous muffin according to claim 1, it is characterised in that: the mica is that silicon handles mica, and selects
The processing of comprehensive silicon cladding and surface-catalyzed reactions is carried out with wet-milling calcinated type mica.
3. a kind of anhydrous muffin according to claim 1, it is characterised in that: the talcum powder is that silicon handles talcum powder,
Subtle talcum powder is selected to carry out the processing of comprehensive silicon cladding and surface-catalyzed reactions.
4. a kind of anhydrous muffin according to claim 1, it is characterised in that: the natural oil include animal fat and
One of vegetable fat, specially lanolin, galam butter, olive oil, grape seed oil or several components mixed.
5. the preparation method of anhydrous muffin according to any one of claims 1 to 4, which comprises the following steps:
1) in agitated kettle, it is put into each component for corresponding to number in A phase one by one, carries out high speed dispersion, revolving speed 2000-3000
Rev/min, the time is 20-50 second, then stops stirring, clears up pot side and upper cover powder, repeat high speed dispersion of progress with
Clear up pot side and upper cover powder；
2) scattered A phase 200g is taken out from pot, and is put into togerther in pulverizer with each component for corresponding to number in B phase, into
Row grinding dispersion and grinding are fine and smooth；
3) it takes out the good component of ground and mixed in step 2) and is reentered into the agitated kettle of A phase, each number will be corresponded in C phase
Group is distributed into spout pouring pot, and the oil-blast switch of spout pouring pot is connected to the agitated kettle of A phase, and starting agitated kettle carries out high-speed stirred
While open oil-blast switch, the component of C phase is disposably sprayed into agitated kettle and is sufficiently mixed with A phase and B phase, close oil spout open
It closes；
4) revolving speed in agitated kettle is adjusted to 500-1500 revs/min of middling speed, stirring is closed after 10-20 seconds, then clears up pot side
With upper cover powder, continue 500-1500 revs/min of middling speed, stir 10-20 seconds, form D phase, stops stirring；
5) discharging is put into D phase in full-automatic pressure mill and carries out press-powder, and first precompressed 2-3 seconds, then pressure 20-40MPa is carried out
Pressure maintaining in 4-6 seconds, molding, demoulding, obtain finished product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113244157A (en) * | 2021-06-04 | 2021-08-13 | 何平蓉 | Anti-darkness makeup powder cake and preparation method thereof |
| CN115252491A (en) * | 2022-07-19 | 2022-11-01 | 浙江名妆化妆品有限公司 | Water-soluble dry powder cake and production process thereof |
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