CN110463693A - A kind of synergist and its application for aqueous pesticide - Google Patents
A kind of synergist and its application for aqueous pesticide Download PDFInfo
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- CN110463693A CN110463693A CN201910857896.8A CN201910857896A CN110463693A CN 110463693 A CN110463693 A CN 110463693A CN 201910857896 A CN201910857896 A CN 201910857896A CN 110463693 A CN110463693 A CN 110463693A
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- synergist
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/24—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients to enhance the sticking of the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of synergist for aqueous pesticide and its application, the synergist includes the raw material of following weight percent: terpinum 5-10%, phytic acid 1-3%, disodium ethylene diamine tetraacetate 5-10%, porphines 0.5-1.5%, emulsifier 10-20%, bleeding agent 5-10%, defoaming agent 0.5-2%, antifreezing agent 1-3%;Surplus is water.Synergistic effect of the synergist provided by the invention due to each component; synergist is enabled to significantly improve wetability, permeability, stability, the adhesiveness etc. of pesticide in aqueous pesticide preparation; promote quick absorption of the plant leaf surface to pesticide; reduce the usage amount of pesticide; so that the drug effect of pesticide enhances; be conducive to preferably play the effect of chemical pesticide and it can be made to increase the preventive effect to harmful organism, reduces cost, preserve the ecological environment.
Description
Technical field
The invention belongs to insecticides adjuvant technical field, specifically a kind of synergist and its application for aqueous pesticide.
Background technique
Insecticides adjuvant itself typically no bioactivity in the processing and application of the formulations of pesticide, but in form formula
In or while being administered be indispensable additive, every kind of insecticides adjuvant has specific function, and what is played the role of plays dilution raw medicine,
What is had helps raw medicine to be evenly dispersed in preparation, and what is had prevents grain cohesion from becoming larger, and what is had increases the wet of particle
Property, adhesiveness or permeability, what is had prevents the decomposition of effective component, the safety etc. for increasing application having, in short, agriculture
The function of medicine auxiliary agent plays drug effect to the maximum extent or helps to apply safely nothing more than the physically or chemically performance for improving pesticide
Medicine, insecticides adjuvant are the progress with formulation and pesticide application technology and develop that auxiliary agent is rarely employed in the inorganic pesticide of early stage, from
Organic agricultural chemicals development after, various auxiliary agents also grow up therewith, with dosage form diversification and performance raising, auxiliary agent also to
Multi items, seriation development, to adapt to the needs of different pesticide species different dosage forms processing.
Aqua is one kind of water-based pesticide agent type, is that water-soluble pesticide is dissolved in the water and adds auxiliary agent and is made
Preparation.The pesticide species that can be made into aqua currently on the market are less, and some traditional pesticides are difficult to be made into water-soluble system
Agent, this also greatly limits the development of water soluble pesticide.Nevertheless, the yield of China's aqua is also very big in recent years, account for about whole
The 15%-20% of a preparation, principal item are gyphosate solutions, and in addition there are also 20% paraquat, 25% prowers and diformazans
Tetrachloro aqueous solvent etc. water-soluble products.
Pesticide synergistic agent is also a kind of insecticides adjuvant, when it is with specific combined use of pesticides, can increase substantially the poison of pesticide
Property and drug effect, are therefore widely used in all kinds of pesticidal preparations.Therefore, study it is a kind of soak, sprawl, osmotic effect is significant,
Stability be used on aqueous pesticide synergist be current market demand.
The disclosure of background above technology contents is only used for auxiliary and understands inventive concept and technical solution of the invention, not
The prior art for necessarily belonging to present patent application shows above content in the applying date of present patent application in no tangible proof
In the case where having disclosed, above-mentioned background technique should not be taken to the novelty and creativeness of evaluation the application.
Summary of the invention
It can be used in improving the wetting of aqueous pesticide, sprawl, permeate, adhere to, stablize it is an object of that present invention to provide a kind of
The synergist of performance, the synergist can be applied very well in the aqueous pesticides such as glyphosate, glufosinate-ammonium, dimehypo, jinggangmeisu.
In order to achieve the goal above, The technical solution adopted by the invention is as follows:
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum 5-
10%, phytic acid 1-3%, disodium ethylene diamine tetraacetate 5-10%, porphines 0.5-1.5%, emulsifier 10-20%, bleeding agent 5-
10%, defoaming agent 0.5-2%, antifreezing agent 1-3%;Surplus is water.
Preferably, the emulsifier includes polyoxyethylene alkylphenol ether, cocoamidopropyl betaine, dodecyl
One of sodium sulfonate, acrylic acid rosin polyoxyethylene sucrose ester, Polyoxyethylene fatty acid amides fatty acid ester or multiple combinations.
Preferably, the bleeding agent include organic silicon infiltration agent, ricinoleic acid butyl ester sodium sulphate, N-Methyl pyrrolidone,
One of N-dodecylpyrrolidone, azone bleeding agent or multiple combinations.
Preferably, the antifreezing agent includes one of glycerine, ethylene glycol, triethanolamine, triisopropanolamine or a variety of
Combination.
Preferably, the defoaming agent is silicone emulsion, polyoxyethylene polyoxypropylene pentaerythrite ether, dimethyl silicone polymer
One of or multiple combinations.
The preparation method of synergist of the present invention, after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, second
Homogenizer is added in edetate disodium, porphines, emulsifier, bleeding agent, defoaming agent, antifreezing agent and water, and high-speed stirred mixing is equal
It is even.
Preferably, the synergist is applied to insecticide, fungicide or the herbicide that dosage form is aqua.It such as applies in careless ammonium
In the aqueous pesticides such as phosphine, glyphosate, dimehypo, jinggangmeisu.
Preferably, the usage amount of the synergist is the 1-10% for accounting for aqueous pesticide mass percent.
Compared with prior art, it advantages of the present invention and has the beneficial effect that
1, terpinum, phytic acid, disodium ethylene diamine tetraacetate is just added in the present invention on the basis of original aqueous pesticide auxiliary agent
Due to the synergistic effect of each component synergist is significantly improved in aqueous pesticide preparation with synergist made from porphines
Wetability, permeability, stability, adhesiveness of pesticide etc. promote quick absorption of the plant leaf surface to pesticide, reduce making for pesticide
Dosage is conducive to preferably play the effect of chemical pesticide and it can be made to increase to harmful organism so that the drug effect of pesticide enhances
Preventive effect, reduce cost, preserve the ecological environment.
2, synergist provided by the invention can be widely applied in aqueous pesticide, have broad spectrum activity, environmental protection, it is degradable, at
The advantages that this is lower, synergy is significant has extensive market application prospect, is suitble to industrialized production.
Specific embodiment
Invention is further described in detail With reference to embodiment.It is emphasized that following the description is only
It is merely exemplary, the range and its application being not intended to be limiting of the invention.
Embodiment 1
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
6%, phytic acid 2.5%, disodium ethylene diamine tetraacetate 5%, porphines 1.8%, cocoamidopropyl betaine 15%, ricinoleic acid
Butyl ester sodium sulphate 6%, rolydimethylsiloxane defoamer 1%, triisopropanolamine 2%;Surplus is water.
Preparation method are as follows: after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, disodium ethylene diamine tetraacetate,
Porphines, cocoamidopropyl betaine, ricinoleic acid butyl ester sodium sulphate, rolydimethylsiloxane defoamer, triisopropanolamine
Homogenizer is added in antifreezing agent and water, and high-speed stirred is uniformly mixed.
Embodiment 2
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
8%, phytic acid 2%, disodium ethylene diamine tetraacetate 7%, porphines 0.8%, Octylphenol polyoxyethylene ether 10%, N- crassitude
Ketone 6%, silicone emulsion 1.5%, ethylene glycol 1.5%;Surplus is water.
Preparation method are as follows: after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, disodium ethylene diamine tetraacetate,
Homogenizer, high-speed stirred is added in porphines, Octylphenol polyoxyethylene ether, N-Methyl pyrrolidone, silicone emulsion, ethylene glycol and water
It is uniformly mixed.
Embodiment 3
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
10%, phytic acid 1.5%, disodium ethylene diamine tetraacetate 5%, porphines 1.2%, dodecyl sodium sulfate 15%, azone bleeding agent
8%, silicone emulsion defoaming agent 1%, glycerine 2.5%;Surplus is water.
Preparation method are as follows: after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, disodium ethylene diamine tetraacetate,
Homogenizer, high speed is added in porphines, dodecyl sodium sulfate, azone bleeding agent, silicone emulsion defoaming agent, glycerine antifreezing agent and water
It is uniformly mixed.
Embodiment 4
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
8%, phytic acid 2.8%, disodium ethylene diamine tetraacetate 7%, porphines 1%, acrylic acid rosin polyoxyethylene sucrose ester 13%, N- 12
Alkyl pyrrolidone bleeding agent 8%, polyoxyethylene polyoxypropylene pentaerythrite ether defoaming agent 1.5%, triisopropanolamine 2.5%;
Surplus is water.
Preparation method are as follows: after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, disodium ethylene diamine tetraacetate,
Porphines, acrylic acid rosin polyoxyethylene sucrose ester, N-dodecylpyrrolidone bleeding agent, polyoxyethylene polyoxypropylene Ji Wusi
Homogenizer is added in alcohol ether defoaming agent, triisopropanolamine antifreezing agent and water, and high-speed stirred is uniformly mixed.
Embodiment 5
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
6%, phytic acid 2%, disodium ethylene diamine tetraacetate 8%, porphines 1.5%, Polyoxyethylene fatty acid amides fatty acid ester 20%, ricinoleic acid butyl ester sulphur
Sour sodium bleeding agent 6%, dimethyl silicone polymer ether defoaming agent 2%, triisopropanolamine 1.5%;Surplus is water.
Preparation method are as follows: after weighing each raw material according to above-mentioned formula, by terpinum, phytic acid, disodium ethylene diamine tetraacetate,
Porphines, Polyoxyethylene fatty acid amides fatty acid ester, ricinoleic acid butyl ester sodium sulphate bleeding agent, dimethyl silicone polymer ether defoaming agent, three isopropyls
Homogenizer is added in hydramine antifreezing agent and water, and high-speed stirred is uniformly mixed.
Comparative example 1
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: coconut oleoyl
Amine propyl betaine 15%, ricinoleic acid butyl ester sodium sulphate 6%, rolydimethylsiloxane defoamer 1%, triisopropanolamine 2%;
Surplus is water.
Comparative example 2
A kind of synergist for aqueous pesticide, the synergist include the raw material of following weight percent: terpinum
10%, phytic acid 1.5%, disodium ethylene diamine tetraacetate 5%, porphines 1.2%, dodecyl sodium sulfate 15%, azone bleeding agent
8%, silicone emulsion defoaming agent 1%, glycerine 2.5%;Surplus is water.
Field trial
10% grass is added with the amount that pesticide quality percentage is 8% in synergist made from embodiment 1-5 and comparative example 1,2
In ammonium phosphine aqua, cauline leaf is watered according to the amount of 1000 milliliter/mu of glufosinate-ammonium and is sprayed, weeds in field is prevented and treated.
Test method: choose former years kind sugarcane harvesting after leave weeds type it is more (weeds be mainly herba setariae viridis, Bermuda grass,
Ageratum conyzoides, rhizome of nutgrass flatsedge etc.), the plot of riotous growth carries out pharmacodynamic test, measures that 8 pieces of 5m × 5m rising trends are close but the grass that do not connect
Ground, wherein the 7 pieces of glufosinate-ammoniumaqua aquas of sprinkling containing embodiment 1-5, comparative example 1,2, the 8th piece is blank control.It is each when sampling
Sampling point area 0.25m2, each cell takes 3 sampling points, and calculates average value.
Control efficiency (%)=(treatment region weeds fresh weight/blank area weeds fresh weight) × 100%
Investigation method: use scissors clip ground above section, weigh fresh weight, sample time be the 3rd day, the 7th day, the 15th
It, the 30th day, investigation result was as shown in table 1.
Synergist of the present invention applies the control efficiency in glufosinate-ammoniumaqua aqua to sugarcane field weeds
It is learnt from above-mentioned test result, the herbicidal effect of glufosinate-ammonium after synergist made from 1-5 of the embodiment of the present invention is added
It is substantially better than the synergist that comparative example is added without terpinum, phytic acid, disodium ethylene diamine tetraacetate and porphines, and weeding is quick bright
It is aobvious to be better than comparative example.
The above content is combine it is specific/further detailed description of the invention for preferred embodiment, cannot
Assert that specific implementation of the invention is only limited to these instructions.General technical staff of the technical field of the invention is come
It says, without departing from the inventive concept of the premise, some replacements or modifications can also be made to the embodiment that these have been described,
And these substitutions or variant are regarded as belonging to the scope of protection of the present invention.
Claims (9)
1. a kind of synergist for aqueous pesticide, it is characterised in that: the synergist includes the raw material of following weight percent:
Terpinum 5-10%, phytic acid 1-3%, disodium ethylene diamine tetraacetate 5-10%, porphines 0.5-1.5%, emulsifier 10-20%, bleeding agent 5-
10%, defoaming agent 0.5-2%, antifreezing agent 1-3%;Surplus is water.
2. being used for the synergist of aqueous pesticide according to claim 1, it is characterised in that: the emulsifier includes alkylphenol
Polyoxyethylene ether, cocoamidopropyl betaine, dodecyl sodium sulfate, acrylic acid rosin polyoxyethylene sucrose ester, polyoxy
One of ethylene fatty acid amide or multiple combinations.
3. being used for the synergist of aqueous pesticide according to claim 1, it is characterised in that: the bleeding agent includes that organosilicon seeps
One of saturating agent, ricinoleic acid butyl ester sodium sulphate, N-Methyl pyrrolidone, N-dodecylpyrrolidone, azone bleeding agent
Or multiple combinations.
4. according to claim 1 be used for aqueous pesticide synergist, it is characterised in that: the antifreezing agent include glycerine,
One of ethylene glycol, triethanolamine, triisopropanolamine or multiple combinations.
5. according to claim 1 be used for aqueous pesticide synergist, it is characterised in that: the defoaming agent be silicone emulsion,
One of polyoxyethylene polyoxypropylene pentaerythrite ether, dimethyl silicone polymer or multiple combinations.
6. a kind of preparation method of the synergist for aqueous pesticide as described in claim 1, it is characterised in that: match according to above-mentioned
After side weighs each raw material, by terpinum, phytic acid, disodium ethylene diamine tetraacetate, porphines, emulsifier, bleeding agent, defoaming agent, antifreeze
Homogenizer is added in agent and water, and high-speed stirred is uniformly mixed.
7. the application of 1 synergist as claimed in claim, it is characterised in that: it is aqua that the synergist, which is applied to dosage form,
Insecticide, fungicide or herbicide.
8. the application of 7 synergist according to claim, it is characterised in that: the synergist is applied to glufosinate-ammonium, grass
Sweet phosphine, dimehypo, jinggangmeisu, in paraquat aqueous pesticide.
9. the application of synergist according to claim 7, it is characterised in that: the usage amount of the synergist is to account for aqueous pesticide
The 1-10% of mass percent.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111528225A (en) * | 2020-05-26 | 2020-08-14 | 山东麒麟农化有限公司 | Synergistic composition for preventing and controlling vegetable plutella xylostella and preparation method thereof |
CN112167262A (en) * | 2020-11-11 | 2021-01-05 | 浙江新安化工集团股份有限公司 | Weeding composition and herbicide |
CN113080199A (en) * | 2021-04-26 | 2021-07-09 | 南开沧州渤海新区绿色化工研究有限公司 | Synergistic composition of herbicide glufosinate |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111528225A (en) * | 2020-05-26 | 2020-08-14 | 山东麒麟农化有限公司 | Synergistic composition for preventing and controlling vegetable plutella xylostella and preparation method thereof |
CN112167262A (en) * | 2020-11-11 | 2021-01-05 | 浙江新安化工集团股份有限公司 | Weeding composition and herbicide |
CN113080199A (en) * | 2021-04-26 | 2021-07-09 | 南开沧州渤海新区绿色化工研究有限公司 | Synergistic composition of herbicide glufosinate |
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